CN108851173A - A kind of cigarette preparation method of mango fragrance and the application in cigarette - Google Patents
A kind of cigarette preparation method of mango fragrance and the application in cigarette Download PDFInfo
- Publication number
- CN108851173A CN108851173A CN201810622684.7A CN201810622684A CN108851173A CN 108851173 A CN108851173 A CN 108851173A CN 201810622684 A CN201810622684 A CN 201810622684A CN 108851173 A CN108851173 A CN 108851173A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- mango
- fragrance
- ethyl alcohol
- mango fragrance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The present invention provides a kind of cigarette preparation methods of mango fragrance：Fresh mature mango is dry, pulverizes and sieves, ethyl alcohol heating extraction, filtering, is concentrated to get mango extractum；The dissolution of mango extractum ethyl alcohol filters removal macromolecular substances using ceramic micro filter film；The organic ultrafiltration membrance filter of microfiltration membranes permeate, removal filtration fraction influence the small-molecule substance of fragrance and mouthfeel, and organic ultrafiltration membrane retention part vacuum distillation concentration obtains mango fragrance.The present invention also provides application of the fragrance in cigarette：Cigarette is diluted with mango fragrance with the nontoxic organic solvent having no irritating odor, pipe tobacco is sprayed on certain proportion and rolls into cigarette.Perfume quantity, the fragrant and sweet protrusion of fruit can be obviously increased after adding the fragrance, fragrance is coordinated, and sweet sense increases, and can reduce irritation and miscellaneous gas, so that flue gas is soft, pleasant impression is comfortable.
Description
Technical field
The invention belongs to cigarette additive preparation technical fields, and in particular to a kind of preparation method of cigarette mango fragrance and
Application in cigarette.
Technical background
For mango as a kind of familiar fruit, vitamin and amino acid rich in are sweet and dilitious, fresh fruit tool
There is strong fragrance.Long guest of Wei et al. extracts volatile component in mango using headspace solid-phase microextraction, carries out gas-chromatography-matter
Spectrum analysis identification.The result shows that volatile component is mainly terpene compound in mango, such as α-terpinolene, δ -3- carene,
These volatile component many are the important components of natural perfume material.Application of the mango product in perfuming cigarette is rarely reported.
General extraction methods, such as egg is all inevitably had using the natural flavor ingredient of Soxhlet extraction method extraction
The impurity such as white matter, starch, wax, not only influence the quality of natural perfume material, but also will affect perfuming cigarette effect, while also can
There is certain influence to the safety of smoking property of cigarette.
Membrane separation technique refers to that the mixture of different-grain diameter molecule on a molecular scale when passing through semi-permeable membrane, realizes selection
Property separation technology.Membrane separation technique can effectively remove while retaining extract original feature fragrance to flue gas sense organ
Quality has the macromolecular substances of negative effect, achievees the purpose that improve extract quality.But it has no and utilizes membrane separation technique point
Tobacco aromaticss are prepared from mango extractum.
It selects membrane separation technique to be separated, purified to the mango extractum of preparation, protein in medicinal extract can be removed, formed sediment
The impurity such as powder, wax, while being retained by ultrafiltration or nanofiltration UF membrane, it also can remove some small-molecule substances for influencing fragrance,
The natural perfume components refined are expected to provide a kind of new method for the utilization of natural perfume material, open up one for perfuming cigarette
New road.
Summary of the invention
It is an object of the invention to be directed to existing for existing tobacco aromaticss, especially mango tobacco aromaticss preparation method not
Foot, provides that a kind of flavouring effect is obvious, the preparation method of impurity few cigarette mango fragrance.The present invention is by following technical side
Case is realized：
To achieve the above object, cigarette provided by the invention mango fragrance preparation method, it includes the following steps：
(1) dry：It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h；
(2) it crushes：Dry mango piece is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；
(3) it extracts：Mango powder is accurately weighed, loading Soxhlet extractor is wrapped with filter paper, is added 3-10 times and measures 50%-
100% ethyl alcohol, is heated to reflux 1-2.5h by 50-90 DEG C of heating temperature.Filtering, filtrate decompression are distilled to no ethyl alcohol and are flowed out, and awns is obtained
Fruit medicinal extract.
(4) micro-filtration UF membrane：It really weighs mango extractum to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20% is added,
Dissolution, dissolved solution N1.It is to be dissolved completely after, filtered using 50-200nm ceramic micro filter film, retention section be N2；
(5)) Ultra filtration membrane：Microfiltration membranes permeate 10-500kd organic membrane filter, retention section are denoted as N3, are denoted as through section
N4。
(6) it takes N3 part reduced pressure to distill to relative density 1.05-1.15, obtains mango fragrance.
The fresh mature mango, the mango comprising originating from Guangxi, Yunnan, Guangdong, Fujian, Taiwan；Originate from India, Meng Jia
Drawing, South East Asia Mainland and one or more of Malay mango and all cultivation mango.
Further, in step (3), it is preferably 5-8 times that amount of alcohol, which is added, and further preferably 5-6 times；Concentration of alcohol
Preferably 70-95%, further preferably 85-90%；Heating temperature is preferably 65-85 DEG C, and further preferably 75-80 DEG C；
Further, in step (4), micro-filtration membrane aperture is preferably 50nm；
Further, in step (5), ultrafiltration membrane aperture is preferably 20-200KD, further preferably 50-100KD；
A kind of application of cigarette mango fragrance of the present invention：By the cigarette nontoxic nonirritant gas of mango fragrance
The organic solvent of taste is diluted, and extension rate is 10-100 times；Before preparing cigarette by the cigarette mango fragrance according to
The mass ratio of 0.02%-1% is sprayed on pipe tobacco, rolls into cigarette.
Further, a kind of application of cigarette mango fragrance, organic solvent diluting multiple are optimized for 20-70 times, into
One-step optimization is 40-50 times；Pipe tobacco adding proportion is optimized for 0.05-0.5%, advanced optimizes as 0.1%-0.3%.
Further, the organic solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any
Mixed liquor of more than two kinds.
A kind of application effect of the cigarette of the present invention with mango fragrance in cigarette, which is characterized in that prepared mango
After fragrance makes an addition to cigarette, perfume quantity, the fragrant and sweet protrusion of fruit can be obviously increased, fragrance is coordinated, and sweet sense increases, and can reduce stimulation
Property with miscellaneous gas so that flue gas is soft, pleasant impression is comfortable.
The invention has the beneficial effects that：
Compared with prior art, UF membrane micro-filtration method is utilized and eliminates a large amount of albumen contained in mango extractum
Matter, pectin, starch, wax, cellulose family and colors are avoided after these ingredients are added to pipe tobacco and are led when burning and sucking
The problem of causing sensory comfort to be deteriorated.In addition, the present invention is eliminated with UF membrane hyperfiltration process influences aroma quality in mango extractum
With perfume quantity and some small-molecule substances excitatory, the suitable flavor component in fragrance is remained as far as possible and is reduced
Miscellaneous gas and irritation, while macromolecular and small molecular weight impurity in mango fragrance are eliminated, so that the application effect of fragrance is more preferable.
Specific embodiment
The present invention is described further with reference to embodiments, but is not limited the scope of the invention in any way.
Embodiment one
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.100g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 90% ethyl alcohol of 500mL, 80 DEG C of heating temperature, is heated to reflux 2h.Filtering, filtrate decompression are distilled to no ethyl alcohol and are flowed out,
Obtain mango extractum.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, the ethyl alcohol of 500mL 20%, dissolution is added
(N1).It is to be dissolved completely after, filtered using 50nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate, which reuses 100kd, to be had
The filtering of machine film, retention section are denoted as N3, are denoted as N4 through section.It takes N3 part reduced pressure to distill to relative density 1.10, obtains cigarette and use awns
Fruity material.Cigarette mango fragrance is taken, ethyl alcohol dilutes 50 times, is sprayed on pipe tobacco according to 0.2% ratio, rolls into cigarette, separately take N1
Part, the same manner operation, as control.
Embodiment two
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.50g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 50% ethyl alcohol of 500mL, 50 DEG C of heating temperature, is heated to reflux 2.5h.Filtering, filtrate decompression are distilled to no ethanol stream
Out, mango extractum is obtained.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, the ethyl alcohol of 500mL 20%, dissolution is added
(N1).It is to be dissolved completely after, filtered using 200nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate reuses 500kd
Organic membrane filter, retention section are denoted as N3, are denoted as N4 through section.It takes N3 part reduced pressure to distill to relative density 1.15, obtains cigarette use
Mango fragrance.Cigarette mango fragrance is taken, propylene glycol dilutes 100 times, is sprayed on pipe tobacco according to 1% ratio, rolls into cigarette.Separately take
The part N1, the same manner operation, as control.
Embodiment three
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.150g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 100% ethyl alcohol of 450mL (dehydrated alcohol), 90 DEG C of heating temperature, is heated to reflux 1h.Filtering, filtrate decompression distill to
No ethyl alcohol outflow, obtains mango extractum.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, is added 500mL's 20%
Ethyl alcohol dissolves (N1).It is to be dissolved completely after, filtered using 100nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate is again
Using 10kd organic membrane filter, retains section and be denoted as N3, be denoted as N4 through section.N3 part reduced pressure is taken to distill to relative density 1.05,
Obtain cigarette mango fragrance.Cigarette mango fragrance is taken, glycerol dilutes 10 times, is sprayed on pipe tobacco according to 0.01% ratio, rolls into
Cigarette.Separately take the part N1, the same manner operation, as control.
Example IV
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.100g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 70% ethyl alcohol of 800mL, 70 DEG C of heating temperature, is heated to reflux 1.5h.Filtering, filtrate decompression are distilled to no ethanol stream
Out, mango extractum is obtained.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, the ethyl alcohol of 500mL 20%, dissolution is added
(N1).It is to be dissolved completely after, filtered using 200nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate, which reuses 50kd, to be had
The filtering of machine film, retention section are denoted as N3, are denoted as N4 through section.It takes N3 part reduced pressure to distill to relative density 1.08, obtains cigarette and use awns
Fruity material.Cigarette mango fragrance is taken, sorbierite dilutes 30 times, is sprayed on pipe tobacco according to 0.5% ratio, rolls into cigarette.Separately take
The part N1, the same manner operation, as control.
Embodiment five
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.100g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 60% ethyl alcohol of 600mL, 60 DEG C of heating temperature, is heated to reflux 2h.Filtering, filtrate decompression are distilled to no ethyl alcohol and are flowed out,
Obtain mango extractum.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, the ethyl alcohol of 500mL 20%, dissolution is added
(N1).It is to be dissolved completely after, filtered using 100nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate reuses 200kd
Organic membrane filter, retention section are denoted as N3, are denoted as N4 through section.It takes N3 part reduced pressure to distill to relative density 1.13, obtains cigarette use
Mango fragrance.Cigarette mango fragrance is taken, xylitol dilutes 80 times, is sprayed on pipe tobacco according to 0.05% ratio, rolls into cigarette.Separately
Take the part N1, the same manner operation, as control.
Embodiment six
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.100g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 75% ethyl alcohol of 400mL, 55 DEG C of heating temperature, is heated to reflux 1.5h.Filtering, filtrate decompression are distilled to no ethanol stream
Out, mango extractum is obtained.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, the ethyl alcohol of 500mL 20%, dissolution is added
(N1).It is to be dissolved completely after, filtered using 50nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate, which reuses 30kd, to be had
The filtering of machine film, retention section are denoted as N3, are denoted as N4 through section.It takes N3 part reduced pressure to distill to relative density 1.07, obtains cigarette and use awns
Fruity material.Cigarette mango fragrance is taken, with ethyl alcohol/mixed with propylene glycol solution (ethyl alcohol：Propylene glycol=1:1) xylitol dilutes 40 times,
It is sprayed on pipe tobacco according to 0.1% ratio, rolls into cigarette.Separately take the part N1, the same manner operation, as control.
Embodiment seven
It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h.Take dry mango
Piece, pulverizer break into coarse powder, cross 10 mesh stainless steel mesh.100g mango powder is accurately weighed, wraps loading Soxhlet extraction with filter paper
Device is added 75% ethyl alcohol of 400mL, 55 DEG C of heating temperature, is heated to reflux 1.5h.Filtering, filtrate decompression are distilled to no ethanol stream
Out, mango extractum is obtained.It accurately weighs 10g mango extractum to be placed in 1000mL beaker, the ethyl alcohol of 500mL 20%, dissolution is added
(N1).It is to be dissolved completely after, filtered using 50nm ceramic micro filter film, retention section be N2；Microfiltration membranes permeate, which reuses 30kd, to be had
The filtering of machine film, retention section are denoted as N3, are denoted as N4 through section.It takes N3 part reduced pressure to distill to relative density 1.07, obtains cigarette and use awns
Fruity material.Cigarette mango fragrance is taken, with xylitol/sorb mixed alkoxide solution (xylitol：Sorbierite=1:1) xylitol dilution 60
Times, it is sprayed on pipe tobacco according to 0.1% ratio, rolls into cigarette.Separately take the part N1, the same manner operation, as control.
Experimental example
1. cigarette mango fragrance analysis of volatile components
In separatory funnel, 20mL20% ethyl alcohol is added with mango fragrance 1.0g in the cigarette prepared in correct amount Example one
Oscillation dissolution, completely rear addition 50mL methylene chloride extraction to be dissolved is for 24 hours.Clear liquid is removed, appropriate anhydrous sodium sulfate is added, is stood
Overnight.It is concentrated into 1mL, carries out GC-MS analysis.
GC-MS condition is：Chromatographic column：HP-5MS capillary column (60m*0.32mm*0.25 μm)；Injector temperature：250
℃；Temperature programming：Then 50 DEG C of maintenance 3min of initial temperature rise to 260 DEG C with 4 DEG C of speed, maintain 5min；Vapourizing temperature：
270℃；Carrier gas：He, 1mL min-1；Split ratio：5:1；Ionization mode：The source EI；Detector temperature：FID, 300 DEG C；Transmission line
Temperature：280℃；Ionizing energy：70eV；Ion source temperature：230℃；Mass scan range：30~700amu；Retrieval spectrum library：
The library NIST11.
According to table 1, cigarette with detecting 31 kinds of substances altogether in mango fragrance.Farnesyl acetone has fresh and sweet fragrant, rose
Rare perfume (or spice) can assign cigarette faint scent note；Trans- squalene is the terpenoid substance of non-pigmented in tobacco leaf, can promote the suction of tobacco leaf
Taste and fragrance, and aroma component can be formed by Degradation and Transformation；Myristic acid has the function of wax, sweet taste and soft flue gas；
Palmitinic acid has effects that increase flue gas sweet taste, wax taste and richness；Ethyl oleate can increase flue gas concentration, so that smoke alcohol
With；Ethyl palmitate soft flue gas and can increase sweet taste, and showing cigarette flavor and taste, certain coke is fragrant and sweet and thick and solid, stays length
Sense；Ethyl linoleate plays the role of increasing sweet taste, soft.These flavor components being enriched with through purification may be that cigarette mango is fragrant
Material, which increases cigarette perfume, improves the material base of mouthfeel.
1 cigarette of table mango fragrance volatile component
2. organoleptic effect of the cigarette with mango fragrance applications in cigarette is evaluated
By 7 sections of cigarette mango fragrance prepared by one-embodiment of embodiment seven, including the N1 awns in seven preparation process
The cigarette of fruity material volume.Transfer to 7 people above judging panel synthesis to smoke panel test, using be not added with the control cigarette of any mango fragrance as pair
According to as a result (table 2) is shown：It, can be obvious after a kind of cigarette of the present invention makes an addition to cigarette with mango fragrance compared with control sample
Increasing perfume quantity, the fragrant and sweet protrusion of fruit, fragrance is coordinated, and sweet sense increases, and can reduce irritation and miscellaneous gas, so that flue gas is soft,
Pleasant impression is comfortable, generally increases fragrance, improvement mouthfeel and removal of impurities drop thorn effect significantly better than conventional mango fragrance.
Influence of 2. cigarette of table with mango fragrance to Sensory Quality of Cigarette
Claims (12)
1. a kind of cigarette preparation method of mango fragrance, which is characterized in that be achieved through the following technical solutions：
(1) dry：It takes fresh mature mango, after peeling, be cut into uniform sheet, is placed in baking oven, 50 DEG C of dry 12h；
(2) it crushes：Dry mango piece is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；
(3) it extracts：Mango powder is accurately weighed, loading Soxhlet extractor is wrapped with filter paper, is added 3-10 times and measures 50%-100% second
Alcohol, is heated to reflux 1-2.5h by 50-90 DEG C of heating temperature.Filtering, filtrate decompression are distilled to no ethyl alcohol and are flowed out, and mango extractum is obtained；
(4) micro-filtration UF membrane：It really weighs mango extractum to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20% is added, dissolve,
Dissolved solution is N1.It is to be dissolved completely after, filtered using 50-200nm ceramic micro filter film, retention section be N2；
(5)) Ultra filtration membrane：Microfiltration membranes permeate 10-500kd organic membrane filter, retention section are denoted as N3, are denoted as N4 through section；
(6) it takes N3 part reduced pressure to distill to relative density 1.05-1.15, obtains mango fragrance.
2. the preparation method of a kind of cigarette mango fragrance according to claim 1, which is characterized in that in step (3), be added
5-8 times is measured 70%-95% ethyl alcohol, 65-85 DEG C of heating temperature, is heated to reflux 1-2.5h.Filtering, filtrate decompression are distilled to no ethyl alcohol
Outflow, obtains mango extractum.
3. the preparation method of a kind of cigarette mango fragrance according to claim 1, which is characterized in that in step (3), be added
5-6 times is measured 85%-90% ethyl alcohol, 75-80 DEG C of heating temperature, is heated to reflux 1-2.5h.Filtering, filtrate decompression are distilled to no ethyl alcohol
Outflow, obtains mango extractum.
4. the preparation method of a kind of cigarette mango fragrance according to claim 1, which is characterized in that in step (4), micro-filtration
Membrane aperture is 50nm.
5. the preparation method of a kind of cigarette mango fragrance according to claim 1, which is characterized in that in step (5), ultrafiltration
Membrane aperture is 20-200KD.
6. the preparation method of a kind of cigarette mango fragrance according to claim 1, which is characterized in that in step (5), ultrafiltration
Membrane aperture is 50-100KD.
7. application of a kind of cigarette of one of -6 the methods preparation with mango fragrance in cigarette according to claim 1, feature
It is, the cigarette is diluted with mango fragrance with the nontoxic organic solvent having no irritating odor, extension rate 10-100
Times；The cigarette is sprayed on pipe tobacco according to the mass ratio of 0.02%-1% with mango fragrance before preparing cigarette, is rolled coiled
Cigarette.
8. application of a kind of cigarette of one of -6 the methods preparation with mango fragrance in cigarette according to claim 1, feature
It is, the cigarette is diluted with mango fragrance with the nontoxic organic solvent having no irritating odor, extension rate 20-70
Times；The cigarette is sprayed on pipe tobacco according to the mass ratio of 0.05-0.5% with mango fragrance before preparing cigarette, is rolled coiled
Cigarette.
9. application of a kind of cigarette of one of -6 the methods preparation with mango fragrance in cigarette according to claim 1, feature
It is, the cigarette is diluted with mango fragrance with the nontoxic organic solvent having no irritating odor, extension rate 40-50
Times；The cigarette is sprayed on pipe tobacco according to the mass ratio of 0.1-0.3% with mango fragrance before preparing cigarette, is rolled coiled
Cigarette.
10. application of a kind of cigarette with mango fragrance in cigarette according to claim 7, which is characterized in that described is organic
Solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any mixed liquor of more than two kinds.
11. application of a kind of cigarette with mango fragrance in cigarette according to claim 8, which is characterized in that described is organic
Solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any mixed liquor of more than two kinds.
12. application of a kind of cigarette with mango fragrance in cigarette according to claim 9, which is characterized in that described is organic
Solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any mixed liquor of more than two kinds.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810622684.7A CN108851173A (en) | 2018-06-15 | 2018-06-15 | A kind of cigarette preparation method of mango fragrance and the application in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810622684.7A CN108851173A (en) | 2018-06-15 | 2018-06-15 | A kind of cigarette preparation method of mango fragrance and the application in cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108851173A true CN108851173A (en) | 2018-11-23 |
Family
ID=64339460
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810622684.7A Withdrawn CN108851173A (en) | 2018-06-15 | 2018-06-15 | A kind of cigarette preparation method of mango fragrance and the application in cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108851173A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111808681A (en) * | 2020-07-20 | 2020-10-23 | 广西中烟工业有限责任公司 | Preparation method of lycium ruthenicum murr spice for cigarettes and application of lycium ruthenicum murr spice in cigarettes |
| CN115067540A (en) * | 2022-07-11 | 2022-09-20 | 湖北中烟工业有限责任公司 | Apple extract for cigarettes and preparation method thereof |
| CN115413814A (en) * | 2022-09-16 | 2022-12-02 | 河南中烟工业有限责任公司 | Preparation method for increasing sweet and fragrant characteristics of cigarette fruits and spice prepared by method |
| CN115558550A (en) * | 2022-09-16 | 2023-01-03 | 中国烟草总公司郑州烟草研究院 | Spice for increasing cigarette smoke concentration characteristics and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104946390A (en) * | 2015-05-31 | 2015-09-30 | 中国烟草总公司郑州烟草研究院 | Method for processing natural perfume used for electronic cigarette |
-
2018
- 2018-06-15 CN CN201810622684.7A patent/CN108851173A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104946390A (en) * | 2015-05-31 | 2015-09-30 | 中国烟草总公司郑州烟草研究院 | Method for processing natural perfume used for electronic cigarette |
Non-Patent Citations (2)
| Title |
|---|
| 国家食品药品监督管理局执业药师资格认证中心组织编写: "《中药学专业知识 2 畅销版》", 31 January 2014, 中国医药科技出版社 * |
| 王娟等: "膜技术在烟用地黄香料加工中的应用", 《香料香精化妆品》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111808681A (en) * | 2020-07-20 | 2020-10-23 | 广西中烟工业有限责任公司 | Preparation method of lycium ruthenicum murr spice for cigarettes and application of lycium ruthenicum murr spice in cigarettes |
| CN115067540A (en) * | 2022-07-11 | 2022-09-20 | 湖北中烟工业有限责任公司 | Apple extract for cigarettes and preparation method thereof |
| CN115413814A (en) * | 2022-09-16 | 2022-12-02 | 河南中烟工业有限责任公司 | Preparation method for increasing sweet and fragrant characteristics of cigarette fruits and spice prepared by method |
| CN115558550A (en) * | 2022-09-16 | 2023-01-03 | 中国烟草总公司郑州烟草研究院 | Spice for increasing cigarette smoke concentration characteristics and preparation method thereof |
| CN115413814B (en) * | 2022-09-16 | 2023-11-21 | 河南中烟工业有限责任公司 | Preparation method for improving sweet characteristics of cigarettes and spice prepared by adopting preparation method |
| CN115558550B (en) * | 2022-09-16 | 2024-03-29 | 中国烟草总公司郑州烟草研究院 | Spice for increasing smoke concentration characteristics of cigarettes and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106307606B (en) | A kind of preparation method of high fragrance tobacco extract | |
| CN106509981B (en) | A kind of preparation method of high-nicotine tobacco extract | |
| CN108851173A (en) | A kind of cigarette preparation method of mango fragrance and the application in cigarette | |
| CN106307604B (en) | tobacco extract, extracting method and application | |
| CN106387990B (en) | High-nicotine tobacco extract and its application | |
| CN108851209B (en) | Tobacco Huai chrysanthemum perfume and preparation method and application of microcapsule thereof | |
| CN109082344B (en) | Tobacco essence perfume, cigarette paper containing tobacco essence perfume and application of cigarette paper | |
| CN106753793B (en) | Preparation method of tea absolute for cigarettes | |
| CN111808681A (en) | Preparation method of lycium ruthenicum murr spice for cigarettes and application of lycium ruthenicum murr spice in cigarettes | |
| CN104004594A (en) | Spice for costustoot flavored cigarettes based on aquilaria leaves, as well as preparation method and application of spice | |
| CN103478885A (en) | Tobacco sheet containing tea flower extractive and preparation method thereof | |
| CN109762664A (en) | A kind of quick-fried pearl tea essence of persistent form cigarette and preparation method thereof | |
| CN113331466A (en) | Fresh and sweet type base for cigarettes and application of fresh and sweet type base in cigarettes | |
| CN107637858B (en) | Plant aroma-causing substance extracted by improved water extraction and alcohol precipitation method, and extraction method and application thereof | |
| CN105146747A (en) | Preparation method of endogenous oily humectant for tobaccos | |
| CN108865438A (en) | A kind of cigarette preparation method of Radix Angelicae Sinensis fragrance and the application in cigarette | |
| CN106167739B (en) | Microcapsule containing green tea extract, preparation method and application thereof | |
| CN107287031A (en) | The aobvious fragrant composition separation of Turkish tobaccos maillard reaction thing prepares method and the application of tobacco additive agent | |
| CN108851172A (en) | A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette | |
| CN111035058B (en) | Preparation method of tar extract in waste cigarette butts and application of tar extract in cigarettes | |
| CN101342011B (en) | Application of black tea mellow wine extract | |
| CN101327041B (en) | Pu'er cooked tea alcohol extract and preparation and use thereof | |
| CN108851210A (en) | A kind of preparation method and application of cigarette mango fragrance and its microcapsules | |
| CN115644494A (en) | Preparation method and application of mixed tobacco reconstituted essence | |
| CN104479867A (en) | Microcapsule purification method and application of dill oil for cigarettes |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181123 |
|
| WW01 | Invention patent application withdrawn after publication |