CN108851172A - A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette - Google Patents
A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette Download PDFInfo
- Publication number
- CN108851172A CN108851172A CN201810621444.5A CN201810621444A CN108851172A CN 108851172 A CN108851172 A CN 108851172A CN 201810621444 A CN201810621444 A CN 201810621444A CN 108851172 A CN108851172 A CN 108851172A
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- Prior art keywords
- cigarette
- fragrance
- siraitia grosvenorii
- preparation
- ethyl alcohol
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The present invention provides a kind of cigarette preparation methods of Siraitia grosvenorii fragrance：Siraitia grosvenorii pulverizes and sieves, alcohol dipping for 24 hours, with certain flow rate seepage pressure effects, obtain a certain amount of percolate, filter, be concentrated to get Luo Han Guo Paste In Foods；The dissolution of Luo Han Guo Paste In Foods ethyl alcohol filters removal macromolecular substances using ceramic micro filter film；The organic ultrafiltration membrance filter of microfiltration membranes permeate, removal filtration fraction influence the small-molecule substance of fragrance and mouthfeel, and organic ultrafiltration membrane retention part vacuum distillation concentration obtains cigarette Siraitia grosvenorii fragrance.The present invention also provides application of the fragrance in cigarette：Cigarette is diluted with Siraitia grosvenorii fragrance, pipe tobacco is sprayed on certain proportion and rolls into cigarette.The rich of cigarette perfume can be obviously increased after adding the fragrance, the smooth feeling of flue gas increases, and sweet sense increases, and can reduce irritation and miscellaneous gas, so that flue gas is soft, pleasant impression is comfortable.
Description
Technical field：
The invention belongs to cigarette additive preparation technical fields, and in particular to a kind of preparation method of cigarette Siraitia grosvenorii fragrance
And the application in cigarette.
Technical background：
Siraitia grosvenorii, the fruit of the perennial liana of Curcurbitaceae.Alias sweating fruit, balloonvine heartseed herb, Semen Momordicae, it is invaluable,
Arhat table, naked tortoise bar are described as " angle fruit " by people, and leaf is heart-shaped, dioecism, summer-flowering, seed in autumn.Mainly originate in
Guangxi Zhuang Autonomous Region Guilin City Yongfu county, the county Long Sheng, the Yongfu county county He Longsheng are that township's plantation history of Siraitia grosvenorii is longer,
Wherein plantation Siraitia grosvenorii in Yongfu has had more than 300 years history, and the county Long Sheng plantation Siraitia grosvenorii has had more than 200 years history, China hundred
/ nine ten Siraitia grosvenoriis originate in the Yongfu county county He Longsheng, Siraitia grosvenorii is the rare local and special products in Guilin, and country ratifies in the first batch
One of dual-purpose of drug and food material, primary efficacy is can be relieving cough and reducing sputum.Fruits nutrition value is very high, containing vitamin C abundant and
Glucoside, fructose, glucose, protein, lipid etc..
Siraitia grosvenorii fragrance is widely used in tobacco aromaticss.This research team long campaigns cigarette is researched and developed with Siraitia grosvenorii fragrance, but
The Siraitia grosvenorii fragrance routinely prepared supplements perfume quantity although helpful to mouthfeel limited.
Percolation is that the plant that will moderately crush is set in percolator, constantly adds solvent by top, solvent seeped medicinal material layer
The method that ingredient is leached during flowing downward belongs to Dynamic Leaching method, and solvent utilization rate is high, and effective component leaches completely,
Leachate can directly be collected.The Siraitia grosvenorii tincture spice of percolation preparation is compared with conventional method, more to cigarette flavor amount supplement
To be obvious, but inevitably with impurity such as protein, starch, waxes, the quality of natural perfume material is influenced to a certain extent, it is right
Also there is also some negative effects for cigarette perfume.
Membrane separation technique refers to that the mixture of different-grain diameter molecule on a molecular scale when passing through semi-permeable membrane, realizes selection
Property separation technology.Membrane separation technique can effectively remove while retaining extract original feature fragrance to flue gas sense organ
Quality has the macromolecular substances of negative effect, achievees the purpose that improve extract quality.But it has no and utilizes membrane separation technique point
Tobacco aromaticss are prepared from Luo Han Guo Paste In Foods.
The present invention selects membrane separation technique to sieve of preparation on the basis of selecting ethanol percolation extraction method enrichment flavor component
Chinese fruit medicinal extract is separated, is purified, and can remove the impurity such as protein in medicinal extract, starch, wax, while passing through ultrafiltration or nanofiltration
UF membrane retention, also can remove some small-molecule substances for influencing fragrance, and the natural perfume components refined are expected to be natural
The utilization of fragrance provides a kind of new method, opens up a new road for perfuming cigarette.
Summary of the invention
It is an object of the invention to be directed to existing for existing tobacco aromaticss, especially momordica grosvenori tobacco flavor preparation method not
Foot, provides that a kind of flavouring effect is obvious, the preparation method of impurity few cigarette Siraitia grosvenorii fragrance.The present invention is by following technology
Scheme is realized：
To achieve the above object, cigarette provided by the invention Siraitia grosvenorii fragrance preparation method, it includes the following steps：
(1) it crushes：Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；
(2) it impregnates：Mangosteen powder is accurately weighed, is placed in percolator, 5-20 times is added and measures 50%-95% ethyl alcohol, is soaked
After impregnate for 24 hours.
(3) seepage pressure effects：With 2-10mL/min speed seepage pressure effects, until obtaining the infiltration of 4-18 times of quality of medicinal material coarse powder quality
It filters after liquid, terminates and extract, percolate filtering is spare；
(4) it is concentrated：The hydraulic distillation of diacolation is flowed out to no ethyl alcohol, obtains Luo Han Guo Paste In Foods.
(5) micro-filtration UF membrane：It really weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the second of 50 times of amounts 20% is added
Alcohol, dissolution, dissolved solution D1.It is to be dissolved completely after, filtered using 50-200nm ceramic micro filter film, retention section be D2；
(6)) Ultra filtration membrane：Microfiltration membranes permeate 10-500kd organic membrane filter, retention section are denoted as D3, are denoted as through section
D4。
(7) it takes D3 part reduced pressure to distill to relative density 1.05-1.15, obtains Siraitia grosvenorii fragrance.
Further, in step (2), it is preferably 6-16 times that amount of alcohol, which is added, and further preferably 8-12 times；Ethyl alcohol is dense
Degree is preferably 55%-85%, and further preferably 60-70% impregnates for 24 hours after wetting.
Further, in step (3), seepage pressure effects flow velocity is preferably 3-7mL/min, further preferably 4-5mL/
min.Percolate collecting amount is preferably 5-15 times of medicinal material coarse powder quality, further preferably 7-11 times.Percolate filtering is spare.
Further, in step (5), micro-filtration membrane aperture is preferably 50nm.
Further, in step (6), ultrafiltration membrane aperture is preferably 20-200KD, further preferably 50-100KD.
A kind of application the invention also discloses cigarette with Siraitia grosvenorii fragrance in cigarette, it is characterised in that：The cigarette is used
Siraitia grosvenorii fragrance is diluted with the nontoxic organic solvent having no irritating odor, and extension rate is 10-100 times；Preparing cigarette
It is preceding that the cigarette is sprayed on pipe tobacco according to the mass ratio of 0.02%-1% with Siraitia grosvenorii fragrance, roll into cigarette.
Further, a kind of application of cigarette Siraitia grosvenorii fragrance, organic solvent diluting multiple are optimized for 20-70 times,
Advanced optimize is 40-50 times；Pipe tobacco adding proportion is optimized for 0.05-0.5%, advanced optimizes as 0.1%-0.3%.
Further, the organic solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any
Mixed liquor of more than two kinds.
A kind of application effect of the cigarette of the present invention with Siraitia grosvenorii fragrance in cigarette, it is characterised in that：Prepared sieve
After Chinese fruity material makes an addition to cigarette, the rich of cigarette perfume can be obviously increased, the smooth feeling of flue gas increases, and sweet sense increases, and energy
Irritation and miscellaneous gas are reduced, so that flue gas is soft, pleasant impression is comfortable.
The invention has the beneficial effects that：
Compared with prior art, Siraitia grosvenorii fragrance is prepared using ethanol percolation extraction method, because being that solvent seeped medicinal material
The method that ingredient is leached during sulfate layer flows downhill is dynamic belongs to Dynamic Leaching method, and solvent utilization rate is high, and effective component has leached
Entirely, the flavouring effect of tobacco aromaticss is prepared significantly better than routine techniques.
Further be utilized UF membrane micro-filtration method eliminate the protein contained in Siraitia grosvenorii fragrance, pectin, starch,
Wax, cellulose family and colors avoid after these ingredients are added to pipe tobacco causes sensory comfort to become when burning and sucking
The problem of difference.In addition, being eliminated with UF membrane hyperfiltration process influences aroma quality and perfume quantity and irritating in Siraitia grosvenorii fragrance
Some small-molecule substances of property, remain the suitable flavor component in fragrance as far as possible and reduce miscellaneous gas and irritation, simultaneously
Macromolecular and small molecular weight impurity in Siraitia grosvenorii fragrance are eliminated, so that the application effect of fragrance is more preferable.
Specific embodiment
The present invention is described further with reference to embodiments, but is not limited the scope of the invention in any way.
Embodiment one
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 11 times of 65% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 5mL/min speed seepage pressure effects, until obtaining medicine
It after the percolate of 10 times of quality of material meal quality, terminates and extracts, percolate filtering is spare；Take the hydraulic distillation of diacolation to no ethanol stream
Out, Luo Han Guo Paste In Foods are obtained.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 50nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 100kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.10, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, ethyl alcohol dilutes 50 times, is sprayed on pipe tobacco according to 0.2% ratio, rolls into cigarette.
Embodiment two
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 20 times of 50% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 2mL/min speed seepage pressure effects, until obtaining medicine
It after the percolate of 18 times of quality of material meal quality, terminates and extracts, percolate filtering is spare；Take the hydraulic distillation of diacolation to no ethanol stream
Out, Luo Han Guo Paste In Foods are obtained.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 200nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 10kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.15, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, propylene glycol dilutes 100 times, is sprayed on pipe tobacco according to 1% ratio, rolls into cigarette.
Embodiment three
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 5 times of 95% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 10mL/min speed seepage pressure effects, until obtaining medicine
It after the percolate of 4 times of quality of material meal quality, terminates and extracts, percolate filtering is spare；Take the hydraulic distillation of diacolation to no ethanol stream
Out, Luo Han Guo Paste In Foods are obtained.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 100nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 20kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.05, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, glycerol dilutes 10 times, is sprayed on pipe tobacco according to 0.01% ratio, rolls into cigarette.
Example IV
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 8 times of 75% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 8mL/min speed seepage pressure effects, until obtaining medicinal material
It after the percolate of 7 times of quality of meal quality, terminates and extracts, percolate filtering is spare；The hydraulic distillation of diacolation to no ethyl alcohol is taken to flow out,
Obtain Luo Han Guo Paste In Foods.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 200nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 50kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.07, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, sorbierite dilutes 30 times, is sprayed on pipe tobacco according to 0.5% ratio, rolls into cigarette.
Embodiment five
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 13 times of 85% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 3mL/min speed seepage pressure effects, until obtaining medicine
It after the percolate of 12 times of quality of material meal quality, terminates and extracts, percolate filtering is spare；Take the hydraulic distillation of diacolation to no ethanol stream
Out, Luo Han Guo Paste In Foods are obtained.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 50nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 200kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.12, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, xylitol dilutes 80 times, is sprayed on pipe tobacco according to 0.05% ratio, rolls into cigarette.
Embodiment six
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 17 times of 60% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 6mL/min speed seepage pressure effects, until obtaining medicine
It after the percolate of 16 times of quality of material meal quality, terminates and extracts, percolate filtering is spare；Take the hydraulic distillation of diacolation to no ethanol stream
Out, Luo Han Guo Paste In Foods are obtained.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 100nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 20kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.09, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, with ethyl alcohol/mixed with propylene glycol solution (ethyl alcohol：Propylene glycol=1:1) xylitol dilution 40
Times, it is sprayed on pipe tobacco according to 0.1% ratio, rolls into cigarette.
Embodiment seven
Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；Mangosteen powder is accurately weighed,
It is placed in percolator, 6 times of 90% ethyl alcohol of amount is added, are impregnated for 24 hours after wetting；With 9mL/min speed seepage pressure effects, until obtaining medicinal material
It after the percolate of 5 times of quality of meal quality, terminates and extracts, percolate filtering is spare；The hydraulic distillation of diacolation to no ethyl alcohol is taken to flow out,
Obtain Luo Han Guo Paste In Foods.
It accurately weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20%, dissolution, after dissolution is added
Solution be D1.It is to be dissolved completely after, filtered using 50nm ceramic micro filter film, retention section be D2；Microfiltration membranes permeate 100kd has
The filtering of machine film, retention section are denoted as D3, are denoted as D4 through section；It takes D3 part reduced pressure to distill to relative density 1.13, obtains Siraitia grosvenorii
Fragrance.
Cigarette Siraitia grosvenorii fragrance is taken, with xylitol/sorb mixed alkoxide solution (xylitol：Sorbierite=1:1) xylitol is dilute
60 times are released, pipe tobacco is sprayed on according to 0.1% ratio, rolls into cigarette.
Experimental example
1. cigarette Siraitia grosvenorii fragrance analysis of volatile components
In separatory funnel, 20mL20% second is added with Siraitia grosvenorii fragrance 1.0g in the cigarette prepared in correct amount Example one
Alcohol oscillation dissolution, completely rear addition 50mL methylene chloride extraction to be dissolved is for 24 hours.Clear liquid is removed, appropriate anhydrous sodium sulfate is added, it is quiet
It sets overnight.It is concentrated into 1mL, carries out GC-MS analysis.
GC-MS condition is：Chromatographic column：HP-5MS capillary column (60m*0.32mm*0.25 μm)；Injector temperature：250
℃；Temperature programming：Then 50 DEG C of maintenance 3min of initial temperature rise to 260 DEG C with 4 DEG C of speed, maintain 5min；Vapourizing temperature：
270℃；Carrier gas：He, 1mL min-1；Split ratio：5:1；Ionization mode：The source EI；Detector temperature：FID, 300 DEG C；Transmission line
Temperature：280℃；Ionizing energy：70eV；Ion source temperature：230℃；Mass scan range：30~700amu；Retrieval spectrum library：
The library NIST11.
According to table 1, cigarette with detecting 24 kinds of substances altogether in Siraitia grosvenorii fragrance.Volatile materials total amount is 2585.41 μ
g/g；The wherein more fanesol of content and the cis- β-farnesene similar with its fragrance, with distinctive green note
Lily of the valley floral scent, and have green fragrant and radix aucklandiae note, the cigarette fragrance of a flower, green fragrant and radix aucklandiae note can be assigned；5 hydroxymethyl furfural has
It is fragrant like caramel, cereal baking breath, fruity, bread, cigarette radix aucklandiae, the fragrance of a flower, fruity and fragrant and sweet can be assigned；Linoleic acid can assign cigarette
Careless fat and the cured sample fragrance of rouge；Palmitinic acid has effects that increase flue gas sweet taste, wax taste and richness；These are enriched with through purification
Flavor component may be cigarette Siraitia grosvenorii fragrance increase cigarette perfume improve mouthfeel material base.
1 cigarette of table Siraitia grosvenorii fragrance volatile component
2. organoleptic effect of the cigarette with Siraitia grosvenorii fragrance applications in cigarette is evaluated
It is extracted by 7 sections of cigarette Siraitia grosvenorii fragrance prepared by one~embodiment of embodiment seven, in addition using alcohol reflux
Conventional method prepares 2 kinds of Siraitia grosvenorii fragrance as reference.The above judging panel's synthesis of 7 people is transferred to smoke panel test, to be not added with any Siraitia grosvenorii
The control cigarette of fragrance is as control, and as a result (table 2) is shown：Compared with control sample, a kind of cigarette Siraitia grosvenorii of the present invention
After fragrance makes an addition to cigarette, the rich of cigarette perfume can be obviously increased, the smooth feeling of flue gas increases, and sweet sense increases, and can reduce
Irritation and miscellaneous gas, so that flue gas is soft, pleasant impression is comfortable.It is obviously good to generally increase fragrance, improvement mouthfeel and removal of impurities drop thorn effect
In conventional Siraitia grosvenorii fragrance.Influence of 2. cigarette of table with Siraitia grosvenorii fragrance to Sensory Quality of Cigarette
| Gloss (5) | Fragrance (32) | Coordinate (6) | Miscellaneous gas (12) | Irritation (20) | Pleasant impression (25) | It is total | |
| Control | 5.00 | 28.00 | 5.00 | 10.20 | 17.20 | 22.00 | 87.40 |
| Conventional perfumes comparison 1 | 5.00 | 28.35 | 5.00 | 10.45 | 17.50 | 22.20 | 88.50 |
| Conventional perfumes comparison 2 | 5.00 | 28.30 | 5.00 | 10.40 | 17.40 | 22.30 | 88.40 |
| One fragrance of embodiment | 5.00 | 28.65 | 5.00 | 10.75 | 17.70 | 22.50 | 89.60 |
| Two fragrance of embodiment | 5.00 | 28.70 | 5.00 | 10.50 | 17.65 | 22.45 | 89.30 |
| Three fragrance of embodiment | 5.00 | 28.50 | 5.00 | 10.55 | 17.95 | 22.50 | 89.25 |
| Example IV fragrance | 5.00 | 28.60 | 5.00 | 10.70 | 17.60 | 22.30 | 89.40 |
| Embodiment five spices | 5.00 | 28.65 | 5.00 | 10.60 | 17.60 | 22.45 | 89.30 |
| Six fragrance of embodiment | 5.00 | 28.65 | 5.00 | 10.65 | 17.60 | 22.50 | 89.40 |
| Seven fragrance of embodiment | 5.00 | 28.60 | 5.00 | 10.60 | 17.65 | 22.50 | 89.35 |
Claims (14)
1. a kind of cigarette preparation method of Siraitia grosvenorii fragrance, which is characterized in that be achieved through the following technical solutions：
(1) it crushes：Dry Siraitia grosvenorii medicinal material is taken, pulverizer breaks into coarse powder, crosses 10 mesh stainless steel mesh；
(2) it impregnates：Mangosteen powder is accurately weighed, is placed in percolator, 5-20 times is added and measures 50%-95% ethyl alcohol, soaked after wetting
Stain is for 24 hours；
(3) seepage pressure effects：With 2-10mL/min speed seepage pressure effects, until obtaining the percolate of 4-18 times of quality of medicinal material coarse powder quality
Afterwards, it terminates and extracts, percolate filtering is spare；
(4) it is concentrated：The hydraulic distillation of diacolation is flowed out to no ethyl alcohol, obtains Luo Han Guo Paste In Foods；
(5) micro-filtration UF membrane：It really weighs Luo Han Guo Paste In Foods to be placed in quantitative glass container, the ethyl alcohol of 50 times of amounts 20% is added, it is molten
Solution, dissolved solution D1.It is to be dissolved completely after, filtered using 50-200nm ceramic micro filter film, retention section be D2；
(6)) Ultra filtration membrane：Microfiltration membranes permeate 10-500kd organic membrane filter, retention section are denoted as D3, are denoted as D4 through section；
(7) it takes D3 part reduced pressure to distill to relative density 1.05-1.15, obtains Siraitia grosvenorii fragrance.
2. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that in step (2), add
Enter 6-16 times and measure 55%-85% ethyl alcohol, is impregnated for 24 hours after wetting.
3. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that in step (2), add
Enter 8-12 times and measure 60%-70% ethyl alcohol, is impregnated for 24 hours after wetting.
4. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that in step (3), with
3-7mL/min speed seepage pressure effects, until terminate and extract after the percolate of acquisition 5-15 times of quality of medicinal material coarse powder quality, percolate
It filters spare.
5. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that in step (3), with
4-5mL/min speed seepage pressure effects, until terminate and extract after the percolate of acquisition 7-11 times of quality of medicinal material coarse powder quality, percolate
It filters spare.
6. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that micro- in step (5)
Filter sizes are 50nm.
7. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that in step (6), surpass
Filter sizes are 20-200KD.
8. the preparation method of a kind of cigarette Siraitia grosvenorii fragrance according to claim 1, which is characterized in that in step (6), surpass
Filter sizes are 50-100KD.
9. application of a kind of cigarette of one of -8 the methods preparation with Siraitia grosvenorii fragrance in cigarette according to claim 1, special
Sign is, the cigarette is diluted with Siraitia grosvenorii fragrance with the nontoxic organic solvent having no irritating odor, extension rate 10-
100 times；The cigarette is sprayed on pipe tobacco according to the mass ratio of 0.02%-1% with Siraitia grosvenorii fragrance before preparing cigarette, is rolled
At cigarette.
10. application of a kind of cigarette of one of -8 the methods preparation with Siraitia grosvenorii fragrance in cigarette according to claim 1, special
Sign is, the cigarette is diluted with Siraitia grosvenorii fragrance with the nontoxic organic solvent having no irritating odor, extension rate 20-
70 times；The cigarette is sprayed on pipe tobacco according to the mass ratio of 0.05-0.5% with Siraitia grosvenorii fragrance before preparing cigarette, is rolled
At cigarette.
11. application of a kind of cigarette of one of -8 the methods preparation with Siraitia grosvenorii fragrance in cigarette according to claim 1, special
Sign is, the cigarette is diluted with Siraitia grosvenorii fragrance with the nontoxic organic solvent having no irritating odor, extension rate 40-
50 times；The cigarette is sprayed on pipe tobacco according to the mass ratio of 0.1-0.3% with Siraitia grosvenorii fragrance before preparing cigarette, is rolled into
Cigarette.
12. application of a kind of cigarette with Siraitia grosvenorii fragrance in cigarette according to claim 9, which is characterized in that described has
Solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any mixed liquor of more than two kinds.
13. application of a kind of cigarette with Siraitia grosvenorii fragrance in cigarette according to claim 10, which is characterized in that described has
Solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any mixed liquor of more than two kinds.
14. application of a kind of cigarette with Siraitia grosvenorii fragrance in cigarette according to claim 11, which is characterized in that described has
Solvent is ethyl alcohol, propylene glycol, sorbierite, xylitol or glycerol, or wherein any mixed liquor of more than two kinds.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810621444.5A CN108851172A (en) | 2018-06-15 | 2018-06-15 | A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810621444.5A CN108851172A (en) | 2018-06-15 | 2018-06-15 | A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette |
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| CN108851172A true CN108851172A (en) | 2018-11-23 |
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| CN (1) | CN108851172A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111567849A (en) * | 2020-06-02 | 2020-08-25 | 江西中烟工业有限责任公司 | Tobacco slice capable of being heated and not combusted |
| CN116392975A (en) * | 2023-04-12 | 2023-07-07 | 江苏中烟工业有限责任公司 | Natural spice separation composite membrane for cigarettes and application thereof |
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| CN104946390A (en) * | 2015-05-31 | 2015-09-30 | 中国烟草总公司郑州烟草研究院 | Method for processing natural perfume used for electronic cigarette |
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| CN104946390A (en) * | 2015-05-31 | 2015-09-30 | 中国烟草总公司郑州烟草研究院 | Method for processing natural perfume used for electronic cigarette |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111567849A (en) * | 2020-06-02 | 2020-08-25 | 江西中烟工业有限责任公司 | Tobacco slice capable of being heated and not combusted |
| CN116392975A (en) * | 2023-04-12 | 2023-07-07 | 江苏中烟工业有限责任公司 | Natural spice separation composite membrane for cigarettes and application thereof |
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Application publication date: 20181123 |