CN111821222A - Agilawood massage oil and preparation method thereof - Google Patents
Agilawood massage oil and preparation method thereof Download PDFInfo
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- CN111821222A CN111821222A CN202010689107.7A CN202010689107A CN111821222A CN 111821222 A CN111821222 A CN 111821222A CN 202010689107 A CN202010689107 A CN 202010689107A CN 111821222 A CN111821222 A CN 111821222A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 239000000341 volatile oil Substances 0.000 claims abstract description 79
- 239000003921 oil Substances 0.000 claims abstract description 72
- 235000019198 oils Nutrition 0.000 claims abstract description 72
- 229910003472 fullerene Inorganic materials 0.000 claims abstract description 60
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 claims abstract description 59
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 32
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 32
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000008117 stearic acid Substances 0.000 claims abstract description 32
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000002480 mineral oil Substances 0.000 claims abstract description 23
- 235000010446 mineral oil Nutrition 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 23
- 238000000605 extraction Methods 0.000 claims abstract description 19
- 239000004006 olive oil Substances 0.000 claims abstract description 16
- 235000008390 olive oil Nutrition 0.000 claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 101
- 239000000706 filtrate Substances 0.000 claims description 36
- 239000002002 slurry Substances 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- 238000000967 suction filtration Methods 0.000 claims description 18
- 238000009210 therapy by ultrasound Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 108010059820 Polygalacturonase Proteins 0.000 claims description 17
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 11
- 108090000790 Enzymes Proteins 0.000 claims description 9
- 102000004190 Enzymes Human genes 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 9
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 230000003301 hydrolyzing effect Effects 0.000 claims description 9
- 230000000415 inactivating effect Effects 0.000 claims description 9
- 239000012074 organic phase Substances 0.000 claims description 9
- 230000003647 oxidation Effects 0.000 abstract description 18
- 238000007254 oxidation reaction Methods 0.000 abstract description 18
- 238000000034 method Methods 0.000 abstract description 6
- 230000002195 synergetic effect Effects 0.000 abstract description 4
- 238000005299 abrasion Methods 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 3
- 235000019441 ethanol Nutrition 0.000 description 30
- 230000000052 comparative effect Effects 0.000 description 23
- 229940088598 enzyme Drugs 0.000 description 8
- 239000003963 antioxidant agent Substances 0.000 description 6
- 230000003078 antioxidant effect Effects 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
- 108010059892 Cellulase Proteins 0.000 description 3
- 229940106157 cellulase Drugs 0.000 description 3
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000012488 sample solution Substances 0.000 description 3
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 2
- 230000031700 light absorption Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 238000002835 absorbance Methods 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 238000001467 acupuncture Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000002199 base oil Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 238000000554 physical therapy Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 239000012088 reference solution Substances 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Birds (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses agilawood massage oil and a preparation method thereof, wherein the agilawood massage essential oil is prepared from the following raw materials: mineral oil, olive oil, GTCC, fullerene, isopropyl myristate, stearic acid and agilawood essential oil. The agilawood massage oil has good oxidation resistance, the oxidation resistance can be remarkably improved by adding the fullerene and the agilawood essential oil, and the fullerene and the agilawood essential oil have a synergistic effect in the aspect of oxidation resistance; the agilawood essential oil with good oxidation resistance is prepared by the preparation method of the agilawood essential oil, the extraction rate is high, the agilawood essential oil can improve the smell, and the agilawood essential oil is fresh and mellow in smell and strong in fragrance without being greasy; the agilawood essential oil can improve the use comfort of the massage oil, and effectively eliminate fatigue and use feeling; in the using process, the addition of the fullerene can enable the frictional resistance and the abrasion to be smaller, so that the massage oil has better fitting property with the skin.
Description
Technical Field
The invention relates to the technical field of massage oil, and particularly relates to agilawood massage oil and a preparation method thereof.
Background
Modern people have faster life rhythm and higher pressure, and in addition, some unhealthy life styles, such as long-term computer facing, frequent staying up all night and the like, cause the problems of rough skin, oil, acne, dry skin and the like.
The agilawood essential oil is prepared by distilling and extracting precious agilawood and is the essence of the agilawood. Massage is a physical therapy means, and acupuncture point stimulation, muscle and bone relaxation, fatigue relief and pressure relief are carried out through massage. The massage oil is used for massage, is skin care oil used for enhancing the massage effect, and usually consists of essential oil and base oil, the massage oil massage is a method of applying the massage oil to a required part and massaging by using a special massage manipulation, and people can massage the body by the massage oil to achieve the effects of losing weight, beautifying, relieving pressure, reducing internal heat, helping emotion to release and the like. The massage oil on the market at present has great defects in the aspects of comfort, fatigue elimination and oxidation resistance.
Disclosure of Invention
The agilawood massage oil has good oxidation resistance and good use comfort, can effectively eliminate fatigue, and is good in use feeling and smell.
The invention adopts the following technical scheme for solving the technical problems:
agilawood massage oil is prepared from the following raw materials in parts by weight: 30-50 parts of mineral oil, 10-25 parts of olive oil, 20-35 parts of GTCC, 0.1-0.4 part of fullerene, 1-10 parts of isopropyl myristate, 5-10 parts of stearic acid and 0.5-2 parts of agilawood essential oil.
The applicant of the invention finds that the agilawood massage oil has good oxidation resistance in experiments of a large amount of agilawood massage oil, wherein the addition of the agilawood essential oil and the fullerene can obviously improve the oxidation resistance, and the agilawood essential oil and the fullerene have good synergistic effect; the agilawood massage oil is good in using comfort, can effectively eliminate fatigue feeling, is good in using feeling, and can remarkably improve the smell and the smell degree due to the addition of the agilawood essential oil, and the agilawood essential oil is fresh and mellow in smell and strong in fragrance and is not greasy; the agilawood essential oil can improve the use comfort of the massage oil, and effectively eliminate fatigue and use feeling; the fullerene can effectively resist oxidation, the fullerene can obviously improve the use feeling, and in the use process, the addition of the fullerene can enable the frictional resistance and the abrasion to become smaller, so that the massage oil and the skin have better fitting performance.
The GTCC is purchased from American-exemplary Biotechnology, Inc. of Guangzhou; the fullerene is oil-soluble fullerene and is purchased from Reynolds Biotechnology Co., Ltd, Guangzhou; other materials are commercially available.
As a preferable scheme, the agilawood massage oil is prepared from the following raw materials in parts by weight: 35-50 parts of mineral oil, 15-25 parts of olive oil, 20-30 parts of GTCC, 0.2-0.4 part of fullerene, 1-8 parts of isopropyl myristate, 6-10 parts of stearic acid and 0.5-1.8 parts of agilawood essential oil.
As a most preferable scheme, the agilawood massage oil is prepared from the following raw materials in parts by weight: 45 parts of mineral oil, 18 parts of olive oil, 25 parts of GTCC, 0.3 part of fullerene, 4 parts of isopropyl myristate, 8 parts of stearic acid and 1 part of agilawood essential oil.
As a preferable scheme, the preparation method of the agilawood essential oil comprises the following steps:
s1: smashing an agilawood raw material to 40-80 meshes, adding deionized water with the weight being 4-7 times that of the agilawood, and carrying out ultrasonic treatment for 30-50 min to obtain slurry;
s2: adding pectinase accounting for 2-5% of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 50-65 ℃ for 1-3 h;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 60-80% ethanol into the first filtrate for extraction, taking an organic phase for suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The applicant of the invention finds that the agilawood essential oil extracted by pectinase has good antioxidant performance and high extraction rate in a large number of agilawood essential oil extraction experiments.
Preferably, the ultrasonic treatment power is 450W in power and 40kHz in frequency.
As a preferable scheme, the ethanol is 70% ethanol, and the weight ratio of the first filtrate to the 70% ethanol is 1: 1.5 to 2.
As a most preferred scheme, the pectase accounts for 3.2% of the weight of the agilawood.
As a most preferred embodiment, the fullerene is an oil-soluble fullerene.
The invention also provides a preparation method of the agilawood massage oil, which comprises the following steps:
(1) adding stearic acid into mineral oil, heating, and stirring until the stearic acid is completely melted;
(2) cooling to 25-30 ℃, adding olive oil, GTCC, fullerene, isopropyl myristate and agilawood essential oil, and uniformly stirring to obtain the agilawood massage oil.
As a preferred scheme, the heating temperature is 70-80 ℃.
The invention has the beneficial effects that: (1) the agilawood massage oil has good oxidation resistance, the oxidation resistance can be remarkably improved by adding the fullerene and the agilawood essential oil, and the fullerene and the agilawood essential oil have a synergistic effect in the aspect of oxidation resistance; (2) the agilawood essential oil with good oxidation resistance is prepared by the preparation method of the agilawood essential oil, the extraction rate is high, the agilawood essential oil can improve the smell, and the agilawood essential oil is fresh and mellow in smell and strong in fragrance without being greasy; the agilawood essential oil can improve the use comfort of the massage oil, and effectively eliminate fatigue and use feeling; (3) the fullerene can effectively resist oxidation, the fullerene can obviously improve the use feeling, and in the use process, the addition of the fullerene can enable the frictional resistance and the abrasion to become smaller, so that the massage oil and the skin have better fitting performance.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The agilawood massage oil is prepared from the following raw materials in parts by weight: 45 parts of mineral oil, 18 parts of olive oil, 25 parts of GTCC, 0.3 part of fullerene, 4 parts of isopropyl myristate, 8 parts of stearic acid and 1 part of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 3.2 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 hours;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 70% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to the 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Example 2
Agilawood massage oil is prepared from the following raw materials in parts by weight: 30 parts of mineral oil, 10 parts of olive oil, 20 parts of GTCC, 0.1-fullerene, 1 part of isopropyl myristate, 5 parts of stearic acid and 0.5 part of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 3.2 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 hours;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 70% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to the 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Example 3
Agilawood massage oil is prepared from the following raw materials in parts by weight: 50 parts of mineral oil, 25 parts of olive oil, 35 parts of GTCC, 0.4 part of fullerene, 10 parts of isopropyl myristate, 10 parts of stearic acid and 2 parts of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 3.2 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 hours;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 70% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to the 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Example 4
Agilawood massage oil is prepared from the following raw materials in parts by weight: 35 parts of mineral oil, 20 parts of olive oil, 25 parts of GTCC, 0.2 part of fullerene, 4 parts of isopropyl myristate, 6 parts of stearic acid and 0.8 part of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 3.2 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 hours;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 70% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to the 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Example 5
The agilawood massage oil is prepared from the following raw materials in parts by weight: 45 parts of mineral oil, 18 parts of olive oil, 25 parts of GTCC, 0.3 part of fullerene, 4 parts of isopropyl myristate, 8 parts of stearic acid and 1 part of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 2 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 hours;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 70% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to the 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Example 6
The agilawood massage oil is prepared from the following raw materials in parts by weight: 45 parts of mineral oil, 18 parts of olive oil, 25 parts of GTCC, 0.3 part of fullerene, 4 parts of isopropyl myristate, 8 parts of stearic acid and 1 part of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 5 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 h;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 70% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to the 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Example 7
The agilawood massage oil is prepared from the following raw materials in parts by weight: 45 parts of mineral oil, 18 parts of olive oil, 25 parts of GTCC, 0.3 part of fullerene, 4 parts of isopropyl myristate, 8 parts of stearic acid and 1 part of agilawood essential oil.
The fullerene is oil-soluble fullerene.
The preparation method of the agilawood essential oil comprises the following steps:
s1: crushing the agilawood raw material to 50 meshes, adding deionized water with the weight 5 times that of the agilawood, and carrying out ultrasonic treatment for 35min to obtain slurry, wherein the power of the ultrasonic treatment power is 450W, and the frequency is 40 kHz;
s2: adding pectinase accounting for 5 percent of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 60 ℃ for 2 h;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 60% ethanol into the first filtrate for extraction, wherein the weight ratio of the first filtrate to 70% ethanol is 1: 1.8; and (4) taking the organic phase, performing suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
The preparation method of the agilawood massage oil comprises the following steps:
(1) adding stearic acid into mineral oil, heating to 75 ℃, and stirring until the stearic acid is completely melted;
(2) cooling to 28 deg.C, adding oleum Olivarum, GTCC, fullerene, isopropyl myristate, and lignum Aquilariae Resinatum essential oil, and stirring to obtain the lignum Aquilariae Resinatum massage oil.
Comparative example 1
Comparative example 1 is different from example 1 in that comparative example 1 does not contain fullerene, and the others are the same.
Comparative example 2
Comparative example 2 differs from example 1 in that comparative example 2 does not contain agilawood essential oil, and the other is the same.
Comparative example 3
Comparative example 3 is different from example 1 in that cellulase is used instead of pectinase in the method for preparing agilawood essential oil described in comparative example 3, and the rest is the same.
To further demonstrate the effect of the present invention, the following test methods were provided:
1. and (3) detecting the oxidation resistance: the skin care massage oils described in examples 1-7 and comparative examples 1-3 were tested for their ability to scavenge DPPH free radicals: preparing a sample solution with the concentration of 0.5mg/mL by using absolute ethyl alcohol as a solvent and massage oil as a solute; to a 1cm quartz cuvette, 2.0mL of the sample solution and 2.0mL of a 1.0X 10 molar concentration4Uniformly mixing a DPPH solution in mol/L, standing in a dark place for 30 minutes, and measuring a light absorption value A at 517nm by taking an ethanol water solution with a volume fraction of 95% as a reference solution; measuring the light absorption value Ao of the mixed solution of 2.0mL of sample solution and 2.0mL of ethanol water solution with the volume fraction of 95% at 517nm by the same method; then, the absorbance A1 at 517nm of 2.0mL of a mixture of DPPH solution with a molar concentration of 1.0X 104mol/L and 2.0mL of an aqueous solution of ethanol with a volume fraction of 95% was measured, and the inhibition was calculated according to the following formula: clearance (%) [1- (A-Ao)/A1]X 100. The test results are shown in Table 1.
2. Calculating the extraction rate of the agilawood essential oil: in the preparation method of the agilawood essential oil, 1kg of the agilawood essential oil is fed, and the extraction rates of the agilawood essential oil in examples 1, 5, 6 and 7 and comparative example 4 are calculated. The test results are shown in Table 1.
TABLE 1 test results
As can be seen from table 1, the agilawood massage oil disclosed by the invention has good antioxidant performance, as can be seen from comparative examples 1-4, the antioxidant performance can be influenced by different proportions of the agilawood massage oil, wherein example 1 is the optimal proportion and has the optimal antioxidant performance, as can be seen from comparative examples 1, 5 and 6, the antioxidant performance can be influenced by different addition amounts of pectinase, wherein example 1 is the optimal addition amount of pectinase, and as can be seen from comparative examples 1 and 7, the antioxidant performance can be influenced by different ethanol concentrations, wherein example 1 is the optimal ethanol concentration; as can be seen from comparative examples 1 and 2, the fullerene and the agilawood essential oil can significantly improve the oxidation resistance, and the fullerene and the agilawood essential oil have a synergistic effect in terms of oxidation resistance, and as can be seen from comparative examples 1 and 3, in the preparation method of the agilawood essential oil, the oxidation resistance is reduced after the pectinase is replaced by the cellulase.
As can be seen from table 1, the extraction rate of the agilawood essential oil of the invention is 0.88%, and as can be seen from comparative example 1 and examples 5 and 6, the addition amount of different pectinases can affect the extraction rate of the agilawood essential oil, wherein example 1 is the optimal addition amount, and as can be seen from comparative example 1 and example 7, different ethanol concentrations can affect the extraction rate of the agilawood essential oil, wherein example 1 is the optimal concentration; comparing example 1 with comparative example 3, it can be seen that the extraction rate of the agilawood essential oil is reduced after the pectinase is replaced by the cellulase.
3. The using effect of the agilawood massage oil prepared in the examples 1-3 and the comparative examples 1-2 is determined: the experimental method comprises the following steps: 50 volunteers were divided into 5 groups (selected from 30-40 years old without skin diseases, male and female were unlimited), the agilawood massage oil 28d prepared in examples 1-3 and comparative examples 1-2 was used to evaluate the comfortableness (less than or equal to 10 min), the fatigue eliminating (less than or equal to 10 min), the use feeling (less than or equal to 10 min) and the smell (less than or equal to 10 min) (each of which was divided into one grade), during the use period, other massage oil products and related products were not used, the test results are shown in table 2, and the test results are the average value of the scores of 10 persons.
TABLE 2 test results
As can be seen from the table 1, the agilawood massage oil disclosed by the invention is comfortable to use, can effectively eliminate fatigue, and is good in use feeling and smell; as can be seen from comparison of the agilawood massage oil in the examples 1-3, the use comfort, the fatigue and the use feeling can be affected by the proportion of different agilawood massage oil; the comparison of example 1 and comparative example 2 shows that the addition of fullerene can significantly improve the use feeling, and the comparison of example 1 and comparative example 3 shows that the agilawood essential oil can significantly improve the use comfort, eliminate the fatigue feeling, the use feeling and the smell.
In light of the foregoing description of preferred embodiments according to the invention, it is clear that many changes and modifications can be made by the person skilled in the art without departing from the scope of the invention. The technical scope of the present invention is not limited to the contents of the specification, and must be determined according to the scope of the claims.
Claims (10)
1. The agilawood massage oil is characterized by being prepared from the following raw materials in parts by weight: 30-50 parts of mineral oil, 10-25 parts of olive oil, 20-35 parts of GTCC, 0.1-0.4 part of fullerene, 1-10 parts of isopropyl myristate, 5-10 parts of stearic acid and 0.5-2 parts of agilawood essential oil.
2. The agilawood massage oil as claimed in claim 1, wherein the agilawood massage oil is prepared from the following raw materials in parts by weight: 35-50 parts of mineral oil, 15-25 parts of olive oil, 20-30 parts of GTCC, 0.2-0.4 part of fullerene, 1-8 parts of isopropyl myristate, 6-10 parts of stearic acid and 0.5-1.8 parts of agilawood essential oil.
3. The agilawood massage oil as claimed in claim 1, wherein the agilawood massage oil is prepared from the following raw materials in parts by weight: 45 parts of mineral oil, 18 parts of olive oil, 25 parts of GTCC, 0.3 part of fullerene, 4 parts of isopropyl myristate, 8 parts of stearic acid and 1 part of agilawood essential oil.
4. The agilawood massage oil as claimed in claim 1, wherein the preparation method of the agilawood essential oil comprises the following steps:
s1: smashing an agilawood raw material to 40-80 meshes, adding deionized water with the weight being 4-7 times that of the agilawood, and carrying out ultrasonic treatment for 30-50 min to obtain slurry;
s2: adding pectinase accounting for 2-5% of the weight of the agilawood into the slurry, and hydrolyzing in a water bath at 50-65 ℃ for 1-3 h;
s3: inactivating enzyme, performing suction filtration, taking a first filtrate, adding 60-80% ethanol into the first filtrate for extraction, taking an organic phase for suction filtration again, and distilling the obtained second filtrate to remove ethanol to obtain the agilawood essential oil.
5. The agilawood massage oil according to claim 4, wherein the ultrasonic treatment power is 450W in power and 40kHz in frequency.
6. The agilawood massage oil as claimed in claim 4, wherein the ethanol is 70% ethanol, and the weight ratio of the first filtrate to the 70% ethanol is 1: 1.5 to 2.
7. The agilawood massage oil according to claim 4, wherein the pectinase is 3.2% of the weight of the agilawood.
8. The agilawood massage oil according to claim 4, wherein the fullerene is an oil-soluble fullerene.
9. The preparation method of the agilawood massage oil as claimed in any one of claims 1 to 7, which is characterized by comprising the following steps:
(1) adding stearic acid into mineral oil, heating, and stirring until the stearic acid is completely melted;
(2) cooling to 25-30 ℃, adding olive oil, GTCC, fullerene, isopropyl myristate and agilawood essential oil, and uniformly stirring to obtain the agilawood massage oil.
10. The preparation method of the agilawood massage oil according to claim 9, wherein the heating temperature is 70-80 ℃.
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