CN1986758A - Alcohol extracted sophora flower extratum and its application in perfuming cigarette - Google Patents
Alcohol extracted sophora flower extratum and its application in perfuming cigarette Download PDFInfo
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- CN1986758A CN1986758A CN 200610128447 CN200610128447A CN1986758A CN 1986758 A CN1986758 A CN 1986758A CN 200610128447 CN200610128447 CN 200610128447 CN 200610128447 A CN200610128447 A CN 200610128447A CN 1986758 A CN1986758 A CN 1986758A
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- sophora flower
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Abstract
The present invention relates to natural perfume, and is especially alcohol extracted sophora flower extractum and its application in perfuming cigarette. The sophora flower extractum is prepared through the following steps: extracting sophora flower with alcohol, solid-liquid separation, clarifying filtration, and distilling concentration to obtain the sophora flower extractum. The sophora flower extractum is used as perfume added into cigarette tobacco shred to increase fragrance, reduce stimulation and bad smell and improve taste. The present invention has simple extraction process and circular utilization of solvent alcohol, and provides one excellent natural perfume for cigarette.
Description
Technical field
The present invention relates to the extraction and the application of natural perfume, be specifically related to a kind of alcohol extracted sophora flower extratum and the application in perfuming cigarette thereof, the sophora flower extractum that utilizes the present invention to obtain has good effect in perfuming cigarette.
Background technology
Essence and flavoring agent is widely used in daily chemical products, food, tobacco, feed and many Industrial products, and natural perfume is because its composition is complicated, fragrance is abundant, fragrance remaining time is the indispensable raw material of preparing essence lastingly.
Sophora flower grows in Chinese scholartree, and Chinese scholartree is a deciduous tree, belongs to the leguminous plants Chinese scholartree.China especially north is very extensive.Sophora flower has strong sweet fragrance, is that people like the fresh flower that eats, and pharmaceutical use is arranged, the action effect that have antibiotic, blood coagulation, refrigerant hemostasis, clears liver and improve vision.
Along with the problem of smoking with health more and more receives publicity, improve the security of sucking of cigarette, the comfort of the objectionable constituent in the reduction cigarette smoke, raising suction is the inevitable development trend of cigarette.
Summary of the invention
Purpose of the present invention just is being based on above-mentioned condition and a kind of alcohol extracted sophora flower extratum of special development and the application in perfuming cigarette thereof, sophora flower extraction using alcohol medicinal extract is applied on the cigarette shreds, can increase fragrance, reducing stimulates and assorted gas, improve the mouthfeel pleasant impression, and this The Application of Technology does not change the existing complete processing of cigarette, can improve the interior quality of cigarette.
The objective of the invention is to realize by following scheme: sophora flower extractum is to make by the following method: sophora flower → alcohol extraction → solid-liquid separation → clarification filtration → distillation concentrates → sophora flower extractum.
In the present invention, described sophora flower can be bright sophora flower, also can be dried sophora flower; Described alcohol concn is 50-100%; Sophora flower/ethanol (KG/KG) is 1: 2-1: 10, and extraction time is 1h-240h, and extraction temperature is 20-80 ℃, and distillation temperature is 80 ℃ during air distillation, and vacuum tightness is 0.01Mpa-0.1Mpa during underpressure distillation, distillation temperature is 15-60 ℃.
Sophora flower extractum of the present invention is joined in the cigarette shreds as spices, can increase fragrance, reduce the gas that stimulates, mixes, improve the mouthfeel pleasant impression.The sophora flower extractum consumption is the 0.01-0.5% of pipe tobacco weight, is that 95% edible ethanol dilutes medicinal extract by dehydrated alcohol or ethanol content earlier, adds in the pipe tobacco by spray pattern again.
Effect of the present invention and benefit are: the alcohol extracted sophora flower extratum method is simpler, easy and simple to handle than general traditional natural perfume extraction method technology, and etoh solvent can recycle and reuse, and there is not solvent contamination in product.Because tobacco flavoring is to be medium with ethanol, being insoluble to the alcoholic acid composition will be difficult for adding in the tobacco, institute's perfuming mostly exists in the solubility in the ethanol, sophora flower extractum with extraction using alcohol can dissolve preferably, easy to use, for tobacco flavoring provides novel, a respond well natural perfume.
Embodiment
To method afford further instruction of the present invention, but do not limit the present invention below by embodiment.
Embodiment 1
With the bright sophora flower 100g of electronic balance weighing, the 3000ml Erlenmeyer flask of packing into equably.Add 1000ml ethanol (concentration is 95% edible ethanol), soak 72h under 40 ℃ of conditions, separation, filtration earlier 80 ℃ of air distillations, are that 0.05-0.1Mpa, distillation temperature are that distillation concentrates under the 15-60 ℃ of condition in vacuum tightness then, get medicinal extract 1g.
Get sophora flower extractum by 0.5% of pipe tobacco weight, be 1% with anhydrous alcohol solution dilution after, spray is added in the flue-cured tobacco pipe tobacco and rolls into cigarette, think through smokeing panel test: the perfuming effect of this product in flue-cured tobacco is obvious, can increase fragrance, reduces the gas that stimulates, mixes, improve mouthfeel, pleasant impression is comparatively comfortable, clean.
Embodiment 2
With the dried sophora flower 100g of electronic balance weighing, the Erlenmeyer flask of packing into equably.Add 1000ml ethanol (concentration 75%), evenly stirring heating is soaked 10h under 80 ℃ of conditions, and separation is filtered, and earlier 80 ℃ of air distillations, is that 0.05-0.1Mpa, distillation temperature are that distillation concentrates under the 15-60 ℃ of condition in vacuum tightness then, gets medicinal extract 1.5g.
Getting sophora flower extractum by 0.1% of pipe tobacco weight, is that 1% spray is added in the flue-cured tobacco pipe tobacco and rolls into cigarette with anhydrous alcohol solution dilution, thinks that through smokeing panel test the perfuming of this product in flue-cured tobacco produces effect, and stimulates, assorted gas alleviates, and mouthfeel has improvement, and pleasant impression is slightly comfortable.
Claims (7)
1, a kind of alcohol extracted sophora flower extratum is characterized in that: it is to make by the following method: sophora flower → alcohol extraction → solid-liquid separation → clarification filtration → distillation concentrates → sophora flower extractum.
2, sophora flower extractum according to claim 1 is characterized in that: described sophora flower is bright sophora flower or dried sophora flower.
3, sophora flower extractum according to claim 1 is characterized in that: used alcohol concn is 50-100%.
4, sophora flower extractum according to claim 1 is characterized in that: sophora flower/ethanol (KG/KG) is 1: 2-1: 10, and extraction time is 1-240h, extraction temperature is 20-80 ℃.
5, sophora flower extractum according to claim 1 is characterized in that: distillation temperature is 80 ℃ when adopting air distillation, adopts underpressure distillation, and vacuum tightness is 0.01Mpa-0.1Mpa, and distillation temperature is 15-60 ℃.
6, the application of sophora flower extractum according to claim 1 in perfuming cigarette is characterized in that: sophora flower extractum of the present invention is joined in the cigarette shreds as spices.
7, the application of sophora flower extractum according to claim 6 in perfuming cigarette, it is characterized in that: the sophora flower extractum consumption is the 0.01-0.5% of pipe tobacco weight, be that 95% edible ethanol dissolves medicinal extract, dilute by dehydrated alcohol or ethanol content earlier, add in the pipe tobacco by spray pattern again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101284472A CN100572514C (en) | 2006-12-22 | 2006-12-22 | Alcohol extracted sophora flower extratum and the application in perfuming cigarette thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101284472A CN100572514C (en) | 2006-12-22 | 2006-12-22 | Alcohol extracted sophora flower extratum and the application in perfuming cigarette thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1986758A true CN1986758A (en) | 2007-06-27 |
| CN100572514C CN100572514C (en) | 2009-12-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2006101284472A Expired - Fee Related CN100572514C (en) | 2006-12-22 | 2006-12-22 | Alcohol extracted sophora flower extratum and the application in perfuming cigarette thereof |
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| CN (1) | CN100572514C (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101889728A (en) * | 2010-07-03 | 2010-11-24 | 中国烟草总公司郑州烟草研究院 | Method for extracting roasted and fermented malt extract by ethanol and application of malt extract in tobacco |
| CN102687904A (en) * | 2012-06-04 | 2012-09-26 | 云南烟草科学研究院 | Chamaemelum nobile extract and application thereof |
| CN103013665A (en) * | 2012-12-13 | 2013-04-03 | 湖北中烟工业有限责任公司 | Preparation method of fenugreek extract Maillard reaction product and application of reaction product in cigarette |
| CN103491810A (en) * | 2011-03-15 | 2014-01-01 | 英美烟草(投资)有限公司 | Method and apparatus for impregnating tobacco industry products with sensate constituents of botanicals |
| CN104087421A (en) * | 2014-07-24 | 2014-10-08 | 中国烟草总公司郑州烟草研究院 | Althaea rosea flower extract coproduction preparation method and applications thereof |
| CN105602729A (en) * | 2015-11-23 | 2016-05-25 | 江西中烟工业有限责任公司 | Extraction method for tulip essence |
| CN106136297A (en) * | 2016-08-24 | 2016-11-23 | 陈佐坚 | A kind of sophora flower wine odor type pipe tobacco |
| CN107637858A (en) * | 2017-09-14 | 2018-01-30 | 云南中烟工业有限责任公司 | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application |
| CN109258370A (en) * | 2018-07-29 | 2019-01-25 | 四川省烟草公司宜宾市公司 | A kind of tobacco planting method improving the sweet fragrant breeze lattice of tobacco leaf |
| CN111418873A (en) * | 2020-03-31 | 2020-07-17 | 广西中烟工业有限责任公司 | Sophora flower sweet-flavor essence for heating non-combustible cigarettes and preparation method thereof |
| CN114794527A (en) * | 2022-03-21 | 2022-07-29 | 河北中烟工业有限责任公司 | Sophora flower extract, preparation method thereof and cigarette flavoring |
-
2006
- 2006-12-22 CN CNB2006101284472A patent/CN100572514C/en not_active Expired - Fee Related
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101889728A (en) * | 2010-07-03 | 2010-11-24 | 中国烟草总公司郑州烟草研究院 | Method for extracting roasted and fermented malt extract by ethanol and application of malt extract in tobacco |
| CN103491810B (en) * | 2011-03-15 | 2016-10-12 | 英美烟草(投资)有限公司 | The method and apparatus impregnating tobacco industry products with the organoleptic component of plant |
| CN103491810A (en) * | 2011-03-15 | 2014-01-01 | 英美烟草(投资)有限公司 | Method and apparatus for impregnating tobacco industry products with sensate constituents of botanicals |
| CN102687904A (en) * | 2012-06-04 | 2012-09-26 | 云南烟草科学研究院 | Chamaemelum nobile extract and application thereof |
| CN103013665A (en) * | 2012-12-13 | 2013-04-03 | 湖北中烟工业有限责任公司 | Preparation method of fenugreek extract Maillard reaction product and application of reaction product in cigarette |
| CN103013665B (en) * | 2012-12-13 | 2014-08-27 | 湖北中烟工业有限责任公司 | Preparation method of fenugreek extract Maillard reaction product and application of reaction product in cigarette |
| CN104087421A (en) * | 2014-07-24 | 2014-10-08 | 中国烟草总公司郑州烟草研究院 | Althaea rosea flower extract coproduction preparation method and applications thereof |
| CN105602729A (en) * | 2015-11-23 | 2016-05-25 | 江西中烟工业有限责任公司 | Extraction method for tulip essence |
| CN106136297A (en) * | 2016-08-24 | 2016-11-23 | 陈佐坚 | A kind of sophora flower wine odor type pipe tobacco |
| CN107637858A (en) * | 2017-09-14 | 2018-01-30 | 云南中烟工业有限责任公司 | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application |
| CN107637858B (en) * | 2017-09-14 | 2020-11-10 | 云南中烟工业有限责任公司 | Plant aroma-causing substance extracted by improved water extraction and alcohol precipitation method, and extraction method and application thereof |
| CN109258370A (en) * | 2018-07-29 | 2019-01-25 | 四川省烟草公司宜宾市公司 | A kind of tobacco planting method improving the sweet fragrant breeze lattice of tobacco leaf |
| CN111418873A (en) * | 2020-03-31 | 2020-07-17 | 广西中烟工业有限责任公司 | Sophora flower sweet-flavor essence for heating non-combustible cigarettes and preparation method thereof |
| CN114794527A (en) * | 2022-03-21 | 2022-07-29 | 河北中烟工业有限责任公司 | Sophora flower extract, preparation method thereof and cigarette flavoring |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100572514C (en) | 2009-12-23 |
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Granted publication date: 20091223 Termination date: 20191222 |