CN109430645A - A kind of novel honeysuckle compound beverage and preparation method thereof - Google Patents
A kind of novel honeysuckle compound beverage and preparation method thereof Download PDFInfo
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- CN109430645A CN109430645A CN201811360100.XA CN201811360100A CN109430645A CN 109430645 A CN109430645 A CN 109430645A CN 201811360100 A CN201811360100 A CN 201811360100A CN 109430645 A CN109430645 A CN 109430645A
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- Prior art keywords
- honeysuckle
- preparation
- ethyl acetate
- compound beverage
- extract
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention provides a kind of novel honeysuckle compound beverage and preparation method thereof, and the honeysuckle compound beverage formula is as follows: raw material: honeysuckle ethyl acetate extract 0.5%-1.0%, honeysuckle subcritical abstraction object 0.5%-1.0%, lycopene 0.1%-0.2%, vine polyphenol 0.1%-0.2%, vitamin E 0.005%-0.008%, Rosa Damascana 0.04%-0.08%；Auxiliary material: white granulated sugar 2%-4%, acesulfame potassium 0.4%-0.6%, citric acid 0.1%-0.2%, xanthan gum 0.05%-0.1%, potassium sorbate 0.06%-0.08%, deionized water 92.532%-96.145%；The preparation method comprises the following steps: the preparation of honeysuckle ethyl acetate extract, the preparation of honeysuckle subcritical abstraction object, ingredient, and dissolution is boiled, mixed, and clarification filtration is filling, sterilization.The present invention is other than using the volatile oil in ethyl acetate high efficiency extraction honeysuckle, by subcritical abstraction technology, using liquid nitrogen as solvent, can high efficiency extraction go out the water-soluble actives such as chlorogenic acid, flavones, polysaccharide, greatly improve the utilization rate of raw material.
Description
Technical field
The invention belongs to food and drink technology field, in particular to a kind of novel honeysuckle compound beverage and its preparation side
Method.
Background technique
Honeysuckle is for the dry flower of the evergreen liana honeysuckle of Caprifoliaceae perennial half or with the flower just opened, and honeysuckle is certainly
Gu is known as clearing heat and detoxicating good medicine, its property sweet cold air fragrance, clear heat with drugs of sweet flavour and cold nature without injuring one's stomach, fragrance thoroughly up to again can eliminating evil, contain
Chlorogenic acid, isochlorogenic acid, amino acid and soluble sugar and other functional ingredient have medicine and health-care effect well, have heat-clearing solution
Poison, dispelling wind and heat from the body function are used for various febrile diseases, such as body heat, dermexanthesis, macular eruption, heat toxin sore carbuncle, abscess of throat disease, equal effect
Significantly, it is commonly used to make tea, decoction, dew is made.
Currently, the production of domestic producer only simple progress honeysuckle tea, the distilled liquid of honeysuckle, or only extract honeysuckle
In active ingredient chlorogenic acid, such as: " distilled liquid of honeysuckle " is the armaticity volatile oil extracted with honeysuckle by vapor distillation method
Water is added to be formulated, some honeysuckle beverage products are to match the cooking liquor addition sweetener etc. that honeysuckle is obtained by boiling
Made of system, these product processes are substantially similar, and be all using a certain fractions of active ingredient of honeysuckle such as volatile oil or
Chlorogenic acid, raw material availability is lower, and many non-extracted active materials are lost if polysaccharide, flavones are unutilized by manufacturer
It abandons, not only causes the pollution of environment, and due to containing the substances such as chlorogenic acid more abundant, flavones, polysaccharide in raffinate residue,
Cause the serious waste of resource.
For this situation, need to improve production technology, invention raw material availability height and the clearing heat and detoxicating gold to work well
Honeysuckle flower composite beverage, to achieve the purpose that make full use of the natural resources, for this purpose, the present invention proposes that a kind of novel honeysuckle is compound
Beverage and preparation method thereof.
Summary of the invention
Of the existing technology in order to solve the problems, such as, the present invention provides a kind of novel honeysuckle compound beverages and its system
Preparation Method, the present invention is other than using the volatile oil in ethyl acetate high efficiency extraction honeysuckle, by subcritical abstraction technology, with
Liquid nitrogen is solvent, can high efficiency extraction go out the water-soluble actives such as chlorogenic acid, flavones, polysaccharide, greatly improve raw material
Utilization rate.
To achieve the goals above, the present invention is to realize by the following technical solutions: a kind of novel honeysuckle is multiple
Beverage and preparation method thereof is closed, the honeysuckle compound beverage formula is as follows: raw material: honeysuckle ethyl acetate extract 0.5%-
1.0%, honeysuckle subcritical abstraction object 0.5%-1.0%, lycopene 0.1%-0.2%, vine polyphenol 0.1%-0.2%,
Vitamin E 0.005%-0.008%, Rosa Damascana 0.04%-0.08%；Auxiliary material: white granulated sugar 2%-4%, acesulfame potassium 0.4%-
0.6%, citric acid 0.1%-0.2%, xanthan gum 0.05%-0.1%, potassium sorbate 0.06%-0.08%, deionized water
92.532%-96.145%；The preparation method comprises the following steps:
Step 1: honeysuckle ethyl acetate extract preparation；Extracting honeysuckle 100g first cleans the sundries such as silt with clear water,
Drying, after crushing, obtains Honeysuckle Flower, and 600mL food level ethyl acetate is added into Honeysuckle Flower, uses supersonic cell
Crusher handles 30min to powder ultrasonic, and filtrate is obtained by filtration, second of addition 500mL food level ethyl acetate ultrasonic wave
Cell pulverization instrument to powder ultrasonic handle 30min, filtrate is obtained by filtration, will twice filtrate merge after, in 35 DEG C, 0.08MPa-
It is concentrated under reduced pressure into no ethyl acetate under conditions of 0.1MPa to steam, obtaining medicinal extract is honeysuckle ethyl acetate extract；
Step 2: honeysuckle subcritical abstraction object preparation；By Honeysuckle Flower filtered in step 1, drying is spare,
Then it puts into and carries out subcritical abstraction in closed extractor, to container vacuum-pumping, inject extractant liquefied ammonia and flood honeysuckle powder
End carries out counter-current extraction, after extraction, extract liquor is introduced into knockout drum and is separated, recycling design, residue, as gold and silver
Flower subcritical abstraction object；
Step 3: ingredient；Suitable raw material is taken according to formula rate and auxiliary material is spare；
Step 4: dissolution；Honeysuckle ethyl acetate extract and the subcritical extraction of honeysuckle are dissolved using portions of de-ionized water
Take object；
Step 5: it boils；White granulated sugar, acesulfame potassium are added in remaining deionized water, 5min-10min is boiled, then plus
Enter into the solution of step 4, then adds lycopene, vine polyphenol, vitamin E, Rosa Damascana, citric acid, xanthan gum respectively
And potassium sorbate；
Step 6: mixing；By the solution in step 5 at 60 DEG C -80 DEG C, mixed well with the stirring of 400r/min speed,
It is settled to required volume, obtains honeysuckle compound beverage；
Step 7: clarification filtration；Honeysuckle compound beverage in step 6 is used into 0.2 μm of -0.45 μm of miillpore filter mistake
Filter carries out clarification filtration；
Step 8: filling；After the completion of filtering, using hot filling form, filling instant capping；
Step 9: sterilization；After canned, maintain temperature 15min-25min to be sterilized, after sterilization, be rapidly cooled to room temperature
It saves.
As a kind of preferred embodiment of the invention, the temperature of hot filling is 80 DEG C -85 DEG C in the step 8.
As a kind of preferred embodiment of the invention, the mixing time in the step 6 is 10min.
As a kind of preferred embodiment of the invention, in the step 2, after extraction, by the molten of all separation and removing
Agent recycling.
As a kind of preferred embodiment of the invention, the extraction temperature in the step 2 is 30 DEG C -50 DEG C, and extracting pressure is
0.3Mpa-0.5Mpa, extraction time 40min-80min.
The raw materials used in the present invention has following characteristic:
Honeysuckle: being known as clearing heat and detoxicating good medicine from ancient times, and the sweet cold air fragrance of its property, clear heat with drugs of sweet flavour and cold nature is without hurting, and fragrance is thoroughly
Up to again can eliminating evil, honeysuckle can dispelling wind-heat, also kind removing summer-heat blood poison is used for various febrile diseases, such as body heat, dermexanthesis, macular eruption, heat
The diseases such as carbuncle pain, abscess of throat, equal significant effect, modern study proves that, honeysuckle contains chlorogenic acid, polysaccharide, cyanidenon glycosides
It, can also strengthen immunity, antitumor, anti-inflammatory, antipyretic, inhibition Deng the fat-soluble equal pharmacological components such as water solubility and linalool
Intestinal absorption cholesterol etc..
Lycopene: it is a kind of natural pigment contained in plant, is primarily present in the mellow fruit of plant of Solanaceae tomato
In reality, it is most one of the powerful antioxidant being found in the plant of nature at present, and lycopene has inoxidizability, right
Cell growth metabolism plays regulating and controlling effect, and the metabolic defence of adjustable cholesterol is cardiovascular, also has and prevents and inhibit tumour, suppression
System mutation reduces nucleic acid damaging, reduces the plurality of health care functions such as cardiovascular disease.
Vine polyphenol: also referred to as Red Wine Polyphenols is extracted from red wine, and grape contains a large amount of polyphenol substance, therefore it extracts
Take object to have apparent anti-oxidation efficacy, it is fermented become grape wine after, polyphenol content more improves, ingredient is more stable, antioxygen
Change ability is substantially improved, and the polyphenolic substance in red wine is more than 50 kinds, is current found polyphenoils most species, anti-oxidant
Substance widest in area.
Vitamin E: being a kind of liposoluble vitamin, is one of most important antioxidant, vitamin E primary efficacy: prolongs
Slow aging, effectively reduces the generation of wrinkle, reduces cell oxygen demand, makes one more have endurance, anti-oxidation protection body cell is exempted from
By the murder by poisoning of free radical, improve lipid-metabolism, prevent coronary heart disease, atherosclerosis, effectively inhibition tumour growth prevent many places
Chronic disease.
Rosa Damascana: Rosa Damascana is the filemot essential oil that rose extracts, it can stimulate immune with landman
System and nervous system, while helping to improve the secretion of endocrine gland, remove organ sclerosis, repair cell, Rosa Damascana tool
There are antibacterial, anti-spasm, sterilization, calmness, benefit body and other effects, and contains citronellol, geraniol, linalool isoreactivity in Rosa Damascana
Substance has effects that clearing heat-fire, lubrication enteron aisle.
The invention has the benefit that
1, the present invention is by ultrasonic extraction, and using food level ethyl acetate as solvent, high efficiency extraction goes out fat-soluble armaticity and waves
Composition is sent out, by subcritical abstraction technology, using liquid nitrogen as solvent, high efficiency extraction goes out the water-soluble actives such as chlorogenic acid, flavones, polysaccharide
Substance greatly improves the utilization rate of raw material.
2, extract of the invention contains most active constituents of honeysuckle, and the basic effect for remaining honeysuckle is made
With while, be added to suitable active ingredient substance and compounded, not only strengthened clearing heat and detoxicating effect, but also increase antioxygen
The effect of change, strengthen immunity, form a kind of beverage of unique flavor.
3, a kind of honeysuckle compound beverage of the invention is formulated safety, good mouthfeel, is easy to receive carrying, Shou Zhongguang has
Wide market application prospect, and simple process, convenient for large-scale production.
Detailed description of the invention
Fig. 1 is a kind of preparation method flow chart of honeysuckle compound beverage；
Specific embodiment
To be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, below with reference to
Specific embodiment, the present invention is further explained.
To avoid repeating, percentage composition refers both to mass percent in following embodiments, the honeysuckle acetic acid second in embodiment
The preparation method of ester extract and honeysuckle subcritical abstraction object is described collectively.
Honeysuckle ethyl acetate extract is prepared by following methods:
Extracting honeysuckle 100g first cleans the sundries such as silt with clear water, and drying after crushing, obtains Honeysuckle Flower, Xiang Jinyin
600mL food level ethyl acetate is added in end in pollen, handles 30min to powder ultrasonic with Ultrasonic cell smash, filters
To filtrate, second of addition 500mL food level ethyl acetate Ultrasonic cell smash handles 30min, mistake to powder ultrasonic
Filter obtain filtrate, will twice filtrate merge after, be concentrated under reduced pressure into no ethyl acetate under conditions of 35 DEG C, 0.08MPa-0.1MPa
It steams, obtaining medicinal extract is honeysuckle ethyl acetate extract.
Honeysuckle subcritical abstraction object is prepared by following methods:
By filtered Honeysuckle Flower in above-mentioned honeysuckle subcritical abstraction object preparation process, drying is spare, then throws
Enter and carry out subcritical abstraction in closed extractor, to container vacuum-pumping, injects extractant liquefied ammonia and flood Honeysuckle Flower, carry out
Counter-current extraction after extraction, extract liquor is introduced into knockout drum and is separated, recycling design, and residue, as honeysuckle are subcritical
Extract.
Embodiment 1:
The every 100mL of honeysuckle compound beverage includes the raw material and auxiliary material of following mass percent, composition of raw materials: honeysuckle second
Acetoacetic ester extract 0.8%, honeysuckle subcritical abstraction object 0.8%, lycopene 0.15%, vine polyphenol 0.15%, dimension life
Plain E0.006%, Rosa Damascana 0.06%；Accessory formula: white granulated sugar 3%, acesulfame potassium 0.5%, citric acid 0.15%, xanthan gum
0.08%, potassium sorbate 0.07%；Surplus is deionized water.
The preparation method of the present embodiment honeysuckle compound beverage, comprising the following steps:
1.: honeysuckle ethyl acetate extract, honeysuckle subcritical abstraction object are added by mass percentage, use deionization
Water dissolution；
2.: weigh white granulated sugar, acesulfame potassium by mass percentage, deionized water added to boil 8min, after be added to solution 1.
In, then by mass percentage respectively add lycopene, vine polyphenol, vitamin E, Rosa Damascana, citric acid, xanthan gum and
Potassium sorbate；
3.: by solution 2. at 70 DEG C, is mixed well with 400r/min speed stirring 10min, be settled to required volume,
Deployed honeysuckle beverage is subjected to clarification filtration using 0.7 μm of miillpore filter membrane filter；
4.: after the completion of filtering, using hot filling form, the temperature of hot filling is 83 DEG C, filling instant capping, after canned,
Temperature 20min is maintained, after sterilization, is rapidly cooled to be stored at room temperature.
Embodiment 2:
The every 100mL of honeysuckle compound beverage includes the raw material and auxiliary material of following mass percent, composition of raw materials: honeysuckle second
Acetoacetic ester extract 0.5%, honeysuckle subcritical abstraction object 0.5%, lycopene 0.1%, vine polyphenol 0.1%, vitamin
E0.005%, Rosa Damascana 0.04%；Accessory formula: white granulated sugar 2%, acesulfame potassium 0.4%, citric acid 0.1%, xanthan gum
0.05%, potassium sorbate 0.06%；Surplus is deionized water.
The preparation method of the present embodiment honeysuckle compound beverage, comprising the following steps:
1.: honeysuckle ethyl acetate extract, honeysuckle subcritical abstraction object are added by mass percentage, use deionization
Water dissolution；
2.: weigh white granulated sugar, acesulfame potassium by mass percentage, deionized water added to boil 5min, after be added to solution 1.
In, then by mass percentage respectively add lycopene, vine polyphenol, vitamin E, Rosa Damascana, citric acid, xanthan gum and
Potassium sorbate；
3.: by solution 2. at 60 DEG C, is mixed well with 400r/min speed stirring 10min, be settled to required volume,
Deployed honeysuckle beverage is subjected to clarification filtration using 0.6 μm of miillpore filter membrane filter；
4.: after the completion of filtering, using hot filling form, the temperature of hot filling is 80 DEG C, filling instant capping, after canned,
Temperature 15min is maintained, after sterilization, is rapidly cooled to be stored at room temperature.
Embodiment 3:
The every 100mL of honeysuckle compound beverage includes the raw material and auxiliary material of following mass percent, composition of raw materials: honeysuckle second
Acetoacetic ester extract 1.0%, honeysuckle subcritical abstraction object 1.0%, lycopene 0.2%, vine polyphenol 0.2%, vitamin
E0.008%, Rosa Damascana 0.08%；Accessory formula: white granulated sugar 4%, acesulfame potassium 0.6%, citric acid 0.2%, xanthan gum
0.1%, potassium sorbate 0.08%；Surplus is deionized water.
The preparation method of the present embodiment honeysuckle compound beverage, comprising the following steps:
1.: honeysuckle ethyl acetate extract, honeysuckle subcritical abstraction object are added by mass percentage, use deionization
Water dissolution；
2.: weigh white granulated sugar, acesulfame potassium by mass percentage, deionized water added to boil 10min, after be added to solution 1.
In, then by mass percentage respectively add lycopene, vine polyphenol, vitamin E, Rosa Damascana, citric acid, xanthan gum and
Potassium sorbate；
3.: by solution 2. at 80 DEG C, is mixed well with 400r/min speed stirring 10min, be settled to required volume,
Deployed honeysuckle beverage is subjected to clarification filtration using 0.8 μm of miillpore filter membrane filter；
4.: after the completion of filtering, using hot filling form, the temperature of hot filling is 85 DEG C, filling instant capping, after canned,
Temperature 25min is maintained, after sterilization, is rapidly cooled to be stored at room temperature.
Embodiment 4:
The clearing heat and detoxicating measure of merit of honeysuckle compound beverage prepared by embodiment 1:
The present invention selects tcm diagnosis excessive internal heat standard are as follows: inflamed eyes, perleche, pharynx by taking the excessive internal heat of Chinese medicine body as an example
Larynx swelling and pain, bleeding gums, furuncle sore first rise, the hot agitation of body, oliguria constipation etc., and symptom as above can be made a definite diagnosis, in 100 made a definite diagnosis
In volunteer, wherein each 25 people of men and women, the age 20-50 years old, without other serious diseases, volunteer was divided into two groups, and one group uses this
Honeysuckle compound beverage, another group is compared using commercially available a certain honeysuckle beverage product, application method are as follows: patient directly drinks
This product is drunk once daily, once drinks 340mL, adhere to being examined honeysuckle compound beverage heat-clearing of the invention using 5 days
The effect of removing toxic substances, the judgment criteria of curative effect are as follows:
Effective: inflamed eyes, perleche, abscess of throat, bleeding gums, furuncle sore first play disappearance, and body heat is irritated significant slow
Solution, oliguria constipation disappear, and urine is salubrious.
Effective: inflamed eyes, perleche, abscess of throat, bleeding gums, furuncle sore first rise, oliguria constipation has larger alleviation.
Invalid: symptom is without substantially changeing.
The result shows that: the clearing heat and detoxicating efficient city for being substantially better than comparison of honeysuckle compound beverage prepared by the present invention
Honeysuckle beverage product is sold, i.e., the honeysuckle compound beverage prepared by the present invention is clearing heat and detoxicating works well.
Embodiment 5:
Below with reference to experimental data to honeysuckle compound beverage of the embodiment of the present invention antioxidation activity aspect effect into
Row evaluation.
Anti-oxidant experiment is carried out using spectrophotometry, using the honeysuckle compound beverage of the preparation of embodiment 1 as experimental group, with
Commercially available a certain honeysuckle beverage product be control group, accurate measuring embodiment 1 prepare honeysuckle compound beverage and it is commercially available certain
One honeysuckle beverage 2mL sequentially adds 0.6mL reaction solution (deoxyribose containing 2.67mmol/L, 0.1mmol/LEDTA
The phosphate buffer that 0.2mol/LPH is 7.4), ferrous sulfate solution 0.2mL, 1.0mmol/L ascorbic acid of 0.4mmol/L
0.05mL and 20mmol/L hydrogenperoxide steam generator 0.05mL in 37 DEG C of heating water bath 15min, then is separately added into 1% malonyl
Thiourea solution and 2% each 1mL of solution of trichloroacetic acid, terminate reaction, then boiling water bath heat 15min, be immediately placed at after taking-up
Cooled on ice returns to zero by blank of distilled water, measures light absorption value at 532nm, obtain Ai, replaces sample with distilled water, measures AO,
The clearance rate of hydroxy radical is calculated according to the following formula, and each sample in triplicate, is averaged, in which: clearance rate (%)=
(1-Ai/AO) × 100%, experimental result:
Experimental group: clearance rate (%)=(1-0.262/0.803) × 100%=67.37%
Control group: clearance rate (%)=(1-0.504/0.803) × 100%=37.24%
The result shows that: honeysuckle compound beverage hydroxy radical (OH) clearance rate prepared by the present invention is substantially better than comparing
Commercially available honeysuckle beverage product, i.e., the present invention prepared by honeysuckle compound beverage antioxidant activity it is good.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention, for this field skill
For art personnel, it is clear that invention is not limited to the details of the above exemplary embodiments, and without departing substantially from spirit of the invention or
In the case where essential characteristic, the present invention can be realized in other specific forms.Therefore, in all respects, should all incite somebody to action
Embodiment regards exemplary as, and is non-limiting, the scope of the present invention by appended claims rather than on state
Bright restriction, it is intended that including all changes that fall within the meaning and scope of the equivalent elements of the claims in the present invention
It is interior.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (5)
1. a kind of novel honeysuckle compound beverage and preparation method thereof, which is characterized in that the honeysuckle compound beverage formula
It is as follows: raw material: honeysuckle ethyl acetate extract 0.5%-1.0%, honeysuckle subcritical abstraction object 0.5%-1.0%, tomato
Red pigment 0.1%-0.2%, vine polyphenol 0.1%-0.2%, vitamin E 0.005%-0.008%, Rosa Damascana 0.04%-
0.08%；Auxiliary material: white granulated sugar 2%-4%, acesulfame potassium 0.4%-0.6%, citric acid 0.1%-0.2%, xanthan gum 0.05%-
0.1%, potassium sorbate 0.06%-0.08%, deionized water 92.532%-96.145%；The preparation method includes following step
It is rapid:
Step 1: honeysuckle ethyl acetate extract preparation；Extracting honeysuckle 100g first cleans the sundries such as silt with clear water, drying,
After crushing, Honeysuckle Flower is obtained, 600mL food level ethyl acetate is added into Honeysuckle Flower, is crushed with supersonic cell
Instrument handles 30min to powder ultrasonic, and filtrate is obtained by filtration, second of addition 500mL food level ethyl acetate supersonic cell
Crusher to powder ultrasonic handle 30min, filtrate is obtained by filtration, will twice filtrate merge after, in 35 DEG C, 0.08MPa-0.1MPa
Under conditions of be concentrated under reduced pressure into no ethyl acetate and steam, obtaining medicinal extract is honeysuckle ethyl acetate extract；
Step 2: honeysuckle subcritical abstraction object preparation；By Honeysuckle Flower filtered in step 1, drying is spare, then
It puts into and carries out subcritical abstraction in closed extractor, to container vacuum-pumping, inject extractant liquefied ammonia and flood Honeysuckle Flower, into
Row counter-current extraction after extraction, extract liquor is introduced into knockout drum and is separated, recycling design, residue, and as honeysuckle Asia is faced
Boundary's extract；
Step 3: ingredient；Suitable raw material is taken according to formula rate and auxiliary material is spare；
Step 4: dissolution；Honeysuckle ethyl acetate extract and honeysuckle subcritical abstraction object are dissolved using portions of de-ionized water；
Step 5: it boils；White granulated sugar, acesulfame potassium are added in remaining deionized water, 5min-10min is boiled, is then added to
In the solution of step 4, then lycopene, vine polyphenol, vitamin E, Rosa Damascana, citric acid, xanthan gum and mountain are added respectively
Potassium sorbate；
Step 6: mixing；By the solution in step 5 at 60 DEG C -80 DEG C, mixed well with the stirring of 400r/min speed, constant volume
To required volume, honeysuckle compound beverage is obtained；
Step 7: clarification filtration；Honeysuckle compound beverage in step 6 is used into 0.2 μm of -0.45 μm of nuclepore membrane filter
Carry out clarification filtration；
Step 8: filling；After the completion of filtering, using hot filling form, filling instant capping；
Step 9: sterilization；After canned, maintain temperature 15min-25min to be sterilized, after sterilization, be rapidly cooled to be stored at room temperature.
2. the novel honeysuckle compound beverage and preparation method thereof of one kind according to claim 1, it is characterised in that: described
The temperature of hot filling is 80 DEG C -85 DEG C in step 8.
3. the novel honeysuckle compound beverage and preparation method thereof of one kind according to claim 1, it is characterised in that: described
Mixing time in step 6 is 10min.
4. the novel honeysuckle compound beverage and preparation method thereof of one kind according to claim 1, it is characterised in that: described
In step 2, after extraction, the solvent recovery cycle of all separation and removing is used.
5. the novel honeysuckle compound beverage and preparation method thereof of one kind according to claim 1, it is characterised in that: described
Extraction temperature in step 2 is 30 DEG C -50 DEG C, extracting pressure 0.3Mpa-0.5Mpa, extraction time 40min-80min.
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| CN113735708A (en) * | 2021-09-30 | 2021-12-03 | 中国药科大学 | Chlorogenic acid extraction method based on subcritical extraction process |
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| 孟祥东: ""金银花挥发油的提取、GC/MS鉴定及其卷烟加香应用研究"", 《中国优秀博硕士学位论文全文数据库(硕士)工程科技Ⅰ辑》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109965165A (en) * | 2019-04-11 | 2019-07-05 | 湖北大别山药业股份有限公司 | A kind of novel sapor distilled liquid of honeysuckle and preparation method thereof |
| CN113735708A (en) * | 2021-09-30 | 2021-12-03 | 中国药科大学 | Chlorogenic acid extraction method based on subcritical extraction process |
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