CN105231450B - A kind of pumpkin lozenge and preparation method thereof - Google Patents
A kind of pumpkin lozenge and preparation method thereof Download PDFInfo
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- CN105231450B CN105231450B CN201510744359.4A CN201510744359A CN105231450B CN 105231450 B CN105231450 B CN 105231450B CN 201510744359 A CN201510744359 A CN 201510744359A CN 105231450 B CN105231450 B CN 105231450B
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- pumpkin
- lozenge
- pawpaw
- tomato
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of pumpkin lozenge and preparation method thereof, the pumpkin lozenge is made up of the raw material of following parts by weight：Pumpkin peel 50~1000, pumpkin 25~500, pumpkin pulp 25~500, pawpaw 10~100, tomato 10~100, xylitol 0.2~20, stevioside 0.1~0.2, peppermint oil 0.01~0.05, dextrin 10~100, glutinous rice 1~10 and propolis 0.1~0.5；The lozenge can slow down or dispelling fatigue, eliminate interior free yl, anti-oxidant, anti-aging, increase it is immune etc., available for anti-organism fatigue, moisturizing beauty treatment etc., it is safe to use, natural green environmental protection, pumpkin, pawpaw, the skin of tomato are utilized simultaneously, the skin slag utilization of resources that goes out of use is played, avoids the effect of the wasting of resources；Method is eaten by cumbersome tradition and is transformed into the new paragon lozenge for facilitating modern to take, without brewing, mouthfeel is good, and compact is easy to carry, and more conveniently and efficiently plays pumpkin effect.
Description
Technical field
The present invention relates to health-care preparation technical field.It is more particularly related to a kind of pumpkin lozenge and its system
Preparation Method.
Background technology
Pumpkin belongs to the annual sprawling herbs plant of Curcurbitaceae Cucurbita, and it is rich in polysaccharide, amino acid, vitamin, Hu
The bioactive ingredients such as radish element, mineral matter, alkaloid, aliphatic acid and pigment.China's TCM investigation thinks, pumpkin bitter, property
It is cold, can anti-inflammatory, analgesic, strong liver, help kidney, reduce blood pressure, being stimulated the secretion of milk for puerpera, tonifying middle-Jiao and Qi.Research shows that pumpkin is to sugar both at home and abroad
Urine disease, particularly type II diabetes there is the effect of notable, and can prevent the nephrosis as caused by diabetes, hepatopathy, high fat of blood and
The diseases such as hypertension occur.Modern medicine study shows that active polysaccharide has the functions such as regulation body blood sugar level in pumpkin.This
Outside, research is found, squash polyoses can improve mouse immune organ mass, the phagocytic function of macrophage, discloses squash polyoses tool
There is immunoregulation effect.Study antitumor action external in squash polyoses body and the influence to hematid immunity function, knot
Fruit shows that squash polyoses can strengthen erythrocyte immune adsorption capacity, has certain antitumor and immunocompetent effect of raising.
Pumpkin peel is rich in functional components such as polysaccharide, organic acid and alkaloids.Pumpkin has anthelmintic action, lives in sanitary condition less preferably
The people in area is often edible can be with expelling parasite, suitable roundworm disease, enterobiasis, taeniasis, snail fever, hookworm disease edible for patients.China
Pumpkin pulp and pumpkin mainly are utilized, but it is limited to the pumpkin peel utilization of resources, and market is not yet using pumpkin peel as the more glycogens of production
Material, lack pumpkin peel preparation, and also without a kind of pumpkin tablet for playing antifatigue effect.Commonly use antifatigue system at present simultaneously
Agent usually contains sexual function class chemicals, hormone or parahormone medicine, stimulant etc., adverse reaction is more and toxic side effect compared with
Greatly.
The content of the invention
It is an object of the invention to solve at least the above, and provide a kind of pumpkin lozenge.The lozenge, which has, to be slowed down
Or dispelling fatigue, remove interior free yl, anti-oxidant, anti-aging, increase immune and other effects, supported available for anti-organism fatigue, moisturizing
Face etc., and using fool proof, natural green environmental protection, while pumpkin, pawpaw, the skin of tomato are utilized, the skin slag utilization of resources is played,
Avoid the effect of the wasting of resources.
The present invention also provides a kind of pumpkin process for preparing buccal lozenge, and mass efficient composition damages during solving traditional preparation methods
Mistake problem, preparation method provided by the invention can preferably preserve active ingredient in raw material in manufacturing process, polysaccharide, Hu in pumpkin
Radish element, organic acid, alkaloid etc., polysaccharide, carrotene, oleanolic acid, ursolic acid, general flavone, polyphenol substance etc. in pawpaw, kind
Abundant vitamin C, lycopene etc. in eggplant.Under the method provided by the present invention, first made with pectinase enzymatic hydrolysis processing raw material many
Active ingredient fully discharges from histocyte, recycles water and ethanol effective component extracting, greatly improve extraction pumpkin peel,
Effective component extraction rate in pawpaw and tomato etc..
Technical scheme provided by the invention is：
A kind of pumpkin lozenge, the pumpkin lozenge are made up of the raw material of following parts by weight：Pumpkin peel 50~1000, pumpkin
25~500, pumpkin pulp 25~500, pawpaw 10~100, tomato 10~100, xylitol 0.2~20, stevioside 0.1~0.2, thin
Lotus oil 0.01~0.05, dextrin 10~100, glutinous rice 1~10 and propolis 0.1~0.5.
Preferably, the pumpkin lozenge is made up of the raw material of following parts by weight：Pumpkin peel 100~500, pumpkin 100~
300th, pumpkin pulp 100~300, pawpaw 20~80, tomato 20~60, xylitol 0.2~10, stevioside 0.1~0.2, peppermint oil
0.02~0.04, dextrin 20~100, glutinous rice 2~5 and propolis 0.1~0.2.
A kind of preparation method of pumpkin lozenge, the preparation method comprise the following steps：
1) it is, 5~10% by pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato vacuum freeze drying to moisture, institute
Dried pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato are stated through Ultrasonic Pulverization, ball milling, powder is made, by manufactured powder
After sieving, powders A is obtained, wherein, the grit number of crossing is 12~120 mesh, and pawpaw uses with tomato belt leather；
2), by powders A described in step 1), pectase and deionized water, Ultrasonic Heating stirring, time 30-40 are added
Minute, then centrifugal filtration, extract solution B is obtained, collects filter residue, wherein the powders A, pectase is 10 with deionized water weight ratio
~15:0.5~2:30~50；
3), by the filter residue described in step 2), ethanol heating and refluxing extraction under vacuum is first added, is filtrated to get and carries
Take liquid C, add water and be heated to reflux extracting again under vacuum, be filtrated to get extract solution D, by extract obtain extract solution C,
Extract solution D mixes with the extract solution B described in step 2), obtains mixed extract E；
4), mixed extract E described in step 2) is concentrated under reduced pressure, concentrate is passed through into hollow fiber filter mistake
After filter, then spray-dried extract powder F is made；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F in step 4) and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, cross 12
~120 eye mesh screens, are made particle, and particle is pressed into lozenge, then slurries G described in lozenge surface spraying last layer is being made,
Drying and forming-film at 60~80 DEG C of temperature, the sterilized processing finished product of lozenge.
Preferably, pumpkin peel described in step 1), pumpkin, pumpkin pulp, pawpaw, tomato vacuum refrigeration do temperature as -40
~-50 DEG C, wherein, before drying, by the pumpkin pulp, pawpaw is cut to 1~5mm thin slice respectively, thinly slices shortening drying
Time.
Preferably, it is 1~2 time with ethanol extraction time in the step 3), each extraction time is 10~20 minutes,
With water extraction time 1~2 time, each extraction time is 20~30 minutes.
Preferably, ethanol heated under vacuum refluxing extraction is used described in step 3), wherein the vacuum pressure is 3.4
~5.8Kpa, heating-up temperature is 40-80 DEG C, described to use water heated under vacuum refluxing extraction, wherein the vacuum pressure is
25~38Kpa, heating-up temperature are 40-80 DEG C.
Preferably, filter residue described in step 3) and water weight ratio are 1~5：10~25, the filter residue is with ethanol weight ratio
1~3：10~20.
Preferably, ethanol described in step 3) is 10~95% ethanol.
Preferably, it is 5-10% to obtain extract powder F water content after being spray-dried in step 3), and this moisture is easy
In compressing.
Preferably, spray drying temperature described in step 4) is 60-80 DEG C.
The present invention comprises at least following beneficial effect：
(1) present invention is by pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato, xylitol, stevioside, peppermint oil, dextrin,
Glutinous rice and propolis are prepared, wherein pawpaw, tomato belt leather use, the present invention by pumpkin peel, pumpkin, pumpkin pulp, pawpaw and
Tomato etc. comprehensively utilizes, and contains pectin, polysaccharide, carrotene, organic acid, alkaloid etc. in pumpkin peel, pumpkin, pumpkin pulp, wood
Contain pectin, polysaccharide, carrotene, oleanolic acid, ursolic acid, general flavone, polyphenol substance etc. in melon, dimension life is contained in tomato skin
Plain C, lycopene etc., synergy so that the present invention, which has, to be slowed down or dispelling fatigue, eliminates interior free yl, anti-oxidant, is resisted
Aging, enhancing are immune and other effects, available for anti-organism fatigue and moisturizing beauty treatment etc., in addition, the present invention contains abundant vitamin
And pectin, pectin have good adsorptivity, Endophytic bacteria toxin and other harmful substances can be bonded and eliminate, in heavy metal
Lead, mercury and radioactive element, detoxication can be played, the present invention can also protect Wei Jiao roads mucous membrane, and use is fool proof,
Natural green environmental protection, pumpkin peel, pawpaw skin, tomato skin generally go out of use, do not use, and causes the wasting of resources, and this hair
It is bright using pumpkin, pawpaw, tomato these skin slags, play the skin slag utilization of resources, avoid the wasting of resources from acting on.
(2) present invention provides preparation method can preserve active ingredient in raw material in manufacturing process, and pectin in pumpkin is more
Sugar, carrotene, organic acid, alkaloid etc., pectin in pawpaw, polysaccharide, carrotene, oleanolic acid, ursolic acid, general flavone are more
Phenol material etc., vitamin C in tomato, lycopene etc., under the method provided by the present invention, first made with pectinase enzymatic hydrolysis processing raw material
Many active ingredient fully discharges from histocyte, then is extracted with series concentration ethanol solution and water, greatly improves extraction
Effective component extraction rate, so as to reduce cost, and finally coat the sticky rice syrup containing propolis on lozenge top layer and form diaphragm, energy
Make active ingredient in pumpkin lozenge be not easy to be oxidized, keep steady quality, ensure lozenge effect, extend the lozenge shelf-life, simultaneously
Pumpkin lozenge is manufactured using the present invention to be easily absorbed by the body, it is quick to play antifatigue effect, length of holding time, by numerous
Trivial tradition eats method and is transformed into the new paragon lozenge for facilitating modern to take, and without brewing, mouthfeel is good, and compact is easy to take
Band, steady quality, dosage is accurate, more conveniently and efficiently plays pumpkin effect.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to example below, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1
A kind of pumpkin lozenge, pumpkin lozenge are made up of the raw material of following parts by weight：Pumpkin peel 50, pumpkin 25, pumpkin pulp
25th, pawpaw 10, tomato 10, xylitol 0.2, stevioside 0.1, peppermint oil 0.01, dextrin 10, glutinous rice 1 and propolis 0.1, pumpkin peel,
Pawpaw skin, tomato skin generally go out of use, and do not use, and cause the wasting of resources, the present invention is by pumpkin peel, pumpkin, pumpkin
Meat, pawpaw, tomato, xylitol, stevioside, peppermint oil, dextrin, glutinous rice and propolis are prepared, pumpkin peel of the present invention, pumpkin
Seed, pumpkin pulp, pawpaw and tomato are comprehensively utilized, pumpkin peel, pumpkin, and polysaccharide, carrotene, organic acid, life are contained in pumpkin pulp
Alkaloids etc., containing polysaccharide, oleanolic acid, ursolic acid, general flavone, polyphenol substance etc. in pawpaw, abundant dimension life is contained in tomato
Plain C, lycopene etc., play synergy so that the present invention have slow down or dispelling fatigue, eliminate interior free yl play it is anti-
Oxidation, anti-aging, increase immune and other effects, available for anti-organism fatigue and moisturizing beauty treatment etc., glutinous rice and propolis make lozenge protection
Film so that lozenge active ingredient is not easy to be oxidized, while is easily absorbed by the body again, can quickly play antifatigue effect, and make
With fool proof, natural green environmental protection, while pumpkin is utilized, pawpaw, these skin slags of tomato, the skin slag utilization of resources is played, is avoided
The wasting of resources acts on.
Pumpkin process for preparing buccal lozenge comprises the following steps：
1) it is, 5% by pumpkin, pumpkin, pumpkin pulp, pawpaw, tomato vacuum freeze drying to moisture, south after drying
Through Ultrasonic Pulverization ball milling, powder is made, it is 120 mesh that powder, which will be made, and cross mesh number in melon skin, pumpkin, pumpkin pulp, pawpaw, tomato
After sieve, powders A is obtained, is freeze-dried active ingredient in preservation raw material more preferable than heated-air drying so that active ingredient is not destroyed
And reduction, Ultrasonic Pulverization and ball milling raw material are in order to which following enzymolysis and extraction are easier to certain mesh number, shorten enzymolysis and extraction
Time；
2) pectase and deionized water are added, by powders A in step 1), powders A, the weight of pectase and deionized water
Than for 10:0.5:30,40 DEG C of stirrings of Ultrasonic Heating, the time is 30 minutes, and extract solution B is obtained after centrifugal filtration, collects filter residue；Adopt
It is first many active ingredient is fully discharged from histocyte with pectinase enzymatic hydrolysis processing raw material with pectinase enzymatic hydrolysis, enters one
Step improves effective component extraction rate；
3), by filter residue in step 2), ethanol heating and refluxing extraction under vacuum is first added, is filtrated to get extract solution C,
Add water to be heated to reflux extracting again under vacuum, be filtrated to get extract solution D, extraction is obtained into extract solution C, extract solution D
Mixed with extract solution B, obtain mixed extract E；Water insoluble ingredients in raw material are extracted with ethanol, cause to heat back under vacuo
The temperature of stream reduces, and is unlikely to the beneficiating ingredient destroyed in raw material, while is heated to reflux the time under vacuum and also shortens, and carries
High extraction efficiency；
4), mixed extract E is concentrated under reduced pressure, by concentrate after hollow fiber filter filters, then through spray
Mist is dried and extract powder F is made；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, 100 eye mesh screens are crossed,
Particle is made in mixed-powder, particle is pressed into lozenge, then slurries G described in last layer is applied lozenge surface is made, in temperature
Drying and forming-film at 60 DEG C, the sterilized processing of lozenge obtain finished product, and finally on lozenge top layer, sticky rice syrup of the coating containing propolis is formed
Diaphragm, pumpkin lozenge can be made to be not easy to be oxidized, ensure lozenge effect and extend the lozenge term of validity, the pumpkin lozenge manufactured
Easily it is absorbed by the body, antifatigue effect is quick.
Embodiment 2
A kind of pumpkin lozenge, pumpkin lozenge are made up of following raw material：Pumpkin peel 1000, pumpkin 500, pumpkin pulp
500th, pawpaw 100, tomato 100, xylitol 20, stevioside 0.2, peppermint oil 0.05, dextrin 100, glutinous rice 10 and propolis 0.5.South
Melon skin, pawpaw skin, tomato skin generally go out of use, and do not use, and cause the wasting of resources, the present invention by pumpkin peel, pumpkin,
Pumpkin pulp, pawpaw, tomato, xylitol, stevioside, peppermint oil, dextrin, glutinous rice and propolis are prepared, pumpkin peel of the present invention, south
Melon seeds, pumpkin pulp, pawpaw and tomato are combined with, in pumpkin peel, pumpkin, pumpkin pulp containing polysaccharide, carrotene, organic acid,
Alkaloid etc., containing oleanolic acid, ursolic acid, general flavone, polyphenol substance etc. in pawpaw, lycopene etc. is contained in tomato skin,
Synergy so that the present invention, which has, to be slowed down or dispelling fatigue, is eliminated interior free yl, anti-oxidant, anti-aging, is increased the work(such as immune
Effect, available for anti-organism fatigue and moisturizing beauty treatment etc., glutinous rice and propolis make lozenge diaphragm so that lozenge active ingredient is not easy
It is oxidized, while is easily absorbed by the body again, can quickly play antifatigue effect, and uses fool proof, natural green environmental protection,
Simultaneously using pumpkin peel, pawpaw skin, tomato skin these skin slags, the skin slag utilization of resources is played, avoids the wasting of resources from acting on.
Pumpkin lozenge preparation side comprises the following steps：
1) before, drying, by pumpkin pulp, pawpaw is cut to 1mm thin slices, by pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato
Vacuum freeze drying temperature is -40 DEG C, is 10% to moisture, pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato after drying
Through Ultrasonic Pulverization, ball milling, powder is made, powder will be made and cross mesh number after 12 mesh sieves, to obtain powders A；Hot blast is compared in freeze-drying
Dry the more preferable active ingredient preserved in raw material so that active ingredient is not destroyed and reduces, and Ultrasonic Pulverization and ball milling raw material arrive
Certain mesh number is in order to which following enzymolysis and extraction are easier, and shortens enzymolysis and extraction time；
2), by powders A, pectase and deionized water are added, Ultrasonic Heating stirs 40 minutes, then centrifugal filtration, is carried
Liquid B is taken, collects filter residue, wherein the powders A, pectase is 15 with deionized water weight ratio:2:50；At pectinase enzymatic hydrolysis
Reason raw material makes many active ingredient fully be discharged from histocyte, further improves effective component extraction rate；
3), by filter residue, it be 10% ethanol first to add concentration, and the weight ratio of filter residue and 10% ethanol is 1：10, in vacuum pressure
Power is that heating-up temperature is 40 DEG C of refluxing extractions 10 minutes under 3.4Kpa, is filtrated to get extract solution, then toward adding 50% second in filter residue
Alcohol extracting 15 minutes, extract solution is filtrated to get, then this proposition liquid twice is mixed to get extract solution C, then water is added toward filter residue,
The weight of filter residue and water ratio is 1：10, heating-up temperature is that 40 DEG C of backflows extract 20 minutes again under being 25Kpa in the pressure of vacuum, mistake
Filter obtains extract solution D, and extract solution C, extract solution D that extraction obtains are mixed with extract solution B, obtain mixed extract E；Use ethanol
Water insoluble ingredients in raw material are extracted, the water soluble ingredient in raw material is extracted with water, cause to be heated to reflux temperature drop under vacuo
It is low, it is unlikely to destroy beneficiating ingredient in raw material, while be heated to reflux the time under vacuum and also shorten, improve extraction efficiency；
4), mixed extract E is concentrated under reduced pressure, by concentrate after hollow fiber filter filters, then through temperature
Spend and the extract powder F that water content is 5% is made for 60 DEG C of spray drying；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, cross 12 eye mesh screens, system
Into particle, particle is pressed into lozenge, then be made lozenge surface apply last layer described in slurries G, be dried under temperature 60 C
Film, finished product is obtained after lozenge sterilization, finally coating the sticky rice syrup containing propolis on lozenge top layer forms diaphragm, can contain pumpkin
Piece is not easy to be oxidized, and ensures lozenge effect and extends lozenge effective shelf-life, manufactures pumpkin lozenge and be easily absorbed by the body,
It is quick to play antifatigue effect.
Embodiment 3
A kind of pumpkin lozenge, pumpkin lozenge are made up of the raw material of following parts by weight：Pumpkin peel 100, pumpkin 100, pumpkin
Meat 100, pawpaw 20, tomato 20, xylitol 0.3, stevioside 0.1, peppermint oil 0.02, dextrin 20, glutinous rice 2 and propolis 0.1.Pumpkin
Skin, pawpaw skin, tomato skin generally go out of use, and do not use, and cause the wasting of resources, the present invention is by pumpkin peel, pumpkin, south
Melon meat, pawpaw, tomato, xylitol, stevioside, peppermint oil, dextrin, glutinous rice and propolis are prepared, and wherein pawpaw, tomato are all
Belt leather utilizes, and pumpkin peel, pumpkin, pumpkin pulp, pawpaw and tomato of the present invention are combined with, pumpkin peel, pumpkin, in pumpkin pulp
Containing polysaccharide, carrotene, organic acid, alkaloid etc., contain oleanolic acid, ursolic acid, general flavone, polyphenol substance in pawpaw skin
Deng containing abundant vitamin C, lycopene etc., synergy in tomato skin so that the present invention, which has, to be slowed down or eliminate tired
Labor, eliminates interior free yl, anti-oxidant, anti-aging, increase it is immune and other effects, available for anti-organism fatigue and moisturizing beauty treatment etc..It is glutinous
Rice and propolis make the diaphragm of lozenge so that the beneficiating ingredient of lozenge is not easy to be oxidized, while is easily absorbed by the body again, energy
It is quick to play antifatigue effect, and using fool proof, natural green environmental protection, while pumpkin peel is make use of, and pawpaw skin, tomato skin
These skin slags, the skin slag utilization of resources is played, avoids the wasting of resources.
The preparation method of pumpkin lozenge comprises the following steps：
1) before, drying, by pumpkin pulp, pawpaw is cut to 5mm thin slice respectively, by pumpkin peel, pumpkin, pumpkin pulp, wood
Vacuum freeze drying at melon, tomato are -50 DEG C in temperature, it is 8% to dry to moisture, pumpkin peel, pumpkin, south after drying
Ball milling, powder is made through Ultrasonic Pulverization in melon meat, pawpaw, tomato, will be made after powder crosses 50 mesh sieves, obtains powders A；Freezing is dry
Beneficiating ingredient in dry preservation raw material more preferable than heated-air drying so that beneficiating ingredient is not destroyed and reduces, Ultrasonic Pulverization and ball milling
Raw material is in order to which following enzymolysis and extraction are easier to certain mesh number, shortens enzymolysis and extraction time；
2) pectase and deionized water are added, by powders A, powders A, the weight ratio of pectase and deionized water is 12:
1.5:38, Ultrasonic Heating stirs 26 minutes, then centrifugal filtration, obtains extract solution B, collects filter residue, and described uses pectase enzyme
Solution using pectinase enzymatic hydrolysis processing raw material many active ingredient is fully discharged from histocyte, further improve effectively into
Divide recovery rate；
3), by filter residue, it is 50% ethanol first to add concentration, and filter residue is 3 with ethanol weight ratio：20, be in the pressure of vacuum
Heating-up temperature is 55 DEG C of refluxing extractions under 5.8Kpa, extracts 20 minutes, is filtrated to get extract solution C, adds water, filter residue and water
Weight ratio is 5：125, in the case where vacuum pressure is 38Kpa, heating-up temperature is that 55 DEG C of backflows are extracted 30 minutes again, is filtrated to get extraction
Liquid, then toward water is added in filter residue, proposition obtains extract solution, and the extract solution that water extraction is got is mixed to get extract solution D, will extract
Mixed to extract solution C, extract solution D with extract solution B, obtain mixed extract E；Water insoluble ingredients in raw material are extracted with ethanol,
Under vacuo so that being heated to reflux temperature reduction, it is unlikely to destroy beneficiating ingredient in raw material, while heat back under vacuum
The stream time also shortens, and improves extraction efficiency, and it is more complete in order to extract to repeat extraction；
4), mixed extract E is concentrated under reduced pressure, by concentrate after hollow fiber filter filters, then through temperature
Spend and the extract powder F that water content is 10% is made for 80 DEG C of spray drying；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, cross 80 eye mesh screens, system
Into particle, particle is pressed into lozenge, then slurries G described in last layer is applied lozenge surface is being made, is dried at 80 DEG C of temperature
Film, finished product is obtained after lozenge sterilization, finally coating the sticky rice syrup containing propolis on lozenge top layer forms diaphragm, can contain pumpkin
Piece is not easy to be oxidized, and ensures lozenge effect and extends lozenge effective shelf-life, the pumpkin lozenge manufactured is easily inhaled by human body
Receive, it is quick to play antifatigue effect.
Embodiment 4
A kind of pumpkin lozenge, pumpkin lozenge are made up of the raw material of following parts by weight：Pumpkin peel 500, pumpkin 300, pumpkin
Meat 300, pawpaw 80, tomato 60, xylitol 10, stevioside 0.2, peppermint oil 0.04, dextrin 100, glutinous rice 5 and propolis 0.2.Pumpkin
Skin, pawpaw skin, tomato skin generally go out of use, and do not use, and cause the wasting of resources, the present invention is by pumpkin peel, pumpkin, south
Melon meat, pawpaw, tomato, xylitol, stevioside, peppermint oil, dextrin, glutinous rice and propolis are prepared, pawpaw, tomato belt leather profit
With pumpkin peel, pumpkin, pumpkin pulp, pawpaw and tomato of the present invention are combined with, pumpkin peel, pumpkin, containing more in pumpkin pulp
Sugar, carrotene, organic acid, alkaloid etc., oleanolic acid, ursolic acid, general flavone, polyphenol substance etc., tomato are contained in pawpaw skin
Contain lycopene in skin, act synergistically, make the present invention have slow down or dispelling fatigue, eliminate interior free yl play antioxygen
Change, anti-aging, increase it is immune and other effects, available for anti-organism fatigue and with moisturizing beauty treatment etc..Glutinous rice and propolis make lozenge protection
Film so that lozenge beneficiating ingredient is not easy to be oxidized, while is easily absorbed by the body again, can quickly play antifatigue effect, and make
With fool proof, natural green environmental protection, while these skin slags of pumpkin peel, pawpaw skin, tomato skin are make use of, play skin slag resource profit
With avoiding the wasting of resources.
The preparation method of pumpkin lozenge comprises the following steps：
1) before, drying, by pumpkin pulp, pawpaw is cut to 3mm thin slice respectively, by pumpkin peel, pumpkin, pumpkin pulp, wood
Melon skin, tomato skin vacuum freeze drying temperature are -45 DEG C, are 6% to moisture, pumpkin peel, pumpkin, pumpkin after drying
Ball milling, powder is made through Ultrasonic Pulverization in meat, pawpaw skin, tomato skin, after powder sieving will be made, obtains powders A, wherein, it is described
The mesh number of sieving is 120 mesh；Freeze-drying it is more more preferable than heated-air drying preservation raw material in beneficiating ingredient so that beneficiating ingredient not by
Destroy and reduce, Ultrasonic Pulverization and ball milling raw material to certain mesh number are digested and extraction is easier in order to following, shorten enzymolysis
And extraction time；
2), by powders A described in step 1), pectase and deionized water, Ultrasonic Heating stirring are added, the time is 36 points
Clock, then centrifugal filtration, extract solution B is obtained, filter residue is collected, wherein the weight ratio of described powders A, pectase and deionized water is
12:1:40；Many active ingredient is fully discharged from histocyte using pectinase enzymatic hydrolysis processing raw material, further improve
Effective component extraction rate；
3), by filter residue described in step 2), it be 70% ethanol first to add concentration, and the weight ratio of filter residue and ethanol is 2：14,
In the case where vacuum pressure is 5Kpa, heating-up temperature is 80 DEG C of refluxing extractions 15 minutes, is filtrated to get extract solution C, adds water, filter residue
Weight ratio with water is 4：20, heating-up temperature is that 80 DEG C of backflows are extracted again under being 30Kpa in the pressure of vacuum, extraction time 2 times,
Each extraction time is 24 minutes, is filtrated to get extract solution D, extraction is obtained into extract solution C, extract solution D mixes with extract solution B,
Obtain mixed extract E；Water insoluble ingredients in raw material are extracted with ethanol, the temperature for causing to be heated to reflux under vacuo reduces,
It is unlikely to the beneficiating ingredient destroyed in raw material, while the time being heated to reflux under vacuum also shortens, and improves extraction effect
Rate；
4), mixed extract E is concentrated under reduced pressure, by concentrate after hollow fiber filter filters, then through temperature
Spend and the extract powder F that water content is 7% is made for 70 DEG C of spray drying；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, 120 eye mesh screens are crossed,
Particle is made, particle is pressed into lozenge, then slurries G described in last layer is applied lozenge surface is being made, is dried at 75 DEG C of temperature
Film forming, finished product is obtained after lozenge sterilizing, finally coating the sticky rice syrup containing propolis on lozenge top layer forms diaphragm, can make pumpkin
Lozenge is not easy to be oxidized, and ensures lozenge effect and extends lozenge effective shelf-life, the pumpkin lozenge manufactured is easily by human body
Absorb, it is quick to play antifatigue effect.
Embodiment 5
A kind of pumpkin lozenge, pumpkin lozenge are made up of the raw material of following parts by weight：Pumpkin peel 700, pumpkin 200, pumpkin
Meat 350, pawpaw skin 60, tomato skin 70, xylitol 15, stevioside 0.15, peppermint oil 0.03, dextrin 50, glutinous rice 4 and propolis 0.1.
Pumpkin peel, pawpaw skin, tomato skin generally go out of use, and do not use, and cause the wasting of resources, the present invention is by pumpkin peel, pumpkin
Seed, pumpkin pulp, pawpaw, tomato, xylitol, stevioside, peppermint oil, dextrin, glutinous rice and propolis are prepared, pawpaw and tomato band
Skin utilizes, and pumpkin peel, pumpkin, pumpkin pulp, pawpaw and tomato of the present invention are combined with, pumpkin peel, pumpkin, contains in pumpkin pulp
There are polysaccharide, carrotene, organic acid, alkaloid etc., contain carrotene in pawpaw, polysaccharide, oleanolic acid, ursolic acid, general flavone,
Polyphenol substance etc., containing abundant vitamin C in tomato, lycopene, synergy is played, there is the present invention and slow down or disappear
Except fatigue, eliminate interior free yl play anti-oxidant, anti-aging, increase it is immune and other effects, available for anti-organism fatigue and and moisturizing
Beauty treatment etc., glutinous rice and propolis make the diaphragm of lozenge so that and lozenge beneficiating ingredient is not easy to be oxidized, while again easily by human body
Absorb, can quickly play antifatigue effect, and using fool proof, natural green environmental protection, while pumpkin peel is utilized, pawpaw skin,
These skin slags of tomato skin, play the skin slag utilization of resources, avoid the wasting of resources from acting on.
The preparation method of pumpkin lozenge comprises the following steps：
1) before, drying, by pumpkin pulp, pawpaw is cut to 3mm thin slice respectively, by pumpkin peel, pumpkin, pumpkin pulp, wood
Melon, tomato vacuum freeze drying temperature be -48 DEG C, to moisture be 7%, dried pumpkin peel, pumpkin, pumpkin pulp,
Ball milling, powder is made through Ultrasonic Pulverization in pawpaw, tomato, after manufactured powder is sieved, obtains powders A, wherein, the sieving
Mesh number be 60 mesh；Beneficiating ingredient in freeze-drying preservation raw material more more preferable than heated-air drying so that beneficiating ingredient is not destroyed
And reduction, Ultrasonic Pulverization and ball milling raw material to certain mesh number be in order to which following enzymolysis and extraction are easier, shorten enzymolysis and
Extraction time；
2), by the powders A described in step 1), pectase and deionized water, Ultrasonic Heating stirring are added, the time is 35 points
Clock, then centrifugal filtration, extract solution B is obtained, filter residue is collected, wherein the weight ratio of the powders A, pectase and deionized water is
15:0.5:50；Many active ingredient is fully discharged from histocyte using pectinase enzymatic hydrolysis processing raw material, further carry
High effective component extraction rate；
3), in filter residue, it is 95% ethanol first to add concentration, and filter residue is 1 with ethanol weight ratio：20, be in vacuum pressure
Heating-up temperature is 50 DEG C of refluxing extractions under 4Kpa, and extraction time is 2 times, and each extraction time is 10 minutes, is filtrated to get extraction
Liquid C, adds water, and the weight ratio of filter residue and water is 5：10, in the case where vacuum pressure is 35Kpa, heating-up temperature is that 60 DEG C of backflows carry again
Take, extraction time 1 time, each extraction time is 20 minutes, is filtrated to get extract solution D, will extract obtained extract solution C, extraction
Liquid D mixes with extract solution B step 2) described, obtains mixed extract E；Water insoluble ingredients in raw material are extracted with ethanol, true
Sky is lower to be heated to reflux temperature reduction, when being unlikely to destroy beneficiating ingredient in raw material, while being heated to reflux under vacuum
Between also shorten, improve extraction efficiency；
4), mixed extract E is concentrated under reduced pressure, by concentrate after hollow fiber filter filters, then through temperature
Spend and the extract powder F that water content is 6% is made for 70 DEG C of spray drying；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, cross 70 eye mesh screens, system
Into particle, particle is pressed into lozenge, then slurries G described in last layer is applied on manufactured lozenge surface, is dried at 65 DEG C of temperature
Film forming, finished product is obtained after the sterilized processing of lozenge, finally coating the sticky rice syrup containing propolis on lozenge top layer forms diaphragm, energy
Make pumpkin lozenge be not easy to be oxidized, ensure lozenge effect and extend lozenge effective shelf-life, the pumpkin lozenge manufactured is easy
It is absorbed by the body, it is quick plays antifatigue effect.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details and shown here as the embodiment with description.
Claims (5)
1. a kind of preparation method of pumpkin lozenge, it is characterised in that the pumpkin lozenge is made up of the raw material of following parts by weight：South
Melon skin 50~1000, pumpkin 25~500, pumpkin pulp 25~500, pawpaw 10~100, tomato 10~100, xylitol 0.2~
20th, stevioside 0.1~0.2, peppermint oil 0.01~0.05, dextrin 10~100, glutinous rice 1~10 and propolis 0.1~0.5；
The preparation method comprises the following steps：
1) it is, 5~10% by pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato vacuum freeze drying to moisture, it is described dry
Pumpkin peel, pumpkin, pumpkin pulp, pawpaw, tomato ball milling, are made powder, manufactured powder are sieved through Ultrasonic Pulverization after dry
Afterwards, powders A is obtained, wherein, the grit number of crossing is 12-120 mesh；Vacuum freeze drying temperature is -40~-50 DEG C, wherein, do
Before dry, the pumpkin pulp, pawpaw are cut to 1~5mm thin slices respectively；
2), by powders A described in step 1), pectase and deionized water are added, Ultrasonic Heating stirring, the time is 30-40 minutes,
Centrifugal filtration again, extract solution B is obtained, collect filter residue, wherein the powders A, pectase is 10~15 with deionized water weight ratio:
0.5~2:30~50；
3), by filter residue described in step 2), by filter residue and ethanol weight than 1~3：10~20 first add ethanol under vacuum
Heating and refluxing extraction, is filtrated to get extract solution C, then by filter residue and water weight ratio is 1~5：10~25 add water in vacuum bar
It is heated to reflux extracting again under part, is filtrated to get extract solution D, extraction is obtained into extract solution C, extract solution D and the step 2) extraction
Liquid B is mixed, and obtains mixed extract E；It it is 1~2 time with ethanol extraction time, each extraction time is 10~20 minutes, uses water
Extraction time 1~2 time, each extraction time are 20~30 minutes；
With ethanol heated under vacuum refluxing extraction, vacuum pressure is 3.4~5.8Kpa, and heating-up temperature is 40-80 DEG C, uses water
Heated under vacuum refluxing extraction, vacuum pressure are 25~38Kpa, and heating-up temperature is 40-80 DEG C；
4), mixed extract E described in step 3) is concentrated under reduced pressure, concentrate is filtered by hollow fiber filter
Afterwards, then spray-dried extract powder F is made；
5) glutinous rice, is worn into slurry, propolis is then added and obtains slurries G with sticky rice syrup mixed dissolution；
6) it is, that extract powder F in step 4) and dextrin, xylitol, stevioside, peppermint oil ball milling mixing is uniform, cross 12~120
Eye mesh screen, particle is made, particle is pressed into lozenge, then slurries G described in lozenge surface spraying last layer is being made, in temperature 60
Drying and forming-film at~80 DEG C, the sterilized processing of lozenge are got product.
2. the preparation method of pumpkin lozenge according to claim 1, it is characterised in that the pumpkin lozenge is by following parts by weight
Raw material be made：Pumpkin peel 100~500, pumpkin 100~300, pumpkin pulp 100~300, pawpaw 20~80, tomato 20~
60th, xylitol 0.2~10, stevioside 0.1~0.2, peppermint oil 0.02~0.04, dextrin 20~100, glutinous rice 2~5 and propolis
0.1~0.2.
3. the preparation method of pumpkin lozenge according to claim 1, it is characterised in that ethanol described in step 3) be 10~
95% ethanol.
4. the preparation method of pumpkin lozenge according to claim 1, it is characterised in that carried after being spray-dried in step 4)
It is 5~10% to take thing powder F water content.
5. the preparation method of pumpkin lozenge according to claim 1, it is characterised in that spray drying temperature is in step 4)
60-80℃。
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| CN106072629A (en) * | 2016-06-11 | 2016-11-09 | 陈清秀 | A kind of Radix et Caulis Opuntiae Dillenii plant buccal tablet and preparation method thereof |
| CN105996003A (en) * | 2016-06-11 | 2016-10-12 | 陈清秀 | Kidney supplementing plant buccal tablets and preparation method thereof |
| CN106072605A (en) * | 2016-06-11 | 2016-11-09 | 陈清秀 | A kind of water chestnut lozenge and preparation method thereof |
| CN106108011A (en) * | 2016-06-25 | 2016-11-16 | 孙凤平 | A kind of water Jambul plant buccal tablet and preparation method thereof |
| CN106360186A (en) * | 2016-09-18 | 2017-02-01 | 天津北洋百川生物技术有限公司 | Preparation method for pumpkin beverage |
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