CN103271860B - Skin care oil containing peony oil and preparation method thereof - Google Patents
Skin care oil containing peony oil and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of skin care oil medicine, in particular to skin care oil medicine containing peony oil and a preparation method thereof. The skin care oil medicine provided by the invention comprises the following components in parts by weight: main ingredients: peony seed oil, caprylic/capric triglyceride, cyclopentasiloxane and 1, 2 - butyl glycol 1-12, wherein the peony oil is peony seed oil or peony essence oil or the mixture of peony seed oil and peony essence oil; auxiliary ingredients: isostearic acid, butylated hydroxytoluene, avocado oil, simmondsia chinensis seed oil, meadowfoam seed oil and macadamia ternifolia seed oil; the skin care oil medicine containing peony oil prepared by the method provided by the invention can remarkably improve of the skin epidermis cell cycle function, promote the microcirculation of the blood capillary of the dermal skin effect, inhibit lipid peroxidation, improve metabolism, delay skin aging process, is provided with anti-wrinkle, moisturizing and whiting effect, people feels smooth and comfortable after the skin care oil medicine is used on the skin, and the skin care oil medicine containing peony oil is provided with better effect to chloasma, aging skin wrinkles, skin cutin hardening peeling and skin chap.
Description
Technical field
The invention belongs to skin care oil technical field of pharmaceuticals, be specifically related to a kind of skin care oil medicine containing peony oil and preparation method thereof.
Background technology
Peony seed oil takes from seed of Paeonia suffruticosa " seed of Flos Moutan ", adopts hot moulding, cold pressing or supercritical CO
2extraction extracts refine and forms.The vegetable oil extracted by seed of Flos Moutan is the distinctive woody macadamia nut oil of China, and nutritious and unique because of it, having medical care effect again, be called " vegetable oil best in the world " by relevant expert, is the treasure in vegetable oil.
In peony seed oil, VA, VE, nicotinic acid, carotene, unsaturated fatty acid content are abundant, to skin, there is fabulous Nutritional Nursing Care effect, can obviously improve skin epidermal cells circulatory function, promote the microcirculation of capillary of skin, the carrying out of anti-lipid peroxidation effect, improve metabolism, delay skin aging process, there is crease-resistant, moisturizing whitening function, use rear skin smooth light, have good effect to chloasma, skin aging wrinkle, skin keratin sclerosis decortication, wrinkled skin.
Real multifunctional raw material---1,2-pentanediol: 1,2-pentanediol (INCI:Pentylene Glycol), as the multifunctional raw material of cosmetics, has long-term safe handling history, meets the cosmetics regulation of the U.S., Europe, Japanese various places.1,2-pentanediol is wetting agent remarkable in cosmetic formulations; Simultaneously can the bioavailability of enhanced activity thing, promote that the effective ingredient in vegetable oil infiltrates skin and realizes effect, experimental data shows that 1,2-pentanediol can make the bioavailability concentration of some functional component increase by more than 10 times; In addition, also having broad spectrum antibiotic activity, is the conventional antipathogenic composition in preservative free formula.
American Avocado Tree (PERSEA GRATISSIMA) oil: American Avocado Tree oil from American Avocado Tree fruit, does not add chemical substance in process by cold press technique extraction.American Avocado Tree oil contains a large amount of vitamin V A, VB1 etc. and several mineral materials, can moisten, soften skin, eliminate skin inflammation, can promote the regeneration of skin cell simultaneously.
Bai Chihua (LIMNANTHES ALBA) seed oil: due to the long-chain fatty acid having an antioxidative effect containing more than 98%, so it is one of the most stable in the world vegetable oil.Excellent emollient, for product creates magnificent quality, also has soft and dry and comfortable skinfeel; Can not be oxidized, increase the shelf-life of product, increase the stability of other oils, also can improve skin resistance to oxidation, make skin often aobvious young nature.
Jojoba (SIMMONDSIA CHINENSIS) seed oil: Jojoba seed oil contains multiple nutritional components, as VE, VC, spermol, protein, mineral etc.The regeneration of skin cell can be promoted, effective especially for cicatrical skin, cicatrix and pox print can be desalinated.In addition, can the fat secretion of balance skin, improve the skin symptoms such as oiliness skin, acne, abscess, eczema.
Macadimia nut (MACADAMIA TERNIFOLIA) seed oil: rich in mineral substances, protein, the natural emollient of multiple unsaturated fatty acid.Fast to skin-permeation rate, for skin brings smooth after using, moisten, the sensation of non-greasy, Cell protection film, repair skin after shining, improve the ability that skin resists extraneous infringement.
Containing multiple important higher fatty acids in peony petal, main based on Palmic acid, linoleic acid plus linolenic acid, unsaturated fatty acid has reduction blood fat, prevents arteriosclerotic effect, if linoleic acid is essential fatty acid, have in human body and can change arachidonic acid into, for synthetic phospholipid, form cellularity, maintain the normal function of all tissues, and synthesis of prostaglandins, be all necessary, linolenic acid is the nutrient that body weight for humans is wanted, there is Tumor suppression transfer, reduce Incidence of CHD, improve the effects such as immunity; Also containing protein in Flos Moutan, the elements such as polyphenols, potassium, calcium, magnesium, phosphorus and vitamin B and carotenoid are a kind of natural nutraceutical agents.As using Flos Moutan as raw material, extract quintessence oil wherein, preparing peony essential oil, is one of optimum feed stock preparing skin care item.
Report about Flos Moutan skin care item is also few, there is the extracting method that patent discloses peony essential oil, in traditional peony essential oil extracting method, take peony petal as raw material, or with the peony petal after oven dry for raw material, and no matter peony petal is in growth course, or in picking process, all inevitably fall to having pollen, and part population is irritated to peony pollen, when peony pollen cannot be stopped completely, pollen can along with the leaching process of peony essential oil, which kind of method no matter is adopted to extract in the peony essential oil obtained, all likely can containing residual peony pollen, thus cause the crowd for peony pollen allergy equally also irritated to peony essential oil.Not all peony essential oil is all suitable for all people group.
Therefore need to improve for above-mentioned method defect, design a kind of processing method fully remaining heat-sensitive materials and active substance in Flos Moutan, Flos Moutan is extracted, obtain that safety is high, the peony essential oil of quality better, with this quintessence oil for raw material, prepare Paeonia suffruticosa skin care oil.
Summary of the invention
In order to solve above-mentioned technical problem, the invention provides a kind of obvious microcirculation improving skin epidermal cells circulatory function, promote capillary of skin, the carrying out of anti-lipid peroxidation effect, improve metabolism, delay skin aging process, there is crease-resistant, moisturizing whitening function, use rear skin smooth light, chloasma, skin aging wrinkle, skin keratin sclerosis decortication, wrinkled skin are had to the skin care oil medicine containing peony seed oil of good effect;
A kind of skin care oil medicine containing peony oil of the present invention, comprises the component of following portions by weight:
Major ingredient:
Peony oil, 30-70;
Caprylic/capric triglyceride 15-40
Ring five polydimethylsiloxane 5-30
1,2-pentanediol 1-12;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Isostearic acid accounts for the heavy 0.1-0.3% of peony oil;
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of peony oil;
American Avocado Tree oil accounts for the heavy 0.01-3% of peony oil;
Jojoba seed oil accounts for the heavy 0.01-3% of peony oil;
White Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of peony oil;
Macadimia nut seed oil accounts for the heavy 0.01-3% of peony oil;
This peony oil is the mixture of peony seed oil or peony essential oil or peony seed oil and peony essential oil.
Preferably, above-mentioned a kind of skin care oil medicine containing peony oil, comprises the component of following portions by weight:
Major ingredient:
Peony oil, 40-60;
Caprylic/capric triglyceride 20-40
Ring five polydimethylsiloxane 10-25
1,2-pentanediol 2-10;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Isostearic acid accounts for the heavy 0.1-0.3% of peony oil;
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of peony oil;
American Avocado Tree oil accounts for the heavy 0.01-3% of peony oil;
Jojoba seed oil accounts for the heavy 0.01-3% of peony oil;
White Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of peony oil;
Macadimia nut seed oil accounts for the heavy 0.01-3% of peony oil;
This peony oil is the mixture of peony seed oil or peony essential oil or peony seed oil and peony essential oil.
Preferred, above-mentioned a kind of skin care oil medicine containing peony oil, comprises the component of following portions by weight:
Major ingredient:
Peony oil, 50;
Caprylic/capric triglyceride 30
Ring five polydimethylsiloxane 20
1,2-pentanediol 5;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Isostearic acid account for peony oil heavy 0.2%,
Butylated hydroxytoluene account for peony oil heavy 0.1%,
American Avocado Tree oil account for peony oil heavy 0.2%,
Jojoba seed oil account for peony oil heavy 0.2%,
White Limnanthes Alba Seed Oil account for peony oil heavy 0.2%,
Macadimia nut seed oil account for peony oil heavy 0.2%;
This peony oil is the mixture of peony seed oil or peony essential oil or peony seed oil and peony essential oil.
Containing a skin care oil medicine its preparation method for peony oil, comprise following step:
Get the peony oil of 30-70 part, add 5-30 part ring five polydimethylsiloxane, be uniformly mixed, then add caprylic/capric triglyceride and the butylated hydroxytoluene of 15-40 part, heating for dissolving below 60 DEG C, is uniformly mixed,
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of peony oil; Slowly add 1, the 2-pentanediol of 1-12 part again, be stirred to transparence, add isostearic acid and be uniformly mixed, above-mentioned isostearic acid accounts for the heavy 0.1-0.3% of peony oil;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil accounts for the heavy 0.01-3% of peony oil, Jojoba seed oil accounts for the heavy 0.01-3% of peony oil, white Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of peony oil, macadimia nut seed oil accounts for the heavy 0.01-3% of peony oil, stir, filter, storage;
Above-mentioned peony oil is the mixture of peony seed oil or peony essential oil or peony seed oil and peony essential oil;
In filtration step, adopt 200-500 mesh sieve aperture.
Containing a skin care oil medicine its preparation method for peony oil,
The peony oil peony seed oil that to be seed of Flos Moutan obtain through cold pressing or hot moulding or supercritical carbon dioxide ways and means;
The peony seed oil adopting common method for cold pressing or hot moulding method to obtain all can be used as raw material peony seed oil of the present invention;
When above-mentioned peony oil is peony essential oil,
Peony essential oil its preparation method is as follows:
(1) extract: pluck fresh peony flower, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, the condition of described supercritical carbon dioxide extraction is: extracting pressure 20-30Mpa, extraction temperature 40-60 DEG C, separator I pressure 8-20Mpa, temperature 45-70 DEG C, separator II pressure 4-l0Mpa, temperature 15-30 DEG C, extraction time 2-4h;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, the condition of molecular distillation is: feeding temperature 40-90 DEG C, vapo(u)rizing temperature 95-180 DEG C, vacuum 5-1000Pa, Paeonia suffruticosa extractum flow 100-2000ml/h, knifing rotating speed 180-550r/min, chilling temperature 10-45 DEG C.
Feeding temperature 60 DEG C, vapo(u)rizing temperature temperature 130 DEG C, vacuum 40Pa, Paeonia suffruticosa extractum flow 200ml/h, knifing rotating speed 380r/min, chilling temperature 25 DEG C.
In above-mentioned step (1) extraction process, pluck fresh peony flower, the at least one in Herba Portulacae and Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), Semen Sinapis is added in fresh peony flower, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and the total amount of described Herba Portulacae and Semen Sinapis Albae or Semen Raphani or Semen Lepidii (Semen Descurainiae) or Semen Sinapis or their mixture accounts for the 0.5-2% of peony petal.
Above-mentioned preparation method also comprises following step: the peony essential oil obtained after distillation of learning from else's experience, and mix with at least one in adjuvant Mel, Aloe polysaccharide, sinapic acid choline ester., the gross weight of adjuvant accounts for the 0.2-1.5% of peony essential oil;
Adjuvant is Aloe polysaccharide and sinapic acid choline ester., and its part by weight is 1:1-3, and the gross weight of adjuvant accounts for the 0.2-1.5% of peony essential oil.
Beneficial effect of the present invention is, the skin care oil medicine containing peony oil adopting above-mentioned method to prepare, obviously improve skin epidermal cells circulatory function, promote the microcirculation of capillary of skin, the carrying out of anti-lipid peroxidation effect, improves metabolism, delay skin aging process, there is crease-resistant, moisturizing whitening function, use rear skin smooth light, have good effect to chloasma, skin aging wrinkle, skin keratin sclerosis decortication, wrinkled skin.
In the present invention, when adopting peony essential oil to be raw material, peony essential oil provide not only the necessary nutrient of human body, and due in peony essential oil preparation process, add the antiallergic material such as Herba Portulacae and Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), Semen Sinapis, make peony essential oil be applicable to all groups and use.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, so that those skilled in the art more understands the present invention, but does not therefore limit the present invention.
Embodiment 1
Get the peony seed oil of 50 parts, the preparation method of this peony seed oil is that common method for cold pressing obtains, and add 20 parts of ring five polydimethylsiloxane, be uniformly mixed, then add Trivent OCG and the butylated hydroxytoluene of 30 parts, heating for dissolving below 60 DEG C, is uniformly mixed,
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony seed oil heavy 0.1%; Slowly add 1, the 2-pentanediol of 5 parts again, be stirred to transparence, add isostearic acid and be uniformly mixed, isostearic acid account for peony seed oil heavy 0.2%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 0.2%, Jojoba seed oil account for peony seed oil heavy 0.2%, white Limnanthes Alba Seed Oil account for peony seed oil heavy 0.2%, macadimia nut seed oil account for peony seed oil heavy 0.2%, stir, filter, storage;
In filtration step, adopt 200-500 mesh sieve aperture.
Below the skin care oil medicine containing peony oil that the method for embodiment 1 prepares, the indexs such as its outward appearance:
Embodiment 2
Get the peony essential oil of 50 parts, add 20 parts of ring five polydimethylsiloxane, be uniformly mixed, then add Trivent OCG and the butylated hydroxytoluene of 30 parts, heating for dissolving below 60 DEG C, is uniformly mixed;
The preparation process of above peony essential oil is as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add Herba Portulacae, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, extraction temperature 50 DEG C, separator I pressure 10Mpa, temperature 55 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 60 DEG C, vapo(u)rizing temperature 120 DEG C, vacuum 40Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 380r/min, chilling temperature 30 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant sinapic acid choline ester., the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, peony essential oil is obtained after mixing, add sinapic acid choline ester., further can prevent human allergy, and add effect that the peony essential oil after sinapic acid choline ester. also has radioprotective, antibacterial, antiinflammatory.
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony essential oil heavy 0.1%; Slowly add 1, the 2-pentanediol of 5 parts again, be stirred to transparence, add isostearic acid and be uniformly mixed, isostearic acid account for peony seed oil heavy 0.2%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 1%, Jojoba seed oil account for peony essential oil heavy 1%, white Limnanthes Alba Seed Oil account for peony essential oil heavy 1%, macadimia nut seed oil account for peony essential oil heavy 1%, stir, filter, storage;
In filtration step, adopt 200-500 mesh sieve aperture.
Comparative example 1
Get the peony essential oil of 50 parts, add 20 parts of ring five polydimethylsiloxane, be uniformly mixed, then add Trivent OCG and the butylated hydroxytoluene of 30 parts, heating for dissolving below 60 DEG C, is uniformly mixed;
The preparation process of above peony essential oil is as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, extraction temperature 50 DEG C, separator I pressure 10Mpa, temperature 55 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(4) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 70 DEG C, vapo(u)rizing temperature 130 DEG C, vacuum 50Pa, Paeonia suffruticosa extractum flow 500ml/h, knifing rotating speed 380r/min, chilling temperature 30 DEG C; The peony essential oil obtained after distillation.
In above peony essential oil, add butylated hydroxytoluene, butylated hydroxytoluene account for peony essential oil heavy 0.1%; Slowly add 1, the 2-pentanediol of 5 parts again, be stirred to transparence, add isostearic acid and be uniformly mixed, isostearic acid account for peony seed oil heavy 0.2%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 1%, Jojoba seed oil account for peony essential oil heavy 1%, white Limnanthes Alba Seed Oil account for peony essential oil heavy 1%, macadimia nut seed oil account for peony essential oil heavy 1%, stir, filter, storage;
In filtration step, adopt 200-500 mesh sieve aperture.
Women between 200 20-30 years is divided into two groups, in these two groups, often organize and have 5 women irritated to Flos Moutan respectively, skin care oil medicine in Example 2 and comparative example 1, allow respectively and often organize librarian use, sooner or later respectively get about 1 gram painting to put on a stern expression and neck, after one month, collect two groups of women respectively to the reaction condition of this skin care oil medicine.
Embodiment 2, in these 100 women, unmanned to Paeonia suffruticosa skin care oil drug allergy, and also compared to before one month, skin is obviously fine and smooth, smooth;
Comparative example 1, in these 100 women, has 4 women to Paeonia suffruticosa skin care oil drug allergy, and before one month, skin is obviously fine and smooth, smooth.
Embodiment 3
Get the peony seed oil of 30 parts, the preparation method of this peony seed oil is that common method for cold pressing obtains, and add 5 parts of ring five polydimethylsiloxane, be uniformly mixed, then add Trivent OCG and the butylated hydroxytoluene of 15 parts, heating for dissolving below 60 DEG C, is uniformly mixed,
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony seed oil heavy 0.05%; Slowly add 1, the 2-pentanediol of 1 part again, be stirred to transparence, add isostearic acid and be uniformly mixed, isostearic acid account for peony seed oil heavy 0.1%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 0.5%, Jojoba seed oil account for peony seed oil heavy 0.5%, white Limnanthes Alba Seed Oil account for peony seed oil heavy 0.5%, macadimia nut seed oil account for peony seed oil heavy 0.5%, stir, filter, storage;
In filtration step, adopt 200-500 mesh sieve aperture.
Embodiment 4
Get the peony seed oil of 30 parts, the preparation method of this peony seed oil is that common hot moulding method obtains, and add 5 parts of ring five polydimethylsiloxane, be uniformly mixed, then add Trivent OCG and the butylated hydroxytoluene of 15 parts, heating for dissolving below 60 DEG C, is uniformly mixed,
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony seed oil heavy 0.15%; Slowly add 1, the 2-pentanediol of 12 parts again, be stirred to transparence, add isostearic acid and be uniformly mixed, isostearic acid account for peony seed oil heavy 0.3%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 3%, Jojoba seed oil account for peony seed oil heavy 3%, white Limnanthes Alba Seed Oil account for peony seed oil heavy 3%, macadimia nut seed oil account for peony seed oil heavy 3%, stir, filter, storage;
In filtration step, adopt 200-500 mesh sieve aperture.
Embodiment 5
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add Herba Portulacae, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, extraction temperature 50 DEG C, separator I pressure 10Mpa, temperature 55 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 50 DEG C, vapo(u)rizing temperature 140 DEG C, vacuum 100Pa, Paeonia suffruticosa extractum flow 600ml/h, knifing rotating speed 480r/min, chilling temperature 20 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant Aloe polysaccharide, the gross weight of Aloe polysaccharide accounts for 1% of peony essential oil, peony essential oil is obtained after mixing, add Aloe polysaccharide, further can prevent human allergy, and add the peony essential oil after Aloe polysaccharide also there is effect that is antibacterial, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 6
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add Herba Portulacae, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, extraction temperature 50 DEG C, separator I pressure 10Mpa, temperature 55 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 70 DEG C, vapo(u)rizing temperature 100 DEG C, vacuum 4Pa, Paeonia suffruticosa extractum flow 700ml/h, knifing rotating speed 280r/min, chilling temperature 30 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant sinapic acid choline ester., the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, peony essential oil is obtained after mixing, add sinapic acid choline ester., further can prevent human allergy, and add effect that the peony essential oil after sinapic acid choline ester. also has radioprotective, antibacterial, antiinflammatory.
Remaining making step is with embodiment 3.
Embodiment 7
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, add Herba Portulacae and Semen Sinapis Albae in fresh peony flower, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, extraction temperature 50 DEG C, separator I pressure 10Mpa, temperature 55 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 55 DEG C, vapo(u)rizing temperature 130 DEG C, vacuum 400Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 380r/min, chilling temperature 10 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant Aloe polysaccharide, the gross weight of Aloe polysaccharide accounts for 1% of peony essential oil, peony essential oil is obtained after mixing, add Aloe polysaccharide, further can prevent human allergy, and add the peony essential oil after Aloe polysaccharide also there is effect that is antibacterial, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 8
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add Herba Portulacae and Semen Sinapis Albae, Semen Raphani, its addition is 1% of peony petal gross weight, its part by weight is 1:1:1, and supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, extraction temperature 50 DEG C, separator I pressure 15Mpa, temperature 35 DEG C, separator II pressure 7Mpa, temperature 20 DEG C, extraction time 2h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae and Semen Sinapis Albae, Semen Raphani, not only can desensitize, and above-mentioned material also has antioxidation, radioprotective, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 60 DEG C, vapo(u)rizing temperature 135 DEG C, vacuum 400Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 430r/min, chilling temperature 20 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant Mel, the gross weight of adjuvant accounts for 0.8% of peony essential oil, peony essential oil is obtained after mixing, add Aloe polysaccharide, further can prevent human allergy, and add the peony essential oil after Aloe polysaccharide also there is effect that is antibacterial, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 9
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add Herba Portulacae, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 30Mpa, extraction temperature 55 DEG C, separator I pressure 20Mpa, temperature 35 DEG C, separator II pressure 10Mpa, temperature 25 DEG C, extraction time 3h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is:
Feeding temperature 45 DEG C, vapo(u)rizing temperature 130 DEG C, vacuum 100Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 350r/min, chilling temperature 25 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant Aloe polysaccharide and sinapic acid choline ester., its part by weight is 1:2, the gross weight of adjuvant accounts for 0.8% of peony essential oil, peony essential oil is obtained after mixing, add Aloe polysaccharide and sinapic acid choline ester., further can prevent human allergy, and add effect that the peony essential oil after Aloe polysaccharide and sinapic acid choline ester. also has radioprotective, antibacterial, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 10
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add Herba Portulacae, addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 25Mpa, extraction temperature 48 DEG C, separator I pressure 10Mpa, temperature 35 DEG C, separator II pressure 6Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned Herba Portulacae also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) distill: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 65 DEG C, vapo(u)rizing temperature 150 DEG C, vacuum 700Pa, Paeonia suffruticosa extractum flow 800ml/h, knifing rotating speed 380r/min, chilling temperature 20 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant sinapic acid choline ester., Mel, gross weight accounts for 1% of peony essential oil, its part by weight is 1:2, peony essential oil is obtained after mixing, add sinapic acid choline ester., Mel, further can prevent human allergy, and add effect that the peony essential oil after sinapic acid choline ester., Mel also has radioprotective, antibacterial, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 11
Take peony essential oil as raw material, wherein peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add that Herba Portulacae addition is peony petal gross weight 1%, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and its condition of supercritical carbon dioxide supercritical extraction is: pressure 25Mpa, extraction temperature 60 DEG C, separator I pressure 10Mpa, temperature 35 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned Herba Portulacae also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) distill: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is: feeding temperature 75 DEG C, vapo(u)rizing temperature 140 DEG C, vacuum 800Pa, Paeonia suffruticosa extractum flow 800ml/h, knifing rotating speed 480r/min, chilling temperature 30 DEG C;
(3) to learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant sinapic acid choline ester., Mel, Aloe polysaccharide, the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, the weight ratio of sinapic acid choline ester., Mel, Aloe polysaccharide is 2:1:1, peony essential oil is obtained after mixing, add sinapic acid choline ester., Mel, Aloe polysaccharide, further can prevent human allergy, and add effect that the peony essential oil after sinapic acid choline ester. also has radioprotective, antibacterial, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 12
With the mixing peony oil of peony essential oil and peony seed oil for raw material, the part by weight of peony essential oil and peony seed oil is that the preparation method of 4:1 peony seed oil adopts common method for cold pressing, peony essential oil preparation process as follows:
(1) extract: pluck fresh peony flower, with fresh Flos Moutan for raw material, in fresh peony flower, add that Herba Portulacae addition is peony petal gross weight 1%, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and its condition of supercritical carbon dioxide supercritical extraction is: pressure 25Mpa, extraction temperature 60 DEG C, separator I pressure 10Mpa, temperature 35 DEG C, separator II pressure 4Mpa, temperature 20 DEG C, extraction time 1.5h; Because inevitably containing residual peony pollen on peony petal, and part population can be irritated to peony pollen, therefore, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned Herba Portulacae also has antioxidation, antidotal effect, makes peony essential oil better act on human body;
The only one week florescence of Flos Moutan, the tender profit of petal, easily mouldy after gathering, not easily preserve peony petal, select fair weather to pluck peony petal, plucking time is 7-10 point in morning, after harvesting, peony petal is placed in container, avoid direct sunlight, because peony petal can dehydration, air-dry in preservation process, original fragrance can volatilize, therefore need to process peony petal as early as possible, within 4 hours preferably after harvesting, carry out extraction process;
(2) distill: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of molecular distillation is:
Feeding temperature 65 DEG C, vapo(u)rizing temperature 120 DEG C, vacuum 50Pa, Paeonia suffruticosa extractum flow 1000ml/h, knifing rotating speed 430r/min, chilling temperature 25 DEG C;
(3) peony essential oil of getting peony seed oil and obtaining after distillation, mix with adjuvant sinapic acid choline ester., Mel, Aloe polysaccharide, the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, the weight ratio of sinapic acid choline ester., Mel, Aloe polysaccharide is 2:1:1, peony essential oil is obtained after mixing, add sinapic acid choline ester., Mel, Aloe polysaccharide, further can prevent human allergy, and adding effect that the peony essential oil after sinapic acid choline ester. also has radioprotective, antibacterial, antiinflammatory, the ratio of peony seed oil and peony essential oil is 1:2.
Remaining making step is with embodiment 2.
Claims (1)
1., containing a preparation method for the skin care oil medicine of peony oil, comprise following step:
Get the peony oil of 30-70 part, add 5-30 part ring five polydimethylsiloxane, be uniformly mixed, add caprylic/capric triglyceride and the butylated hydroxytoluene of 15-40 part again, heating for dissolving below 60 DEG C, is uniformly mixed, and the butylated hydroxytoluene added is the 0.05-0.15% that peony oil weighs; Slowly add 1, the 2-pentanediol of 1-12 part again, be stirred to transparence, add isostearic acid and be uniformly mixed, described isostearic acid is the 0.1-0.3% that peony oil weighs;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil and macadimia nut seed oil again, the 0.01-3% that American Avocado Tree oil is the heavy 0.01-3% of peony oil, Jojoba seed oil is the heavy 0.01-3% of peony oil, white Limnanthes Alba Seed Oil is the heavy 0.01-3% of peony oil, macadimia nut seed oil weighs for peony oil, stir, filter, storage; In described filtration step, adopt 200-500 mesh sieve aperture;
Described peony oil is the mixture of peony essential oil or peony seed oil and peony essential oil;
Peony seed oil is obtained through cold pressing or hot moulding or supercritical carbon dioxide ways and means by seed of Flos Moutan;
The preparation method of peony essential oil is as follows:
(1) extract: pluck fresh peony flower, the at least one in Herba Portulacae, Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), Semen Sinapis is added in fresh peony flower, the gross weight of at least one in described Herba Portulacae, Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), Semen Sinapis or their mixture is the 0.5-2% of peony petal, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of described carbon dioxide supercritical fluid extraction is: pressure 28MPa, extraction temperature 50 DEG C, separator I pressure 15MPa, temperature 55 DEG C, separator II pressure 8 MPa, temperature 20 DEG C, extraction time 2h;
(2) molecular distillation: adopt the method for molecular distillation to extract Paeonia suffruticosa extractum, obtain peony essential oil, its condition of described molecular distillation is: feeding temperature 60 DEG C, vapo(u)rizing temperature 130 DEG C, vacuum 40Pa, Paeonia suffruticosa extractum flow 200mL/h, knifing rotating speed 380r/min, chilling temperature 25 DEG C;
Learn from else's experience the peony essential oil that obtains after distillation, mix with adjuvant, described adjuvant is Aloe polysaccharide and sinapic acid choline ester., and the part by weight of Aloe polysaccharide and sinapic acid choline ester. is 1:1-3, and the gross weight of adjuvant is the 0.2-1.5% of peony essential oil.
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| CN105038946A (en) * | 2015-06-24 | 2015-11-11 | 洛阳国花坊牡丹生物科技有限公司 | Peony essential oil supercritical CO2 extraction method |
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