CN107137316A - A kind of stem of noble dendrobium lip gloss and preparation method thereof - Google Patents
A kind of stem of noble dendrobium lip gloss and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/671—Vitamin A; Derivatives thereof, e.g. ester of vitamin A acid, ester of retinol, retinol, retinal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a kind of stem of noble dendrobium lip gloss, it is made up of (parts by weight) following component：20 30 parts of the stem of noble dendrobium, 10 15 parts of peppermint, 5 10 parts of aloe stoste, 58 parts of olive oil, 58 parts of maize germ oil, 10 15 parts of sunflower oil, 12 16 parts of cod-liver oil, 25 parts of vitamin A, 10 13 parts of collagen protein powder, 25 parts of glycerine, 38 parts of triglyceride, 58 parts of beeswax, 57 parts of purified water.Product stem of noble dendrobium lip gloss of the present invention can keep the plump and elasticity of lip, prevent the generation of lip wrinkle, refrigerant, comfortable sense can be brought to lip, with preferable fungistatic effect, edible.
Description
Technical field
The present invention relates to technical field of skin care, more particularly to a kind of stem of noble dendrobium lip gloss and preparation method thereof.
Background technology
Lip belongs to mucosal sites, comprises only a small amount of melanin, is not enough to prevent the injury of sunlight, along with lip regardless of
Some relatively thin and artificial bad habits of grease, cuticula etc. are secreted, may all cause lip peeling occur, dry and cracked or even cheilitis
Symptom.Lip gloss is that one kind is applied to lip, and protection lip is dry and cracked, while increasing the cosmetics of woman charm.At present on the market
Lip gloss mainly focus on beautifying lip and moisten the function of lip, function more single, repair is not obvious, for cheilitis not
Certain therapeutic effect can be played, or even portioned product instead results in lip and occurred due to adding artificial synthesized chemicals
The phenomenons such as quick, decortication.
The content of the invention
For in place of above the deficiencies in the prior art, the present invention provides a kind of stem of noble dendrobium lip gloss, and the stem of noble dendrobium lip gloss can be with
The plump and elasticity of lip is kept, the generation of lip wrinkle is prevented, refrigerant, comfortable sense can be brought to lip, and have
Preferable fungistatic effect.
To solve above technical problem, the technical scheme that the present invention takes is as follows：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：20-30 parts of the stem of noble dendrobium, 10-15 parts of peppermint, aloe is former
5-10 parts of liquid, 5-8 parts of olive oil, 5-8 parts of maize germ oil, 10-15 parts of sunflower oil, 12-16 parts of cod-liver oil, vitamin A 2-
5 parts, 10-13 parts of collagen protein powder, 2-5 parts of glycerine, 3-8 parts of triglyceride, 5-8 parts of beeswax, 5-7 parts of purified water.
It is preferred that, a kind of stem of noble dendrobium lip gloss that the present invention is provided is made up of (parts by weight) following component：20 parts of the stem of noble dendrobium is thin
10 parts of lotus, 5 parts of aloe stoste, 5 parts of olive oil, 8 parts of maize germ oil, 12 parts of sunflower oil, 12 parts of cod-liver oil, vitamin A 5
Part, 10 parts of collagen protein powder, 5 parts of glycerine, 3 parts of triglyceride, 5 parts of beeswax, 5 parts of purified water.
Accordingly, present invention also offers a kind of preparation method of stem of noble dendrobium lip gloss, its preparation method is comprised the steps of：
(1) stem of noble dendrobium of recipe quantity is weighed, is crushed, 200-300 mesh sieves is crossed, obtains Dendrobium, in mass ratio 1:8~10 by powder
End is mixed with absolute ethyl alcohol, extracts 1-2h, and filter residue, in mass ratio 1 are collected in filtering:10~12 mix filter residue with water, add 2-
5% cellulase, keeps 40 DEG C of -50 DEG C of water-bath 0.5-1h, and rise bath temperature is the 95-100 DEG C of enzyme that goes out, and is cooled down, filtering,
Absolute ethyl alcohol extraction 1-2h is added in filtrate, filtering is collected and ethyl acetate and water are added in filter residue, filter residue, and water is collected in extraction
Phase, is concentrated under reduced pressure, freeze-drying, obtains stem of noble dendrobium freeze-dried powder；The peppermint for weighing recipe quantity is crushed, and is crossed 400-500 mesh sieves, is obtained thin
Charged powders, in mass ratio 1:5 mix powder and water, boiling 0.5-1h, and cooling, filtering take filtrate to be freeze-dried, and obtain peppermint jelly
Dry powder；Stem of noble dendrobium freeze-dried powder is mixed with peppermint freeze-dried powder, it is standby.
(2) by fresh aloe vanes cleaning and sterilization, epidermis is pruned, is beaten with pulverizer, the aloe body of paste after mashing
Squeezed, remove solids, take the juice squeezed out to carry out homogeneous, filtering again, aloe stoste is made, it is standby；
(3) collagen protein powder and water of recipe quantity are taken, collagen liquid is obtained after being uniformly mixed, into collagen liquid
Glycerine, the triglyceride of recipe quantity are sequentially added, 60~75 DEG C are heated to, stirring mixing 20-30min is cooled down after stirring
It is standby to room temperature；
(4) aloe stoste, olive oil, maize germ oil, sunflower oil, cod-liver oil, the beeswax of recipe quantity is taken to be well mixed,
Heated in 85-100 thermostat water baths, 30-40min is stirred under 110~130r/m rotating speed, be cooled to 40-45 DEG C, add step
Suddenly the vitamin A of (1), the product of step (3) and recipe quantity, stirs, and pours into lipstick tube, and solidification can be used.
It is preferred that, the stem of noble dendrobium in stem of noble dendrobium lip gloss of the present invention includes HERBA DENDROBII, dendrobium candidum, Dendrobidium huoshanness, horse
One or more in the whip stem of noble dendrobium.
A kind of proportioning mechanism of each component of stem of noble dendrobium lip gloss of the present invention is as follows：
The stem of noble dendrobium：Main active in the stem of noble dendrobium is：Dendrobine, dendrobium polysaccharide, dendramine, nobilonine etc., stem of noble dendrobium tool
There are antibacterial, anti-oxidant, antitumor, raising immunity and protection nerve.
Peppermint：The main active of peppermint is menthol, and peppermint external application plays the role of anti-inflammatory, local anaesthesia, analgesic, antipruritic,
Peppermint has special aromatic odor and cool feeling, can mitigate the sense of discomfort caused by cheilitis.
Aloe：Aloe not only has moisturizing, antibacterial, the effect of anti-inflammatory, while playing sun-proof function, can effectively prevent
Injury of the ultraviolet to lip.
Beeswax：There is the fragrance of honey；Have functions that inducing astrigency, sore, myogenic, wind-dispelling are moisturized and detoxified with blood.In formula
In play a part of bond, healing harelip wound.
Cod-liver oil：Rich in vitamin E and vitamin B2, play a part of anti-oxidant, reparation cuticula, while having moist
The effect of lip.
Olive oil：Rich in abundant monounsaturated fatty acids, i.e. oleic acid and linoleic acid, leukotrienes, also vitamin A, dimension
Raw element B, vitamin D, vitamin E, vitamin K and polyphenoils etc..Because olive oil contains polyphenol and lipopolysaccharide components, so
It is beneficial to keep moisture, eliminates and delay cheilogramma to occur, prevents lip decortication from splitting, smooth, the olive oil for making lip become again
The also function of radiation proof.
Maize germ oil：Contain abundant unrighted acid (based on oleic acid and linoleic acid), vitamin E and Polyphenols
Material, and play the role of good pretty and dazzling skin, it is skin moisturizing, fills indispensable nutriment.
Sunflower oil：Sunflower oil 90% is unrighted acid, and its Linoleic acid accounts for 66% or so, also contains vitamin
A, B, D and E, the nutritional ingredient such as phytosterol, phosphatide, carrotene.The linoleic acid that it contains, is aliphatic acid needed by human, has
Help human development and Physiological effect, for preventing dry skin and scales of skin that peel off hypertrophy from also having positive role.Due in sunflower oil
Also containing reduces the consumption of vitamin A in more vitamin A, E, therefore this formula, or even selection is no longer individually added into dimension
Raw element E.
Vitamin A：With the effect for safeguarding Skin Cell function, skin emolliency can be made delicate, moisten epidermis, promote pole
Property active material release, keep lip it is moist, smooth, flexible.
Collagen protein powder：Collagen has the effect such as pure natural moisturizing, whitening, wrinkle resistant, nti-freckle.Collagen and human body skin
The structure of skin collagen is similar, is that non-soluble fiber shape contains in glycoprotein, molecule rich in a large amount of amino acid and hydrophilic group, has
Certain surface-active and good compatibility, simultaneously because contain substantial amounts of hydroxyl in its molecule, therefore it has fairly good
Moisture-keeping function.
Glycerine：Glycerine can make skin keep soft, and high resilience is not damaged and dried by dust, weather etc..
Triglyceride：The ability of elastic fibers regeneration is improved, improves wrinkle, promotes collagen synthesis and hyaluronic acid
Generation.
Compared with prior art, the beneficial effects of the invention are as follows：Product stem of noble dendrobium lip gloss of the present invention can keep lip
Plump and elasticity, prevents the generation of lip wrinkle, has good therapeutic effect to cheilitis, can be brought to lip refrigerant, easypro
Suitable sense, and harmful chemical substance, environment protection health, edible are free of in product of the present invention.
Embodiment
The invention will now be further described with reference to specific embodiments, advantages of the present invention and feature will be with description and
It is apparent, but the ripple A Hu scopes of the present invention are not limited to following examples.
Embodiment 1
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：
20 parts of HERBA DENDROBII, 10 parts of peppermint, 5 parts of aloe stoste, 5 parts of olive oil, 8 parts of maize germ oil, sunflower oil 12
Part, 12 parts of cod-liver oil, 5 parts of vitamin A, 10 parts of collagen protein powder, 5 parts of glycerine, 3 parts of triglyceride, 5 parts of beeswax, purifying
5 parts of water.
Preparation method is as follows：
(1) HERBA DENDROBII of recipe quantity is weighed, is crushed, 300 mesh sieves is crossed, obtains Dendrobium, in mass ratio 1:10 by powder
Mixed with absolute ethyl alcohol, extract 1h, filter residue, in mass ratio 1 are collected in filtering:10 mix filter residue with water, add 5% fiber
Plain enzyme, keeps 40 DEG C of water-bath 1h, and rise bath temperature is 95 DEG C of enzymes that go out, and is cooled down, filtering, and absolute ethyl alcohol extraction is added in filtrate
2h, filtering is collected and ethyl acetate and water is added in filter residue, filter residue, and extraction is collected aqueous phase, is concentrated under reduced pressure, and is freeze-dried,
Obtain stem of noble dendrobium freeze-dried powder；The peppermint for weighing recipe quantity is crushed, and is crossed 500 mesh sieves, is obtained peppermint powder, in mass ratio 1:5 by powder and water
Mixing, boiling 1h, cooling, filtering take filtrate to be freeze-dried, obtain peppermint freeze-dried powder；Stem of noble dendrobium freeze-dried powder is mixed with peppermint freeze-dried powder
Close, it is standby.
(2) by fresh aloe vanes cleaning and sterilization, epidermis is pruned, is beaten with pulverizer, the aloe body of paste after mashing
Squeezed, remove solids, take the juice squeezed out to carry out homogeneous, filtering again, aloe stoste is made, it is standby；
(3) collagen protein powder and water of recipe quantity are taken, collagen liquid is obtained after being uniformly mixed, into collagen liquid
Glycerine, the triglyceride of recipe quantity are sequentially added, 60 DEG C are heated to, stirring mixing 20min is cooled to room temperature after stirring,
It is standby；
(4) aloe stoste, olive oil, maize germ oil, sunflower oil, cod-liver oil, the beeswax of recipe quantity is taken to be well mixed,
Heated in 100 DEG C of thermostat water baths, 30min is stirred under 130r/m rotating speed, be cooled to 40 DEG C, add step (1), step
(3) product and the vitamin A of recipe quantity, stir, and pour into lipstick tube, and solidification can be used.
Embodiment 2：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：
20 parts of HERBA DENDROBII, 10 parts of stem of Eyeshaped Dendrobium, 15 parts of peppermint, 5 parts of aloe stoste, 8 parts of olive oil, maize germ oil 5
Part, 10 parts of sunflower oil, 12 parts of cod-liver oil, 2 parts of vitamin A, 13 parts of collagen protein powder, 5 parts of glycerine, triglyceride 8
Part, 8 parts of beeswax, 7 parts of purified water.
Preparation method is as follows：
(1) stem of noble dendrobium of recipe quantity is weighed, is crushed, 300 mesh sieves is crossed, obtains Dendrobium, in mass ratio 1:8 by powder with it is anhydrous
Ethanol is mixed, and extracts 1h, and filter residue, in mass ratio 1 are collected in filtering:12 mix filter residue with water, add 5% cellulase, protect
40 DEG C of DEG C of water-bath 1h are held, rise bath temperature is 95 DEG C of enzymes that go out, and is cooled down, filtering, absolute ethyl alcohol extraction 2h, mistake are added in filtrate
Filter, collects and ethyl acetate and water is added in filter residue, filter residue, and extraction is collected aqueous phase, is concentrated under reduced pressure, and is freeze-dried, obtains the stem of noble dendrobium
Freeze-dried powder；The peppermint for weighing recipe quantity is crushed, and is crossed 500 mesh sieves, is obtained peppermint powder, in mass ratio 1:5 mix powder and water, steam
0.5h is boiled, cooling, filtering take filtrate to be freeze-dried, obtain peppermint freeze-dried powder；Stem of noble dendrobium freeze-dried powder is mixed with peppermint freeze-dried powder, it is standby
With.
(2) by fresh aloe vanes cleaning and sterilization, epidermis is pruned, is beaten with pulverizer, the aloe body of paste after mashing
Squeezed, remove solids, take the juice squeezed out to carry out homogeneous, filtering again, aloe stoste is made, it is standby；
(3) collagen protein powder and water of recipe quantity are taken, collagen liquid is obtained after being uniformly mixed, into collagen liquid
Glycerine, the triglyceride of recipe quantity are sequentially added, 75 DEG C are heated to, stirring mixing 30min is cooled to room temperature after stirring,
It is standby；
(4) aloe stoste of recipe quantity is taken, olive oil, maize germ oil, sunflower oil, cod-liver oil, beeswax are well mixed,
Heated in 90 DEG C of thermostat water baths, 40min is stirred under 120r/m rotating speed, be cooled to 45 DEG C, add step (1), step (3)
Product and recipe quantity vitamin A, stir, pour into lipstick tube, solidification can be used.
Embodiment 3：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：
25 parts of dendrobium candidum, 15 parts of peppermint, 10 parts of aloe stoste, 8 parts of olive oil, 5 parts of maize germ oil, sunflower oil 15
Part, 16 parts of cod-liver oil, 2 parts of vitamin A, 13 parts of collagen protein powder, 2 parts of glycerine, 5 parts of triglyceride, 5 parts of beeswax, purifying
5 parts of water.
Preparation method is as follows：
(1) stem of noble dendrobium of recipe quantity is weighed, is crushed, 300 mesh sieves is crossed, obtains Dendrobium, in mass ratio 1:8 by powder with it is anhydrous
Ethanol is mixed, and extracts 2h, and filter residue, in mass ratio 1 are collected in filtering:12 mix filter residue with water, add 2% cellulase, protect
50 DEG C of water-bath 0.5h are held, rise bath temperature is 100 DEG C of enzymes that go out, and is cooled down, filtering, absolute ethyl alcohol extraction 1h are added in filtrate,
Filtering, collects and ethyl acetate and water is added in filter residue, filter residue, and extraction is collected aqueous phase, is concentrated under reduced pressure, and is freeze-dried, obtains stone
Dry measure used in former times freeze-dried powder；The peppermint for weighing recipe quantity is crushed, and is crossed 400 mesh sieves, is obtained peppermint powder, in mass ratio 1:5 mix powder and water,
Boiling 0.5h, cooling, filtering, takes filtrate to be freeze-dried, obtains peppermint freeze-dried powder；Stem of noble dendrobium freeze-dried powder is mixed with peppermint freeze-dried powder,
It is standby.
(2) by fresh aloe vanes cleaning and sterilization, epidermis is pruned, is beaten with pulverizer, the aloe body of paste after mashing
Squeezed, remove solids, take the juice squeezed out to carry out homogeneous, filtering again, aloe stoste is made, it is standby；
(3) collagen protein powder and water of recipe quantity are taken, collagen liquid is obtained after being uniformly mixed, into collagen liquid
Glycerine, the triglyceride of recipe quantity are sequentially added, 75 DEG C are heated to, stirring mixing 30min is cooled to room temperature after stirring,
It is standby；
(4) aloe stoste, olive oil, maize germ oil, sunflower oil, cod-liver oil, the beeswax of recipe quantity is taken to be well mixed,
Heated in 85 DEG C of thermostat water baths, 30min is stirred under 110r/m rotating speed, be cooled to 45 DEG C, add step (1), step (3)
Product and recipe quantity vitamin A, stir, pour into lipstick tube, solidification can be used.
Embodiment 4：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：
25 parts of Dendrobidium huoshanness, 15 parts of peppermint, 10 parts of aloe stoste, 5 parts of olive oil, 5 parts of maize germ oil, sunflower oil
10-15 parts, 12 parts of cod-liver oil, 3-Hydroxyretinol part, 10 parts of collagen protein powder, 2 parts of glycerine, 5 parts of triglyceride, 5 parts of beeswax,
7 parts of purified water.
Preparation method is as follows：
(1) stem of noble dendrobium of recipe quantity is weighed, is crushed, 250 mesh sieves is crossed, obtains Dendrobium, in mass ratio 1:8 by powder with it is anhydrous
Ethanol is mixed, and extracts 1.5h, and filter residue, in mass ratio 1 are collected in filtering:10~12 mix filter residue with water, add 3% fiber
Plain enzyme, keeps 45 DEG C of water-bath 1h, and rise bath temperature is 95 DEG C of enzymes that go out, and is cooled down, filtering, and absolute ethyl alcohol extraction is added in filtrate
1h, filtering is collected and ethyl acetate and water is added in filter residue, filter residue, and extraction is collected aqueous phase, is concentrated under reduced pressure, and is freeze-dried,
Obtain stem of noble dendrobium freeze-dried powder；The peppermint for weighing recipe quantity is crushed, and is crossed 500 mesh sieves, is obtained peppermint powder, in mass ratio 1:5 by powder and water
Mixing, boiling 0.5h, cooling, filtering take filtrate to be freeze-dried, obtain peppermint freeze-dried powder；By stem of noble dendrobium freeze-dried powder and peppermint freeze-dried powder
Mixing, it is standby.
(2) by fresh aloe vanes cleaning and sterilization, epidermis is pruned, is beaten with pulverizer, the aloe body of paste after mashing
Squeezed, remove solids, take the juice squeezed out to carry out homogeneous, filtering again, aloe stoste is made, it is standby；
(3) collagen protein powder and water of recipe quantity are taken, collagen liquid is obtained after being uniformly mixed, into collagen liquid
Glycerine, the triglyceride of recipe quantity are sequentially added, 70 DEG C are heated to, stirring mixing 20-30min is cooled to room after stirring
Temperature, it is standby；
(4) aloe stoste, olive oil, maize germ oil, sunflower oil, cod-liver oil, the beeswax of recipe quantity is taken to be well mixed,
Heated in 90 DEG C of thermostat water baths, 30-40min is stirred under 120r/m rotating speed, be cooled to 40 DEG C, add step (1), step
(3) product and the vitamin A of recipe quantity, stir, and pour into lipstick tube, and solidification can be used.
Comparative example 1：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：10 parts of HERBA DENDROBII, 4 parts of peppermint, aloe stoste 2
Part, 2 parts of olive oil, 4 parts of maize germ oil, 7 parts of sunflower oil, 10 parts of cod-liver oil, 1 part of vitamin A, 6 parts of collagen protein powder,
1 part of glycerine, 2 parts of triglyceride, 3 parts of beeswax, 2 parts of purified water.
Preparation method：It is same as Example 1.
Comparative example 2：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：35 parts of HERBA DENDROBII, 20 parts of peppermint, aloe stoste
17 parts, 10 parts of olive oil, 17 parts of maize germ oil, 20 parts of sunflower oil, 22 parts of cod-liver oil, 14 parts of vitamin A, collagen
14 parts of powder, 6 parts of glycerine, 15 parts of triglyceride, 10 parts of beeswax, 28 parts of purified water.
Preparation method：It is same as Example 1.
Comparative example 3：
A kind of stem of noble dendrobium lip gloss, is made up of (parts by weight) following component：It is same as Example 1.
Preparation method：
The olive oil of heating recipe quantity, maize germ oil, sunflower oil, cod-liver oil, purified water, sequentially add recipe quantity
The stem of noble dendrobium, peppermint, aloe stoste, decoct it is withered after pull the dregs of a decoction out, add beeswax, stirred evenly after melting, cross 250~300 mesh dusting covers, cooling
To 50 DEG C~60 DEG C, vitamin A, collagen protein powder, 2-5 parts of glycerine, triglyceride are added, stirs, obtains finished product.
Comparative example 4：
A kind of lip gloss, is made up of (parts by weight) following component：
(stem of noble dendrobium replaces with the root of Dahurain angelica, and peppermint replaces with rhodiola root, and triglyceride replaces with lactic acid tetradecane base ester, beeswax
Replace with Brazil wax).15 parts of the root of Dahurain angelica, 10 parts of rhodiola root, 8 parts of butter fruit, 5 parts of olive oil, 10 parts of maize germ oil, sunflower
12 parts of seed oil, 5 parts of cod-liver oil, 6 parts of vitamin A, 8 parts of collagen protein powder, 7 parts of glycerine, 3 parts of lactic acid tetradecane base ester, Brazil
5 parts of palm wax, 7 parts of purified water.
Preparation method：It is same as Example 1.
Experimental example 1：Organoleptic indicator determines
Above-described embodiment 1-4 and comparative example 1-4 sample are taken, its outward appearance, color and luster, odor type (the results are shown in Table 1) are investigated respectively.
The organoleptic indicator's measurement result of table 1
According to above measurement result, the sample of embodiment 1 to embodiment 4 is on outward appearance, color and luster and odor type than comparative example 1
Show excellent to comparative example 4；Comparative example 1 and comparative example 2 use the preparation method of the present invention, but the content and the present invention of each component
Difference, outward appearance difference more of the present invention, color and luster and odor type substantially conform to regulation, and particularly the sample of comparative example 2 is because of liquid component content
Larger, sample setting time is longer, is unfavorable for industrialization；Comparative example 3 is prescription of the present invention, but employs traditional preparation side
Method, its rough surface has stomata, and color and luster and odor type are against regulation；The prescription of comparative example 4 is different from the present invention, preparation method and sheet
Invention is identical, and as a result its outward appearance, color and luster, odor type are undesirable.The smooth pore-free of product surface of the present invention, color and luster, odor type
Meet regulation.
Test example 2：Microbial Challenge is tested
Experimental method：
Experimental strain includes staphylococcus aureus, Pseudomonas aeruginosa, Escherichia coli, Candida albicans, black-koji mould.Experiment
Preceding that each bacterium is inoculated in suitable culture medium, incubated 48 hours of 37 DEG C of bacterium, incubated 72 hours of 28 DEG C of mould is chosen
Select typical bacterium colony that certain density bacterium and mould suspension are made in the culture medium of sterilizing.
Embodiment 1 is weighed to the sample of embodiment 4, comparative example 1 to each 100g of sample of comparative example 4, in the container for adding sterilizing,
Mixed cell suspension is added, is fully mixed.Every gram of sample is 5 × 10 containing amount of bacteria6CFU/g or CFU/ml, amount containing mould be 3 ×
104CFU/g or CFU/ml.It is subsequently placed at 28 DEG C.Connect bacterium 0,7,14,21,28 days sampling analyses：Accurately weigh 10g samples
Product, are added in the conical flask containing glass pellet and 90ml sterile salines, and fully shaking is mixed, and this suspension is 1：10 dilutions
Liquid；Then 1 is pressed with physiological saline again：10 dilute successively.By bacteria containing amount in flat board tilt-pour process count samples.
Criterion：
If plus after bacterium 7 days survival bacterium amount in 100CFU/g (CFU/mL) below, 0CFU/g (CFU/ were all down in 28 days
ML), then it can be considered that antiseptic effect is outstanding, tested by challenging；If bacterium amount of being survived at the 7th day is in 1000CFU/g (CFU/
ML) below, then it is considered as and scrapes；If bacterium amount of being survived at 7 days is in more than 1000CFU/g (CFU/mL), then it is assumed that do not have
Antiseptic effect.
Table 2：Microbial Challenge experimental result (bacterium) unit：CFU/g
Table 3：Microbial Challenge experimental result (fungi) unit：CFU/g
Test result indicates that：Embodiment 1 to embodiment 4 sample from the 7th day, the survival bacterium amount in sample<10CFU/g
(ml), illustrate that inventive samples have the inhibitory or killing effect of extra-heavy to microorganism, tested by challenging, product is being produced, preserves and made
Used time is not easy microbial contamination very much.Comparative example 1 to comparative example 4 sample at the 28th day, survival bacterium amount exists in sample
102CFU/g(ml)-103CFU/g (ml), illustrates that comparative example 1 is poor to the fungistatic effect of the sample of comparative example 4；In the prescription of comparative example 1
Each component content is reduced, and the reduction that particularly stem of noble dendrobium, aloe etc. have the component content of bactericidal action causes the sample of comparative example 1
Antibacterial effect is deteriorated；The reason for bactericidal action of comparative example 2 is reduced be probably in prescription nutritional ingredient cross Sheng, moisture is more, has
Beneficial to the growth with bacterium, fungi.The preparation method refined enough without use of the sample of comparative example 3, it is impossible to play in sample
Main active component；The sample of comparative example 4 substituted for the main active of the present invention, and the prescription can not play good sterilization
Effect.
It with the addition of the traditional Chinese medicine ingredients such as the stem of noble dendrobium, peppermint, aloe in product prescription of the present invention, the stem of noble dendrobium has antibacterial, anti-oxidant, anti-
Tumour, improve immunity and the protection multiple efficacies such as nerve, peppermint plays the role of anti-inflammatory, local anaesthesia, analgesic, antipruritic, has simultaneously
Special aromatic odor and cool feeling, can mitigate the sense of discomfort caused by cheilitis.Aloe not only has moisturizing, antibacterial, anti-inflammatory
Effect, while playing sun-proof function, can effectively prevent injury of the ultraviolet to lip.These traditional Chinese medicine ingredients and other components
Between there is certain synergistic function so that product of the present invention not only has very high fungistatic effect, and can give lip
Bring refrigerant, comfortable sense in portion.
In the preparation technology of product of the present invention, the stem of noble dendrobium and the active component of peppermint are carried out by process for refining in step (1)
Extract, the stem of noble dendrobium and peppermint is played maximum effect in this prescription；Aloe stoste, step is made using simple process in step (2)
(3) collagen protein powder and glycerine, triglyceride are further prepared into viscous fluid, the use of the viscous fluid can make this
Invention product keeps continuing simple and elegant good odor type；Step (4) sets optimised process step and parameter, passes through the step and parameter
Obtained lipstick has good color and luster, outward appearance smoothly fine and smooth, and do not fray skin, with good moisture-keeping function.
The smooth fine and smooth pore-free of product appearance obtained by prescription of the present invention and preparation technology, odor type and color and luster bacterium meet
Relevant regulations, can keep the plump and elasticity of lip, prevent the generation of lip wrinkle, can be brought to lip refrigerant, comfortable
Sense, with preferable antibacterial, edible.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
God is with principle, and any modification, equivalent substitution and improvements done etc. should be included within the scope of protection of the invention.
Claims (4)
1. a kind of stem of noble dendrobium lip gloss, it is characterised in that be made up of (parts by weight) following component：20-30 parts of the stem of noble dendrobium, peppermint 10-15
Part, 5-10 parts of aloe stoste, 5-8 parts of olive oil, 5-8 parts of maize germ oil, 10-15 parts of sunflower oil, 12-16 parts of cod-liver oil,
2-5 parts of vitamin A, 10-13 parts of collagen protein powder, 2-5 parts of glycerine, 3-8 parts of triglyceride, 5-8 parts of beeswax, purified water
5-7 parts.
2. a kind of stem of noble dendrobium lip gloss according to claim 1, it is characterised in that be made up of (parts by weight) following component：Stone
20 parts of dry measure used in former times, 10 parts of peppermint, 5 parts of aloe stoste, 5 parts of olive oil, 8 parts of maize germ oil, 12 parts of sunflower oil, 12 parts of cod-liver oil,
5 parts of vitamin A, 10 parts of collagen protein powder, 5 parts of glycerine, 3 parts of triglyceride, 5 parts of beeswax, 5 parts of purified water.
3. a kind of stem of noble dendrobium lip gloss according to claim any one of 1-2, it is characterised in that its preparation method is comprising following
Step：
(1) stem of noble dendrobium of recipe quantity is weighed, is crushed, 200-300 mesh sieves is crossed, obtains Dendrobium, in mass ratio 1:8~10 by powder with
Absolute ethyl alcohol is mixed, and extracts 1-2h, and filter residue, in mass ratio 1 are collected in filtering:10~12 mix filter residue with water, add 2-5%
Cellulase, keep 40 DEG C of -50 DEG C of water-bath 0.5-1h, rise bath temperature is 95-100 DEG C of enzyme that goes out, and is cooled down, filtering, in filter
Absolute ethyl alcohol extraction 1-2h is added in liquid, filtering is collected and ethyl acetate and water are added in filter residue, filter residue, and aqueous phase is collected in extraction,
It is concentrated under reduced pressure, is freeze-dried, obtains stem of noble dendrobium freeze-dried powder；The peppermint for weighing recipe quantity is crushed, and is crossed 400-500 mesh sieves, is obtained peppermint
Powder, in mass ratio 1:5 mix powder and water, boiling 0.5-1h, and cooling, filtering take filtrate to be freeze-dried, and obtain peppermint and freeze
Powder；Stem of noble dendrobium freeze-dried powder is mixed with peppermint freeze-dried powder, it is standby；
(2) by fresh aloe vanes cleaning and sterilization, epidermis is pruned, is beaten with pulverizer, the aloe body of paste after mashing is carried out
Squeezing, removes solids, takes the juice squeezed out to carry out homogeneous, filtering again, and aloe stoste is made, standby；
(3) collagen protein powder and water of recipe quantity are taken, collagen liquid is obtained after being uniformly mixed, into collagen liquid successively
Glycerine, the triglyceride of recipe quantity are added, 60~75 DEG C are heated to, stirring mixing 20-30min is cooled to room after stirring
Temperature, it is standby；
(4) aloe stoste, olive oil, maize germ oil, sunflower oil, cod-liver oil, the beeswax of recipe quantity is taken to be well mixed, 85-
Heated in 100 DEG C of thermostat water baths, 30-40min is stirred under 110~130r/m rotating speed, be cooled to 40-45 DEG C, add step
Suddenly the vitamin A of (1), the product of step (3) and recipe quantity, stirs, and pours into lipstick tube, and solidification can be used.
4. a kind of stem of noble dendrobium lip gloss according to claim any one of 1-3, it is characterised in that the stem of noble dendrobium includes golden hairpin stone
One or more in dry measure used in former times, dendrobium candidum, Dendrobidium huoshanness, stem of Eyeshaped Dendrobium.
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| CN111297784A (en) * | 2019-12-19 | 2020-06-19 | 中国农业科学院农产品加工研究所 | Natural lip balm containing dendrobe components and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107982164A (en) * | 2017-11-10 | 2018-05-04 | 浙江工业大学 | A kind of pure natural lip preparation containing dendrobium candidum ultrafine powder and preparation method thereof |
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| CN107137316B (en) | 2021-02-26 |
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