CN106727237A - A kind of nourishing type lipstick and preparation method thereof - Google Patents
A kind of nourishing type lipstick and preparation method thereof Download PDFInfo
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- CN106727237A CN106727237A CN201611218091.1A CN201611218091A CN106727237A CN 106727237 A CN106727237 A CN 106727237A CN 201611218091 A CN201611218091 A CN 201611218091A CN 106727237 A CN106727237 A CN 106727237A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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Abstract
The present invention relates to a kind of nourishing type lipstick, it is constituted by moistening moisturizing component, antioxidant composition, promoting blood circulation rush absorbent components, anti-inflammatory component of releiving, natural pigment, excipient component and helper component.Present invention also offers the preparation method of above-mentioned nourishing type lipstick.Can not only assign lip naturally ruddy beautiful color and luster using nourishing type lipstick of the invention, improve because drying that cheilogramma caused by water shortage is deep, lip decortication situation, and can effectively resist injury of the ultraviolet to skin of lip, delay skin of lip aging, long-term use can improve that skin of lip is obscure, make the state that it returns to ruddy health.Nourishing type lipstick of the invention is safe All Pure Nature formula, is particularly suitable for lip sensitive group and uses.
Description
Technical field
The present invention relates to cosmetic field, more specifically it relates to a kind of nourishing type lipstick and preparation method thereof.
Background technology
Lip is the extension of skin of face, is connected with mucous membrane in oral cavity, and its cuticula is thinner than general skin, and again without hair
The accessory organs such as capsule, sebaceous glands, sweat gland, it is especially sensitive to drying, low temperature environment, easily there is microgroove, water shortage, decortication, dry and cracked
Etc. phenomenon.And skin of lip basalis is relatively thin, without melanocyte, self-protection and the external injury ability of defence, for a long time
Under ultraviolet irradiation, lip is easily aging, lip discoloration depth.So seeming particularly to the nursing such as the moist of lip, moisturizing, sun-proof
It is important.
Lipstick is a kind of conventional lip makeups product, and the color and luster of beauty can be provided for lip, makes its delicate and charming brilliant, for
Crucial touch is played a part of in face's makeups.Lipstick on current market generally only focuses on attractive in appearance and skin sense, and have ignored to making
The health care and maintenance of user's lip, it is difficult to accomplish that both there are beautifying functions, and with moisturizing, moisturizing and anti-ageing healthy work(of waiting for a long time
Effect, long-term use is easily caused dry and cracked lip, decortication, sensitivity.Therefore, a good lipstick will be, it is necessary to will beautify organic with maintenance
With reference to.
The content of the invention
Be to solve problem above, the invention provides a kind of nourishing type lipstick, its by moisten moisturizing component, anti-oxidant group
Divide, promoting blood circulation promotees absorbent components, anti-inflammatory component of releiving, natural pigment, excipient component and helper component composition.
Preferably, the moist moisturizing component includes：The jojoba oil of 20-25 weight portions, the spiny dogfish of 10-15 weight portions
Alkane, the rice bran oil of 5-10 weight portions, the cocoa butter of 4-5 weight portions, the honey of 1-3 weight portions, the tuberose of 1-3 weight portions are extracted
Thing.
Preferably, the antioxidant composition includes：The vitamin E of 2-5 weight portions and the sweet osmanthus pericarp of 0.1-0.5 weight portions
Melanin.
Preferably, the promoting blood circulation promotees absorbent components includes：The angelica extract of 2-5 weight portions, the idesia of 4-7 weight portions
Oil, the peony seed oil of 1-3 weight portions, the safflower seed oil of 1-3 weight portions.
Preferably, the anti-inflammatory component of releiving includes：The Sage extract of 1-3 weight portions.
Preferably, the natural pigment includes：The capsorubin of 3-5 weight portions, the alkermes of 0-4 weight portions, 0.1-
The sweet osmanthus pericarp melanin of 0.5 weight portion.
Preferably, the excipient component includes：The beeswax of 10-15 weight portions, the Brazil wax of 2-5 weight portions, 3-6 weights
Candelila wax, the rice bran wax and helper component of 3-4 weight portions of part are measured, the helper component includes：The Ma Ling of 1-2 weight portions
Sweet potato starch (preventing from perspiring, there is provided smooth skin sense), the Salvia japonica essential oil (imparting faint scent) of 0.1-0.3 weight portions.
Preferably, the nourishing type lipstick includes following component：The jojoba oil of 20-25 weight portions, 10-15 weight portions
Saualane, the rice bran oil of 5-10 weight portions, the cocoa butter of 4-5 weight portions, the honey of 1-3 weight portions, the tuberose of 1-3 weight portions
Extract, the vitamin E of 2-5 weight portions, the sweet osmanthus pericarp melanin of 0.1-0.5 weight portions, the beeswax of 10-15 weight portions, 2-5
The Brazil wax of weight portion, the candelila wax of 3-6 weight portions, the rice bran wax of 3-4 weight portions, the Radix Angelicae Sinensis of 2-5 weight portions are extracted
Thing, the idesia oil of 4-7 weight portions, the peony seed oil of 1-3 weight portions, the safflower seed oil of 1-3 weight portions, the mouse of 1-3 weight portions
Tail grass extract, the capsorubin of 3-5 weight portions, the alkermes of 0-4 weight portions, the farina of 1-2 weight portions, 0.1-
The Salvia japonica essential oil of 0.3 weight portion.
Present invention also offers a kind of preparation method of above-mentioned nourishing type lipstick, it is comprised the following steps：
1) sweet osmanthus pericarp melanin, capsorubin are well mixed with alkermes and farina, add part
Jojoba oil grinds, and obtains mill base；
2) remaining jojoba oil, saualane, rice bran oil, idesia oil, peony seed oil, safflower seed oil, vitamin E are mixed
Stir；
3) in step 2) cocoa butter, beeswax, Brazil wax, candelila wax, rice bran wax are added in the mixture that obtains, plus
Heat obtains oil mixture to 85 DEG C or so；
4) tuberose extract, angelica extract, Sage extract are mixed, are heated to 85 DEG C or so, add honey,
Be sufficiently stirred for, be added to step 3) obtained in oil mixture, be well mixed；
5) by step 1) mill base be added to step 4) mixture in, in stirring 10min under 300-500r/min；
6) mixture is cooled to 60 DEG C or so, adds Salvia japonica essential oil, mixing forms lotion；
7) lotion is injected into and is preheating in 35-40 DEG C of mould in advance, be positioned at 5-10 DEG C, taken after 30 minutes
Go out the demoulding, that is, obtain the nourishing type lipstick；
Preferably, the sweet osmanthus pericarp melanin is obtained by following steps：
1) by 1:5 weight extracts 36h than the sweet osmanthus pericarp is mixed with the ammonia spirit of pH=10.5 at 25 DEG C,
Skin slag is filtered to remove, sweet osmanthus pericarp melanin leaching liquor is obtained；
2) the sweet osmanthus pericarp melanin leaching liquor is taken into supernatant in 30-35min is centrifuged under 3000-3500r/min,
PH is adjusted to 2.5 with the HCl solution of 2mol/L, melanin deposition is separated out, 12h is stored at room temperature, and is centrifugally separating to obtain precipitation, i.e.,
Sweet osmanthus pericarp melanin crude product；
3) the sweet osmanthus pericarp melanin crude product is hydrolyzed into 2h with the HCl of 1mol/L at 100 DEG C, suction filtration, then successively
Filter residue is washed with chloroform, ethyl acetate, 95% ethanol, neutrality is finally washed with distilled water to, then by filter residue at 60-80 DEG C
Lower drying obtains described refined sweet osmanthus pericarp melanin to constant weight；
The capsorubin is obtained by following steps：
1) by dry pimiento, remove seed is shredded, 40 mesh sieves is crossed after crushing, the Paprika is pressed 1：9 weight ratio adds
Enter 15% NaOH solution, in extracting 2h, intermittent stirring at 55 DEG C；
2) filtering removal alkali lye, filter residue is washed with deionized to neutrality, is obtained except the capsicum skin powder after peppery；
3) will remove it is peppery after capsicum skin powder wrapped with filter paper, loaded on apparatus,Soxhlet's in, with acetone extraction, carried at 70 DEG C
4-5h is taken, the acetone extract of capsorubin is obtained；
4) acetone extract of the capsorubin is concentrated by evaporation, is dried to constant weight at 60-80 DEG C, obtain described peppery
Green pepper red pigment；
The angelica extract is obtained by with water in extraction Radix Angelicae Sinensis at 85 DEG C；
The Sage extract is obtained by with water in extraction rat-tail grass meal at 100 DEG C；
The tuberose extract is obtained in extracting dry tuberose at 65 DEG C by with water.
Jojoba oil is mainly senior unsaturated wax ester in the present invention, and its permeability is stronger than triglyceride, moisturizing effect
It is good.Jojoba oil can form one layer of very thin oil film on skin, can not only reduce the loss of transepidermal water but also not influence skin
The breathing of skin, soft and non-greasy is very salubrious comfortable, is excellent moist moisturizing ingredient.Saualane is a kind of group of sebum
Point, and skin affinity is by force, the saualane in lipstick can be combined together with sebum film, and one layer of natural screen is formed in skin surface
Barrier, with moisture-keeping function.Rice bran oil is rich in vitamin E, and oxidation resistance is strong, also contains abundant oryzanol, phosphatide, spiny dogfish
Various active skull cap components such as alkene, phytosterol, have to skin and moisten health-care efficacy.The fusing point of cocoa butter is about 34-38 DEG C,
It is a kind of existing hardness and melting speed lipid faster, provides perfect soft and moist sense of touch can to lip.Honey main component
It is carbohydrate, accounts for more than the 3/4 of honey total amount, wherein based on fructose and glucose, micro mineral matter and dimension is contained in honey
Raw plain and various enzymes, protein, amino acid etc., can improve the nutrition condition on skin of lip surface, to lip in lipstick
With nourishing effect.《Cosmetics plant material is complete works of》Record, tuberose extract can improve the water content of cuticula：Will be late fragrant
Beautiful water extract is configured to 0.01% solution, applies skin, determines cutaneous application sample and blank examination after 100min respectively
The electrical conductivity of sample, and compare with aloe extract, conductivity value is respectively:The μ s/cm of tuberose 126, the μ s/cm of aloe 111, blank
The μ s/cm of sample 35, the moistening effect of tuberose extract is more excellent than aloe extract, can effectively improve the aqueous of cuticula
Amount.
Vitamin E in the present invention, is conventional antioxidant also known as tocopherol.Sweet osmanthus pericarp melanin has excellent
Inoxidizability, can both prevent the oxidation of lipstick itself, injury of the ultraviolet to skin of lip can also be resisted.There is research table
Bright, the antioxidation activity of sweet osmanthus pericarp melanin is four times of ascorbic acid.With conventional antioxidant 2,6- di-t-butyl -4- first
Base phenol (BHT) is contrasted, and sweet osmanthus pericarp melanin is to Fe3+Reducing power be far longer than BHT.Sweet osmanthus pericarp melanin can show
Write the lipid peroxidation for suppressing yolk.
Angelica extract has and activates blood circulation and disperses blood clots, improves skin microcirculation, the effect of tough blood vessel in the present invention, may also suppress
The membrane lipid peroxidatio that superoxide radical causes, it is obvious to improving the caused colour of skin dimness effect of oxidation.Peony seed oil is unsaturated
Up to more than 90%, wherein alpha-linolenic acid content is up to 40% to content of fatty acid, circulated with promoting blood circulation and removing blood stasis, improvement skin blood,
Promote the function of cytothesis, you can taking orally again can external application.Also contain micro VA, VE, niacin, carrot in peony seed oil
Element etc., has nutritive effect, delay skin aging to skin.Safflower seed oil contains about 80% linoleic acid, and its penetration is strong, can
To effectively facilitate the absorption of active component.Idesia oil is a kind of new plant oil sources developed in the present invention, is being made up
Application is yet there are no in product, its linoleic acid content is up to 70%, and containing abundant vitamin E, skin is to the oily absorbability
Fabulous, being blended with rush improves the function of blood microcirculation.The present invention coordinates idesia oil, peony seed oil and safflower seed oil should
In for lipstick, infiltration and absorption of the skin of lip to effect material can be promoted.
Sage extract has anti-inflammatory in the present invention.Pharmacological research is carried out to Sage extract, finds it to glimmering
Light element enzyme has activation, and concentration is 0.1% 50% alcoholic extract, and the activation rate to uciferase activity reaches
141.1%, there is obvious anti-scytitis.
Capsorubin in the present invention, is extracted from capsicum skin, belongs to one kind of carotenoid, bright in colour, thermally-stabilised
Property is good, is natural colouring agent.Alkermes are a kind of natural pigments extracted from cochineal body, and chemical constitution belongs to anthraquinone
Class, stable in physicochemical property is considered safest natural pigment.
Brazil wax fusing point is 82-86 DEG C in the present invention, and quality is hard, and glossiness is high.Make excipients in lipstick, together
When assign product gloss.Candelila wax structure is fine, and quality is harder more crisp, and shrinkage factor is small, and sense of touch is smooth, can be effectively improved lipstick
Ductility, improve lipstick heat endurance, make the color and luster of lipstick more natural.Beeswax has good plastotype and stripping
Property, contribute to the shaping and the demoulding of lipstick.The fusing point of rice bran wax is shared at 80-85 DEG C with Brazil wax, improves the steady of lipstick
It is qualitative.
Salvia japonica essential oil has pure and fresh fragrance, has calm and double effects of releiving concurrently.It is blue that the essential oil can significantly inhibit leather
The infection that family name's positive bacteria and Gram-negative bacteria cause, is commonly used in dental care product.Salvia japonica essential oil is used in the present invention
Simple and elegant comfortable fragrance can be provided, it may have certain antibacterial effect.Farina has stronger oil absorption, not only can be with
Lipstick " perspiration " is prevented, makes lotion more stable, and the loss of lip moisture can be reduced, strengthen the tack of lipstick pigment.
The mutual cooperation of above material, makes lipstick of the invention to assign skin of lip naturally ruddy beautiful color
Pool, improves the situation deep because drying decortication caused by water shortage, cheilogramma, and can effectively resist ultraviolet to skin of lip
Injury, delays skin of lip aging, and long-term use can improve that skin of lip is obscure or bloodless situation, and return to it
The state of ruddy health.Raw material used in the present invention is all safety natural products high, and being especially suitable for lip sensitive group makes
With.
Brief description of the drawings
Fig. 1 is the anti-oxidant induction time statistical chart of sample 1-3.
Specific embodiment
Principle of the invention and feature are described below in conjunction with example, example is served only for explaining the present invention, and
It is non-for limiting the scope of the present invention.
Embodiment 1
Formula is (by weight)：25 parts of jojoba oil, 15 parts of saualane, 7 parts of rice bran oil, 4 parts of cocoa butter, 2 parts of honey, evening
Fragrant 2 parts of extract of jade, 3 parts of vitamin E, 0.2 part of sweet osmanthus pericarp melanin, 12 parts of beeswax, 4 parts of Brazil wax, candelila wax
3 parts, 3 parts of rice bran wax, 3 parts of angelica extract, 5 parts of idesia oil, 2 parts of peony seed oil, 1 part of safflower seed oil, Sage extract 2
Part, capsicum is red 3 parts, 2 parts of alkermes, 2 parts of farina, 0.1 part of Salvia japonica essential oil.
Preparation method：
1) 0.2 part of sweet osmanthus pericarp melanin, 3 parts of capsorubins are mixed with 2 parts of alkermes and 2 parts of farinas
Uniformly, to add 5 parts of jojoba oils to grind to form fine and smooth pulpous state standby；
2) by 20 parts of jojoba oils, 15 portions of saualanes, 7 portions of rice bran oils, 3 portions of vitamin Es, 5 portions of idesia oils, 2 portions of tree peonies
Seed oil, 1 part of safflower seed oil are well mixed；
3) in step 2) 4 parts of cocoa butters, 12 parts of beeswaxs, 4 parts of Brazil waxs, 3 parts of candelila waxes, 3 are added in mixture
Part rice bran wax, is heated to 85 DEG C, and mixture is formed after fusing；
4) 2 parts of tuberose extracts, 3 parts of angelica extracts, 2 parts of Sage extracts are mixed, is heated to 85 DEG C, then add
Enter 2 parts of honey, be sufficiently stirred for, be added to step 3) oil phase in, be well mixed；
5) by step 1) mill base be added to step 4) mixture in, stir 10min under 400r/min；
6) by step 5) mixture be cooled to 60 DEG C, add 0.1 part of Salvia japonica essential oil, mixing forms lotion；
7) lotion is injected into and is preheating in 35 DEG C of mould in advance, be positioned under the conditions of 10 DEG C, taken after 30 minutes
Go out the demoulding, that is, obtain the nourishing type lipstick.
Embodiment 2
Formula is (by weight)：20 parts of jojoba oil, 15 parts of saualane, 8 parts of rice bran oil, 5 parts of cocoa butter, 3 parts of honey, evening
Fragrant 3 parts of extract of jade, 4 parts of vitamin E, 0.1 part of sweet osmanthus pericarp melanin, 12 parts of beeswax, 5 parts of Brazil wax, candelila wax
3 parts, 2 parts of rice bran wax, 4 parts of angelica extract, 4 parts of idesia oil, 2 parts of peony seed oil, 2 parts of safflower seed oil, Sage extract 2
Part, 3 parts of capsorubin, 2 parts of alkermes, 1 part of farina, 0.2 part of Salvia japonica essential oil.
Preparation method：
1) 0.2 part of sweet osmanthus pericarp melanin, 3 parts of capsorubins are mixed with 2 parts of alkermes and 2 parts of farinas
Uniformly, to add 5 parts of jojoba oils to grind to form fine and smooth pulpous state standby；
2) by 15 parts of jojoba oils, 15 parts of saualanes, 8 parts of rice bran oils, 4 parts of vitamins, 4 parts of idesia oils, 2 parts of peony seeds
Oil, 2 parts of safflower seed oils are well mixed；
3) in step 2) 5 parts of cocoa butters, 12 parts of beeswaxs, 5 parts of Brazil waxs, 3 parts of candelila waxes, 2 are added in mixture
Part rice bran wax, is heated to 85 DEG C, and mixture is formed after fusing；
4) 3 parts of tuberose extracts, 4 parts of angelica extracts, 2 parts of Sage extracts are mixed, is heated to 85 DEG C, then add
Enter 3 parts of honey, be sufficiently stirred for, be added to step 3) oil phase in, be well mixed；
5) by step 1) mill base be added to step 4) mixture in, stir 10min under 350r/min；
6) by step 5) mixture be cooled to 60 DEG C, add 0.2 part of Salvia japonica essential oil, mixing forms lotion；
7) lotion is injected into and is preheating in 40 DEG C of mould in advance, be positioned under the conditions of 8 DEG C, taken out after 30 minutes
The demoulding, that is, obtain the nourishing type lipstick.
Embodiment 3
Formula is (by weight)：20 parts of jojoba oil, 16 parts of saualane, 5 parts of rice bran oil, 4 parts of cocoa butter, 2 parts of honey, evening
Fragrant 3 parts of extract of jade, 4 parts of vitamin E, 0.2 part of sweet osmanthus pericarp melanin, 10 parts of beeswax, 4 parts of Brazil wax, candelila wax
6 parts, 3 parts of rice bran wax, 3 parts of angelica extract, 4 parts of idesia oil, 3 parts of peony seed oil, 1 part of safflower seed oil, Sage extract 2
Part, 4 parts of capsorubin, 2 parts of farina, 0.1 part of Salvia japonica essential oil.
Preparation method：
1) 0.2 part of sweet osmanthus pericarp melanin, 4 parts of capsorubins and 2 parts of farinas are well mixed, add 5 parts
It is standby that jojoba oil grinds to form fine and smooth pulpous state；
2) by 15 parts of jojoba oils, 16 portions of saualanes, 5 portions of rice bran oils, 4 portions of vitamin Es, 4 portions of idesia oils, 3 portions of tree peonies
Seed oil, 1 part of safflower seed oil are well mixed；
3) in step 2) 4 parts of cocoa butters, 10 parts of beeswaxs, 4 parts of Brazil waxs, 6 parts of candelila waxes, 3 are added in mixture
Part rice bran wax, is heated to 85 DEG C, and mixture is formed after fusing；
4) 3 parts of tuberose extracts, 3 parts of angelica extracts, 2 parts of Sage extracts are mixed, is heated to 85 DEG C, then add
Enter 2 parts of honey, be sufficiently stirred for, be added to step 3) oil phase in, be well mixed；
5) by step 1) mill base be added to step 4) mixture in, stir 10min under 400r/min；
6) by step 5) mixture be cooled to 60 DEG C, add 0.1 part of Salvia japonica essential oil, mixing forms lotion；
7) lotion is injected into and is preheating in 40 DEG C of mould in advance, be positioned under the conditions of 10 DEG C, taken after 30 minutes
Go out the demoulding, that is, obtain the nourishing type lipstick.
Embodiment 4
Formula is (by weight)：25 parts of jojoba oil, 10 parts of saualane, 6 parts of rice bran oil, 4 parts of cocoa butter, 3 parts of honey, evening
Fragrant 3 parts of extract of jade, 2 parts of vitamin E, 0.3 part of sweet osmanthus pericarp melanin, 12 parts of beeswax, 4 parts of Brazil wax, candelila wax
4 parts, 3 parts of rice bran wax, 5 parts of angelica extract, 5 parts of idesia oil, 3 parts of peony seed oil, 2 parts of safflower seed oil, Sage extract 3
Part, 3 parts of capsorubin, 2 parts of alkermes, 2 parts of farina, 0.2 part of Salvia japonica essential oil.
Preparation method：
1) 0.3 part of sweet osmanthus pericarp melanin, 3 parts of capsorubins are mixed with 2 parts of alkermes and 2 parts of farinas
Uniformly, to add 5 parts of jojoba oils to grind to form fine and smooth pulpous state standby；
2) by 20 parts of jojoba oils, 10 portions of saualanes, 6 portions of rice bran oils, 2 portions of vitamin Es, 5 portions of idesia oils, 3 portions of tree peonies
Seed oil, 2 parts of safflower seed oils are well mixed；
3) in step 2) 4 parts of cocoa butters, 12 parts of beeswaxs, 4 parts of Brazil waxs, 4 parts of candelila waxes, 3 are added in mixture
Part rice bran wax, is heated to 85 DEG C, and mixture is formed after fusing；
4) 3 parts of tuberose extracts, 5 parts of angelica extracts, 3 parts of Sage extracts are mixed, is heated to 85 DEG C, then add
Enter 3 parts of honey, be sufficiently stirred for, be added to step 3) oil phase in, be well mixed；
5) by step 1) mill base be added to step 4) mixture in, stir 10min under 350r/min；
6) by step 5) mixture be cooled to 60 DEG C, add 0.2 part of Salvia japonica essential oil, mixing forms lotion；
7) lotion is injected into and is preheating in 37 DEG C of mould in advance, be positioned under the conditions of 8 DEG C, taken out after 30 minutes
The demoulding, that is, obtain the nourishing type lipstick.
In the embodiment above, the following institute of extracting method of angelica extract, Sage extract, tuberose extract
State.
The extracting method of angelica extract：Take angelica root and clean drying, be cut into the sheet of 0.5cm left and right thicknesses, fibrous root is cut
Into segment, according to 1:5 feed liquid weight leaches 3 hours, cooled and filtered than adding deionized water at 85 DEG C, and filter residue is with equally
Method extract again 2 times, merging filtrate is centrifuged 30min under 3500-4000r/min, takes supernatant, is concentrated under reduced pressure into substance
Long-pending 50%.
The extracting method of Sage extract：Salvia japonica meal is taken appropriate, according to 1:10 feed liquid weight than addition go from
Sub- water soaked overnight, decocts 1.5h, cooled and filtered at 100 DEG C, filter residue decocts 1.5h again at 100 DEG C, merging filtrate,
30min is centrifuged under 3500-4000r/min, supernatant is taken, the 50% of original volume is concentrated under reduced pressure into.
The extracting method of tuberose extract：Tuberose dried flower is washed with deionized water only, drying, according to 1:15 liquid material
Weight is than adding deionized water.4.5h is leached at 60 DEG C, is filtered, the same method of filter residue is extracted 2 times again, merging filtrate,
30min is centrifuged under 3500-4000r/min, supernatant is taken, the 50% of original volume is concentrated under reduced pressure into.
Ocular estimate
Take each 6 of the nourishing type lipstick of embodiment of the present invention 1-4, respectively take 3 be respectively placed in -15 DEG C, at a temperature of 45 DEG C
Storage recovers to observe the cosmetic variation of lipstick lotion to room temperature after 3 months.Lipstick is intact to keep former rod-like morphology, is rich in light
Pool, apparent exquisiteness, without perspiring, tiltedly collapse, the bad phenomenon such as decorative pattern, crackle.
Inoxidizability is evaluated
A kind of inoxidizability of material has correlation with delay skin aging.Sweet osmanthus pericarp melanin is used in the present invention
As one of colouration component, while as functional component, using its high antioxidant, coordinating with vitamin E, lip skin is protected
Skin, anti-aging.
The present invention verifies sweet osmanthus pericarp melanin in formula to the influence of lipstick antioxygenic property using Rancimat methods.
The general principle of Rancimat methods be under certain hot conditions to sample in be passed through certain flow air, make sample accelerate oxygen
Change, the volatile small molecule for producing such as aldehyde, ketone, acid will be aoxidized and imported in distilled water, record the conductivity variations situation of water, and
Induction time is obtained, induction time is more long, show that sample inoxidizability stability is stronger.
As shown in table 1,3 groups of samples are designed according to embodiment 2, only changes antioxidant, the antioxidant composition of sample 1 is given birth to tie up
Plain E and sweet osmanthus pericarp melanin, the antioxidant composition of sample 2 is vitamin E and 2,6- di-tert-butyl-4-methy phenol (BHT),
The antioxidant composition of sample 3 is vitamin E.
The sample 1-3 component situations of table 1
The present invention is determined according to Rancimat methods using the type Oxidation of Fat and Oils steady testing instrument of Switzerland Metrohm 743.Weigh
3.0g each sample at 110 DEG C, air induced oxidation is passed through with the flow velocity of 20L/h, respectively to each antioxidant in reaction tube
Oxidation resistance in the sample is evaluated.Experimental result is as shown in Figure 1.
By the anti-oxidant induction curves of Fig. 1, the induction time of sample 3 is 7.83h, and the induction time of sample 2 is 10.76h, sample
The induction time of product 1 is 15.34h.The induction time of sample 3 is most short, and sample 2 takes second place, and the induction time of sample 1 is most long.Experiment knot
Fruit explanation sweet osmanthus pericarp melanin is significantly stronger than 2,6 di tert butyl 4 methyl phenol (BHT) to the inoxidizability ability of lipstick.
Efficacy assessments
The present invention evaluates effect of nourishing type lipstick by trying out rear effect.Choose altogether 100 lip dryings, peeling,
Obscure female consumer, the age is 18-40 Sui.It is divided into 5 groups, every group of 20 people.The taste for being prepared using above-described embodiment 1-4 respectively
The type of supporting lipstick, compares with certain the middle and high end lipstick commercially bought, and after 3 months, feedback information is collected, as a result such as table
Shown in 2.
The nourishing type lipstick of the embodiment 1-4 of table 2 is counted with the using effect of comparative example
As can be seen from Table 2, embodiment 1-4 and comparative example have different degrees of improvement to lip aridity, but implement
The improvement degree of example 1-4 will be significantly better than comparative example；Embodiment 1-4 has different degrees of improvement to lip color, but comparative example is imitated
Fruit is not obvious.Comprehensive Correlation, improvement of the embodiment 4 to skin of lip is most notable.As can be seen here, embodiment of the present invention nourishing type mouthful
It is red to be effectively improved skin of lip drying, the phenomenon of peeling, and have more significant improvement lip color, help lip color dimness person to recover strong
Effect of Kang Hongrun.
The foregoing is only presently preferred embodiments of the present invention, be not intended to limit the invention, it is all it is of the invention spirit and
Within principle, any modification, equivalent substitution and improvements made etc. should be included within the scope of the present invention.
Claims (10)
1. a kind of nourishing type lipstick, it is characterised in that promote absorbent components by moistening moisturizing component, antioxidant composition, promoting blood circulation, releive
Anti-inflammatory component, natural pigment, excipient component and helper component composition.
2. nourishing type lipstick according to claim 1, it is characterised in that the moist moisturizing component includes：20-25 weight
The jojoba oil, the saualane of 10-15 weight portions, the rice bran oil of 5-10 weight portions, the cocoa butter of 4-5 weight portions, 1-3 weight of part
The honey, the tuberose extract of 1-3 weight portions of part.
3. nourishing type lipstick according to claim 1, it is characterised in that the antioxidant composition includes：2-5 weight portions
The sweet osmanthus pericarp melanin of vitamin E and 0.1-0.5 weight portions.
4. nourishing type lipstick according to claim 1, it is characterised in that the promoting blood circulation promotees absorbent components to be included：2-5 weight
The angelica extract, the idesia oil of 4-7 weight portions, the peony seed oil of 1-3 weight portions, the safflower seed oil of 1-3 weight portions of part.
5. nourishing type lipstick according to claim 1, it is characterised in that the anti-inflammatory component of releiving includes：1-3 weight portions
Sage extract.
6. nourishing type lipstick according to claim 1, it is characterised in that the natural pigment includes：3-5 weight portions it is peppery
Green pepper red pigment, the alkermes of 0-4 weight portions, the sweet osmanthus pericarp melanin of 0.1-0.5 weight portions.
7. nourishing type lipstick according to claim 1, it is characterised in that the excipient component includes：10-15 weight portions
Beeswax, the Brazil wax of 2-5 weight portions, the candelila wax of 3-6 weight portions, the rice bran wax and helper component of 3-4 weight portions,
The helper component includes：The farina of 1-2 weight portions and the Salvia japonica essential oil of 0.1-0.3 weight portions.
8. the nourishing type lipstick according to any one of claim 1-7, it is characterised in that the nourishing type lipstick include with
Lower composition：The jojoba oil of 20-25 weight portions, the saualane of 10-15 weight portions, the rice bran oil of 5-10 weight portions, 4-5 weight portions
Cocoa butter, the honey of 1-3 weight portions, the tuberose extract of 1-3 weight portions, the vitamin E of 2-5 weight portions, 0.1-0.5
The sweet osmanthus pericarp melanin of weight portion, the angelica extract of 2-5 weight portions, the idesia oil of 4-7 weight portions, 1-3 weight portions
Peony seed oil, the safflower seed oil of 1-3 weight portions, the Sage extract of 1-3 weight portions, the capsorubin of 3-5 weight portions, 10-
The beeswax of 15 weight portions, the Brazil wax of 2-5 weight portions, the candelila wax of 3-6 weight portions, the rice bran wax of 3-4 weight portions, 0-
The alkermes of 4 weight portions, the farina of 1-2 weight portions, the Salvia japonica essential oil of 0.1-0.3 weight portions.
9. a kind of preparation method of nourishing type lipstick as claimed in claim 8, it is characterised in that comprise the following steps：
1) sweet osmanthus pericarp melanin, capsorubin are well mixed with alkermes and farina, add part flash
Bar oil grinding, obtains mill base；
2) remaining jojoba oil, saualane, rice bran oil, idesia oil, peony seed oil, safflower seed oil, vitamin E are mixed and is stirred
Mix uniform；
3) in step 2) cocoa butter, beeswax, Brazil wax, candelila wax, rice bran wax are added in the mixture that obtains, it is heated to
85 DEG C or so, obtain oil mixture；
4) tuberose extract, angelica extract, Sage extract are mixed, is heated to 85 DEG C or so, add honey, fully
Stirring, is added to step 3) obtained in oil mixture, be well mixed；
5) by step 1) mill base be added to step 4) mixture in, in stirring 10min under 300-500r/min；
6) mixture is cooled to 60 DEG C or so, adds Salvia japonica essential oil, mixing forms lotion；
7) lotion is injected into and is preheating in 35-40 DEG C of mould in advance, be positioned at 5-10 DEG C, take out de- after 30 minutes
Mould, that is, obtain the nourishing type lipstick.
10. preparation method according to claim 9, it is characterised in that the sweet osmanthus pericarp melanin passes through following steps
Obtain：
1) by 1:5 weight extracts 36h than the sweet osmanthus pericarp is mixed with the ammonia spirit of pH=10.5 at 25 DEG C, filters
The sweet osmanthus pericarp, obtains sweet osmanthus pericarp melanin leaching liquor；
2) by the sweet osmanthus pericarp melanin leaching liquor in 30-35min is centrifuged under 3000-3500r/min, supernatant is taken, is used
The HCl solution of 2mol/L adjusts pH to 2.5, separates out melanin deposition, is stored at room temperature 12h, is centrifugally separating to obtain precipitation, i.e. osmanthus
Flowers and fruits hull melanin crude product；
3) the sweet osmanthus pericarp melanin crude product is hydrolyzed into 2h, suction filtration, then successively with three with the HCl of 1mol/L at 100 DEG C
Chloromethanes, ethyl acetate, 95% ethanol washing sweet osmanthus pericarp melanin filter residue, are finally washed with distilled water to neutrality, then by institute
State sweet osmanthus pericarp melanin filter residue to be dried at 60-80 DEG C to constant weight, that is, obtain refined sweet osmanthus pericarp melanin；
The capsorubin is obtained by following steps：
1) by dry pimiento, remove seed is shredded, 40 mesh sieves is crossed after crushing, the pimiento is pressed 1：9 weight is than adding 15%
NaOH solution, 2h, intermittent stirring are extracted at 55 DEG C；
2) filtering removal alkali lye, filter residue is washed with deionized to neutrality, is obtained except the capsicum skin powder after peppery；
3) the capsicum skin powder except after peppery is wrapped with filter paper, loaded on apparatus,Soxhlet's in, with acetone extraction, carried at 70 DEG C
4-5h is taken, the acetone extract of capsorubin is obtained；
4) acetone extract of the capsorubin is evaporated concentration, is dried to constant weight at 60-80 DEG C, obtain described peppery
Green pepper red pigment；
The angelica extract is obtained by with water in extraction angelica root at 85 DEG C；
The Sage extract is obtained by with water in extraction rat-tail grass meal at 100 DEG C；
The tuberose extract is obtained in extracting dry tuberose at 65 DEG C by with water.
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| CN107903655A (en) * | 2017-10-18 | 2018-04-13 | 湖北科技学院 | The method and its application of melanin are extracted in a kind of pericarp from sweet osmanthus |
| CN108670940A (en) * | 2018-08-30 | 2018-10-19 | 佛山市欧若拉生物科技有限公司 | A kind of jasmine fragrance lipstick and preparation method thereof |
| CN110075012A (en) * | 2019-05-20 | 2019-08-02 | 湖北大学 | The application of idesia oil and cosmetics and tyrosinase activity inhibitor |
| JP2019151561A (en) * | 2018-02-28 | 2019-09-12 | 株式会社コーセー | Cosmetic or skin external preparation |
| CN111374929A (en) * | 2018-12-27 | 2020-07-07 | 深圳市蔡府实业有限公司 | Lipstick |
| CN111904897A (en) * | 2020-09-16 | 2020-11-10 | 上海海盈通感光材料有限公司 | Nourishing type lip cosmetic and preparation method thereof |
| CN113855590A (en) * | 2021-09-28 | 2021-12-31 | 力精化学品(上海)有限公司 | Lip cosmetic composition |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107903655A (en) * | 2017-10-18 | 2018-04-13 | 湖北科技学院 | The method and its application of melanin are extracted in a kind of pericarp from sweet osmanthus |
| JP2019151561A (en) * | 2018-02-28 | 2019-09-12 | 株式会社コーセー | Cosmetic or skin external preparation |
| JP7254447B2 (en) | 2018-02-28 | 2023-04-10 | 株式会社コーセー | Cosmetics and external skin preparations |
| CN108670940A (en) * | 2018-08-30 | 2018-10-19 | 佛山市欧若拉生物科技有限公司 | A kind of jasmine fragrance lipstick and preparation method thereof |
| CN111374929A (en) * | 2018-12-27 | 2020-07-07 | 深圳市蔡府实业有限公司 | Lipstick |
| CN110075012A (en) * | 2019-05-20 | 2019-08-02 | 湖北大学 | The application of idesia oil and cosmetics and tyrosinase activity inhibitor |
| CN111904897A (en) * | 2020-09-16 | 2020-11-10 | 上海海盈通感光材料有限公司 | Nourishing type lip cosmetic and preparation method thereof |
| CN113855590A (en) * | 2021-09-28 | 2021-12-31 | 力精化学品(上海)有限公司 | Lip cosmetic composition |
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