CN103184102A - Extraction method and application of agilawood essential oil - Google Patents
Extraction method and application of agilawood essential oil Download PDFInfo
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- CN103184102A CN103184102A CN2013100135733A CN201310013573A CN103184102A CN 103184102 A CN103184102 A CN 103184102A CN 2013100135733 A CN2013100135733 A CN 2013100135733A CN 201310013573 A CN201310013573 A CN 201310013573A CN 103184102 A CN103184102 A CN 103184102A
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Abstract
The invention relates to an extraction method of agilawood essential oil, which comprises the following steps: firstly, cutting down aquilaria sinensis trees, removing white wood and carving into agilawood slices; grinding the agilawood slices into agilawood powder with specification of 40 meshes; then adding the agilawood powder into an extraction kettle by normal butane and directly extracting agilawood essential oil by adopting a subcritical fluid extraction technology under the extraction conditions that extraction time is 0.5 to 1.5 hours, analysis temperature is 60 DEG C, extraction temperature is 50 DEG C and extraction pressure is 0.4 Mpa to 0.5MPa; and then adding slags obtained after extracting the agilawood essential oil for the first time into the extraction kettle by 95 percent of ethanol to carry out extraction for the second time under the same extraction conditions in the process of extracting the agilawood essential oil for the first time. The invention aims to provide the extraction method and application of the agilawood essential oil.
Description
Technical field
The present invention relates to a kind of extracting process, be specifically related to the application of a kind of agalloch eaglewood extracts essential oil method and agalloch eaglewood essential oil.
Background technology
Agalloch eaglewood tool promoting the circulation of QI to relieve pain, warming middle-JIAO to arrest vomiting, helping inspiration to relieve asthma, tranquilizing by nourishing the heart, the effect of the sending down abnormally ascending of promoting blood circulation, in treatment and prevention coronary heart disease, stenocardia, myocardial ischemia, diseases such as irregular pulse have significant curative effect.And traditional technology only adopts single extraction to extract the agalloch eaglewood essential oil, and obtainable linaloe oil is limited.Linaloe oil is very golden expensive, and how obtaining more linaloe oil becomes the purpose that everybody falls over each other to strive in the industry.
Summary of the invention
The object of the invention provides a kind of agalloch eaglewood extracts essential oil method.Twice extraction of this process using, relatively other technologies can obtain more linaloe oil, for the raw material sources of agalloch eaglewood series product find a new approach.
Another object of the present invention provides the application of agalloch eaglewood essential oil.
The present invention has adopted following technical proposals:
A kind of agalloch eaglewood extracts essential oil method, felling Lignum Aquilariae Resinatum tree is removed the whitewood earlier, carves the agalloch eaglewood thin slice; Again the agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves; Then the agalloch eaglewood powder is added to extraction kettle with normal butane, adopt the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil, its extraction conditions: extraction time is 0.5～1 hour, and 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa; Be added to extraction kettle with 95% ethanol and carry out extracting second time extraction agalloch eaglewood essential oil extracting for the first time slag behind the agalloch eaglewood essential oil subsequently, its extraction conditions: extraction time is 0.5～1.5 hour, 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa.
Embodiment extracts one of application of agalloch eaglewood essential oil, with the agalloch eaglewood essential oil of extraction using alcohol, adds Laoshan wingceltis essential oil 1 ‰, adds ethanol 98%, and an amount of fixing agent is deployed into the Ligaloes perfumes that gives off a strong fragrance.Wherein fixing agent is face cream.
Embodiment, two of the application of extraction agalloch eaglewood essential oil, evenly make the muscle pressure of to releive by agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersant that the subcritical fluid extraction technology is extracted, skin had skin moisten effect agalloch eaglewood massage oil, wherein agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersion agent volume percent are: agalloch eaglewood essential oil 4%～8%, flores aurantii essential oil 1%～3%, cypress essential oil 1%～3%, sweet almond oil 86%～94%.
The present invention has following advantage and effect:
1, the present invention is added to extraction kettle to the agalloch eaglewood powder with normal butane, adopt the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil, be added to extraction kettle with 95% ethanol and carry out extracting the second time extracting for the first time slag behind the agalloch eaglewood essential oil subsequently, twice extraction conditions is identical, production technique is simple, the relative other technologies of technology of the present invention can obtain more linaloe oil, for the raw material sources of agalloch eaglewood series product find a new approach.
2, use the agalloch eaglewood essential oil of extraction using alcohol, add Laoshan wingceltis essential oil 1 ‰, add ethanol 98%, an amount of fixing agent, be deployed into the Ligaloes perfumes that gives off a strong fragrance, the agalloch eaglewood essential oil has multi-efficiency to human body, as: improve the gas field, the pressure of releiving, anti-strongly fragrant, the conditioning body and mind and promote health new city metabolism etc. of sleeping peacefully.The santal essential oil is to the multiple curative effect of skin tool, is fit to aging, drying and lack of water skin.Urging property is strengthened and is breathed and urinary system, the treatment cellulitis.
3, agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and the dispersant of being extracted by the subcritical fluid extraction technology evenly made the agalloch eaglewood massage oil, and this agalloch eaglewood massage oil muscle pressure of can releiving has the skin moisten effect to skin.
Embodiment
The present invention is described in further detail below in conjunction with embodiment, but embodiments of the present invention are not limited thereto.
Embodiment, a kind of agalloch eaglewood extracts essential oil method, felling Lignum Aquilariae Resinatum tree is removed the whitewood earlier, carves the agalloch eaglewood thin slice; Again the agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves; Then the agalloch eaglewood powder is added to extraction kettle with normal butane, adopt the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil, its extraction conditions: extraction time is 1 hour, and 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa; Be added to extraction kettle with 95% ethanol and carry out extraction second time extracting for the first time slag behind the agalloch eaglewood essential oil subsequently, its extraction conditions is: by the same extraction conditions extraction agalloch eaglewood essential oil that extracts the agalloch eaglewood essential oil first time.
Extract one of application of agalloch eaglewood essential oil, with the agalloch eaglewood essential oil of extraction using alcohol, add Laoshan wingceltis essential oil 1 ‰, add ethanol 98%, an amount of face cream is deployed into the Ligaloes perfumes that gives off a strong fragrance as fixing agent.
Two of the application of extraction agalloch eaglewood essential oil, evenly make the muscle pressure of to releive by agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersant that the subcritical fluid extraction technology is extracted, skin had skin moisten effect agalloch eaglewood massage oil, wherein agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersion agent volume percent are: agalloch eaglewood essential oil 4%～8%, flores aurantii essential oil 1%～3%, cypress essential oil 1%～3%, sweet almond oil 86%～94%.
Claims (5)
1. an agalloch eaglewood extracts essential oil method is characterized in that, felling Lignum Aquilariae Resinatum tree is removed the whitewood earlier, carves the agalloch eaglewood thin slice; Again the agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves; Then the agalloch eaglewood powder is added to extraction kettle with normal butane, adopts the subcritical fluid extraction technology directly to extract the agalloch eaglewood essential oil; Be added to extraction kettle with 95% ethanol and carry out extracting second time extraction agalloch eaglewood essential oil extracting for the first time slag behind the agalloch eaglewood essential oil subsequently.
2. according to the described agalloch eaglewood extracts essential oil of claim 1 method, it is characterized in that: for the first time extraction conditions and for the second time extraction conditions be: extraction time is 0.5～1.5 hour, and 60 ℃ of resolution temperatures extract 50 ℃ of temperature, and extraction pressure is 0.4～0.5MPa.
3. the application of the described agalloch eaglewood essential oil of claim 1 is characterized in that, with the agalloch eaglewood essential oil of extraction using alcohol, adds Laoshan wingceltis essential oil 1 ‰, adds ethanol 98%, and an amount of fixing agent is deployed into the Ligaloes perfumes that gives off a strong fragrance.
4. the application of the described agalloch eaglewood essential oil of claim 2 is characterized in that, fixing agent is face cream.
5. the application of the described agalloch eaglewood essential oil of claim 1, it is characterized in that, evenly make the muscle pressure of to releive by agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersant that the subcritical fluid extraction technology is extracted, skin had skin moisten effect agalloch eaglewood massage oil, wherein agalloch eaglewood essential oil, flores aurantii essential oil, cypress essential oil, sweet almond oil and dispersion agent volume percent are: agalloch eaglewood essential oil 4%～8%, flores aurantii essential oil 1%～3%, cypress essential oil 1%～3%, sweet almond oil 86%～94%.
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| CN2013100135733A CN103184102A (en) | 2013-01-14 | 2013-01-14 | Extraction method and application of agilawood essential oil |
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| CN2013100135733A CN103184102A (en) | 2013-01-14 | 2013-01-14 | Extraction method and application of agilawood essential oil |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103351954A (en) * | 2013-07-11 | 2013-10-16 | 大连卓尔高科技有限公司 | Process for extracting eaglewood essential oil by using supercritical carbon dioxide |
| CN103520435A (en) * | 2013-10-11 | 2014-01-22 | 中山市国林沉香科学研究所 | Agilawood health care essential oil |
| CN103740467A (en) * | 2014-01-27 | 2014-04-23 | 陆燕 | Method for extracting plant essential oil |
| CN103789094A (en) * | 2014-01-21 | 2014-05-14 | 广州大学 | Method for extracting agilawood essential oil from agilawood chips |
| CN103923749A (en) * | 2014-04-30 | 2014-07-16 | 海口蜜香树科技有限公司 | Method for extracting Chinese eaglewood essential oil |
| CN104087420A (en) * | 2014-07-16 | 2014-10-08 | 贵州省华烁生物科技有限公司 | Subcritical extraction method capable of improving antioxidant activity of volatile oil in agarwood leaves |
| CN104792722A (en) * | 2015-04-30 | 2015-07-22 | 华南农业大学 | Method for establishing agilawood oil content near infrared spectral prediction model |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
| CN104830528A (en) * | 2015-04-23 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and use method of aquilaria wood perfume |
| CN105647647A (en) * | 2016-01-07 | 2016-06-08 | 安阳市晶华油脂工程有限公司 | Energy-saving agilawood essential oil extraction complete plant and low-temperature extraction technique thereof |
| CN106176411A (en) * | 2016-08-22 | 2016-12-07 | 广州市香事文化传播有限公司 | A kind of agilawood essential oil and preparation method thereof |
| CN106833899A (en) * | 2017-02-07 | 2017-06-13 | 珠海市玖鑫化妆品有限公司 | The preparation technology and essential oil Deacne pack of a kind of linaloe oil |
| CN107216950A (en) * | 2017-07-29 | 2017-09-29 | 郑永如璧 | Agilawood spray and agilawood tobacco tar preparation method |
| CN107299002A (en) * | 2017-08-09 | 2017-10-27 | 中国热带农业科学院农产品加工研究所 | The extracting method of agilawood essential oil |
| CN110934797A (en) * | 2019-12-25 | 2020-03-31 | 芜湖市茅王香料植物科技有限公司 | Production process of lavender perfume capable of soothing nerves and helping sleep |
| CN111821222A (en) * | 2020-07-17 | 2020-10-27 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood massage oil and preparation method thereof |
| CN112159722A (en) * | 2020-09-01 | 2021-01-01 | 梁勇 | Preparation method of agilawood essential oil |
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| CN1500477A (en) * | 2002-11-13 | 2004-06-02 | 丛繁滋 | Quick result aerosol with plant aroma and its preparation |
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| CN101129316A (en) * | 2007-08-30 | 2008-02-27 | 中国热带农业科学院热带生物技术研究所 | Ligaloes perfumes and method of producing the same |
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103351954A (en) * | 2013-07-11 | 2013-10-16 | 大连卓尔高科技有限公司 | Process for extracting eaglewood essential oil by using supercritical carbon dioxide |
| CN103520435A (en) * | 2013-10-11 | 2014-01-22 | 中山市国林沉香科学研究所 | Agilawood health care essential oil |
| CN103789094A (en) * | 2014-01-21 | 2014-05-14 | 广州大学 | Method for extracting agilawood essential oil from agilawood chips |
| CN103740467A (en) * | 2014-01-27 | 2014-04-23 | 陆燕 | Method for extracting plant essential oil |
| CN103923749A (en) * | 2014-04-30 | 2014-07-16 | 海口蜜香树科技有限公司 | Method for extracting Chinese eaglewood essential oil |
| CN104087420A (en) * | 2014-07-16 | 2014-10-08 | 贵州省华烁生物科技有限公司 | Subcritical extraction method capable of improving antioxidant activity of volatile oil in agarwood leaves |
| CN104087420B (en) * | 2014-07-16 | 2016-03-30 | 贵州省华烁生物科技有限公司 | A kind of subcritical extraction method improving volatile oil anti-oxidant activity in eaglewood leaf |
| CN104830528A (en) * | 2015-04-23 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and use method of aquilaria wood perfume |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
| CN104792722A (en) * | 2015-04-30 | 2015-07-22 | 华南农业大学 | Method for establishing agilawood oil content near infrared spectral prediction model |
| CN104830537B (en) * | 2015-04-30 | 2018-05-18 | 东莞波顿香料有限公司 | A kind of preparation method and applications of agalloch eaglewood hydrosol |
| CN105647647A (en) * | 2016-01-07 | 2016-06-08 | 安阳市晶华油脂工程有限公司 | Energy-saving agilawood essential oil extraction complete plant and low-temperature extraction technique thereof |
| CN106176411A (en) * | 2016-08-22 | 2016-12-07 | 广州市香事文化传播有限公司 | A kind of agilawood essential oil and preparation method thereof |
| CN106833899A (en) * | 2017-02-07 | 2017-06-13 | 珠海市玖鑫化妆品有限公司 | The preparation technology and essential oil Deacne pack of a kind of linaloe oil |
| CN107216950A (en) * | 2017-07-29 | 2017-09-29 | 郑永如璧 | Agilawood spray and agilawood tobacco tar preparation method |
| CN107299002A (en) * | 2017-08-09 | 2017-10-27 | 中国热带农业科学院农产品加工研究所 | The extracting method of agilawood essential oil |
| CN110934797A (en) * | 2019-12-25 | 2020-03-31 | 芜湖市茅王香料植物科技有限公司 | Production process of lavender perfume capable of soothing nerves and helping sleep |
| CN111821222A (en) * | 2020-07-17 | 2020-10-27 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood massage oil and preparation method thereof |
| CN112159722A (en) * | 2020-09-01 | 2021-01-01 | 梁勇 | Preparation method of agilawood essential oil |
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Application publication date: 20130703 |