CN113274326B - Lip balm - Google Patents
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- CN113274326B CN113274326B CN202110577689.4A CN202110577689A CN113274326B CN 113274326 B CN113274326 B CN 113274326B CN 202110577689 A CN202110577689 A CN 202110577689A CN 113274326 B CN113274326 B CN 113274326B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention belongs to the technical field of daily chemical products, and particularly relates to a lip balm. The lip balm comprises the following components: coconut oil, olive oil, shea butter, beeswax, folic acid compounds, peach flower extract, honeysuckle flower extract, chrysanthemum flower extract and safflower extract. The lip balm has the effects of supplementing water, preserving moisture and weakening lip marks, and can improve the immunity to the external dry environment.
Description
Technical Field
The invention belongs to the technical field of daily chemical products, and particularly relates to a lip balm.
Background
Daily application of skin cream to the dry lips has no effect. The lip is required to be moistened, and can be maintained for a long time, and can stay on the surface of the lips without penetrating, namely the lip balm. Although the lip balm cannot be said to be universal, the main components contained in the lip balm are specific to the special requirements of the lip skin, and can provide a barrier for the lips to lock moisture, so that the lips are ruddy and glossy, and the effects of moistening and protecting the lips are achieved. Lip balms are also known as lipsticks, lip sticks, which are in the form of sticks, pencils, creams, etc., but most commonly are in the form of sticks.
The lip balms daily chemical products in the market only have the effects of simple lip wetting and beautifying, and partial lip chapping, peeling, pigment deposition and other adverse reactions can be caused after long-time use, so that discomfort can be caused to the skin; most medical ointments sold in pharmacies generally contain hormone chemical components, and skin inflammatory response can be caused after long-term use; some lipstick-like alternative products are available in the market, and the degree of moistening of lips is insufficient, so that foreign body sensation is easy to generate. Can bring harm to the vast consumers after long-time use.
The lip balm in the prior art is various, for example, chinese patent application CN110101612A discloses that the lip balm raw material comprises, by weight, 20-25 parts of polybutene, 15-20 parts of wheat germ oil, 20-30 parts of triglyceride, 8-13 parts of polyethylene, 1-3 parts of camellia seed oil, 1-5 parts of pentaerythritol ester, 0.01-0.1 part of tocopherol esterified substance, 1-5 parts of diisostearyl malate, 1-5 parts of candelilla wax and 1-5 parts of di-diglycerol polyacyl adipate-2, and the lip balm can effectively improve the problem of thick and greasy feeling during use and effectively lock water.
Chinese patent application CN102793638A discloses a lip balm comprising grease, wax and an additive, wherein the wax is natural animal fat accounting for 22-42% of the mass of the lip balm, the grease is jojoba seed oil accounting for 56-70% of the mass of the lip balm, the additive contains sodium hyaluronate and osmanthus fragrans essence, and the mass percentage of the additive is 2-8% of the lip balm. The moisturizing lip balm disclosed by the invention adopts natural animal fat, can permeate skin, can maintain long-time moisturizing, and meanwhile, sodium hyaluronate in the additive has a good moisturizing effect, and the osmanthus fragrans essence brings a delicate natural hanging flower fragrance.
Disclosure of Invention
In order to overcome the technical problems, the invention provides a lip balm. The lip balm has the effects of supplementing water, preserving moisture and weakening lip marks, and can improve the immunity to the external dry environment.
In order to achieve the above object, the technical scheme provided by the invention is as follows:
a lip balm, comprising the following components: coconut oil, olive oil, shea butter, beeswax, folic acid compounds, peach flower extract, honeysuckle flower extract, chrysanthemum flower extract and safflower extract.
Preferably, the lip balm comprises the following components in parts by weight: 20-40 parts of coconut oil, 25-30 parts of olive oil, 20-30 parts of shea butter, 10-30 parts of beeswax, 0.001-0.05 part of folic acid compounds, 2-8 parts of peach blossom extract, 2-6 parts of honeysuckle flower extract, 2-8 parts of chrysanthemum extract and 2-10 parts of safflower extract.
Preferably, the lip balm comprises the following components in parts by weight: 30 parts of coconut oil, 28 parts of olive oil, 25 parts of shea butter, 20 parts of beeswax, 0.003 part of folic acid compounds, 5 parts of peach blossom extract, 4 parts of honeysuckle flower extract, 5 parts of chrysanthemum extract and 6 parts of safflower extract.
Preferably, the folic acid compounds are one or more of folic acid, leucovorin, L-methyl folic acid, folic acid medicinal salt, folic acid or folic acid medicinal salt active metabolite and substances capable of being metabolized and/or generating folic acid in vivo.
Preferably, the preparation method of the peach blossom extract comprises the following steps:
s1: drying and pulverizing flos persicae, adding petroleum ether, and reflux extracting to obtain petroleum ether extractive solution and residue;
s2: drying the residue, removing petroleum ether, soaking in ethanol, reflux extracting, and filtering to obtain primary filtrate and residue;
s3: reflux extracting the residue with ethanol, and filtering to obtain secondary filtrate;
s4: mixing the primary filtrate and the secondary filtrate, recovering ethanol under reduced pressure, and drying to obtain flos persicae extract.
Preferably, in S1, the mesh number of the pulverization is 20-30 mesh;
preferably, in S1, the weight of the petroleum ether is 6-8 times of the dry weight of the peach blossom.
Preferably, in S1, the temperature of petroleum ether extraction is 40-50 ℃;
preferably, in S1, the reflux extraction time is 2-3 hours.
Preferably, in S2, the ethanol is 6-8 times of the residue mass, the ethanol mass concentration is 60-75%, and the soaking time is 1-1.5h.
Preferably, in S2, the extraction time is 1-1.5h.
Preferably, in S3, the ethanol is used in an amount which is 6-8 times the mass of the filter residue, the mass concentration of the ethanol is 60-75%, and the extraction time is 1-1.5h.
Preferably, the preparation method of the honeysuckle extract comprises the following steps: weighing flos Lonicerae, adding into ethanol water solution, soaking under negative pressure, decocting under heating, and filtering; decolorizing the obtained filtrate, and concentrating to obtain flos Lonicerae extract.
Preferably, the mass concentration of the ethanol aqueous solution is 45-75%, and the dosage is 4-8 times of the mass of the honeysuckle.
Preferably, the negative pressure condition is a pressure of 20-60kpa.
Preferably, the preparation method of the chrysanthemum extract comprises the following steps: crushing chrysanthemum to obtain superfine chrysanthemum powder; mixing flos Chrysanthemi superfine powder with deionized water, heating and stirring for extraction, filtering, and concentrating under reduced pressure to obtain flos Chrysanthemi extract.
Preferably, the heating temperature is that heating to 60-80deg.C for 30-60min, and boiling for 1-2 hr.
Preferably, the preparation method of the safflower extract comprises the following steps:
a: adding safflower into ethanol, leaching at normal temperature, and separating leaching liquor and residues;
b: concentrating the leaching solution at 70-80deg.C, and separating concentrated solution and ethanol;
c: and (c) performing normal-temperature leaching-concentrating cyclic operation on the residues for 1-2 times by using ethanol, mixing the prepared concentrated solution with the concentrated solution obtained in the step (B), and drying to obtain the safflower extract.
Another object of the present invention is to provide a method for preparing the lip balm, comprising the steps of:
(1) Uniformly mixing olive oil, coconut oil and shea butter to obtain mixed oil;
(2) Adding Cera flava, flos persicae extract, flos Lonicerae extract, flos Chrysanthemi extract, carthami flos extract and folic acid compounds into mixed oil, heating to completely melt, dispersing uniformly, defoaming, sterilizing, pouring into lipstick tube while hot, and naturally cooling and solidifying to obtain lip balm.
Preferably, in step (2), the heating temperature is 65-70 ℃.
Compared with the prior art, the invention has the technical advantages that:
(1) The lip balm provided by the invention can supplement folic acid, and most of raw materials adopted by the lip balm are substances rich in moisturizing components, so that the lip balm can effectively supplement water and moisturize the skin of lips, lighten the lips, prevent cheilitis, inhibit bacteria and diminish inflammation.
(2) The lip balm provided by the invention can improve the immunity to the external dry environment. Meanwhile, the lip balm is low in production cost, simple in preparation process and suitable for industrial production.
(3) The peach blossom extract, the honeysuckle flower extract, the chrysanthemum extract and the safflower extract provided by the invention have better synergistic effect, can effectively promote the moisturizing effect, and simultaneously have the effects of inhibiting bacteria and preventing cheilitis.
Detailed Description
The present invention will be described by way of specific examples, to facilitate understanding and grasping of the technical solution of the present invention, but the present invention is not limited thereto. The experimental methods described in the following examples are all conventional methods unless otherwise specified; the reagents and materials, unless otherwise specified, are commercially available.
Example 1
(1) Preparation of peach blossom extract:
s1: drying flos persicae, pulverizing to 20 mesh, adding petroleum ether 8 times the dry weight of flos persicae, and reflux extracting at 40deg.C for 3 hr to obtain petroleum ether extractive solution and residue;
s2: drying the residue to remove petroleum ether, adding 6 times of 75% ethanol, soaking for 1 hr, reflux extracting for 1.5 hr, and filtering to obtain primary filtrate and residue;
s3: reflux-extracting the residue with 6 times of 75% ethanol for 1 hr, and filtering to obtain secondary filtrate;
s4: mixing the primary filtrate and the secondary filtrate, recovering ethanol under reduced pressure, and drying to obtain flos persicae extract.
(2) Preparation of honeysuckle extract:
weighing flos Lonicerae, adding into 8 times of 45% ethanol water solution, soaking under 60kpa condition, decocting for 2 hr, and filtering; decolorizing the obtained filtrate, and concentrating to obtain flos Lonicerae extract.
(3) Preparation of chrysanthemum extract:
crushing chrysanthemum to obtain superfine chrysanthemum powder; mixing flos Chrysanthemi superfine powder with deionized water, stirring, heating to 60deg.C, extracting for 60min, boiling for 1 hr, filtering, and concentrating under reduced pressure to obtain flos Chrysanthemi extract.
(4) Preparation of safflower extract:
a: adding safflower into ethanol, leaching at normal temperature, and separating leaching liquor and residues;
b: concentrating the leaching solution at 80 ℃ to obtain concentrated solution 1;
c: extracting the residue with ethanol at normal temperature, concentrating to obtain concentrated solution 2, mixing concentrated solution 2 with concentrated solution 1, and drying to obtain Carthami flos extract.
Example 2
(1) Preparation of peach blossom extract:
s1: drying flos persicae, pulverizing to 30 mesh, adding petroleum ether 6 times the dry weight of flos persicae, and reflux extracting at 50deg.C for 2 hr to obtain petroleum ether extractive solution and residue;
s2: drying the residue to remove petroleum ether, adding 6 times of 60% ethanol, soaking for 1.5 hr, reflux extracting for 1 hr, and filtering to obtain primary filtrate and residue;
s3: reflux-extracting the filter residue with 6 times of 60% ethanol for 1.5 hr, and filtering to obtain secondary filtrate;
s4: mixing the primary filtrate and the secondary filtrate, recovering ethanol under reduced pressure, and drying to obtain flos persicae extract.
(2) Preparation of honeysuckle extract:
weighing flos Lonicerae, adding into 4 times of 75% ethanol water solution, soaking under 20kpa condition, decocting for 2 hr, and filtering; decolorizing the obtained filtrate, and concentrating to obtain flos Lonicerae extract.
(3) Preparation of chrysanthemum extract:
crushing chrysanthemum to obtain superfine chrysanthemum powder; mixing flos Chrysanthemi superfine powder with deionized water, stirring, heating to 60deg.C, extracting for 30min, boiling for 2 hr, filtering, and concentrating under reduced pressure to obtain flos Chrysanthemi extract.
(4) Preparation of safflower extract:
a: adding safflower into ethanol, leaching at normal temperature, and separating leaching liquor and residues;
b: concentrating the leaching solution at 70 ℃ to obtain concentrated solution 1;
c: and (3) carrying out normal-temperature leaching-concentrating cyclic operation on the residues for 2 times by using ethanol to respectively prepare concentrated solution 2 and concentrated solution 3, mixing the concentrated solution 2 and the concentrated solution 3 with the concentrated solution 1, and drying to obtain the safflower extract.
Example 3
The lip balm comprises the following components in parts by weight: 30 parts of coconut oil, 28 parts of olive oil, 25 parts of shea butter, 20 parts of beeswax, 0.003 part of folic acid, 5 parts of peach blossom extract, 4 parts of honeysuckle flower extract, 5 parts of chrysanthemum extract and 6 parts of safflower extract.
The preparation method of the lip balm comprises the following steps:
(1) Uniformly mixing olive oil, coconut oil and shea butter to obtain mixed oil;
(2) Adding Cera flava, flos persicae extract, flos Lonicerae extract, flos Chrysanthemi extract, carthami flos extract and folic acid into mixed oil, heating at 70deg.C to completely melt, dispersing uniformly, defoaming, sterilizing, pouring into lipstick tube while hot, and naturally cooling and solidifying to obtain lip balm.
Among them, the peach flower extract, the honeysuckle flower extract, the chrysanthemum flower extract and the safflower extract used in this example were all derived from the product of example 1.
Example 4
The lip balm comprises the following components in parts by weight: 20 parts of coconut oil, 25 parts of olive oil, 20 parts of shea butter, 10 parts of beeswax, 0.001 part of L-methyl folic acid, 2 parts of peach blossom extract, 2 parts of honeysuckle flower extract, 2 parts of chrysanthemum extract and 2 parts of safflower extract.
The preparation method of the lip balm comprises the following steps:
(1) Uniformly mixing olive oil, coconut oil and shea butter to obtain mixed oil;
(2) Adding Cera flava, flos persicae extract, flos Lonicerae extract, flos Chrysanthemi extract, carthami flos extract and L-methyl folic acid into mixed oil, heating at 65deg.C to completely melt, dispersing uniformly, defoaming, sterilizing, pouring into lipstick tube while hot, and naturally cooling and solidifying to obtain lip gloss.
Among them, the peach flower extract, the honeysuckle flower extract, the chrysanthemum flower extract and the safflower extract used in this example were all derived from the product of example 2.
Example 5
The lip balm comprises the following components in parts by weight: 40 parts of coconut oil, 30 parts of olive oil, 30 parts of shea butter, 30 parts of beeswax, 0.05 part of leucovorin, 8 parts of peach blossom extract, 6 parts of honeysuckle flower extract, 8 parts of chrysanthemum extract and 10 parts of safflower extract.
The preparation method of the lip balm comprises the following steps:
(1) Uniformly mixing olive oil, coconut oil and shea butter to obtain mixed oil;
(2) Adding Cera flava, flos persicae extract, flos Lonicerae extract, flos Chrysanthemi extract, carthami flos extract and leucovorin into mixed oil, heating at 70deg.C to completely melt, dispersing uniformly, defoaming, sterilizing, pouring into lipstick tube while hot, and naturally cooling and solidifying to obtain lip balm.
Among them, the peach flower extract, the honeysuckle flower extract, the chrysanthemum flower extract and the safflower extract used in this example were all derived from the product of example 1.
Comparative example 1
The only difference compared to example 3 is that the peach flower extract is replaced by the rose flower extract, the rest of the operations being unchanged.
The lip balm comprises the following components in parts by weight: 30 parts of coconut oil, 28 parts of olive oil, 25 parts of shea butter, 20 parts of beeswax, 0.003 part of folic acid, 5 parts of rose extract, 4 parts of honeysuckle extract, 5 parts of chrysanthemum extract and 6 parts of safflower extract.
The procedure of the preparation method of lip gloss is the same as in example 3.
The preparation method of the rose extract is the same as that of the peach blossom extract in the example 1, and the rest extracts are the same as in the example 3.
Comparative example 2
The difference compared with example 3 is only that the chrysanthemum extract is replaced by the honeysuckle extract, and the rest of the operation is unchanged.
The lip balm comprises the following components in parts by weight: 30 parts of coconut oil, 28 parts of olive oil, 25 parts of shea butter, 20 parts of beeswax, 0.003 part of folic acid, 5 parts of peach blossom extract, 9 parts of honeysuckle flower extract and 6 parts of safflower extract.
The procedure of the preparation method of lip gloss is the same as in example 3.
Wherein the source of each extract was the same as in example 3.
Comparative example 3
The only difference compared to example 3 is that the safflower extract is replaced by peach kernel extract.
The lip balm comprises the following components in parts by weight: 30 parts of coconut oil, 28 parts of olive oil, 25 parts of shea butter, 20 parts of beeswax, 0.003 part of folic acid, 5 parts of peach blossom extract, 4 parts of honeysuckle flower extract, 5 parts of chrysanthemum extract and 6 parts of peach kernel extract.
The procedure of the preparation method of lip gloss is the same as in example 3.
The preparation method of the peach kernel extract is the same as that of the safflower extract in the embodiment 1:
a: pulverizing semen Persicae, adding into ethanol, leaching at normal temperature, and separating out leaching solution and residue;
b: concentrating the leaching solution at 80 ℃ to obtain concentrated solution 1;
c: extracting the residue with ethanol at normal temperature, concentrating to obtain concentrated solution 2, mixing concentrated solution 2 and concentrated solution 1, and drying to obtain semen Persicae extract.
The remaining extracts were as in example 3.
Comparative example 4
The only difference compared to example 3 is the preparation of the peach flower extract, the rest of the procedure being unchanged.
Preparation of peach blossom extract:
s1: drying flos persicae, pulverizing to 20 mesh, adding petroleum ether 8 times the dry weight of flos persicae, and reflux extracting at 40deg.C for 3 hr to obtain petroleum ether extractive solution and residue;
s2: drying the residue to remove petroleum ether, adding 12 times of 75% ethanol, soaking for 1 hr, reflux extracting for 3 hr, and filtering to obtain filtrate; recovering ethanol under reduced pressure, and drying to obtain flos persicae extract.
Comparative example 5
The only difference compared with example 3 is that the preparation method of the honeysuckle extract is different, and the rest operation is unchanged.
Preparation of honeysuckle extract:
weighing flos Lonicerae, adding into 8 times of 45% ethanol water solution, soaking under normal pressure, decocting for 2 hr, and filtering; decolorizing the obtained filtrate, and concentrating to obtain flos Lonicerae extract.
Comparative example 6
The only difference compared to example 3 is that the extracts are all from commercial products.
A lip balm was prepared in the same manner as in example 3.
The procedure of the preparation method of lip gloss is the same as in example 3.
Peach blossom extract, honeysuckle flower extract, chrysanthemum flower extract and safflower extract are all from commercial products (western An Yunuo bioengineering limited).
Effect example
1. Moisture retention test
45 women between 25-35 years of age were selected as subjects, and were divided into 9 groups (examples 3-5 and comparative examples 1-6), each group of 5 persons, who were allowed to rest in a stable environment at 20.+ -. 5 ℃ and 50.+ -. 5% relative humidity throughout the test period. At the beginning of the experiment, cleaning lips of a subject, coating a lipstick, measuring 3 times each time by using a Comeometer CM825 measuring instrument produced by Germany, taking an average value (T), and testing the moisture content of skin horny layer of the lips; the average water content (T0) 2h before application, the average water content (T1) 1h after application and the average water content (T4) 4h were recorded separately, and the average water loss rate for each group was calculated. Water loss = (T1-T4)/t1×100%; the smaller the water loss value, the better the lip skin barrier, indicating a better water-locking effect of the product. The results are shown in Table 1.
Table 1 moisturizing data
| Test group | T0(AU) | T1(AU) | T4(AU) | Water loss rate% |
| Example 3 | 50.32 | 81.21 | 73.29 | 9.75 |
| Example 4 | 51.26 | 79.36 | 71.68 | 9.68 |
| Example 5 | 48.67 | 79.41 | 70.25 | 11.54 |
| Comparative example 1 | 53.07 | 61.38 | 49.22 | 19.81 |
| Comparative example 2 | 52.61 | 67.29 | 52.19 | 22.44 |
| Comparative example 3 | 50.22 | 60.58 | 49.37 | 18.50 |
| Comparative example 4 | 51.69 | 73.27 | 61.58 | 15.95 |
| Comparative example 5 | 49.18 | 69.11 | 53.17 | 23.06 |
| Comparative example 6 | 50.67 | 51.23 | 38.69 | 24.48 |
Therefore, the lip balm provided by the invention has a good moisturizing effect, and meanwhile, the composition of raw materials and the preparation method thereof have a certain influence on the moisturizing effect.
2. Antibacterial effect
Will be 1X 10 5 The cfu/g bacterial liquid is evenly coated on a flat plate, and then the lip balms prepared in the embodiment 3-5 and the comparative examples 1-6 are evenly coated on the surface of the flat plate; meanwhile, the culture time was 10min, the number of bacteria surviving (cfu/g) on the plate was measured, and the number of bacteria surviving was compared with the number of bacteria in the original bacterial liquid to obtain a sterilization rate (%), and the results are shown in Table 2.
TABLE 2 antibacterial rate%
Therefore, the lip balm provided by the invention has a good antibacterial effect, and meanwhile, the composition of raw materials and the preparation method thereof have a certain influence on the antibacterial effect.
The foregoing detailed description is directed to one of the possible embodiments of the present invention, which is not intended to limit the scope of the invention, but is to be accorded the full scope of all such equivalents and modifications so as not to depart from the scope of the invention.
Claims (4)
1. The lip balm comprises the following components in parts by weight: 20-40 parts of coconut oil, 25-30 parts of olive oil, 20-30 parts of shea butter, 10-30 parts of beeswax, 0.001-0.05 part of folic acid compounds, 2-8 parts of peach blossom extract, 2-6 parts of honeysuckle flower extract, 2-8 parts of chrysanthemum extract and 2-10 parts of safflower extract;
the preparation method of the peach blossom extract comprises the following steps:
s1: drying and pulverizing flos persicae, adding petroleum ether, and reflux extracting to obtain petroleum ether extractive solution and residue;
s2: drying the residue, removing petroleum ether, soaking in ethanol, reflux extracting, and filtering to obtain primary filtrate and residue;
s3: reflux extracting the residue with ethanol, and filtering to obtain secondary filtrate;
s4: mixing the primary filtrate and the secondary filtrate, recovering ethanol under reduced pressure, and drying to obtain flos persicae extract;
wherein, in S1, the number of the crushed meshes is 20-30 meshes; the weight of the petroleum ether is 6-8 times of the dry weight of the peach blossom, the petroleum ether is extracted at 40-50 ℃, and the reflux extraction time is 2-3h;
s2, the ethanol dosage is 6-8 times of the mass of the medicine residues, the mass concentration of the ethanol is 60-75%, and the soaking time is 1-1.5h; the extraction time is 1-1.5h;
s3, the ethanol consumption is 6-8 times of the mass of the filter residue, the mass concentration of the ethanol is 60-75%, and the extraction time is 1-1.5h;
the preparation method of the honeysuckle extract comprises the following steps: weighing flos Lonicerae, adding into ethanol water solution, soaking under negative pressure, decocting under heating, and filtering; decolorizing the obtained filtrate, and concentrating to obtain flos Lonicerae extract;
wherein the mass concentration of the ethanol aqueous solution is 45-75%, and the dosage is 4-8 times of the mass of the honeysuckle; the negative pressure condition is that the pressure is 20-60kpa;
the preparation method of the chrysanthemum extract comprises the following steps: crushing chrysanthemum to obtain superfine chrysanthemum powder; mixing flos Chrysanthemi superfine powder with deionized water, heating and stirring for extraction, filtering, and concentrating under reduced pressure to obtain flos Chrysanthemi extract;
wherein the heating temperature is that heating to 60-80deg.C for 30-60min, boiling and extracting for 1-2 hr;
the preparation method of the safflower extract comprises the following steps:
a: adding safflower into ethanol, leaching at normal temperature, and separating leaching liquor and residues;
b: concentrating the leaching solution at 70-80deg.C, and separating concentrated solution and ethanol;
c: c, performing normal-temperature leaching-concentrating cyclic operation on the residues for 1-2 times by using ethanol, mixing the prepared concentrated solution with the concentrated solution obtained in the step B, and drying to obtain the safflower extract;
the folic acid compounds are one or more of folic acid, leucovorin, L-methyl folic acid, folic acid medicinal salt, folic acid or folic acid medicinal salt active metabolite and substances capable of being metabolized and/or generating folic acid in vivo.
2. Lip balm according to claim 1, characterized in that it comprises the following components in parts by weight: 30 parts of coconut oil, 28 parts of olive oil, 25 parts of shea butter, 20 parts of beeswax, 0.003 part of folic acid compounds, 5 parts of peach blossom extract, 4 parts of honeysuckle flower extract, 5 parts of chrysanthemum extract and 6 parts of safflower extract.
3. The method of preparing a lip balm according to claim 1, comprising the steps of:
(1) Uniformly mixing olive oil, coconut oil and shea butter to obtain mixed oil;
(2) Adding Cera flava, flos persicae extract, flos Lonicerae extract, flos Chrysanthemi extract, carthami flos extract and folic acid compounds into mixed oil, heating to completely melt, pouring into lipstick tube while it is hot, and naturally cooling and solidifying to obtain the lip balm.
4. The method of preparing a lip balm according to claim 3, wherein in the step (2), the heating temperature is 65-70 ℃.
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| US7695727B2 (en) * | 2006-10-11 | 2010-04-13 | Wyeth Llc | Botanical butter stick lip balm |
| CN106974873A (en) * | 2017-01-06 | 2017-07-25 | 施娜 | It is a series of that there is medicinal efficacy, the coloured Chinese medicine lipstick of health care function |
| CN107811916A (en) * | 2017-11-20 | 2018-03-20 | 南京科技职业学院 | A kind of natural herb moist lip protector |
| CN109091447A (en) * | 2018-10-24 | 2018-12-28 | 王真松 | A kind of moist lip protector |
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| 徐怀德,刘邻渭,李元瑞,刘兴华,李彦萍.几种干花成分分析及玫瑰花饮料加工技术研究.西北农林科技大学学报(自然科学版).2003,(第03期),全文. * |
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