CN110652482B - Skin moistening oil containing lotus extract - Google Patents
Skin moistening oil containing lotus extract Download PDFInfo
- Publication number
- CN110652482B CN110652482B CN201911052553.0A CN201911052553A CN110652482B CN 110652482 B CN110652482 B CN 110652482B CN 201911052553 A CN201911052553 A CN 201911052553A CN 110652482 B CN110652482 B CN 110652482B
- Authority
- CN
- China
- Prior art keywords
- oil
- lotus
- leaf extract
- skin
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Molecular Biology (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Emergency Medicine (AREA)
- Biophysics (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a skin-moistening oil containing a lotus extract, which consists of the following components in percentage by mass: 50-70% of tea oil, 10-30% of sweet almond oil, 1-10% of lotus essential oil, 0.1-2% of willow leaf extract, 0.1-1% of lotus leaf extract, 5-15% of caprylic/capric triglyceride, 2-5% of hydrogenated lecithin, 0.1-1% of vitamin E, 0.1-1% of squalene and 0.01-0.1% of erucamide. Also discloses a preparation method of the skin moisturizing oil. The skin moistening oil is prepared by compounding the lotus essential oil, the lotus leaf extract and the willow leaf extract through reasonable compounding and the cooperation of the caprylic/capric triglyceride and the phospholipid, has elegant fragrance, is not pungent, can protect and repair cells and tissues, has the effects of resisting aging, improving the immunity of the body and the like, can moisten the skin and promote the healthy growth of the skin.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to skin moisturizing oil containing a lotus extract.
Background
Lotus (Lotus flower): belongs to the family Nymphaeaceae of Ranunculaceae, is a generic name of two plants in the Nelumbo, and is a perennial aquatic herb flower in the Nelumbo. Underground stems are long and thick, have long nodes and leaves are round. In the flowering period of 6-9 months, the flowers grow on the tops of the pedicels, most of the petals are embedded in the receptacle, and the flowers have red, pink, white, purple and other colors, or have colored lines and rims. The lotus essential oil has the effects of whitening skin, lightening spots, diminishing inflammation, resisting acne, moistening, nourishing, repairing, tranquilizing, resisting allergy, stimulating blood circulation, enhancing memory and refreshing. The natural lotus essential oil anti-allergy factor eliminates and discharges stubborn skin allergy factors, can effectively treat various allergens in the skin, thoroughly and harmlessly solves various skin allergy phenomena, strengthens the natural health care toxin expelling function of the skin, keeps the proliferation and regeneration of cells with contact balance, and effectively improves abnormal skin and aged skin. The essential oil extracted from flos Nelumbinis has certain inhibitory effect on Staphylococcus aureus, Escherichia coli, and Proteus vulgaris, and has good chelating effect on metal ions.
The lotus leaf is different from the lotus, and the extract is generally obtained by taking dried and crushed lotus leaves as a raw material, adopting cellulase pretreatment, dilute hydrochloric acid extraction, ultrasonic-assisted extraction, combining extracting solutions, alkalizing and concentrating. However, the lotus leaf extract is different in substances extracted by water and organic solvents, and the water extract has better effect on skin, is non-irritant and has different compatibility with other substances.
The folium Salicis Babylonicae is leaf of Salicaceae Salicis Babylonicae of Salicales, and has effects of clearing away heat and toxic materials, promoting diuresis and relieving swelling. The willow leaf extract has a good treatment effect on chronic liver injury, and also has the effect of removing superoxide radicals. The willow leaf water extract has an anti-tumor effect, and the compatibility of the willow leaf water extract and essential oil is poor at present.
At present, the field of application of the lotus extract is very limited, other effects of the lotus extract cannot be fully developed, and currently, a skin moistening oil containing the lotus extract is urgently needed to fully develop and expand the performance and application range of the lotus extract and provide a basis for further development of the lotus extract industry.
Disclosure of Invention
In order to solve the problems, the invention provides the skin moistening oil containing the lotus extract, the skin moistening oil is prepared by compounding the lotus essential oil, the lotus leaf extract and the willow leaf extract through reasonable compounding, and the synergism of the caprylic/capric triglyceride and the phospholipid is added, so that the prepared skin moistening oil is elegant in flavor, not pungent, capable of protecting and repairing cells and tissues, has the effects of resisting aging, improving the immunity of the body and the like, and can moisten the skin and promote the healthy growth of the skin.
The invention is realized by the following technical scheme:
a skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 50-70% of tea oil, 10-30% of sweet almond oil, 1-10% of lotus essential oil, 0.1-2% of willow leaf extract, 0.1-1% of lotus leaf extract, 5-15% of caprylic/capric triglyceride, 2-5% of hydrogenated lecithin, 0.1-1% of vitamin E, 0.1-1% of squalene and 0.01-0.1% of erucamide.
Tea oil: the main oil base of the skin-moistening oil, the tea oil in the experiment is the commercial tea oil which is winterized, the acidity of unsaturated fat of the tea oil is higher, the antioxidant activity is good, and the tea oil is an excellent percutaneous penetration enhancer.
Lotus essential oil, lotus extract picked from May to July every year, mainly comprising pentadecane, palmitic acid, caryophyllene oxide, 1-caryophyllene, alpha-terpineol, heneicosane, 8-heptadecene and the like as main components by a solvent extraction method, has a certain inhibiting effect on staphylococcus aureus, escherichia coli and proteus and has a better chelating effect on metal ions. The lotus essential oil has very stable smell.
Sweet almond oil: the viscosity is low, the skin-moistening oil is fresh and not greasy, and the viscosity in the skin-moistening oil is effectively reduced. The content of linoleic acid in the sweet almond oil is higher, and the viscosity of the grease is inversely related to the unsaturation degree of fatty acid.
Vitamin E: is a fat-soluble antioxidant separated and extracted from deodorized distillate of vegetable oil.
Squalene: is a fat-soluble antioxidant separated and extracted from deodorized distillate of vegetable oil. The squalene has certain anti-aging effect on skin. The squalene is a substance closest to the natural oil secretion of a human body, has excellent skin-friendly performance, contains lower squalene content in the willow leaf extract and the lotus extract, and can well improve the permeability of active substances in the skin moistening oil by increasing the content of the squalene.
Preferably, the skin moistening oil containing the lotus extract consists of the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
Preferably, the preparation method of the lotus leaf extract comprises the following steps: cleaning and airing lotus leaves, crushing, adding 5-6 times of extraction liquid by mass, soaking for 2-4 hours at 30-50 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain a lotus leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The lotus leaf extract completely reserves natural substance components and nutritional compositions in the lotus leaf extract, is rich in lotus leaf flavone, can effectively remove DPPH free radicals, and reduces the facial melanin content of a subject.
Preferably, the extraction method of the willow leaf extract comprises the steps of cleaning, airing and crushing willow leaves, adding 5-6 times of extraction liquid by mass, soaking for 2-4 hours at 30-50 ℃, filtering to remove residues, centrifuging supernate, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The extraction method of the willow leaves is various, generally solvent extraction, microwave-assisted extraction or ultrasonic-assisted extraction is carried out, the extract is generally flavone, tax is adopted as a solvent for extraction in the method, the extract contains water-soluble substances, the extraction method is simple and convenient, the extract is a new natural antioxidant resource, the extract is usually applied to the treatment of diabetes, the extract is rarely applied to emollient oil and is easy to cause skin allergy, and the main reason is that the actual using effect of the extract is not substantially improved compared with polysaccharide such as hyaluronic acid and the like, and the tolerance of human skin to the willow leaf extract is different. The application of the lotus extract in the skin-moistening oil has obvious synergistic effect on the lotus extract. Mainly, substances in the salix leaf extract can form intermolecular crosslinking with the lotus extract, and the film forming property of the substances is combined, so that the active substances of the lotus extract can continuously act, and the salix leaf extract has better antioxidant property.
The preparation method of the skin-moistening oil containing the lotus essential oil extract comprises the following steps:
(1) adding the salix leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating and uniformly mixing at 55-75 ℃, and performing ultrasonic treatment and high-speed shearing at the shearing speed of 10000-13000 rpm for 0.5-1 min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 80-120 MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Advantageous effects
1. The skin moisturizing oil disclosed by the invention can be used for remarkably reducing the MDA content of the skin, increasing the SOD and CAT contents and improving the photoaging of the skin, and the moisture retention is also superior to that of the commercially available care oil; the skin moistening oil has good use sensory experience, can effectively reduce the loss of moisturizing factors in the dermis, maintains the functions of elastic fibers and collagen fibers in the dermis, avoids the reduction of skin tension and elasticity, and delays the aging characteristics of wrinkles, tarnish skin and the like of the skin.
2. According to the invention, the lotus extract, the lotus leaf extract and the willow leaf extract are compounded, so that the biological safety is high, the three substances have a synergistic effect, and under the synergistic effect of the components, the skin-moistening lotion has an excellent skin-moistening effect, can play roles of nursing, repairing skin and the like more safely and durably, and does not need to be added with other functional components.
3. The lotus extract and the essential oil are used as main components, so that the lotus extract and the essential oil have high biological safety, have a remarkable moisturizing effect, and have elegant and lasting fragrance; the lotus leaf extract and the willow leaf extract are not easy to be mutually dissolved with components such as essential oil after being extracted by water, and the lotus leaf extract and the willow leaf extract are coated in liposome of phospholipid and caprylic capric glyceride and are better fused with the essential oil to form uniform and stable transparent liquid which is not suitable for layering. The skin caring oil has effects of keeping moisture, caring skin, resisting oxidation, scavenging free radicals, enhancing epidermal cell activity, promoting skin metabolism, delaying skin aging, and improving market value.
4. The extract of folium Salicis Babylonicae obtained by water extraction has antiaging effect, and can be used for reconstructing the junction between dermis and epidermis and promoting collagen fiber generation. In addition, the product has strong free radical scavenging ability, is a good antioxidant, and has antiaging effect.
5. The composition has the advantages of simple preparation, natural and safe raw materials, no need of organic reagents and other auxiliaries, safety, mildness, no stimulation, no toxic or side effect, short process period, low pollution and low energy consumption.
Detailed Description
The following examples are given for the detailed implementation and specific operation of the present invention, but the scope of the present invention is not limited to the following examples.
Tea tree essential oil used as follows
Example 1
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 51.5% of tea oil, 30% of sweet almond oil, 1% of lotus essential oil, 0.1% of willow leaf extract, 0.1% of lotus leaf extract, 15% of caprylic/capric triglyceride, 2.09% of hydrogenated lecithin, 0.1% of vitamin E, 0.1% of squalene and 0.01% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of the extractive solution, soaking at 30 deg.C for 2 hr, filtering to remove residue, centrifuging the supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 5 times of extraction liquid by mass, soaking for 2 hours at 30 ℃, filtering to remove residues, centrifuging supernate, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 55 deg.C, mixing, performing ultrasonic treatment, and shearing at high speed of 10000rpm for 1min to obtain liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 80MPa, taking out the liquid when the liquid is transparent, and naturally cooling to room temperature to obtain the skin moistening oil.
Example 2
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 61% of tea oil, 10% of sweet almond oil, 5% of lotus essential oil, 1% of willow leaf extract, 1% of lotus leaf extract, 15% of caprylic/capric triglyceride, 5% of hydrogenated lecithin, 1% of vitamin E, 0.9% of squalene and 0.1% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 6 times of the extract, soaking at 50 deg.C for 4 hr, filtering to remove residue, centrifuging the supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 6 times of extraction liquid by mass, soaking for 4 hours at 50 ℃, filtering to remove residues, centrifuging supernate, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 75 ℃, uniformly mixing, performing ultrasonic treatment, and performing high-speed shearing at 13000rpm for 0.5min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Example 3
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of extractive solution, soaking at 38 deg.C for 3 hr, filtering to remove residue, centrifuging supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 6 times of extract liquor, soaking for 3 hours at 38 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain the willow leaf extract; the extraction liquid consists of isopropyl palmitate and water according to a mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 60 ℃, uniformly mixing, performing ultrasonic treatment, and performing high-speed shearing at 12000rpm for 1min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Comparative example 1
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.7% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of extractive solution, soaking at 38 deg.C for 3 hr, filtering to remove residue, centrifuging supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the lotus leaf extract into hydrogenated lecithin and caprylic capric triglyceride, heating at 60 deg.C, mixing, performing ultrasonic treatment, and shearing at high speed of 12000rpm for 1min to obtain liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid when the liquid is transparent, and naturally cooling to room temperature to obtain the skin moistening oil.
Comparative example 2
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 1.0% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 6 times of extraction liquid, soaking for 3 hours at 38 ℃, filtering to remove residues, centrifuging supernate, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 60 deg.C, mixing, performing ultrasonic treatment, and shearing at high speed of 12000rpm for 1min to obtain liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Comparative example 3
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of 25% ethanol extract, soaking at 38 deg.C for 3 hr, filtering to remove residue, centrifuging supernatant, purifying, and concentrating to obtain folium Nelumbinis extract.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 6 times of extract liquor, soaking for 3 hours at 38 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 60 ℃, uniformly mixing, performing ultrasonic treatment, and performing high-speed shearing at 12000rpm for 1min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Comparative example 4
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of extractive solution, soaking at 38 deg.C for 3 hr, filtering to remove residue, centrifuging supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 25% ethanol extract liquid with the mass 6 times that of the willow leaves, soaking for 3 hours at 38 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 60 ℃, uniformly mixing, performing ultrasonic treatment, and performing high-speed shearing at 12000rpm for 1min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Comparative example 5
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.1% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E and 0.5% of squalene.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of extractive solution, soaking at 38 deg.C for 3 hr, filtering to remove residue, centrifuging supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 6 times of extract liquor, soaking for 3 hours at 38 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
(1) adding the willow leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating at 60 ℃, uniformly mixing, performing ultrasonic treatment, and performing high-speed shearing at 12000rpm for 1min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 120MPa, taking out the liquid when the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
Comparative example 6
A skin moistening oil containing a lotus extract comprises the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
The preparation method of the lotus leaf extract comprises the following steps: cleaning folium Nelumbinis, air drying, pulverizing, adding 5 times of extractive solution, soaking at 38 deg.C for 3 hr, filtering to remove residue, centrifuging supernatant, purifying, and concentrating to obtain folium Nelumbinis extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.01: 10.
The extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 6 times of extract liquor, soaking for 3 hours at 38 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain the willow leaf extract; the extraction liquid is composed of isopropyl palmitate and water according to the mass ratio of 0.02: 10.
The preparation method of the skin moisturizing oil comprises the following steps:
heating tea oil and sweet almond oil to 50 ℃, adding other raw materials in parts by mass, directly stirring, carrying out high-pressure homogenization circulating treatment under the pressure of 120MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
And (3) performance testing:
1. the emollient oils prepared in examples 1 to 3 and comparative examples 1 to 6 were left at 25 ℃ for 3 months, and the change of the emollient oil was observed.
2. The skin oils prepared in examples 1 to 3 and comparative examples 1 to 6 were subjected to sensory evaluation, and the color, moisture, absorbency, oily feeling and odor of the skin oils applied to the skin were evaluated, respectively.
Table-sensory evaluation table
Scoring
3. According to the requirements of the human skin patch test of 'cosmetic hygiene standard 2015 edition', selecting qualified patch materials and testees. The subject is required to have not recently used antihistamines or immunosuppressants, or to have not used any anti-inflammatory drugs at the site of the subject. 20uL of each test sample was dropped onto a piece of filter paper and placed in a spotting apparatus. The plaque test device with the test substance is applied to the curved side of the forearm of the tested person by using a non-irritating adhesive tape, and is lightly pressed by the palm to be uniformly applied to the skin for 24 hours. The interval is 30min after the spot tester is removed, and the skin reaction is observed after the indentation disappears. 30 people per group.
Example 1 produced 1 case of erythema; example 2 no erythema was produced; example 3 produced no erythema. Comparative example 1 produced 2 erythema examples; comparative example 2 produced 6 erythema; comparative example 3 produced 5 erythema examples; comparative example 4 produced 5 erythema; comparative example 5 produced 3 erythema; comparative example 6 produced 6 erythema examples.
The emollient oil can also be applied to human skin in the form of a lotion or cream.
It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.
Claims (2)
1. The skin moisturizing oil containing the lotus extract is characterized by comprising the following components in percentage by mass: 50-70% of tea oil, 10-30% of sweet almond oil, 1-10% of lotus essential oil, 0.1-2% of willow leaf extract, 0.1-1% of lotus leaf extract, 5-15% of caprylic/capric triglyceride, 2-5% of hydrogenated lecithin, 0.1-1% of vitamin E, 0.1-1% of squalene and 0.01-0.1% of erucamide;
the preparation method of the lotus leaf extract comprises the following steps: cleaning and airing lotus leaves, crushing, adding 5-6 times of extraction liquid by mass, soaking for 2-4 hours at 30-50 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain a lotus leaf extract; the extraction liquid consists of isopropyl palmitate and water according to the mass ratio of 0.01: 10;
the extraction method of the willow leaf extract comprises the steps of cleaning willow leaves, airing, crushing, adding 5-6 times of extraction liquid by mass, soaking for 2-4 hours at 30-50 ℃, filtering to remove residues, centrifuging supernatant, purifying and concentrating to obtain the willow leaf extract; the extraction liquid consists of isopropyl palmitate and water according to the mass ratio of 0.02: 10;
the preparation method of the skin-moistening oil containing the lotus essential oil extract comprises the following steps:
(1) adding the salix leaf extract and the lotus leaf extract into hydrogenated lecithin and caprylic/capric triglyceride, heating and uniformly mixing at 55-75 ℃, and performing ultrasonic treatment and high-speed shearing at the shearing speed of 10000-13000 rpm for 0.5-1 min to obtain a liquid phase;
(2) heating tea oil and sweet almond oil to 50 ℃, adding erucamide, slowly adding a liquid phase, then adding lotus essential oil, tea tree essential oil, vitamin E and squalene, carrying out high-pressure homogenization circulation treatment under the pressure of 80-120 MPa, taking out the liquid until the liquid is transparent, and naturally cooling to room temperature to obtain the skin moisturizing oil.
2. The skin oil containing the lotus extract as claimed in claim 1, which is characterized by comprising the following components in percentage by mass: 58.2% of tea oil, 22% of sweet almond oil, 3% of lotus essential oil, 0.2% of willow leaf extract, 0.5% of lotus leaf extract, 11.05% of caprylic/capric triglyceride, 4% of hydrogenated lecithin, 0.5% of vitamin E, 0.5% of squalene and 0.05% of erucamide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911052553.0A CN110652482B (en) | 2019-10-31 | 2019-10-31 | Skin moistening oil containing lotus extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911052553.0A CN110652482B (en) | 2019-10-31 | 2019-10-31 | Skin moistening oil containing lotus extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110652482A CN110652482A (en) | 2020-01-07 |
| CN110652482B true CN110652482B (en) | 2022-07-05 |
Family
ID=69042522
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911052553.0A Active CN110652482B (en) | 2019-10-31 | 2019-10-31 | Skin moistening oil containing lotus extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110652482B (en) |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103405377A (en) * | 2013-08-15 | 2013-11-27 | 江南大学 | Natural skin whitening and protecting composition and application thereof in cosmetics |
| CN104666126A (en) * | 2015-02-06 | 2015-06-03 | 深圳唯美度生物科技有限公司 | Liquid preparation employing horse oil as active component |
| CN105997612A (en) * | 2016-05-16 | 2016-10-12 | 合肥工业大学 | Skin-whitening, wrinkle-resisting and skin-protecting oil and preparing method thereof |
| CN107625674A (en) * | 2016-07-18 | 2018-01-26 | 无锡市天爱装饰工程有限公司 | A kind of willow leaf toner and preparation method thereof |
-
2019
- 2019-10-31 CN CN201911052553.0A patent/CN110652482B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN110652482A (en) | 2020-01-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104188885B (en) | A kind of moist humidity-preserving type Asian puccoon lip gloss and preparation method thereof | |
| WO2018036356A1 (en) | Peach gum mask | |
| CN107550771A (en) | Salubrious camellia makeup remover of quality and preparation method thereof | |
| CN105106655B (en) | A kind of prosthetic burn and scald ointment and preparation method thereof | |
| KR101997177B1 (en) | Shampoo composition for improving state of scalp and hair | |
| CN109771348B (en) | Whitening, moisturizing and wrinkle-removing face cream rich in natural product extract components and preparation method thereof | |
| CN109771337A (en) | A kind of fat of Oromaius norvaehollandeae lip-stick and preparation method thereof | |
| KR20130113729A (en) | The functional beauti-pacl and its manufacturing method | |
| CN107375095A (en) | A kind of whitening, moisturizing essence and preparation method thereof | |
| WO2018036358A1 (en) | Peach gum mask | |
| CN106333880B (en) | toner based on thin emulsion and preparation method thereof | |
| CN113679640A (en) | Natural nourishing skin-cleaning skin-care acne-removing facial cleansing gel and preparation method thereof | |
| KR101498609B1 (en) | Manufacturing method of bodylotion using herb and bodylotion made by that manufacturing method | |
| CN113143820A (en) | Anti-aging composition and preparation method thereof | |
| KR20140145278A (en) | Cosmetic composition containing Cimicifuga heracleifolia extract, Cornus officinalis extract and Geranium nepalense extract for skin convergence and elasticity effect | |
| CN110613663A (en) | Skin repairing composition, skin care product and preparation method thereof | |
| CN105832612A (en) | Safe pore refining type cleansing oil and preparing method thereof | |
| CN110652482B (en) | Skin moistening oil containing lotus extract | |
| KR20210040522A (en) | Cosmetic composition, cosmetic mask pack comprisint the same and preperation method of the cosmetic composition | |
| CN107441340B (en) | Hand and foot chap cream for relieving swelling, pain and itching and nourishing skin and preparation method thereof | |
| CN109646329A (en) | It is a kind of to drop the essential oil content in freckle cream and preparation method thereof that smells good | |
| CN105796408B (en) | Composition of plant extracts and its application in cosmetics and fluid composition and preparation method thereof of removing ornaments and formal dress | |
| CN111481487B (en) | Whitening skin care composition containing herba Violae extract and preparation method thereof | |
| KR20090111980A (en) | Cosmetic composition for improving acne containing extracts of natural substance | |
| JP6391879B1 (en) | Beauty method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |