CN102406581B - Skin protecting composite with function of tightening skin - Google Patents
Skin protecting composite with function of tightening skin Download PDFInfo
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- CN102406581B CN102406581B CN2011103839132A CN201110383913A CN102406581B CN 102406581 B CN102406581 B CN 102406581B CN 2011103839132 A CN2011103839132 A CN 2011103839132A CN 201110383913 A CN201110383913 A CN 201110383913A CN 102406581 B CN102406581 B CN 102406581B
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Abstract
The invention provides a skin protecting composite with a function of tightening skin. The skin protecting composite comprises fresh milk, olive oil, wych-hazel extract, hydrolyzed soy protein and artemia extract. The invention also provides a cosmetic product containing the skin protecting composite, such as anti-wrinkling cream, anti-wrinkling lotion, which has the functions of tightening skin (particularly increasing skin elasticity, smoothing winkles and improving moistening strength), and delaying skin ageing.
Description
Technical field
The invention relates to a kind of skin care compositions with the skin effect of compacting, particularly about a kind of skin care compositions with the skin that efficiently compacts, prevention skin aging that is applied to cosmetics, and the cosmetics that comprise said composition, it mainly comprises fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia (ARTEMIA) extract etc.
Background technology
In recent years, cosmetics circle are advocated natural functional component are added among all kinds of skin-protection products.
Skin aging is the skin aging phenomenon that is caused by natural cause or non-natural cause.People's rear skin histology of being born is day by day flourishing, and function is active gradually, will begin to degenerate when arriving certain age, and this degeneration is often slowly carried out unconsciously people.The growth stage of skin histology generally ended at about 25 years old, had this phase of person to be " bent angle of skin ", carried out simultaneously with aging from after this growth, Elastic fibers is chap gradually, the old phase of 40～50 the beginning of the year, wearing out of skin is slowly obvious, although degree of aging can vary with each individual.
Skin aging is the intrinsic physiological mechanism of human senility and the coefficient results of infringement such as expose to the weather in the external world, environmental pollution.Reasonably nutrition can partly suppress the physiological aging, but is difficult to protect skin not to be subjected to the impact of external environment.Only has the presenility of crossing that could suppress skin by replenish nutrient in good time.
The body nutritive equilibrium is very important to keeping healthy skin, and skin is youthened, and will greatly accelerate skin aging but ignore this point.Known some nutrient substance lacks, and such as vitamin C, vitamin B complex and essential fatty acid, can cause various dermatitis and other dermatosis.If slight shortage the (this situation ubiquity but often out in the cold), may not can cause clinical symptoms, but affected the ability of skin healing and renewal.
Skin aging is embodied in the several respects such as skin elasticity, wrinkle of skin and roughness, moist intensity usually.Use moisturizer skin protection simple in the daily life obviously is inadequate for the prevention skin aging.The factor meetings such as environment, sunlight and pressure impel skin ageing to accelerate so that free radical injures skin greatly.At this time skin also easily goes out a little speckles, and the phenomenons such as microgroove are so need to use the antioxidative skin care item.Years cause health aging, and skin metabolism slows down, the collagen protein of skin and elastic fiber degeneration.It has been generally acknowledged that the skin-protection product that needs to use Rosemary Extract to slow down the aging of skin, the skin care item that for example can select some energy stimulation collagens to generate.
Summary of the invention
One object of the present invention is to provide a kind of skin care compositions with the skin effect of compacting, said composition comprises that by multiple natural animal-plant composition fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia (ARTEMIA) extract etc. form, stable in properties, have total care skin particularly compact skin, the prevention skin aging effect.
Another object of the present invention is to provide a kind of cosmetics that comprise described skin care compositions, can directly act on the human body skin surface, total care skin, the effect of reach the skin that compacts, preventing skin aging.
Another object of the present invention is to provide a kind of method for preparing described cosmetics, by rational production technology, the described skin care compositions of fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia (ARTEMIA) extract that comprises is used for the production of cosmetics, preparing stable in properties, and the cosmetics with effects such as the skin that well compacts, prevention skin agings (mainly being skin care, wrinkle removing, increase skin elasticity).
At first, the invention provides a kind of moisture-keeping composition, said composition is comprised of fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract.
Among the present invention, the all commercially available acquisitions of described fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract, also can prepare voluntarily according to the record of prior art, each extract should meet correlated quality standard-required (for example fresh milk should meet the requirement of GB6914).
Fresh milk (sweet milk) contains outside high-quality protein, fat, the carbohydrate, also contain abundant vitamin and mineral, especially vitamin B2, B12 and calcium, these materials all are that human body growth promoter and metabolism are necessary, through Transdermal absorption, fresh cow milk almost can provide whole skin nutrients.Lot of documents record fresh milk has profit skin, the lung that nourishes heart, relieving heat toxin, delay skin aging, make skin keep the effects such as smooth pliable is delicate.
Olive oil is green health food.Olive oil is the fruit of the olive tree (Olea europaea L.) after cutting one's eye-teeth by collection, extract through squeezing.Olive oil contains the nutritional labeling of multiple needed by human body, and its fatty acid and multiple natural grease soluble vitamin are very favourable to nourishing skin.Directly use the olive oil skin protection can prevent wrinkle of skin and coarse.Make skin recover natural elasticity, gloss and tender has special absorbability to ultraviolet, is to prevent that burning sun from tanning by the sun and the superior good merchantable brand of severe cold frost to skin damage.Olive oil is easy to absorb with rear clearly oiliness, is the safe and reliable cosmetic good merchantable brand of a kind of pure natural.
Hamamelis virginiana is to be grown in Northeastern United States one with the plant in the forest, contain abundant active component and aromatic substance in the branch of Radix Hamamelidis Mollis and the bark, behind distillation extraction, can increase the special odor of Radix Hamamelidis Mollis, obtain having the nature convergence, nourishing and promote transparent, the supernatant liquid of vasoconstrictor effects.Radix Hamamelidis Mollis extracting solution skinfeel height is pleasant fresh and clean, can in time replenish skin moisture, is easy to absorb, and has the Lavender Extract effect, can be used for the balance conditioning of oiliness skin.
Hydrolyzed soybean protein is Glycinemax (Semen sojae atricolor) extract, is rich in the peptide with the respiratory chain protein similar.The present invention uses it for the preparation skin care compositions, can significantly promote skin vision and sensory effect, and for example better skin apparent structure has moisture-keeping function and cosmetic result.
Artemia (ARTEMIA) extract; it is a kind of halomereid extract; mainly contain GP4G, enter human body after, can change rapidly ATP into; moment magnitude of recruitment; " wake " cell because of old and feeble or " dormancy " affected by environment up, activate various physiological activities and the metabolism of Skin Cell, improve the synthetic of the protein that plays a crucial role in the epidermis; the function that also has the DNA protection and repair plays an important role to numerous cell metabolism procedures.
Among the present invention, studied the different characteristics character of fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract, considered the interaction between each component, obtain a kind of skin care compositions with these materials are composite, can directly act on human body or be further used for mutually producing cosmetics and act on human body as adding, has synergism for the skin that compacts, can reach wrinkle removing, increase skin elasticity, improve and moisten the intensity texts, thereby the skin that can compact, prevention skin aging have good skin-care effect.
According to preferred specific embodiments of the present invention, as follows to the prescription of described olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract among the present invention:
Olive oil: outward appearance: transparent yellow green liquid; Refraction index (20 ℃): 1.46-1.48; Relative density: 0.9160-0.9250; Acid value (mgKOH/g)≤0.5; Peroxide value (meq/kg)≤15; Oleic acid (%) 〉=72; Moisture and volatile matter content (%)≤0.05; Impurity (%)≤0.01.
Hamamelis virginiana extracting solution: outward appearance: colourless transparent liquid; PH value (10% aqueous solution): 5～6.5; Index of refraction (20 ℃): 1.4160～1.4200; Relative density (20 ℃): 1.03～1.036.
Hydrolyzed soybean protein: outward appearance: transparency liquid; Color: yellow; PH (20 ℃): 4.0～5.0; Density, g/cm
3(20 ℃): 1.06～1.09; Refractive index (20 ℃): 1.365～1.385; Protein content (Lowry method) g/kg:1.5～3.5; Potassium sorbate content %:0.10～0.16; Sodium benzoate content %:0.240～0.30.
Artemia extract: outward appearance: transparency liquid; PH (20 ℃): 5.0～6.0; Density (20 ℃) g/m
3: 1.00～1.02; Refractive index (20 ℃): 1.33～1.34; Solid content: 12.0～18.0g/kg; GP4G content 145～195ppm.
According to specific embodiments of the present invention, in the skin care compositions of the present invention, the weight proportion of described fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract is 3～10: 2～4: 2～4: 0.5～1.5: 1～2; Most preferred weight proportion is 4～6: 3: 3: 1: 1.5 (except indicating especially, ratio described in the present invention and content are part by weight and content).Each component of this ratio is used for the production of cosmetics, compact in skin (wrinkle removing, increase skin elasticity, improve and the moisten intensity) effect giving cosmetics, can guarantee that resulting cosmetics have popular acceptable excellent flavor and good stability.
On the other hand, the present invention also provides described skin care compositions to compact the skin composition for the preparation of the application in the cosmetics in conduct.Specifically, described cosmetics be for improve skin moisturizing intensity, improve wrinkle of skin and roughness, the increase skin elasticity, that is, mainly be used to the skin that compacts, crease-resistant.
On the other hand, the present invention also provides a kind of cosmetics, comprising the skin care compositions with the skin effect of compacting of the present invention.According to specific embodiments of the present invention, described cosmetics are emulsified make-ups, for example can be cold cream frost or facial treatment milk.According to the preferred embodiments of the invention, the weight content of described skin care compositions in cosmetics is 5%～20%, can for example cream frost or emulsion have different content according to the concrete kind difference of cosmetics.Preferred, guaranteeing under the total content prerequisite of described skin care compositions in cosmetics, in (take the gross weight of cosmetics as benchmark) scope that the fresh milk in the described skin care compositions, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, the weight content of artemia extract in these cosmetics should be controlled at respectively 3%～10%, 2%～4%, 2%～4%, 0.5%～1.5%, 1%～2%; Most preferred, the content of fresh milk wherein in cosmetics is more than 5%.
Among the present invention, described skin care compositions with the skin effect of compacting can be to add to mutually in the described cosmetics as adding.According to specific embodiments of the present invention, cosmetics of the present invention are except comprising described skin care compositions with the skin effect of compacting, selecting of other components can be carried out according to the routine operation in this area, for example can comprise oil phase and water that some are conventional, other that commonly use in the field under perhaps further comprising add phases.In some emulsified make-ups, generally include emulsifying agent, excipient (thickening) agent, also can add basic material and necessary additive that cosmetics contain usually, emollient (vegetable oil for example for example, white oil, animal oil and derivant thereof etc.), wetting agent (glycerol for example, propylene glycol, 1,3-butanediol etc.), essence, deionized water, antioxidant, antiseptic etc., also can add some nutritional labelings, the application of these concrete compositions and consumption can be selected according to the concrete kind of described cosmetics, perhaps add according to convention amount, this is easy to grasp for a person skilled in the art.
When concrete production, can according to conventional production method, adding phase time, the skin care compositions with the skin effect of compacting of the present invention be added in the described cosmetics.Also can be that the olive oil in the skin care compositions of the present invention is sneaked in the oil phase of cosmetics, and other components be added as adding mutually.Skin care compositions of the present invention adds the cosmetics such as cream frost or emulsion to particularly in the skin care item, by controlling rational addition and suitable process conditions, can the structure of product not damaged, stability to cosmetics can not brought adverse influence, can not cause the quality problems such as variable color, layering.
For example, in a typical emulsified make-up of the present invention (protective skin cream or cold cream etc.), prescription is:
Fresh milk: 5%～10%
Olive oil: 2%～4%
Radix Hamamelidis Mollis extracting solution: 2%～4%
Hydrolyzed soybean protein: 0.5%～1.5%
Artemia (ARTEMIA) extract forms: 1%～2%
Emulsifying agent: 0.5%～10.0%
Emollient: 5%～40%
Excipient thickening agent: 0.1%～10%
Wetting agent: 5%～30%
Nutrition, functional components: optionally, formula ratio
Antiseptic: convention amount (hygienic standards for cosmetics regulation)
Antioxidant: convention amount
Deionized water: surplus.
On the other hand, the present invention also provides a kind of method for preparing described cosmetics, and the raw material of described cosmetics forms and comprises oil phase, water and the skin care compositions with the skin effect of compacting of the present invention, and the method comprises:
Make first oil phase and the water of cosmetic material carry out preliminary emulsifying, the temperature of adjusting this emulsification system adds fresh milk when being lower than 60 ℃, after stirring, then be cooled to 35～40 ℃, add olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract (as other interpolation phases are arranged in the prescription, in this step, add other and add phase), system further requires complete operation according to prescription after the cooling through stirring.
Wherein, the olive oil in the skin care compositions with the skin effect of compacting of the present invention also can be to sneak into first in the oil phase of cosmetic material, that is, the production of cosmetics of the present invention also can be to carry out in such a way:
Make first oil phase (having sneaked into the olive oil in the skin care compositions of the present invention) and the water of cosmetic material carry out preliminary emulsifying, the temperature of adjusting this emulsification system adds fresh milk when being lower than 60 ℃, after stirring, then be cooled to 35～40 ℃, add Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract (as other interpolation phases are arranged in the prescription, in this step, add other and add phase), system further requires complete operation according to prescription after the cooling through stirring.
In sum, the invention provides a kind of skin care compositions that is formed by fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract combination and the skin protection cosmetics that makes thus, for increasing skin elasticity, improve wrinkle of skin, improving skin moisturizing intensity and have synergism, can Rosemary Extract, slowing down skin aging, and cosmetic product outward appearance, inherent quality that the present invention produces can maintain a long-term stability.
The specific embodiment
Below describe the beneficial effect of implementation process of the present invention and generation in detail by specific embodiment, be intended to help the reader to understand better essence of the present invention and characteristics, but not as the restriction to this case practical range.
In following scheme description of the present invention and the prescription, used fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia (ARTEMIA) extract are commercially available.Wherein:
Fresh milk: meet the GB6914 requirement;
Olive oil: outward appearance: transparent yellow green liquid; Refraction index (20 ℃): 1.46～1.48; Relative density: 0.9160～0.9250; Acid value (mgKOH/g)≤0.5; Peroxide value (meq/kg)≤15; Oleic acid (%) 〉=72; Moisture and volatile matter content (%)≤0.05; Impurity (%)≤0.01; Supply producer: east, BeiJing, China Wan Hua International Trading Company Ltd; Trade name: set greatly the board olive oil;
Hamamelis virginiana extracting solution: outward appearance: colourless transparent liquid; PH value (10% aqueous solution): 5～6.5; Abnormal smells from the patient: special odor; Index of refraction (20 ℃) 1.4160～1.4200; Relative density (20 ℃) 1.03～1.036; Supply producer: the fragrant Shanghai company limited of moral; Marque: Extrapone Witch Hazel Dist.CL;
Hydrolyzed soybean protein: outward appearance: transparency liquid; Abnormal smells from the patient: characteristic odor; Color: yellow; PH (20 ℃): 4.0～5.0; Density, g/cm
3(20 ℃) 1.06～1.09; Refractive index (20 ℃) 1.365～1.385; Protein content (Lowry method) g/kg:1.5～3.5; Potassium sorbate content %:0.10～0.16; Sodium benzoate content %:0.240～0.30; Supply producer: the chemical (Shanghai) Co., Ltd. of leading special product; Marque DYNACHONDRINE ISR;
Artemia extract: outward appearance: transparency liquid; Abnormal smells from the patient: characteristic odor; PH (20 ℃) 5.0～6.0; Density, g/m3 (20 ℃) 1.00～1.02; Refractive index (20 ℃) 1.33～1.34; Solid content, g/kg (105 ℃) 12.0～18.0; GP4G content ppm (HPLC) 145～195; Supply producer: the chemical (Shanghai) Co., Ltd. of leading special product; Marque GP4G.
Embodiment 1: protective skin cream
The present embodiment provides a kind of crease-shedding skin-care cream, its prescription following (W%):
Glycerol hard acid esters: 3
Cetearyl alcohol: 5
Glycerol: 10
Propylene glycol: 10
Hydrogenation gathers certain herbaceous plants with big flowers alkene 5
Fresh milk: 5
Olive oil 3
Radix Hamamelidis Mollis extracting solution 3
Hydrolyzed soybean protein 1
Artemia (ARTEMIA) extract forms 1.5
Spermol polyethers-20: 1
Cocoanut oil alcohol sodium sulfovinate: 0.5
Hydroxyethyl-cellulose: 0.7
Antiseptic: an amount of
Essence: an amount of
Deionized water: surplus.
When the cosmetics of preparation the present embodiment, carry out according to following technique:
Accurately take by weighing various materials by prescription for subsequent use;
In oil phase pretreatment tank, the oil phase material (propylene glycol, cetearyl alcohol, stearin, the poly-certain herbaceous plants with big flowers alkene of hydrogenation, olive oil) that accurately takes by weighing is dropped in the still, start simultaneously agitator, be heated to 92～98 ℃, start simultaneously agitator, material is melted fully;
In water pretreatment tank, all drop into the glycerol in the prescription in the still, start stirring, and slowly be sprinkled in still with powder type hydroxyethyl-cellulose, make it fully disperse (must guard against and form pimple), other material of the water that then will accurately take by weighing (water, spermol polyethers-20, cocoanut oil alcohol sulfuric ester are received) drops in the still, is heated to 92～98 ℃, is stirred to evenly;
Filtered oil phase thing sucks through in the emulsion tank of preheating, rear suction aqueous-phase material, and starting successively scraper plate stirring, rapid stirring, homogenizer (starting emulsifying kettle rapid stirring and homogenizer approximately 10～12 minutes), emulsifying this moment temperature in the kettle should not be lower than 85 ℃.After carrying out vacuum emulsification, insulated and stirred is started the chiller cooling after 10～15 minutes again;
When temperature drops to 55～60 ℃, add and add phase (fresh milk, essence) when temperature drops to 35～40 ℃, add Hamamelis virginiana, hydrolyzed soy egg, white artemia (ARTEMIA) extract, antiseptic, continue to stir, when temperature continues to drop to 30 ℃ when spending, after the assay was approved discharging.
The crease-shedding skin-care cream of the present embodiment is without unacceptable abnormal flavour.Be applied in skin surface, salubrious, skinfeel is good.Through repeatedly heat-resisting (40 ± 1 ℃, after 24 hours recovery room temperatures), cold-resistant (15 ± 1 ℃, 24 hours recovery room temperatures) destructive testing, system is normal, without variable color, lamination.The every sense index of product, physical and chemical index, sanitary index all meet corresponding national standard.
The result of use experiment of the protective skin cream of embodiment 1
Method: for the protective skin cream of checking the present embodiment in the skin that compacts, effect aspect crease-resistant, selects 40 volunteers to carry out the effectiveness experiment, adopt double blinding design, the contrast experiment compares investigation.40 volunteers do not limit healthy population for the men and women, and the age, one group of 10 people were divided into 4 groups at random between 50～56 years old.Wherein the A group is for using the protective skin cream of the embodiment of the invention 1; The experiment of B group is compared with the protective skin cream of the embodiment of the invention 1 with protective skin cream, added fresh milk, olive oil and artemia (ARTEMIA) extract of equivalent, do not add Hamamelis virginiana extracting solution and hydrolyzed soybean protein, other effect components are identical, and are in shortage alternative with deionized water; The experiment of C group is compared with the protective skin cream of the embodiment of the invention 1 with protective skin cream, Hamamelis virginiana extracting solution and the hydrolyzed soybean protein of equivalent have been added, do not add fresh milk, olive oil and artemia (ARTEMIA) extract, other effect components are identical, and are in shortage alternative with deionized water; The experiment of D group is compared with the protective skin cream of the embodiment of the invention 1 with protective skin cream, does not add fresh milk, olive oil, artemia extract, Hamamelis virginiana extracting solution and hydrolyzed soybean protein, but substitutes with deionized water, and other effect components are identical.
Four groups of A, B, C, D require once described protective skin cream of for each person every day early, middle and late use, and using method spreads upon face in right amount for getting, and loop gently to Emulsion to absorb fully.
Every user is carried out regular follow-up investigation, adopts skinanalysis apparatus (Derma-Expert MC760), per 10 days for the one-phase test once, testing the position is the both sides cheek.To skin recover natural elasticity, improve wrinkle of skin and coarse, improve several respects such as moistening intensity and test and go forward side by side line number according to one's analysis.Outcome record is in following table.
The skin elasticity test annotates 1
Annotate 1:D
0Volunteer both sides cheek is carried out respectively flexibility test, set up archives, be recorded as basic value, after the experiment beginning, increase 〉=5 than basic value, for improving volunteer's number.
Annotate 2: represented numerical value is the meansigma methods of the shown data of skinanalysis apparatus in the table, and (the 10th day data deduct the 0th day data D to volunteer's skin elasticity value
10-D
0), (the 20th day data deduct the 10th day data D
20-D
10) larger, elasticity is better.
The test of skin friction power annotates 1
Annotate 1:D
0Volunteer both sides cheek is carried out respectively friction testing, set up archives, be recorded as basic value, after the experiment beginning, reduce 〉=10 than basic value, for improving volunteer's number.
Annotate 2: represented numerical value is the meansigma methods of the shown data of skinanalysis apparatus in the table, volunteer's skin friction power (D
10-D
0), (D
20-D
10) less, skin surface is more level and smooth, and wrinkle is more shallow.
The test of skin moisture content annotates 1
Annotate 1:D
0Volunteer both sides cheek is carried out respectively the test of skin moisture content, and measuring condition is 20 ℃ of temperature and relative humidity 40～60%, sets up archives, is recorded as basic value, after the experiment beginning, increases 〉=5 than basic value, for improving volunteer's number.
Annotate 2: represented numerical value is the meansigma methods of the shown data of skinanalysis apparatus in the table, volunteer's skin water content (D
10-D
0), (D
20-D
10) larger, skin is more moist.
Interpretation:
Can find out from above embodiment and result of use contrast: the skin elasticity aspect, the skin elasticity number of A group tester after 20 days obviously promoted than other three groups (not containing or contain part skin care compositions composition), recover the pliability of skin, although and two groups of B, C have valid data, but the improvement number is compared still lower, and the D group is basic not to be improved; Skin friction power aspect, A group tester skin friction value shows the reduction of certain amplitude, and the skin smoothness is effectively improved, and wrinkle obviously shoals, and B, C group tester has the part improver, but the skin sense organ is very unobvious, and the D group is basic not to be improved; Skin moisture content aspect, the testing result demonstration, the tester is than three groups of B, C, D for the A group, and water content rises, and moist degree is improved.
Embodiment 2: facial treatment milk
The present embodiment provides a kind of crease-resistant facial treatment milk, its prescription following (W%):
Glyceryl stearate: 1.5
Cetearyl alcohol: 1
Glycerol: 10
Propylene glycol: 10
Hydrogenation gathers certain herbaceous plants with big flowers alkene: 5
Fresh milk: 6
Olive oil: 3.5
Radix Hamamelidis Mollis extracting solution: 2.5
Hydrolyzed soybean protein: 1.5
Artemia (ARTEMIA) extract forms: 1
Spermol polyethers-20: 1
Cocoanut oil alcohol sodium sulfovinate: 0.5
Hydroxyethyl-cellulose: 0.3
Antiseptic: an amount of
Essence: an amount of
Deionized water: surplus.
When the cosmetics of preparation the present embodiment, carry out according to following technique:
Accurately take by weighing each material by prescription for subsequent use; In oil phase pretreatment tank, the oil phase material (propylene glycol, cetearyl alcohol, stearin, the poly-certain herbaceous plants with big flowers alkene of hydrogenation, olive oil) that accurately takes by weighing is dropped in the still, start simultaneously agitator, be heated to 92～98 ℃, start simultaneously agitator, material is melted fully; In water pretreatment tank, all drop into the glycerol in the prescription in the still, start stirring, and slowly be sprinkled in still with powder type hydroxyethyl-cellulose, make it fully disperse (must guard against and form pimple), other material of the water that then will accurately take by weighing (water, spermol polyethers-20, cocoanut oil alcohol sulfuric ester are received) drops in the still, is heated to 92～98 ℃, is stirred to evenly;
Filtered oil phase thing sucks through in the emulsion tank of preheating, rear suction aqueous-phase material, and starting successively scraper plate stirring, rapid stirring, homogenizer (starting emulsifying kettle rapid stirring and homogenizer approximately 10～12 minutes), emulsifying this moment temperature in the kettle should not be lower than 85 ℃.After carrying out vacuum emulsification, insulated and stirred is started the chiller cooling after 10～15 minutes again;
When temperature drops to 55～60 ℃, add and add phase (fresh milk, essence), stir, when continuing to cool to 35～40 ℃, add Hamamelis virginiana, hydrolyzed soy egg, white artemia (ARTEMIA) extract, antiseptic, stir, continue to cool to 30 ℃ when spending, after the assay was approved discharging.
The facial treatment milk of the present embodiment is without unacceptable abnormal flavour.Be applied in skin surface, salubrious, skinfeel is good.Through repeatedly heat-resisting (40 ± 1 ℃, after 24 hours recovery room temperatures), cold-resistant (5 ± 1 ℃, 24 hours recovery room temperatures) destructive testing, system is normal, without muddiness, variable color, lamination.The every sense index of product, physical and chemical index, sanitary index all meet corresponding national standard.
The result of use experiment of the facial treatment milk of embodiment 2
Method: for the facial treatment milk of checking the present embodiment in the skin that compacts, effect aspect crease-resistant, selects 30 volunteers to carry out the effectiveness experiment, adopt double blinding design, the contrast experiment compares investigation.30 volunteers do not limit healthy population for the men and women, and the age, one group of 10 people were divided into 3 groups at random between 50～56 years old.Wherein the A group is for using the facial treatment milk of the embodiment of the invention 2; The experiment of B group is compared with the facial treatment milk of the embodiment of the invention 2 with facial treatment milk, fresh milk, olive oil and the artemia extract of equivalent have been added, do not add Hamamelis virginiana extracting solution and hydrolyzed soybean protein, other effect components are identical, and are in shortage alternative with deionized water; The experiment of C group is compared with the facial treatment milk of the embodiment of the invention 2 with facial treatment milk, Hamamelis virginiana extracting solution and the hydrolyzed soybean protein of equivalent have been added, do not add fresh milk, olive oil and artemia (ARTEMIA) extract, other effect components are identical, and are in shortage alternative with deionized water.
Three groups of A, B, C require once described skin care milk of for each person every day early, middle and late use, and using method spreads upon face in right amount for getting, and loop gently to Emulsion to absorb fully.
Every user is carried out regular follow-up investigation, adopts skinanalysis apparatus (Derma-Expert MC760), per 10 days for the one-phase test once, testing the position is the both sides cheek.To skin recover natural elasticity, improve wrinkle of skin and coarse, improve several respects such as moistening intensity and test and go forward side by side line number according to one's analysis.
The skin elasticity test annotates 1
Annotate 1:D
0Volunteer both sides cheek is carried out respectively flexibility test, set up archives, be recorded as basic value, after the experiment beginning, the basis is straight increases 〉=5, for improving volunteer's number.
Annotate 2: represented numerical value is the meansigma methods of the shown data of skinanalysis apparatus in the table, volunteer's skin elasticity value (D
10-D
0), (D
20-D
10) larger, elasticity is better.
The test of skin friction power annotates 1
Annotate 1:D
0Volunteer both sides cheek is carried out respectively friction testing, set up archives, be recorded as basic value, after the experiment beginning, reduce 〉=10 than basic value, for improving volunteer's number.
Annotate 2: represented numerical value is the meansigma methods of the shown data of skinanalysis apparatus in the table, volunteer's skin friction power (D
10-D
0), (D
20-D
10) less, skin surface is more level and smooth, and wrinkle is more shallow.
The test of skin moisture content annotates 1
Annotate 1:D
0Volunteer both sides cheek is carried out respectively the test of skin moisture content, set up archives, be recorded as basic value, after the experiment beginning, increase 〉=5 than basic value, for improving volunteer's number.
Annotate 2: represented numerical value is the meansigma methods of the shown data of skinanalysis apparatus in the table, volunteer's skin water content (D
10-D
0), (D
20-D
10) larger, skin is more moist.
Interpretation
Can find out from above embodiment and result of use contrast, the skin elasticity aspect, the A group is used the tester of the facial treatment milk that contains skin care compositions, skin elasticity number after 20 days was obviously promoted than other two groups (containing the part functional component), recover the pliability of skin, although and two groups of B, C have valid data, it is still lower that the improvement number is compared; Skin friction power aspect, A group tester skin friction value shows the reduction of certain amplitude, and the skin smoothness is effectively improved, and wrinkle obviously shoals, and B, C group tester has the part improver, but the skin sense organ is very unobvious; Skin moisture content aspect, the testing result demonstration, the tester is than two groups of B, C for the A group, and water content rises, and moist degree is improved.
Conclusion: skin care compositions of the present invention effect aspect wrinkle removing, increase skin elasticity, the moist intensity of raising is remarkable.Each component in the compositions is composite to have a significant cooperative effect, with after make skin increase elasticity, recover the pliability of skin, delay the appearance of wrinkle, poor for skin elasticity, tarnish, old and feeble too early crowd, often use, can make skin smoothly careful, glittering and translucent, make it beautiful one new, delicate fitness is takeed good care of skin comprehensively.
Claims (9)
1. skin care compositions, said composition is comprised of fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract; Wherein, the weight proportion of described fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract is 3～10: 2～4: 2～4: 0.5～1.5: 1～2.
2. skin care compositions according to claim 1, wherein, described olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract quality require as follows:
Olive oil: outward appearance: transparent yellow green liquid; 20 ℃ of refraction indexs: 1.46～1.48; Relative density: 0.9160～0.9250; Acid value≤0.5mgKOH/g; Peroxide value≤15meq/kg; Oleic acid 〉=72%; Moisture and volatile matter content≤0.05%; Impurity≤0.01%;
Hamamelis virginiana extracting solution: outward appearance: colourless transparent liquid; 10% pH value of water solution: 5～6.5; 20 ℃ of indexs of refraction: 1.4160～1.4200; 20 ℃ of relative densities: 1.03～1.036;
Hydrolyzed soybean protein: outward appearance: transparency liquid; Color: yellow; 20 ℃ of pH:4.0～5.0; 20 ℃ of density, g/cm
3: 1.06～1.09; 20 ℃ of refractive indexs: 1.365～1.385; Protein content: 1.5～3.5g/kg; Potassium sorbate content: 0.10%～0.16%; Sodium benzoate content: 0.240%～0.30%;
Artemia extract: outward appearance: transparency liquid; 20 ℃ of pH:5.0～6.0; 20 ℃ of density g/m
3: 1.00～1.02; 20 ℃ of refractive indexs: 1.33～1.34; Solid content: 12.0～18.0g/kg; GP4G content 145～195ppm.
3. skin care compositions according to claim 1, wherein, the weight proportion of described fresh milk, olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract is 4～6: 3: 3: 1: 1.5.
4. the application of each described skin care compositions of claim 1～3 in producing cosmetics.
5. application according to claim 4, wherein said cosmetics are for improving skin moisturizing intensity, improving wrinkle of skin and degree of roughness, perhaps for increasing skin elasticity.
6. cosmetics wherein contain each described skin care compositions of claim 1～3.
7. cosmetics according to claim 6, wherein, the weight content of described skin care compositions in these cosmetics is 0.5%～20%.
8. according to claim 6 or 7 described cosmetics, it is anti-wrinkling cream frost or crease-resistant emulsion.
9. the production method of each described cosmetics of claim 6～8, the raw material of these cosmetics forms and comprises oil phase, water and 1～3 each described skin care compositions, and the method comprises:
Make first oil phase and the water of cosmetic material carry out preliminary emulsifying, the temperature of adjusting this emulsification system adds fresh milk when being lower than 60 ℃, after stirring, then be cooled to 35～40 ℃, add olive oil, Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract, system is through stirring the further discharging that is up to the standards of lowering the temperature; Perhaps,
First olive oil is sneaked into the oil phase of cosmetic material, make oil phase and water carry out preliminary emulsifying, the temperature of adjusting this emulsification system adds fresh milk when being lower than 60 ℃, after stirring, then be cooled to 35～40 ℃, add Hamamelis virginiana extracting solution, hydrolyzed soybean protein, artemia extract, system is through stirring the further discharging that is up to the standards of lowering the temperature.
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| CN103284928A (en) * | 2013-07-02 | 2013-09-11 | 孙佳丽 | Medicine for shrinking enlarged pores by utilizing egg white and preparation method thereof |
| CN103340786A (en) * | 2013-07-05 | 2013-10-09 | 上海珍馨化工科技有限公司 | Witch hazel toner |
| CN103494754B (en) * | 2013-08-27 | 2015-09-23 | 星彤（上海）化妆品科技有限公司 | Hair-loss preventing and hair-restoring shampoo of herbal essences and biochemical component formula and preparation method thereof |
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| CN105078873A (en) * | 2014-05-16 | 2015-11-25 | 天津强微特生物科技有限公司 | Biological skin protecting composition with tightening and whitening effects |
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| CN105193677A (en) * | 2015-10-29 | 2015-12-30 | 桂林华诺威基因药业有限公司 | Composition with acne removal efficacy |
| CN105310972A (en) * | 2015-10-29 | 2016-02-10 | 桂林华诺威基因药业有限公司 | Anti-wrinkle skin care product |
| CN105193702A (en) * | 2015-10-29 | 2015-12-30 | 桂林华诺威基因药业有限公司 | Skin-care composition with repairing, regeneration and senescence delaying functions |
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| CN105193694A (en) * | 2015-10-29 | 2015-12-30 | 桂林华诺威基因药业有限公司 | Skin care product with whitening and freckle-removing functions |
| CN105596273B (en) * | 2015-11-24 | 2017-03-29 | 广州市花安堂生物科技有限公司 | Clear Virgin's milk liquid of a kind of Shu Run and preparation method thereof |
| CN107019664A (en) * | 2016-04-06 | 2017-08-08 | 广州暨大美塑生物科技有限公司 | A kind of elite breast for alleviating local wrinkle and preparation method thereof |
| CN106420560B (en) * | 2016-10-19 | 2019-05-14 | 广东丸美生物技术股份有限公司 | Skin matrix and its preparation and application with moisturizing and sensitive skin effect of releiving |
| CN107595703A (en) * | 2017-10-14 | 2018-01-19 | 李丹丹 | A kind of Chinese medicine composition and its purposes in aesthetic care products as astringent |
| US20220133622A1 (en) * | 2020-10-30 | 2022-05-05 | Mary Kay Inc. | Instant effect eye cream |
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| CN102125511B (en) * | 2010-01-19 | 2015-04-29 | 上海华银日用品有限公司 | Tendering, whitening and moisturizing cream and preparation method thereof |
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