CN103271860A - Skin care oil containing peony oil and preparation method thereof - Google Patents

Skin care oil containing peony oil and preparation method thereof Download PDF

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CN103271860A
CN103271860A CN2013102409047A CN201310240904A CN103271860A CN 103271860 A CN103271860 A CN 103271860A CN 2013102409047 A CN2013102409047 A CN 2013102409047A CN 201310240904 A CN201310240904 A CN 201310240904A CN 103271860 A CN103271860 A CN 103271860A
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oil
peony
paeonia suffruticosa
seed oil
heavy
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CN103271860B (en
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余洪智
王昌涛
毛文岳
吴震生
安华婉
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HEZE YAOSHUN PEONY BIOTECH CO Ltd
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HEZE YAOSHUN PEONY BIOTECH CO Ltd
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Abstract

The invention belongs to the technical field of skin care oil, in particular to skin care oil containing peony oil and a preparation method thereof. The skin care oil provided by the invention comprises the following components in parts by weight: main ingredients: peony seed oil, caprylic/capric triglyceride, cyclopentasiloxane and 1, 2 - butyl glycol 1-12, wherein the peony oil is peony seed oil or peony essence oil or the mixture of peony seed oil and peony essence oil; auxiliary ingredients: isostearic acid, butylated hydroxytoluene, avocado oil, simmondsia chinensis seed oil, meadowfoam seed oil and macadamia ternifolia seed oil; the skin care oil containing peony oil prepared by the method provided by the invention can remarkably improve of the skin epidermis cell cycle function, promote the microcirculation of the blood capillary of the dermal skin effect, inhibit lipid peroxidation, improve metabolism, delay skin aging process, is provided with anti-wrinkle, moisturizing and whiting effect, people feels smooth and comfortable after the skin care oil is used on the skin, and the skin care oil containing peony oil is provided with better effect to chloasma, aging skin wrinkles, skin cutin hardening peeling and skin chap.

Description

A kind of skin protection oil that contains Paeonia suffruticosa oil and preparation method thereof
Technical field
The invention belongs to skin protection oil tech field, be specifically related to a kind of skin protection oil that contains Paeonia suffruticosa oil and preparation method thereof.
Background technology
Peony seed oil is taken from seed of Paeonia suffruticosa " seed of Flos Moutan ", adopts hot moulding, cold pressing or supercritical CO 2Extraction extracts refine and forms.The vegetable oil that is extracted by seed of Flos Moutan is the distinctive woody macadamia nut oil of China, and is nutritious and unique because of it, and medical care effect is arranged again, is called " in the world best vegetable oil " by the relevant expert, is the treasure in the vegetable oil.
In the peony seed oil, VA, VE, nicotinic acid, carotene, unsaturated fatty acid content enrich, skin had fabulous nutrition nursing role, can obviously improve epiderm skin cell cycle function, promote the microcirculation of capillary of skin, the carrying out that suppresses lipid peroxidation, improve metabolism, the delaying decrepitude of skin process, crease-resistant, the whitening function of preserving moisture is arranged, use the back skin smooth light, chloasma, skin aging wrinkle, skin keratin sclerosis decortication, wrinkled skin are had good effect.
Real multifunctional raw material---1,2-pentanediol: 1,2-pentanediol (INCI:Pentylene Glycol), as the multifunctional raw material of cosmetics, have long-term safe handling history, meet the cosmetics rules of the U.S., Europe, Japanese various places.1,2-pentanediol is wetting agent remarkable in the cosmetic formulations; Bioavailability that simultaneously can the enhanced activity thing promotes effective ingredient in the vegetable oil to infiltrate skin and realizes effect that experimental data shows that 1,2-pentanediol can make the bioavailability concentration of some functional component increase more than 10 times; In addition, also having broad spectrum antibiotic activity, is the antipathogenic composition commonly used in the preservative free prescription.
American Avocado Tree (PERSEA GRATISSIMA) oil: American Avocado Tree oil from the American Avocado Tree fruit, does not add chemical substance by the technology extraction of colding pressing in the process.American Avocado Tree oil contains a large amount of vitamin V A, VB1 etc. and several mineral materials, can moisten, soften skin, eliminates the skin inflammation, can promote the regeneration of skin cell simultaneously.
Bai Chihua (LIMNANTHES ALBA) seed oil: owing to contain the long-chain fatty acid that has the antioxidative effect more than 98%, so it is one of the most stable in the world vegetable oil.Good emollient is created magnificent quality for product, also has soft and dry and comfortable skin sense; Can oxidation, increase the shelf-life of product, increase the stability of other oils, also can improve the skin resistance to oxidation, make skin often show young nature.
Jojoba (SIMMONDSIA CHINENSIS) seed oil: Jojoba seed oil contains multiple nutritional components, as VE, VC, spermol, protein, mineral etc.Can promote the regeneration of skin cell, effective especially for the skin of cicatrix, can desalinate cicatrix and pox seal.In addition, fat secretion that can the balance skin improves skin symptoms such as oiliness skin, acne, abscess, eczema.
Macadimia nut (MACADAMIA TERNIFOLIA) seed oil: rich in mineral substances, protein, the natural emollient of multiple unsaturated fatty acid.Fast to dermal osmosis speed, it is smooth to use the back to bring as skin, moisten, and the sensation of non-greasy, the protection cell membrane is repaired and is shone the back skin, improves the ability that skin is resisted extraneous infringement.
Contain multiple important higher fatty acids in the peony petal, mainly based on Palmic acid, linoleic acid plus linolenic acid, unsaturated fatty acid has blood fat reducing, prevents arteriosclerotic effect, be essential fatty acid as linoleic acid, have in the human body and can change arachidonic acid into, for synthetic phospholipid, form cellularity, keep the normal function of all tissues, and synthesis of prostaglandins, all be necessary, linolenic acid is the nutrient that body weight for humans is wanted, have the inhibition neoplasm metastasis, reduce effects such as Incidence of CHD, raising immunity; Also containing element and vitamin B and carotenoid such as protein, polyphenols, potassium, calcium, magnesium, phosphorus in the Flos Moutan, is a kind of natural nourishing healthy material.As with Flos Moutan as raw material, extract quintessence oil wherein, prepare the Flos Moutan quintessence oil, be one of optimum feed stock of preparation skin care item.
Report about the Flos Moutan skin care item is also few, patent disclosure has been arranged Flos Moutan extracts essential oil method, in traditional Flos Moutan method of extraction of essential oil, be raw material with the peony petal, or with the oven dry after peony petal be raw material, and no matter peony petal is in growth course, still in the harvesting process, all inevitably can fall to having pollen, and the part crowd is to peony pollen allergy, can't stop under the situation of peony pollen fully, pollen can be along with Flos Moutan extracts essential oil process, no matter adopt which kind of method to extract in the peony essential oil that obtains, all might contain residual peony pollen, thereby cause crowd for peony pollen allergy equally also to Flos Moutan quintessence oil allergy.Not all Flos Moutan quintessence oil all is suitable for all crowds.
Therefore need improve at above-mentioned method defective, design a kind of processing method that has fully kept heat-sensitive materials and active substance in the Flos Moutan, Flos Moutan is extracted, obtain peony essential oil safe, quality better, be raw material with this quintessence oil, prepare Paeonia suffruticosa skin protection oil.
Summary of the invention
In order to solve above-mentioned technical problem, the invention provides a kind of obvious microcirculation that improves epiderm skin cell cycle function, promotes capillary of skin, the carrying out that suppresses lipid peroxidation, improve metabolism, the delaying decrepitude of skin process, crease-resistant, the whitening function of preserving moisture is arranged, use the back skin smooth light, chloasma, skin aging wrinkle, skin keratin sclerosis decortication, wrinkled skin are had the skin protection oil that contains peony seed oil of good effect;
A kind of skin protection oil that contains Paeonia suffruticosa oil of the present invention comprises the component of following portions by weight:
Major ingredient:
Paeonia suffruticosa oil, 30-70;
Caprylic/capric triglyceride 15-40
Encircle five polydimethylsiloxane 5-30
1,2-pentanediol 1-12;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Isostearic acid accounts for the heavy 0.1-0.3% of Paeonia suffruticosa oil;
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of Paeonia suffruticosa oil;
American Avocado Tree oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Jojoba seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
White Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Macadimia nut seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
This Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil.
Preferably, above-mentioned a kind of skin protection oil that contains Paeonia suffruticosa oil comprises the component of following portions by weight:
Major ingredient:
Paeonia suffruticosa oil, 40-60;
Caprylic/capric triglyceride 20-40
Encircle five polydimethylsiloxane 10-25
1,2-pentanediol 2-10;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Isostearic acid accounts for the heavy 0.1-0.3% of Paeonia suffruticosa oil;
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of Paeonia suffruticosa oil;
American Avocado Tree oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Jojoba seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
White Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Macadimia nut seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
This Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil.
Preferred, above-mentioned a kind of skin protection oil that contains Paeonia suffruticosa oil comprises the component of following portions by weight:
Major ingredient:
Paeonia suffruticosa oil, 50;
Caprylic/capric triglyceride 30
Encircle five polydimethylsiloxane 20
1,2-pentanediol 5;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Isostearic acid account for Paeonia suffruticosa oil heavy 0.2%,
Butylated hydroxytoluene account for Paeonia suffruticosa oil heavy 0.1%,
American Avocado Tree oil account for Paeonia suffruticosa oil heavy 0.2%,
Jojoba seed oil account for Paeonia suffruticosa oil heavy 0.2%,
White Limnanthes Alba Seed Oil account for Paeonia suffruticosa oil heavy 0.2%,
Macadimia nut seed oil account for Paeonia suffruticosa oil heavy 0.2%;
This Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil.
A kind of skin protection oil its preparation method that contains Paeonia suffruticosa oil comprises following step:
Get the Paeonia suffruticosa oil of 30-70 part, add 5-30 part and encircle five polydimethylsiloxane, mix, add caprylic/capric triglyceride and the butylated hydroxytoluene of 15-40 part again, 60 ℃ of following heating for dissolving, mix,
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of Paeonia suffruticosa oil; Slowly add 1 of 1-12 part again, the 2-pentanediol is stirred to transparence, adds isostearic acid and mixes, and above-mentioned isostearic acid accounts for the heavy 0.1-0.3% of Paeonia suffruticosa oil;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil accounts for that Paeonia suffruticosa oil heavy 0.01-3%, Jojoba seed oil account for the heavy 0.01-3% of Paeonia suffruticosa oil, white Limnanthes Alba Seed Oil accounts for heavy 0.01-3%, the macadimia nut seed oil of Paeonia suffruticosa oil and accounts for the heavy 0.01-3% of Paeonia suffruticosa oil, stir, filter, store;
Above-mentioned Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil;
In the filtration step, adopt 200-500 mesh sieve aperture.
A kind of skin protection oil its preparation method that contains Paeonia suffruticosa oil,
Paeonia suffruticosa oil passes through the peony seed oil that cold pressing or hot moulding or supercritical carbon dioxide ways and means obtain for seed of Flos Moutan;
The peony seed oil that adopts common method for cold pressing or hot moulding method to obtain all can be used as raw material peony seed oil of the present invention;
When above-mentioned Paeonia suffruticosa oil is the Flos Moutan quintessence oil,
Flos Moutan quintessence oil its preparation method is as follows:
(1) extraction: pluck fresh peony flower, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, the condition of described supercritical carbon dioxide extraction is: extracting pressure 20-30Mpa, extraction temperature 40-60 ℃, separator I pressure 8-20Mpa, temperature 45-70 ℃, separator II pressure 4-l0Mpa, temperature 15-30 ℃, extraction time 2-4h;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, the condition of molecular distillation is: feeding temperature 40-90 ℃, vapo(u)rizing temperature 95-180 ℃, vacuum 5-1000Pa, Paeonia suffruticosa extractum flow 100-2000ml/h, knifing rotating speed 180-550r/min, chilling temperature 10-45 ℃.
60 ℃ of feeding temperatures, 130 ℃ of vapo(u)rizing temperature temperature, vacuum 40Pa, Paeonia suffruticosa extractum flow 200ml/h, knifing rotating speed 380r/min, 25 ℃ of chilling temperatures.
In above-mentioned step (1) extraction process, pluck fresh peony flower, in fresh peony flower, add at least a in Herba Portulacae and Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), the Semen Sinapis, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and the total amount of described Herba Portulacae and Semen Sinapis Albae or Semen Raphani or Semen Lepidii (Semen Descurainiae) or Semen Sinapis or their mixture accounts for the 0.5-2% of peony petal.
Above-mentioned preparation method also comprises following step: the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, and with at least a mixing the in adjuvant Mel, Aloe polysaccharide, the sinapic acid choline ester., the gross weight of adjuvant accounts for the 0.2-1.5% of peony essential oil;
Adjuvant is Aloe polysaccharide and sinapic acid choline ester., and its part by weight is 1:1-3, and the gross weight of adjuvant accounts for the 0.2-1.5% of peony essential oil.
Beneficial effect of the present invention is, the skin protection oil that contains Paeonia suffruticosa oil that adopts above-mentioned method to prepare, obviously improve epiderm skin cell cycle function, promote the microcirculation of capillary of skin, suppress the carrying out of lipid peroxidation, improve metabolism, the delaying decrepitude of skin process, crease-resistant, the whitening function of preserving moisture is arranged, use the back skin smooth light, chloasma, skin aging wrinkle, skin keratin sclerosis decortication, wrinkled skin are had good effect.
Among the present invention, when adopting the Flos Moutan quintessence oil to be raw material, the Flos Moutan quintessence oil not only provides human body necessary nutrient, and because in Flos Moutan quintessence oil preparation process, added antiallergic materials such as Herba Portulacae and Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), Semen Sinapis, made the Flos Moutan quintessence oil be fit to all groups and use.
The specific embodiment
Below in conjunction with specific embodiment the present invention is done further explanation, so that those skilled in the art more understands the present invention, but therefore do not limit the present invention.
Embodiment 1
Get 50 parts peony seed oil, the preparation method of this peony seed oil is that common method for cold pressing obtains, and adds 20 parts of ring five polydimethylsiloxane, mixes, and adds 30 parts Trivent OCG and butylated hydroxytoluene again, 60 ℃ of following heating for dissolving, mix,
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony seed oil heavy 0.1%; Slowly add again 5 parts 1, the 2-pentanediol is stirred to transparence, add isostearic acid and mix, isostearic acid account for peony seed oil heavy 0.2%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 0.2%, Jojoba seed oil account for peony seed oil heavy 0.2%, white Limnanthes Alba Seed Oil account for peony seed oil heavy 0.2%, macadimia nut seed oil account for peony seed oil heavy 0.2%, stir, filter, store;
In the filtration step, adopt 200-500 mesh sieve aperture.
Below be the skin protection oil that contains Paeonia suffruticosa oil that the method for embodiment 1 prepares, indexs such as its outward appearance:
Figure 2013102409047100002DEST_PATH_IMAGE001
Embodiment 2
Get 50 parts Flos Moutan quintessence oil, add 20 parts of ring five polydimethylsiloxane, mix, add 30 parts Trivent OCG and butylated hydroxytoluene again, 60 ℃ of following heating for dissolving, mix;
The preparation process of above Flos Moutan quintessence oil is as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, add Herba Portulacae in fresh peony flower, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 10Mpa, 55 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 60 ℃ of feeding temperatures, 120 ℃ of vapo(u)rizing temperatures, vacuum 40Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 380r/min, 30 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with the adjuvant sinapic acid choline ester., the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, get the Flos Moutan quintessence oil after the mixing, add sinapic acid choline ester., can further prevent the human allergy, and add the effect that Flos Moutan quintessence oil behind the sinapic acid choline ester. also has radioprotective, antibiotic, antiinflammatory.
Add butylated hydroxytoluene, butylated hydroxytoluene account for the Flos Moutan quintessence oil heavy 0.1%; Slowly add again 5 parts 1, the 2-pentanediol is stirred to transparence, add isostearic acid and mix, isostearic acid account for peony seed oil heavy 0.2%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 1%, Jojoba seed oil account for the Flos Moutan quintessence oil heavy 1%, white Limnanthes Alba Seed Oil account for the Flos Moutan quintessence oil heavy 1%, macadimia nut seed oil account for the Flos Moutan quintessence oil heavy 1%, stir, filter, store;
In the filtration step, adopt 200-500 mesh sieve aperture.
Comparative Examples 1
Get 50 parts Flos Moutan quintessence oil, add 20 parts of ring five polydimethylsiloxane, mix, add 30 parts Trivent OCG and butylated hydroxytoluene again, 60 ℃ of following heating for dissolving, mix;
The preparation process of above Flos Moutan quintessence oil is as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 10Mpa, 55 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(4) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 70 ℃ of feeding temperatures, 130 ℃ of vapo(u)rizing temperatures, vacuum 50Pa, Paeonia suffruticosa extractum flow 500ml/h, knifing rotating speed 380r/min, 30 ℃ of chilling temperatures; The Flos Moutan quintessence oil that after distillation, obtains.
In above Flos Moutan quintessence oil, add butylated hydroxytoluene, butylated hydroxytoluene account for the Flos Moutan quintessence oil heavy 0.1%; Slowly add again 5 parts 1, the 2-pentanediol is stirred to transparence, add isostearic acid and mix, isostearic acid account for peony seed oil heavy 0.2%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 1%, Jojoba seed oil account for the Flos Moutan quintessence oil heavy 1%, white Limnanthes Alba Seed Oil account for the Flos Moutan quintessence oil heavy 1%, macadimia nut seed oil account for the Flos Moutan quintessence oil heavy 1%, stir, filter, store;
In the filtration step, adopt 200-500 mesh sieve aperture.
200 women of 20-30 between year are divided into two groups, in these two groups, every group has 5 women respectively to Flos Moutan allergy, get the skin protection oil in embodiment 2 and the Comparative Examples 1, allow every group of personnel use respectively, sooner or later respectively get to be coated with about 1 gram and put on a stern expression and neck, after one month, collect two groups of women respectively to the reaction condition of this skin protection oil.
Embodiment 2, and is unmanned irritated to Paeonia suffruticosa skin protection oil among these 100 women, and before one month, skin is obviously fine and smooth, smooth;
Comparative Examples 1 among these 100 women, has 4 women irritated to Paeonia suffruticosa skin protection oil, and before one month, skin is obviously fine and smooth, smooth.
Embodiment 3
Get 30 parts peony seed oil, the preparation method of this peony seed oil is that common method for cold pressing obtains, and adds 5 parts of ring five polydimethylsiloxane, mixes, and adds 15 parts Trivent OCG and butylated hydroxytoluene again, 60 ℃ of following heating for dissolving, mix,
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony seed oil heavy 0.05%; Slowly add again 1 part 1, the 2-pentanediol is stirred to transparence, add isostearic acid and mix, isostearic acid account for peony seed oil heavy 0.1%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 0.5%, Jojoba seed oil account for peony seed oil heavy 0.5%, white Limnanthes Alba Seed Oil account for peony seed oil heavy 0.5%, macadimia nut seed oil account for peony seed oil heavy 0.5%, stir, filter, store;
In the filtration step, adopt 200-500 mesh sieve aperture.
Embodiment 4
Get 30 parts peony seed oil, the preparation method of this peony seed oil is that common hot moulding method obtains, and adds 5 parts of ring five polydimethylsiloxane, mixes, and adds 15 parts Trivent OCG and butylated hydroxytoluene again, 60 ℃ of following heating for dissolving, mix,
Add butylated hydroxytoluene, butylated hydroxytoluene account for peony seed oil heavy 0.15%; Slowly add again 12 parts 1, the 2-pentanediol is stirred to transparence, add isostearic acid and mix, isostearic acid account for peony seed oil heavy 0.3%;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil account for peony seed oil heavy 3%, Jojoba seed oil account for peony seed oil heavy 3%, white Limnanthes Alba Seed Oil account for peony seed oil heavy 3%, macadimia nut seed oil account for peony seed oil heavy 3%, stir, filter, store;
In the filtration step, adopt 200-500 mesh sieve aperture.
Embodiment 5
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, add Herba Portulacae in fresh peony flower, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 10Mpa, 55 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 50 ℃ of feeding temperatures, 140 ℃ of vapo(u)rizing temperatures, vacuum 100Pa, Paeonia suffruticosa extractum flow 600ml/h, knifing rotating speed 480r/min, 20 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with the adjuvant Aloe polysaccharide, the gross weight of Aloe polysaccharide accounts for 1% of peony essential oil, get the Flos Moutan quintessence oil after the mixing, add Aloe polysaccharide, can further prevent the human allergy, and the Flos Moutan quintessence oil that adds behind the Aloe polysaccharide also has effect antibiotic, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 6
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, add Herba Portulacae in fresh peony flower, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 10Mpa, 55 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 70 ℃ of feeding temperatures, 100 ℃ of vapo(u)rizing temperatures, vacuum 4Pa, Paeonia suffruticosa extractum flow 700ml/h, knifing rotating speed 280r/min, 30 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with the adjuvant sinapic acid choline ester., the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, get the Flos Moutan quintessence oil after the mixing, add sinapic acid choline ester., can further prevent the human allergy, and add the effect that Flos Moutan quintessence oil behind the sinapic acid choline ester. also has radioprotective, antibiotic, antiinflammatory.
Remaining making step is with embodiment 3.
Embodiment 7
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, add Herba Portulacae and Semen Sinapis Albae in fresh peony flower, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 10Mpa, 55 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 55 ℃ of feeding temperatures, 130 ℃ of vapo(u)rizing temperatures, vacuum 400Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 380r/min, 10 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with the adjuvant Aloe polysaccharide, the gross weight of Aloe polysaccharide accounts for 1% of peony essential oil, get the Flos Moutan quintessence oil after the mixing, add Aloe polysaccharide, can further prevent the human allergy, and the Flos Moutan quintessence oil that adds behind the Aloe polysaccharide also has effect antibiotic, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 8
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: plucking fresh peony flower, is raw material with fresh Flos Moutan, adds Herba Portulacae and Semen Sinapis Albae, Semen Raphani in fresh peony flower, its addition is 1% of peony petal gross weight, its part by weight is 1:1:1, and supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and its condition of supercritical carbon dioxide supercritical extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 15Mpa, 35 ℃ of temperature, separator II pressure 7Mpa, 20 ℃ of temperature, extraction time 2h; Because inevitably can contain residual peony pollen on the peony petal, and the part crowd can be to peony pollen allergy, therefore, add above-mentioned Herba Portulacae and Semen Sinapis Albae, Semen Raphani, not only can desensitize, and above-mentioned material also has antioxidation, radioprotective, antidotal effect, makes peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 60 ℃ of feeding temperatures, 135 ℃ of vapo(u)rizing temperatures, vacuum 400Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 430r/min, 20 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with adjuvant Mel, the gross weight of adjuvant accounts for 0.8% of peony essential oil, get the Flos Moutan quintessence oil after the mixing, add Aloe polysaccharide, can further prevent the human allergy, and the Flos Moutan quintessence oil that adds behind the Aloe polysaccharide also has effect antibiotic, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 9
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, add Herba Portulacae in fresh peony flower, its addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 30Mpa, 55 ℃ of extraction temperature, separator I pressure 20Mpa, 35 ℃ of temperature, separator II pressure 10Mpa, 25 ℃ of temperature, extraction time 3h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned material also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is:
45 ℃ of feeding temperatures, 130 ℃ of vapo(u)rizing temperatures, vacuum 100Pa, Paeonia suffruticosa extractum flow 300ml/h, knifing rotating speed 350r/min, 25 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with adjuvant Aloe polysaccharide and sinapic acid choline ester., its part by weight is 1:2, the gross weight of adjuvant accounts for 0.8% of peony essential oil, get the Flos Moutan quintessence oil after the mixing, add Aloe polysaccharide and sinapic acid choline ester., can further prevent the human allergy, and add the effect that Flos Moutan quintessence oil behind Aloe polysaccharide and the sinapic acid choline ester. also has radioprotective, antibiotic, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 10
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, add Herba Portulacae in fresh peony flower, addition is 1% of peony petal gross weight, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, its condition of supercritical carbon dioxide supercritical extraction is: pressure 25Mpa, 48 ℃ of extraction temperature, separator I pressure 10Mpa, 35 ℃ of temperature, separator II pressure 6Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned Herba Portulacae also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 65 ℃ of feeding temperatures, 150 ℃ of vapo(u)rizing temperatures, vacuum 700Pa, Paeonia suffruticosa extractum flow 800ml/h, knifing rotating speed 380r/min, 20 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with adjuvant sinapic acid choline ester., Mel, gross weight accounts for 1% of peony essential oil, its part by weight is 1:2, get the Flos Moutan quintessence oil after the mixing, add sinapic acid choline ester., Mel, can further prevent the human allergy, and add the effect that Flos Moutan quintessence oil behind sinapic acid choline ester., the Mel also has radioprotective, antibiotic, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 11
Be raw material with the Flos Moutan quintessence oil, wherein the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, adding the Herba Portulacae addition in fresh peony flower is 1% of peony petal gross weight, and supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and its condition of supercritical carbon dioxide supercritical extraction is: pressure 25Mpa, 60 ℃ of extraction temperature, separator I pressure 10Mpa, 35 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned Herba Portulacae also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is: 75 ℃ of feeding temperatures, 140 ℃ of vapo(u)rizing temperatures, vacuum 800Pa, Paeonia suffruticosa extractum flow 800ml/h, knifing rotating speed 480r/min, 30 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, mix with adjuvant sinapic acid choline ester., Mel, Aloe polysaccharide, the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, the weight ratio of sinapic acid choline ester., Mel, Aloe polysaccharide is 2:1:1, get the Flos Moutan quintessence oil after the mixing, add sinapic acid choline ester., Mel, Aloe polysaccharide, can further prevent the human allergy, and add the effect that Flos Moutan quintessence oil behind the sinapic acid choline ester. also has radioprotective, antibiotic, antiinflammatory.
Remaining making step is with embodiment 2.
Embodiment 12
Mixing Paeonia suffruticosa oil with Flos Moutan quintessence oil and peony seed oil is raw material, and the part by weight of Flos Moutan quintessence oil and peony seed oil is that the preparation method of 4:1 peony seed oil adopts common method for cold pressing, the Flos Moutan quintessence oil preparation process as follows:
(1) extraction: pluck fresh peony flower, be raw material with fresh Flos Moutan, adding the Herba Portulacae addition in fresh peony flower is 1% of peony petal gross weight, and supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and its condition of supercritical carbon dioxide supercritical extraction is: pressure 25Mpa, 60 ℃ of extraction temperature, separator I pressure 10Mpa, 35 ℃ of temperature, separator II pressure 4Mpa, 20 ℃ of temperature, extraction time 1.5h; Because inevitably can contain residual peony pollen on the peony petal, and therefore the part crowd can be to peony pollen allergy,, add above-mentioned Herba Portulacae, not only can desensitize, and above-mentioned Herba Portulacae also has antioxidation, antidotal effect, make peony essential oil better act on human body;
The florescence of Flos Moutan is a week only, and the tender profit of petal is mouldy easily after gathering, be difficult for preserving peony petal, select fine weather to pluck peony petal, plucking time is 7-10 point in morning, after the harvesting, peony petal is placed container, avoid the sunlight direct projection, because peony petal meeting dehydration, air-dry in the preservation process, original fragrance can volatilize, therefore need handle peony petal as early as possible, be preferably within 4 hours after the harvesting and extract processing;
(2) distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, its condition of molecular distillation is:
65 ℃ of feeding temperatures, 120 ℃ of vapo(u)rizing temperatures, vacuum 50Pa, Paeonia suffruticosa extractum flow 1000ml/h, knifing rotating speed 430r/min, 25 ℃ of chilling temperatures;
(3) the Flos Moutan quintessence oil of getting peony seed oil and after distillation, obtaining, mix with adjuvant sinapic acid choline ester., Mel, Aloe polysaccharide, the gross weight of sinapic acid choline ester. accounts for 1% of peony essential oil, the weight ratio of sinapic acid choline ester., Mel, Aloe polysaccharide is 2:1:1, get the Flos Moutan quintessence oil after the mixing, add sinapic acid choline ester., Mel, Aloe polysaccharide, can further prevent the human allergy, and the Flos Moutan quintessence oil behind the adding sinapic acid choline ester. also has the effect of radioprotective, antibiotic, antiinflammatory, and the ratio of peony seed oil and Flos Moutan quintessence oil is 1:2.
Remaining making step is with embodiment 2.

Claims (10)

1. skin protection oil that contains Paeonia suffruticosa oil comprises the component of following portions by weight:
Major ingredient:
Paeonia suffruticosa oil 30-70, caprylic/capric triglyceride 15-40;
Encircle five polydimethylsiloxane 5-30;
1,2-pentanediol 1-12;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Described isostearic acid accounts for the heavy 0.1-0.3% of Paeonia suffruticosa oil;
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of Paeonia suffruticosa oil;
American Avocado Tree oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Jojoba seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
White Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Macadimia nut seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Described Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil.
2. a kind of skin protection oil that contains Paeonia suffruticosa oil as claimed in claim 1 comprises the component of following portions by weight:
Major ingredient:
Paeonia suffruticosa oil 40-60,
Caprylic/capric triglyceride 20-40;
Encircle five polydimethylsiloxane 10-25;
1,2-pentanediol 2-10;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Described isostearic acid accounts for the heavy 0.1-0.3% of Paeonia suffruticosa oil;
Butylated hydroxytoluene accounts for the heavy 0.05-0.15% of Paeonia suffruticosa oil;
American Avocado Tree oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Jojoba seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
White Limnanthes Alba Seed Oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Macadimia nut seed oil accounts for the heavy 0.01-3% of Paeonia suffruticosa oil;
Described Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil.
3. a kind of skin protection oil that contains Paeonia suffruticosa oil as claimed in claim 1 comprises the component of following portions by weight:
Major ingredient:
Paeonia suffruticosa oil 50, caprylic/capric triglyceride 30
Encircle five polydimethylsiloxane 20
1,2-pentanediol 5;
Adjuvant:
Isostearic acid, butylated hydroxytoluene, American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil;
Described isostearic acid account for Paeonia suffruticosa oil heavy 0.2%,
Butylated hydroxytoluene account for Paeonia suffruticosa oil heavy 0.1%,
American Avocado Tree oil account for Paeonia suffruticosa oil heavy 0.2%,
Jojoba seed oil account for Paeonia suffruticosa oil heavy 0.2%,
White Limnanthes Alba Seed Oil account for Paeonia suffruticosa oil heavy 0.2%,
Macadimia nut seed oil account for Paeonia suffruticosa oil heavy 0.2%;
Described Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil.
4. a kind of skin protection oil its preparation method that contains Paeonia suffruticosa oil as claimed in claim 1 comprises following step:
Get the Paeonia suffruticosa oil of 30-70 part, add 5-30 part and encircle five polydimethylsiloxane, mix, the caprylic/capric triglyceride and the butylated hydroxytoluene that add 15-40 part again 60 ℃ of following heating for dissolving, mix, add butylated hydroxytoluene, butylated hydroxytoluene accounts for the heavy 0.05-0.15% of Paeonia suffruticosa oil; Slowly add 1 of 1-12 part again, the 2-pentanediol is stirred to transparence, adds isostearic acid and mixes, and described isostearic acid accounts for the heavy 0.1-0.3% of peony seed oil;
Add American Avocado Tree oil, Jojoba seed oil, white Limnanthes Alba Seed Oil, macadimia nut seed oil again, American Avocado Tree oil accounts for that Paeonia suffruticosa oil heavy 0.01-3%, Jojoba seed oil account for the heavy 0.01-3% of Paeonia suffruticosa oil, white Limnanthes Alba Seed Oil accounts for heavy 0.01-3%, the macadimia nut seed oil of Paeonia suffruticosa oil and accounts for the heavy 0.01-3% of Paeonia suffruticosa oil, stir, filter, store;
Described Paeonia suffruticosa oil is the mixture of peony seed oil or Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil;
In the described filtration step, adopt 200-500 mesh sieve aperture.
5. a kind of skin protection oil its preparation method that contains Paeonia suffruticosa oil as claimed in claim 1 is characterized in that when described Paeonia suffruticosa oil was peony seed oil, peony seed oil passed through cold pressing or hot moulding or supercritical carbon dioxide ways and means by seed of Flos Moutan and obtains;
When described Paeonia suffruticosa oil was the mixture of Flos Moutan quintessence oil or peony seed oil and Flos Moutan quintessence oil, the preparation method of Flos Moutan quintessence oil was as follows:
(1) extraction: pluck fresh peony flower, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, the condition of described supercritical carbon dioxide extraction is: extracting pressure 20-30Mpa, extraction temperature 40-60 ℃, separator I pressure 8-20Mpa, temperature 45-70 ℃, separator II pressure 4-l0Mpa, temperature 15-30 ℃, extraction time 2-4h;
(2) molecular distillation: adopt the method for molecular distillation that Paeonia suffruticosa extractum is extracted, get peony essential oil, the condition of molecular distillation is: feeding temperature 40-90 ℃, vapo(u)rizing temperature 95-180 ℃, vacuum 5-1000Pa, Paeonia suffruticosa extractum flow 100-2000ml/h, knifing rotating speed 180-550r/min, chilling temperature 10-45 ℃.
6. according to the described a kind of skin protection oil its preparation method that contains Paeonia suffruticosa oil of claim 5, it is characterized in that, its condition of described carbon dioxide supercritical fluid extraction is: pressure 28Mpa, 50 ℃ of extraction temperature, separator I pressure 15Mpa, 55 ℃ of temperature, separator II pressure 8Mpa, 20 ℃ of temperature, extraction time 2h.
7. according to the described a kind of skin protection oil its preparation method that contains Paeonia suffruticosa oil of claim 5, it is characterized in that, its condition of described molecular distillation is: 60 ℃ of feeding temperatures, 130 ℃ of vapo(u)rizing temperature temperature, vacuum 40Pa, Paeonia suffruticosa extractum flow 200ml/h, knifing rotating speed 380r/min, 25 ℃ of chilling temperatures.
8. according to the method for extracting peony essential oil in the described fresh peony flower of claim 5, it is characterized in that, in described step (1) extraction process, pluck fresh peony flower, in fresh peony flower, add Herba Portulacae, Semen Sinapis Albae, Semen Raphani, Semen Lepidii (Semen Descurainiae), Semen Sinapis, at least a, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum, and the total amount of described Herba Portulacae and Semen Sinapis Albae or Semen Raphani or Semen Lepidii (Semen Descurainiae) or Semen Sinapis or their mixture accounts for the 0.5-2% of peony petal.
9. according to the method for extracting peony essential oil in the described fresh peony flower of claim 5, it is characterized in that, in described step (1) extraction process, pluck fresh peony flower, add sinapic acid choline ester. in fresh peony flower, supercritical carbon dioxide extraction prepares Paeonia suffruticosa extractum.
10. according to the method for extracting peony essential oil in the described fresh peony flower of claim 5, it is characterized in that, described preparation method also comprises following step: the Flos Moutan quintessence oil that obtains after the distillation of learning from else's experience, with at least a mixing the in adjuvant Herba Portulacae extract, Mel, Aloe polysaccharide, the sinapic acid choline ester., the gross weight of adjuvant accounts for the 0.2-1.5% of peony essential oil;
Described adjuvant is Aloe polysaccharide and sinapic acid choline ester., and its part by weight is 1:1-3, and the gross weight of adjuvant accounts for the 0.2-1.5% of peony essential oil.
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CN105411882A (en) * 2015-12-21 2016-03-23 天津贝世康科技有限公司 Skin-care composition with peony extract and application of skin-care composition
CN107088179A (en) * 2016-06-13 2017-08-25 北京国济众芳中医药研究所 Skin care oil for preventing and alleviating senile skin chap and its production and use
CN106074284A (en) * 2016-07-16 2016-11-09 尹治华 A kind of moistening skin beautifying beautifying facial mask and preparation method thereof
CN106265262A (en) * 2016-08-25 2017-01-04 周荣 A kind of preparation method of natural cosmetic water
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CN111939093B (en) * 2020-08-26 2023-04-07 广州市逸轩精细化工有限公司 Bath oil with foaming and moistening effects, and its preparation method
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