CN110585074B - Application of rose essential oil balm in cosmetics - Google Patents
Application of rose essential oil balm in cosmetics Download PDFInfo
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- CN110585074B CN110585074B CN201911006626.2A CN201911006626A CN110585074B CN 110585074 B CN110585074 B CN 110585074B CN 201911006626 A CN201911006626 A CN 201911006626A CN 110585074 B CN110585074 B CN 110585074B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
Abstract
The invention provides application of rose essential oil balm in cosmetics, belonging to the technical field of cosmetics. The application of the rose essential oil balm in cosmetics; the preparation method of the rose essential oil balm comprises the following steps: fresh rose flowers and extraction solvent were mixed in a 1 g: mixing 1-3 ml of the rose essential oil and the rose essential oil, performing subcritical extraction under a dark condition, collecting extract liquor, and removing an extraction solvent in the extract liquor to obtain the rose essential oil balm. The invention adopts the rose essential oil balm to replace rose essential oil to prepare the cosmetics, can effectively reduce the production cost of the cosmetics and simultaneously play the skin care role of the rose essential oil. The cosmetic containing the rose essential oil balm has the effects of mild nourishing, repairing and moisturizing the skin after long-term use, and has no toxic or side effect.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to application of rose essential oil balm in cosmetics.
Background
The rose is a shrub formed by upright fallen leaves of Rosa in Rosaceae, has bright color, pleasant fragrance and high oil content, is an important special economic plant in China, and is one of important ornamental and production dual-purpose flowers in the world. It can be enjoyed by people, and is also an important raw material for precious traditional Chinese medicinal materials, food industry, spice industry and the like. Modern pharmacological technical analysis shows that the rose contains abundant volatile oil, various phenols, phenethyl alcohol, benzyl alcohol, nerol, organic acid, pigment and the like, and has the effects of oxidation resistance, inflammation resistance, convergence, cleanness and the like. The rose can be directly used as spice and can be used as additive in skin care products such as facial cleanser, hand cream, skin lotion and the like.
The rose essential oil is rich in aromatic compounds, has strong fragrance and good permeability, can stimulate epidermal cell metabolism and a human nervous system, and has good moistening and relieving effects. The rose water is rich in phenethyl alcohol, and compounds such as flavonoid, mineral substances and the like are also contained, so that the rose water has the effects of improving skin color, regulating water-oil balance and enhancing skin vitality. Meanwhile, researches prove that the rose water can inhibit bacteria and diminish inflammation, and can be compounded with other components to prepare the preservative. The rose essential oil has excellent permeability and good fusion, stimulates the metabolism of epidermal cells and activates the regeneration of the epidermal cells; on the other hand, the medicine can stimulate the nervous system of a human body, the fragrance enters the brain from the olfactory nervous system, and the anterior lobe of the brain is stimulated to secrete two hormones, namely the caffeine and the enkephalin, so that the human body presents the optimal state; in addition, the rose essential oil can inhibit oxygen free radical activity, prevent pigmentation, and regulate skin internal environment.
At present, the rose cosmetics in the market are mostly prepared from rose essential oil or rose hydrosol as raw materials, but the cost for preparing the rose cosmetics is high due to the high production cost of the rose essential oil, so that the selection of consumers is limited.
Disclosure of Invention
In view of the above, the present invention aims to provide an application of a rose essential oil balm in cosmetics, which can reduce the cost of the prepared cosmetics and has the same skin care effect as the rose essential oil cosmetics.
The invention provides application of rose essential oil balm in cosmetics; the preparation method of the rose essential oil balm comprises the following steps:
fresh rose flowers and extraction solvent were mixed in a 1 g: mixing 1-3 ml of the rose essential oil and the rose essential oil, performing subcritical extraction under a dark condition, collecting extract liquor, and removing an extraction solvent in the extract liquor to obtain the rose essential oil balm.
Preferably, the extraction solvent is one of propane, butane and tetrafluoroethane.
Preferably, the temperature of the subcritical extraction is 40-50 ℃, the pressure of the subcritical extraction is 0.40-0.50 MPa, the extraction times of the subcritical extraction are 2-4 times, and the time of each extraction is 30-60 min.
Preferably, the cosmetic comprises rose scent facial cleanser, rose repairing moisturizing emulsion and the like.
Preferably, the rose repairing moisturizing emulsion comprises the following components in parts by weight: 1-3 parts of squalane, 1-3 parts of propylene glycol, 3-5 parts of olive oil, 3-5 parts of tocopherol, 3-5 parts of hyaluronic acid, 1-3 parts of an amino acid humectant, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol.
Preferably, the rose-fragrance facial cleanser comprises the following components in parts by weight: 1-3 parts of glycerin, 0.5-1 part of propylene glycol, 0.3-0.5 part of lauric acid, 0.3-0.3 part of polyethylene glycol-1500.1, 0.1-0.5 part of glycerol stearate, 1-2 parts of potassium cocoyl glycinate, 3-5 parts of aloe leaf extract, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol.
The invention provides a rose repairing and moisturizing emulsion which comprises the following components in parts by weight: 1-3 parts of squalane, 1-3 parts of propylene glycol, 3-5 parts of olive oil, 3-5 parts of tocopherol, 3-5 parts of hyaluronic acid, 1-3 parts of an amino acid humectant, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol; the preparation method of the rose essential oil balm is the preparation method of the rose essential oil balm in the application.
The invention provides application of rose essential oil balm in cosmetics, and the rose essential oil balm is used for replacing rose essential oil to prepare the cosmetics, so that the production cost of the cosmetics can be effectively reduced, and the skin care effect of the rose essential oil can be exerted. Experiments prove that the rose essential oil balm prepared by the invention has the special fragrance and taste of rose, the fragrance of the rose essential oil balm is closer to the fragrance of fresh flowers than the fragrance of rose essential oil, but the fragrance of the rose essential oil does not drift. GC-MS detection and analysis show that the rose essential oil balm has low lipid content, 10-30% of lipid content and 50-60% of essential oil content, the main components of the rose essential oil balm are citronellol, geraniol, linalool, phenethyl alcohol, farnesol, nerol, alkane compounds and the like, the rose essential oil balm has the quality superior to that of the traditional rose extract, and the rose essential oil balm has the effects of improving skin color, regulating water-oil balance and enhancing skin vitality, and can also effectively inhibit oxygen radical activity, prevent pigment deposition and regulate and control the internal environment of skin.
The invention provides a rose repairing and moisturizing emulsion, which adopts a scientific and technological moisturizing formula, is rich in nutrient components, and hyaluronic acid and an amino acid moisturizing agent which are fully moisturized are matched with rose essential oil balm and rose hydrosol, so that the rose repairing and moisturizing emulsion can be quickly absorbed by skin, moisturize the skin, relieve the dryness of the skin, supplement the nutrient and moisturizing components of the skin, increase the elasticity of the skin, tighten the skin and enable the skin to be glossy and full of vitality. Meanwhile, the rose repairing moisturizing emulsion provided by the invention has the effects of mild nourishing, repairing, moisturizing and moistening the skin after long-term use, and has no toxic or side effect.
Detailed Description
The invention provides application of rose essential oil balm in cosmetics; the preparation method of the rose essential oil balm comprises the following steps: fresh rose flowers and extraction solvent were mixed in a 1 g: mixing 1-3 ml of the rose essential oil and the rose essential oil, performing subcritical extraction under a dark condition, collecting extract liquor, and removing an extraction solvent in the extract liquor to obtain the rose essential oil balm.
In the present invention, the extraction solvent is preferably one of propane, butane and tetrafluoroethane. The temperature of the subcritical extraction is preferably 40-50 ℃, and more preferably 45 ℃. The pressure of the subcritical extraction is preferably 0.40-0.50 MPa, and more preferably 0.45 MPa. The extraction frequency of the subcritical extraction is preferably 2-4 times, and the time of each extraction is preferably 30-60 min, and more preferably 40-50 min. The apparatus for subcritical extraction is not particularly limited in the present invention, and a subcritical extraction method well known in the art may be employed. 100g of rose essential oil balsam is dissolved in 200 ml of hexane, the obtained hexane solution is subjected to alkaline alumina column chromatography and washed by hexane to separate out all rose wax, the wax content of the rose essential oil balsam is found to be low, the wax content is about 10-30 percent and is far lower than that of the rose extract prepared by the traditional process by 40-60 percent, and no waste water is generated in the whole production process of the rose essential oil balsam.
In the present invention, the cosmetic preferably includes a rose scent type cleansing milk or a rose repairing moisturizing lotion, etc.
In the invention, the rose repairing and moisturizing emulsion preferably comprises the following components in parts by weight: 1-3 parts of squalane, 1-3 parts of propylene glycol, 3-5 parts of olive oil, 3-5 parts of tocopherol, 3-5 parts of hyaluronic acid, 1-3 parts of an amino acid humectant, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol; more preferably comprises the following components in parts by weight: 2 parts of squalane, 2 parts of propylene glycol, 4 parts of olive oil, 4 parts of tocopherol, 4 parts of hyaluronic acid, 2 parts of an amino acid humectant, 15 parts of rose essential oil balm and 30 parts of rose hydrosol. The sources of the components in the rose repairing moisturizing emulsion are not particularly limited in the invention, and the sources well known in the field can be adopted. The preparation method of the rose repairing and moisturizing emulsion preferably comprises the steps of mixing and stirring the components in parts by weight, carrying out ultrasonic homogenization, sterilizing and canning to obtain the rose moisturizing emulsion. The mixing and stirring conditions are preferably 50-60 ℃ and the temperature is kept for 10-30 min. The homogenizing method is preferably to homogenize on a homogenizer for 3-10 min. The method of sterilization and filling is not particularly limited in the present invention, and a method known in the art may be used.
In the invention, the rose-fragrance facial cleanser comprises the following components in parts by weight: 1-3 parts of glycerin, 0.5-1 part of propylene glycol, 0.3-0.5 part of lauric acid, 0.3-0.3 part of polyethylene glycol-1500.1, 0.1-0.5 part of glycerol stearate, 1-2 parts of potassium cocoyl glycinate, 3-5 parts of aloe leaf extract, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol. The preparation method of the rose scent facial cleanser is not particularly limited, and the preparation method of the rose restoring and moisturizing emulsion is adopted. The rose fragrance type facial cleanser can effectively remove oil stains and moisten facial skin.
The invention provides a rose repairing and moisturizing emulsion which comprises the following components in parts by weight: 1-3 parts of squalane, 1-3 parts of propylene glycol, 3-5 parts of olive oil, 3-5 parts of tocopherol, 3-5 parts of hyaluronic acid, 1-3 parts of an amino acid humectant, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol; the preparation method of the rose essential oil balm is the preparation method of the rose essential oil balm in the application.
In the present invention, the preparation method of the rose repairing moisturizing emulsion is the same as the preparation method of the rose repairing moisturizing emulsion described above, and is not described herein again. The application method of the rose repairing and moisturizing emulsion is characterized in that a proper amount of rose repairing and moisturizing emulsion is uniformly coated on clean skin. The rose repairing and moisturizing emulsion can be rapidly absorbed by skin, moisturizes the skin, relieves the dryness of the skin, supplements skin nutrition and moisturizing components, increases the elasticity of the skin, tightens the skin and enables the skin to be glossy and full of vitality. The skin care cream has the effects of mild nourishing, repairing, moisturizing and moistening the skin after long-term use, and has no toxic or side effect.
The following examples are provided to illustrate the use of the rose essential oil balm of the present invention in cosmetics, but they should not be construed as limiting the scope of the present invention.
Example 1
1. A production method of rose essential oil balm comprises the following steps:
5000g of fresh rose flowers are placed in a subcritical extraction tank, and the weight ratio of the fresh rose flowers to the subcritical extraction tank is 1 kg: mixing 3L of the mixture with liquid propane, and performing subcritical extraction for 40min for 4 times at 45 deg.C under 0.45MPa in dark condition; after the subcritical extraction is finished, extracting an extract liquid; evaporating and desolventizing the extract liquor, compressing and liquefying the evaporated gas solvent by a diaphragm compressor, and then recovering the solvent; and desolventizing the extract to obtain 1175.8g of rose essential oil balm with the extraction rate of 23.52%. 100g of rose essential oil balm was dissolved in 200 ml of hexane, and the resultant hexane solution was subjected to column chromatography using basic alumina and washed with hexane to separate 15.28 g of total rose wax, and the wax content of the rose essential oil balm was found to be low, about 15.28%.
2. Preparation method of rose repairing moisturizing lotion
The following ingredients were accurately weighed: 1g of squalane, 3g of propylene glycol, 3g of olive oil, 5g of tocopherol, 3g of hyaluronic acid, 3g of amino acid humectant, 10g of rose essential oil balm prepared by the method and 40g of rose hydrosol. Mixing and stirring the components, and preserving heat for 10 minutes at the temperature of 50 ℃; and then carrying out ultrasonic homogenization for 3min, sterilizing and canning to obtain the rose moisturizing emulsion.
3. Preparation method of rose fragrance facial cleanser
The following ingredients were accurately weighed: 1g of glycerin, 0.5g of propylene glycol, 0.3g of lauric acid, 0.1g of polyethylene glycol-1500.1 g of glyceryl stearate, 1g of potassium cocoyl glycinate, 3g of aloe leaf extract, 10g of the rose essential oil balm prepared above and 40g of rose hydrosol. Mixing the above materials, stirring, and keeping the temperature at 50 deg.C for 10 min; and then carrying out ultrasonic homogenization for 3min, sterilizing and canning to obtain the rose fragrance facial cleanser.
Comparative example 1
1. A production method of rose essential oil balm comprises the following steps:
5000g of fresh rose flowers are placed in a subcritical extraction tank, and the weight ratio of the fresh rose flowers to the subcritical extraction tank is 1 kg: mixing 3L of the mixture with liquid propane, and performing subcritical extraction for 40min under the conditions of extraction temperature of 30 ℃, extraction pressure of 0.3MPa and light shielding for 4 times; after the subcritical extraction is finished, extracting an extract liquid; evaporating and desolventizing the extract liquor, compressing and liquefying the evaporated gas solvent by a diaphragm compressor, and then recovering the solvent; and after the extraction liquid is desolventized, 853.2g of rose essential oil balm is obtained, and the extraction rate is 17.06%. 100g of rose essential oil balm was dissolved in 200 ml of hexane, and the resultant hexane solution was subjected to column chromatography using basic alumina and washed with hexane to separate 38.95 g of total rose wax, and the wax content of the rose essential oil balm was found to be about 38.95%.
2. Preparation method of rose repairing moisturizing lotion
The following ingredients were accurately weighed: 1g of squalane, 3g of propylene glycol, 3g of olive oil, 5g of tocopherol, 3g of hyaluronic acid, 3g of amino acid humectant, 10g of rose essential oil balm prepared by the method and 40g of rose hydrosol. Mixing and stirring the components, and preserving heat for 10 minutes at the temperature of 50 ℃; and then carrying out ultrasonic homogenization for 3min, sterilizing and canning to obtain the rose moisturizing emulsion.
3. Preparation method of rose fragrance facial cleanser
The following ingredients were accurately weighed: 1g of glycerin, 0.5g of propylene glycol, 0.3g of lauric acid, 0.1g of polyethylene glycol-1500.1 g of glyceryl stearate, 1g of potassium cocoyl glycinate, 3g of aloe leaf extract, 10g of rose essential oil balm prepared by the method and 40g of rose hydrosol. Mixing the above materials, stirring, and keeping the temperature at 50 deg.C for 10 min; and then carrying out ultrasonic homogenization for 3min, sterilizing and canning to obtain the rose fragrance facial cleanser.
Comparative example 2
A production method of rose essential oil balm comprises the following steps:
5000g of fresh rose flowers are placed in a subcritical extraction tank, and the weight ratio of the fresh rose flowers to the subcritical extraction tank is 1 kg: mixing 3L of the mixture with liquid propane, and performing subcritical extraction for 40min for 4 times at extraction temperature of 55 deg.C and extraction pressure of 0.55MPa under dark condition; after the subcritical extraction is finished, extracting an extract liquid; evaporating and desolventizing the extract liquor, compressing and liquefying the evaporated gas solvent by a diaphragm compressor, and then recovering the solvent; and desolventizing the extractive solution to obtain 926.5g of rose essential oil balm with extraction rate of 18.53%. 100g of rose essential oil balm was dissolved in 200 ml of hexane, and the resultant hexane solution was subjected to column chromatography using basic alumina and washed with hexane to separate 25.86g of total rose wax, and the wax content of the rose essential oil balm was found to be about 25.86%.
2. Preparation method of rose repairing moisturizing lotion
The following ingredients were accurately weighed: 1g of squalane, 3g of propylene glycol, 3g of olive oil, 5g of tocopherol, 3g of hyaluronic acid, 3g of amino acid humectant, 10g of rose essential oil balm prepared by the method and 40g of rose hydrosol. Mixing and stirring the components, and preserving heat for 10 minutes at the temperature of 50 ℃; and then carrying out ultrasonic homogenization for 3min, sterilizing and canning to obtain the rose moisturizing emulsion.
3. Preparation method of rose fragrance facial cleanser
The following ingredients were accurately weighed: 1g of glycerin, 0.5g of propylene glycol, 0.3g of lauric acid, 0.1g of polyethylene glycol-1500.1 g of glyceryl stearate, 1g of potassium cocoyl glycinate, 3g of aloe leaf extract, 10g of rose essential oil balm prepared by the method and 40g of rose hydrosol. Mixing the above materials, stirring, and keeping the temperature at 50 deg.C for 10 min; and then carrying out ultrasonic homogenization for 3min, sterilizing and canning to obtain the rose fragrance facial cleanser.
Example 2
1. A production method of rose essential oil balm comprises the following steps:
5000g of fresh rose flowers are placed in a subcritical extraction tank, and the weight ratio of the fresh rose flowers to the subcritical extraction tank is 1 kg: mixing 2L of the mixture with liquid butane, and performing subcritical extraction for 3 times at 40 deg.C under 0.40MPa in dark condition for 60 min; after the subcritical extraction is finished, extracting an extract liquid; evaporating and desolventizing the extract liquor, compressing and liquefying the evaporated gas solvent by a diaphragm compressor, and then recovering the solvent; and desolventizing the extractive solution to obtain 1085.5g of rose essential oil balm with extraction rate of 21.71%. 100g of rose essential oil balm was dissolved in 200 ml of hexane, and the resultant hexane solution was subjected to column chromatography using basic alumina and washed with hexane to separate 18.65g of total rose wax, and the wax content of the rose essential oil balm was found to be about 18.65%.
2. Preparation method of rose repairing moisturizing lotion
The following ingredients were accurately weighed: 3g of squalane, 1g of propylene glycol, 5g of olive oil, 3g of tocopherol, 5g of hyaluronic acid, 1g of amino acid humectant, 20g of rose essential oil balm prepared by the method and 20g of rose hydrosol. Mixing and stirring the components, and preserving heat for 20 minutes at the temperature of 60 ℃; and then carrying out ultrasonic homogenization for 8min, sterilizing and canning to obtain the rose moisturizing emulsion.
3. Preparation method of rose fragrance facial cleanser
The following ingredients were accurately weighed: 3g of glycerin, 0.5g of propylene glycol, 0.5g of lauric acid, 0.5g of polyethylene glycol-1500.1 g of glyceryl stearate, 1g of potassium cocoyl glycinate, 5g of aloe leaf extract, 10g of rose essential oil balm prepared by the method and 40g of rose hydrosol. Mixing the above materials, stirring, and keeping the temperature at 60 deg.C for 20 min; and then carrying out ultrasonic homogenization for 8min, sterilizing and canning to obtain the rose fragrance facial cleanser.
Example 3
1. A production method of rose essential oil balm comprises the following steps:
5000g of fresh rose flowers are placed in a subcritical extraction tank, and the weight ratio of the fresh rose flowers to the subcritical extraction tank is 1 kg: mixing 1L of the material-solvent ratio with liquid tetrafluoroethane, and performing subcritical extraction for 30min under the conditions of extraction temperature of 50 ℃, extraction pressure of 0.5MPa and light shielding for 4 times; after the subcritical extraction is finished, extracting an extract liquid; evaporating and desolventizing the extract liquor, compressing and liquefying the evaporated gas solvent by a diaphragm compressor, and then recovering the solvent; and desolventizing the extract to obtain 1142.5g of rose essential oil balm with extraction rate of 22.85%.
100g of rose essential oil balm was dissolved in 200 ml of hexane, and the resultant hexane solution was subjected to column chromatography using basic alumina and washed with hexane to separate out 23.65 g of total rose wax, and the wax content of the rose essential oil balm was found to be about 23.65%.
2. Preparation method of rose repairing moisturizing lotion
The following ingredients were accurately weighed: 2g of squalane, 2g of propylene glycol, 4g of olive oil, 4g of tocopherol, 4g of hyaluronic acid, 2g of an amino acid humectant, 15g of the rose essential oil balm prepared by the method and 30g of rose hydrosol. Mixing and stirring the components in parts by weight, and keeping the temperature at 60 ℃ for 30 minutes; and then carrying out ultrasonic homogenization for 10min, sterilizing and canning to obtain the rose moisturizing emulsion.
3. Preparation method of rose fragrance facial cleanser
The following ingredients were accurately weighed: 1g of glycerin, 1g of propylene glycol, 0.3g of lauric acid, 1500.3g of polyethylene glycol-ester, 0.1g of glyceryl stearate, 2g of coconut oil acyl potassium glycinate, 3g of aloe leaf extract, 20g of rose essential oil balm prepared by the method and 20g of rose hydrosol. Mixing the above materials, stirring, and keeping the temperature at 60 deg.C for 20 min; and then carrying out ultrasonic homogenization for 8min, sterilizing and canning to obtain the rose fragrance facial cleanser.
Example 4
The rose moisturizing emulsion and the rose-flavor facial cleanser prepared in the embodiments 1 to 3 of the invention are randomly distributed to 100 persons for use, the rose moisturizing emulsion and the rose-flavor facial cleanser prepared in the comparative examples 1 to 2 are randomly distributed to another 100 persons for use, and the return visit tracking after the trial is carried out. After the testers use for a period of time, people who use the rose moisturizing emulsion and the rose-flavor facial cleanser prepared in the embodiments 1 to 3 feed back that the skin is tender and tender, feel moist and smooth, and have remarkable nourishing effect, while people who use the rose moisturizing emulsion and the rose-flavor facial cleanser prepared in the comparative examples 1 to 2 feed back the effect generally, and have little effect on caring the skin. The rose moisturizing emulsion and the rose scent facial cleanser prepared by the method contain rose essential oil balm and rose hydrosol, contain rich rose components, and can effectively promote cell regeneration, prevent skin aging and smooth skin fine lines.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (5)
1. The application of the rose essential oil balm in cosmetics; the preparation method of the rose essential oil balm comprises the following steps:
fresh rose flowers and extraction solvent were mixed in a 1 g: mixing 1-3 ml of the rose essential oil and the rose essential oil, performing subcritical extraction under a dark condition, collecting extract liquor, and removing an extraction solvent in the extract liquor to obtain rose essential oil balm;
the temperature of the subcritical extraction is 40-45 ℃, the pressure of the subcritical extraction is 0.40-0.45 MPa, the extraction times of the subcritical extraction are 2-4 times, and the time of each extraction is 30-60 min; the extraction solvent is propane.
2. The use according to claim 1, wherein the cosmetic comprises a rose-scented facial cleanser or a rose repairing moisturizing lotion.
3. The use according to claim 2, wherein the rose repairing moisturizing emulsion comprises the following components in parts by weight: 1-3 parts of squalane, 1-3 parts of propylene glycol, 3-5 parts of olive oil, 3-5 parts of tocopherol, 3-5 parts of hyaluronic acid, 1-3 parts of an amino acid humectant, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol.
4. The use of claim 2, wherein the rose-scent facial cleanser comprises the following components in parts by weight: 1-3 parts of glycerin, 0.5-1 part of propylene glycol, 0.3-0.5 part of lauric acid, 0.3-0.3 part of polyethylene glycol-1500.1, 0.1-0.5 part of glycerol stearate, 1-2 parts of potassium cocoyl glycinate, 3-5 parts of aloe leaf extract, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol.
5. The rose repairing and moisturizing emulsion is characterized by comprising the following components in parts by weight: 1-3 parts of squalane, 1-3 parts of propylene glycol, 3-5 parts of olive oil, 3-5 parts of tocopherol, 3-5 parts of hyaluronic acid, 1-3 parts of an amino acid humectant, 10-20 parts of rose essential oil balm and 20-40 parts of rose hydrosol;
the method for preparing the rose essential oil balm is the method for preparing the rose essential oil balm in the application of claim 1.
Priority Applications (1)
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