CN107216950A - Agilawood spray and agilawood tobacco tar preparation method - Google Patents
Agilawood spray and agilawood tobacco tar preparation method Download PDFInfo
- Publication number
- CN107216950A CN107216950A CN201710634312.1A CN201710634312A CN107216950A CN 107216950 A CN107216950 A CN 107216950A CN 201710634312 A CN201710634312 A CN 201710634312A CN 107216950 A CN107216950 A CN 107216950A
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- Prior art keywords
- agalloch eaglewood
- agilawood
- tobacco tar
- essential oil
- temperature
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 27
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 27
- 239000007921 spray Substances 0.000 title claims abstract description 9
- 238000002360 preparation method Methods 0.000 title claims description 14
- 239000000341 volatile oil Substances 0.000 claims abstract description 36
- 230000000694 effects Effects 0.000 claims abstract description 9
- 238000000194 supercritical-fluid extraction Methods 0.000 claims abstract description 3
- 241000271309 Aquilaria crassna Species 0.000 claims description 93
- 238000000605 extraction Methods 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 16
- 238000005507 spraying Methods 0.000 claims description 16
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- 238000000926 separation method Methods 0.000 claims description 12
- 239000002304 perfume Substances 0.000 claims description 10
- 235000013599 spices Nutrition 0.000 claims description 10
- 239000002023 wood Substances 0.000 claims description 10
- 239000012530 fluid Substances 0.000 claims description 8
- 238000005516 engineering process Methods 0.000 claims description 7
- 238000000227 grinding Methods 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 7
- 241001265525 Edgeworthia chrysantha Species 0.000 claims description 6
- 238000000889 atomisation Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 2
- 239000001569 carbon dioxide Substances 0.000 claims description 2
- 238000002955 isolation Methods 0.000 claims description 2
- 239000005416 organic matter Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 8
- 239000003921 oil Substances 0.000 abstract description 6
- 238000002156 mixing Methods 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract description 3
- 239000003595 mist Substances 0.000 abstract 4
- 239000000779 smoke Substances 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 1
- 239000003205 fragrance Substances 0.000 description 4
- 239000002893 slag Substances 0.000 description 4
- 241001533085 Aquilaria sinensis Species 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 150000003384 small molecules Chemical class 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 235000019504 cigarettes Nutrition 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 238000004114 suspension culture Methods 0.000 description 2
- 239000011800 void material Substances 0.000 description 2
- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 1
- 241000984061 Aquilaria Species 0.000 description 1
- 235000009414 Elaeocarpus kirtonii Nutrition 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 208000031361 Hiccup Diseases 0.000 description 1
- 235000013584 Tabebuia pallida Nutrition 0.000 description 1
- 244000236151 Tabebuia pallida Species 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 208000019790 abdominal distention Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 210000003127 knee Anatomy 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 230000003902 lesion Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N sec-butylidene Natural products CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- RXHIKAIVEMAPRU-JRIGQVHBSA-N sequiterpene Natural products C1=C(C)[C@@H](OC(C)=O)[C@H](O)[C@@]2(O)[C@H](C)CC[C@@H](C(C)=C)[C@H]21 RXHIKAIVEMAPRU-JRIGQVHBSA-N 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 210000004916 vomit Anatomy 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a method for preparing agilawood smoke oil and agilawood mist spray, which comprises the steps of firstly crushing the agilawood smoke oil and agilawood mist spray by a low-temperature crusher at a low temperature, then filtering the agilawood by agilawood, performing supercritical extraction, and finally separating, purifying and blending the agilawood smoke oil and the agilawood mist spray. The invention provides a method for preparing agilawood tobacco tar by purifying agilawood essential oil and blending agilawood mist, which greatly enhances the absorption effect of a human body of a user.
Description
Technical field
The invention belongs to essential oil technical field, more specifically, more particularly to a kind of agalloch eaglewood is sprayed and agalloch eaglewood tobacco tar
Preparation method.
Background technology
Agalloch eaglewood is that Thymelaeceae agalloch eaglewood category (Aquilaria agalocha Roxb.) or Thymelaeceae agalloch eaglewood belong to suspension culture of Aquilaria sinensis
Resinous position in [Aquilaria sinensis (Lour.) Gilg] trees.The main northeast for originating from the South Asian Subcontinent,
Indonesia archipelago and Papua New Guinea archipelago, referred to as import agalloch eaglewood；China agalloch eaglewood mainly originate from Guangdong, Hainan,
The provinces and regions such as Yunnan, Fujian, referred to as Home-made occluder.Mainly in flavor component for sequiterpene and its containing oxygen derivative in agalloch eaglewood
Class, aromatic compound, aliphatic acid and its lipid and chromogen ketone etc..Agalloch eaglewood is from agallochum by exterior injury or sheet
The secreted resin of the influence such as body lesion, it is parasitic by the microorganism invasion of Menanotus flavoliven, in thalline in the presence of enzyme,
It there occurs a series of changes, and through a kind of special material rich in fragrance formed by depositing for many years.
Agalloch eaglewood has many uses, and clinically there is agalloch eaglewood to have a sending down abnormally ascending middle benefit gas for it, and warm kidney receives effect of gas.The circulation of vital energy in the wrong direction is controlled to breathe heavily
Breath, vomits hiccup, and abdominal distention, waist and knee void is cold, and large intestine void is secret, and urine gas drenches, the effect of man's cold sperm.
At present, in the prior art, the method for agalloch eaglewood Edgeworthia chrysantha is varied, such as Publication No. CN103184102A invention
A kind of extracting method of agilawood essential oil of patent application publication, this method has steps of, and first cuts down suspension culture of Aquilaria sinensis tree, removes white
Wood, carves agalloch eaglewood thin slice；Agalloch eaglewood thin slice is ground into the agalloch eaglewood powder of 40 mesh sieves again；Then agalloch eaglewood powder is added to extraction with normal butane
Kettle is taken, agilawood essential oil is directly extracted using subcritical fluid extraction technology；Slag after the agilawood essential oil that then first time is extracted
Extraction kettle is added to 95% ethanol and carries out second of extraction extraction agilawood essential oil；Wherein, first time extraction conditions and second of extraction
The condition is taken to be：Extraction time is 0.5-1.5h, and resolution temperature is 60 DEG C, and 50 DEG C of Extracting temperature, extraction pressure is 0.4-
0.5MPa.Above-mentioned patent application methods described is substantially that agalloch eaglewood face cream is extracted, and this face cream oil content is very high, price
Extremely expensive, thus deducted a percentage split-phase is to simple, without polishing purification technique, thus obtained agilawood essential oil product price is also very
It is high.
Meanwhile, at present, for agilawood essential oil utilization rate than relatively low, it is impossible to be that human body largely absorbs, reach treatment
Effect.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of agalloch eaglewood proposed is sprayed and agalloch eaglewood
The preparation method of tobacco tar.
To achieve the above object, the present invention provides following technical scheme：
A kind of agalloch eaglewood spraying and the preparation method of agalloch eaglewood tobacco tar, comprise the following steps：
S1, choose perfume (or spice)：For more than 7 years agallochums, after Edgeworthia chrysantha, peeling went rotten wood to choose perfume (or spice), it is therefore an objective to choose agalloch eaglewood from agallochum
Elect；
S2, the agalloch eaglewood low-temperature grinding that will be singled out, attrition grinding is carried out using Lowtemperaturepulverizer, and the pulverizer has automatic drop
Temperature function；
S3, supercritical extract：Extracted using carbon dioxide supercritical extraction technology, super critical CO 2 technology is to set up
CO 2 fluid has the isolation technics in special solubility effect to organic matter in the supercritical state；
S4, separating-purifying：The purpose of separating-purifying is to separate impurity, improve its it is pure from fat, moisture, wherein moisture will
Less than 5%, essential oil can be made to preserve for a long time；
S5, blend：Agalloch eaglewood tobacco tar can be blent into spray with agalloch eaglewood, agalloch eaglewood spraying is blent using atomization, with 450-550 grams of small group
Molecular water blends 1 gram of agilawood essential oil；Agalloch eaglewood tobacco tar：Agilawood essential oil with 80-120 grams of edible glycerol than 1.5 grams, at a high speed
Blend and form under rotation.
It is preferred that, the one-level separating technology parameter setting of supercritical extract operation is as follows：Extracting pressure 20-21Mpa, temperature
44-48 DEG C, CO 2 fluid flow is 2.5-7.0L/h, and separating pressure is 8Mpa, and separation temperature is all 40 DEG C, collects agalloch eaglewood
Essential oil.
It is preferred that, second of extraction conditions is：Extraction time is 0.5-1.5h, and resolution temperature is 60 DEG C, Extracting temperature 50
DEG C, extraction pressure is 0.4-0.5MPa.
It is preferred that, in S2, wood chip is ground into the agalloch eaglewood powder of 20-80 mesh.
The technique effect and advantage of the present invention：A kind of spraying of agalloch eaglewood and the preparation method of agalloch eaglewood tobacco tar that the present invention is provided,
First crushed with Lowtemperaturepulverizer under low-temperature condition, then the supercritical extract after agalloch eaglewood is filtered, is finally separating and carries
The pure agalloch eaglewood tobacco tar that blends into is sprayed with agalloch eaglewood, and the heat-sensitive ingredients of fragrance are not only protected to greatest extent, thus product fragrance is pure
Just and completely, appearance uniform is transparent, good fluidity.The present invention proposes that a kind of agalloch eaglewood purifies out agilawood essential oil, then by blending out
Agalloch eaglewood is sprayed, and the production method of agalloch eaglewood tobacco tar greatly enhances user's absorption of human body effect.
Brief description of the drawings
Fig. 1 is process chart of the invention.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.Based on the embodiment in the present invention, those of ordinary skill in the art are not before creative work is made
The every other embodiment obtained is put, the scope of protection of the invention is belonged to.
Embodiment 1
A kind of agalloch eaglewood spraying and the preparation method of agalloch eaglewood tobacco tar, comprise the following steps：
S1, choose perfume (or spice)：For more than 7 years agallochums, after Edgeworthia chrysantha, peeling went rotten wood to choose perfume (or spice), it is therefore an objective to choose agalloch eaglewood from agallochum
Elect；
S2, the agalloch eaglewood that will be singled out carry out low-temperature grinding using Lowtemperaturepulverizer, and wood chip is ground into the agalloch eaglewood powder of 20 mesh, described
Pulverizer has automatic cooling function
S3, supercritical extract：Agalloch eaglewood is filtered, agalloch eaglewood is put into supercritical extract device and extracted, one-level separation, one-level separation
Technological parameter sets as follows：Extracting pressure 20Mpa, 44 DEG C of temperature, CO 2 fluid flow is 2.5L/h, and separating pressure is
8Mpa, separation temperature is all 40 DEG C, collects agilawood essential oil；Slag after the agilawood essential oil that then first time is extracted is added to extractor
Carry out second of extraction and extract agilawood essential oil；Second of extraction conditions be：Extraction time is 0.5h, and resolution temperature is 60 DEG C, is carried
Temperature 50 C is taken, extraction pressure is 0.4MPa；
S4, separating-purifying：The purpose of separating-purifying is to separate impurity, improve its it is pure from fat, moisture, wherein moisture will
Less than 5%, essential oil can be made to preserve for a long time；
S5, blend：Agalloch eaglewood tobacco tar can be blent into spray with agalloch eaglewood, agalloch eaglewood spraying is blent using atomization, with 450 grams of small molecule
Water blends 1 gram of agilawood essential oil；Agalloch eaglewood tobacco tar：Agilawood essential oil with 80 grams of edible glycerol than 1.5 grams, is hooked in the case where high speed rotates
Convert and form.
Embodiment 2
A kind of agalloch eaglewood spraying and the preparation method of agalloch eaglewood tobacco tar, comprise the following steps：
S1, choose perfume (or spice)：For more than 7 years agallochums, after Edgeworthia chrysantha, peeling went rotten wood to choose perfume (or spice), it is therefore an objective to choose agalloch eaglewood from agallochum
Elect；
S2, the agalloch eaglewood that will be singled out carry out low-temperature grinding using Lowtemperaturepulverizer, and wood chip is ground into the agalloch eaglewood powder of 60 mesh, described
Lowtemperaturepulverizer has automatic cooling function；
S3, supercritical extract：Agalloch eaglewood is filtered, agalloch eaglewood is put into supercritical extract device and extracted, one-level separation, one-level separation
Technological parameter sets as follows：Extracting pressure 20-21Mpa, 44-48 DEG C of temperature, CO 2 fluid flow is 5.5L/h, separation pressure
Power is 8Mpa, and separation temperature is all 40 DEG C, collects agilawood essential oil；Slag after the agilawood essential oil that then first time is extracted is added to extraction
Take device to carry out second of extraction and extract agilawood essential oil；Second of extraction conditions be：Extraction time is 01.2h, and resolution temperature is 60
DEG C, 50 DEG C of Extracting temperature, extraction pressure is 0.45MPa；
S4, separating-purifying：The purpose of separating-purifying is to separate impurity, improve its it is pure from fat, moisture, wherein moisture will
Less than 5%, essential oil can be made to preserve for a long time；
S5, blend：Agalloch eaglewood tobacco tar can be blent into spray with agalloch eaglewood, agalloch eaglewood spraying is blent using atomization, with 500 grams of small molecule
Water blends 1 gram of agilawood essential oil；Agalloch eaglewood tobacco tar：Agilawood essential oil with 100 grams of edible glycerol than 1.5 grams, in the case where high speed rotates
Blend and form.
Embodiment 3
A kind of agalloch eaglewood spraying and the preparation method of agalloch eaglewood tobacco tar, comprise the following steps：
S1, choose perfume (or spice)：For more than 7 years agallochums, after Edgeworthia chrysantha, peeling went rotten wood to choose perfume (or spice), it is therefore an objective to choose agalloch eaglewood from agallochum
Elect；
S2, the agalloch eaglewood that will be singled out carry out low-temperature grinding using Lowtemperaturepulverizer, and wood chip is ground into the agalloch eaglewood powder of 80 mesh, described
Lowtemperaturepulverizer has automatic cooling function；
S3, supercritical extract：Agalloch eaglewood is filtered, agalloch eaglewood is put into supercritical extract device and extracted, one-level separation, one-level separation
Technological parameter sets as follows：Extracting pressure 21Mpa, 48 DEG C of temperature, CO 2 fluid flow is 7.0L/h, and separating pressure is
8Mpa, separation temperature is all 40 DEG C, collects agilawood essential oil；Slag after the agilawood essential oil that then first time is extracted is added to extractor
Carry out second of extraction and extract agilawood essential oil；Second of extraction conditions be：Extraction time is 1.5h, and resolution temperature is 60 DEG C, is carried
Temperature 50 C is taken, extraction pressure is 0.5MPa；
S4, separating-purifying：The purpose of separating-purifying is to separate impurity, improve its it is pure from fat, moisture, wherein moisture will
Less than 5%, essential oil can be made to preserve for a long time；
S5, blend：Agalloch eaglewood tobacco tar can be blent into spray with agalloch eaglewood, agalloch eaglewood spraying is blent using atomization, with 550 grams of small molecule
Water blends 1 gram of agilawood essential oil；Agalloch eaglewood tobacco tar：Agilawood essential oil with 120 grams of edible glycerol than 1.5 grams, in the case where high speed rotates
Blend and form.
In summary：A kind of spraying of agalloch eaglewood and the preparation method of agalloch eaglewood tobacco tar that the present invention is provided, first with Lowtemperaturepulverizer
Extracted under low temperature conditions, then the supercritical extract after agalloch eaglewood is filtered, is finally separating purification and blends into agilawood cigarette
Oil is sprayed with agalloch eaglewood, not only protects the heat-sensitive ingredients of fragrance to greatest extent, thus product aroma of pure and complete, and outward appearance is equal
It is even transparent, good fluidity.The present invention proposes that a kind of agalloch eaglewood purifies out agilawood essential oil, then is sprayed by blending out agalloch eaglewood, agilawood cigarette
The production method of oil, greatly enhances user's absorption of human body effect.
Finally it should be noted that：The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic,
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention's
Within protection domain.
Claims (4)
1. a kind of agalloch eaglewood spraying and the preparation method of agalloch eaglewood tobacco tar, it is characterised in that comprise the following steps：
S1, choose perfume (or spice)：For more than 7 years agallochums, after Edgeworthia chrysantha, peeling went rotten wood to choose perfume (or spice), it is therefore an objective to choose agalloch eaglewood from agallochum
Elect；
S2, the agalloch eaglewood low-temperature grinding that will be singled out, attrition grinding is carried out using Lowtemperaturepulverizer, and the pulverizer has automatic drop
Temperature function；
S3, supercritical extract：Extracted using carbon dioxide supercritical extraction technology, super critical CO 2 technology is to set up
CO 2 fluid has the isolation technics in special solubility effect to organic matter in the supercritical state；
S4, separating-purifying：The purpose of separating-purifying is to separate impurity, improve its it is pure from fat, moisture, wherein moisture will
Less than 5%, essential oil can be made to preserve for a long time；
S5, blend：Agalloch eaglewood tobacco tar can be blent into spray with agalloch eaglewood, agalloch eaglewood spraying is blent using atomization, with 450-550 grams of small group
Molecular water blends 1 gram of agilawood essential oil；Agalloch eaglewood tobacco tar：Agilawood essential oil with 80-120 grams of edible glycerol than 1.5 grams, at a high speed
Blend and form under rotation.
2. a kind of agalloch eaglewood spraying according to claim 1 and the preparation method of agalloch eaglewood tobacco tar, it is characterised in that：Overcritical extraction
The one-level separating technology parameter setting of extract operation is as follows：Extracting pressure 20-21Mpa, 44-48 DEG C of temperature, CO 2 fluid stream
Measure as 2.5-7.0L/h, separating pressure is 8Mpa, separation temperature is all 40 DEG C, collects agilawood essential oil.
3. a kind of agalloch eaglewood spraying according to claim 1 and the preparation method of agalloch eaglewood tobacco tar, it is characterised in that：Second of extraction
The condition is taken to be：Extraction time is 0.5-1.5h, and resolution temperature is 60 DEG C, and 50 DEG C of Extracting temperature, extraction pressure is 0.4-0.5MPa.
4. a kind of agalloch eaglewood spraying according to claim 1 and the preparation method of agalloch eaglewood tobacco tar, it is characterised in that：In S2,
Wood chip is ground into the agalloch eaglewood powder of 20-80 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710634312.1A CN107216950A (en) | 2017-07-29 | 2017-07-29 | Agilawood spray and agilawood tobacco tar preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710634312.1A CN107216950A (en) | 2017-07-29 | 2017-07-29 | Agilawood spray and agilawood tobacco tar preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107216950A true CN107216950A (en) | 2017-09-29 |
Family
ID=59954578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710634312.1A Pending CN107216950A (en) | 2017-07-29 | 2017-07-29 | Agilawood spray and agilawood tobacco tar preparation method |
Country Status (1)
| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108002997A (en) * | 2017-12-15 | 2018-05-08 | 中国医学科学院药用植物研究所海南分所 | A kind of Lignum Aquilariae Resinatum extract and its application with preventing or arresting vomiting effect |
| CN108542976A (en) * | 2018-07-12 | 2018-09-18 | 草本搭档有限公司 | A kind of agalloch eaglewood spray formula and preparation method thereof |
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|---|---|---|---|---|
| CN103184102A (en) * | 2013-01-14 | 2013-07-03 | 中山市国林沉香科学研究所 | Extraction method and application of agilawood essential oil |
| CN103627527A (en) * | 2013-06-30 | 2014-03-12 | 金玛瑙香水（明光）有限公司 | Extraction method of agilawood essential oil |
| CN105011349A (en) * | 2014-04-30 | 2015-11-04 | 上海绿馨电子科技有限公司 | Electronic cigarette oil containing agilawood extract and preparation method thereof |
| CN105105316A (en) * | 2015-07-14 | 2015-12-02 | 深圳合创源生物科技有限公司 | Agilawood essential oil atomized liquid and preparation method thereof |
-
2017
- 2017-07-29 CN CN201710634312.1A patent/CN107216950A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103184102A (en) * | 2013-01-14 | 2013-07-03 | 中山市国林沉香科学研究所 | Extraction method and application of agilawood essential oil |
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Application publication date: 20170929 |