CN1990001A - Process for extracting total saponin from papermulberry fruit - Google Patents
Process for extracting total saponin from papermulberry fruit Download PDFInfo
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- CN1990001A CN1990001A CNA2005102008916A CN200510200891A CN1990001A CN 1990001 A CN1990001 A CN 1990001A CN A2005102008916 A CNA2005102008916 A CN A2005102008916A CN 200510200891 A CN200510200891 A CN 200510200891A CN 1990001 A CN1990001 A CN 1990001A
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- fructus broussonetiae
- total saponin
- extraction
- papermulberry fruit
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a method which extracts total soap glucoside from papermulberry fruit. It follows below steps to preparing: drying and disintegrating the papermulberry fruit and getting the papermulberry fruit powder as A material; extracting A material through mechanical squeeze or carbon dioxide supercritical extraction device, separating the papermulberry fruit peach oil and the resulting mixture is B material; extracting and refinishing B material with organic solvent and getting papermulberry fruit total soap glucoside. The invention uses mechanical squeeze or carbon dioxide supercritical extraction device to removing papermulberry fruit peach oil, then refines and extracts the material using flavouring alcohol, the got total soap glucoside extraction rate >=1.84% which is higher then other methods extraction rate(0.51%) in prior technology 3.5 times. At the same time it solves the question of effective ingredients easily lost better, raises the rate of extraction but also solves the problems of removing impurities, improving purity and decreasing cost while increasing the rate of extraction, so achieves the purpose of the invention. The extracted papermulberry fruit total soap glucoside has many effects and can be used as processing raw materials of medicines and health products.
Description
Technical field
The present invention relates to a kind of method of from plant seed, extracting Saponin, particularly a kind of method of from Fructus Broussonetiae, extracting total Saponin.
Background technology
Broussonetia papyrifera claims papermulberry again, lemon wood, and the deciduous tree of moraceae plants (Broussonetia papyrifera (L.) vent), dioecism, there is distribution in national most of area, grows in the hillside, and the limit, gully mostly is wild, and a small amount of cultivation is arranged.Compendium of Material Medica claims its fruit (Fructus Broussonetiae) to have functions such as " enriching yin and nourishing kidney, liver heat removing and eyesight improving obey for a long time that flesh is not old, the strengthening bone and muscle of making light of one's life by commiting suicide, aid yang qi, tonify deficiency consumptive disease, strong waist knee joint, beneficial color ".Modern technologies research, Fructus Broussonetiae (Broussonetia papyrifera seed) contains physiological material Saponin and Fructus Broussonetiae oil, has multiple efficacies.Can reduce fat, suppress tumor, blood fat reducing, atherosclerosis, blood sugar lowering prevents diabetes, improves immunity, health invigorating, control senile dementia, defying age.Because saponin content is low in the Fructus Broussonetiae, traditional method extraction effective component extraction rate is low, and the Saponin purity that obtains is not high.Therefore people fail to extract the Fructus Broussonetiae Saponin and are used for health care and medical treatment.
Summary of the invention
The objective of the invention is to, a kind of method of extracting Saponin from Fructus Broussonetiae is provided.This method can improve extraction ratio and obtain the raw material of highly purified Saponin as the processing drugs and health care products.
Technical scheme of the present invention.From Fructus Broussonetiae, extract the method for total Saponin, it is characterized in that: make by following step;
A, the Fructus Broussonetiae drying pulverized after, cross the 40-60 mesh sieve, the Papermulberry Fruit that obtains is the A product;
B, the A product are isolated paper mulberry peach oil by mechanical expression; Or, paper mulberry peach oil extract and separate is gone out in the A product input carbon dioxide supercritical fluid extraction device; Remaining mixture is the B product;
C, with the B product with the refining extraction of organic solvent, the total Saponin of Fructus Broussonetiae.
Above-mentioned extracts in the method for total Saponin from Fructus Broussonetiae, and step b is that the A product are isolated paper mulberry peach oil by the mechanical expression method; Or the A product are dropped in the carbon dioxide supercritical fluid extraction device, controlled pressure extracts under 5mpa-30mpa, temperature 40-50 ℃ condition, goes out the paper mulberry peach is separating of oil; Remaining mixture is the B product.
In the aforesaid method of extracting total Saponin from Fructus Broussonetiae, step C is: with B product with ethanol through the refining extraction of apparatus,Soxhlet's, get the total Saponin of Fructus Broussonetiae.
In the aforesaid method of extracting total Saponin from Fructus Broussonetiae, step C is: B product are extracted through apparatus,Soxhlet's is refining with 95% edible ethanol, and must the total Saponin of Fructus Broussonetiae.
The present invention adopts the mechanical expression method of passing through earlier, or supercritical CO
2Extract and separate is removed paper mulberry peach oil, the refining method of extracting of reuse edible ethanol, total Saponin extraction ratio 〉=1.84% of gained is higher more than 3.5 times than other industrial extraction method extraction ratios (0.51%) of the prior art.The present invention has solved the problem that active ingredient is run off easily better, has also solved preferably when having improved extraction ratio and has removed impurity, improved purity, and the problem that reduces cost has reached purpose of the present invention.The Fructus Broussonetiae Saponin that the present invention extracts has the study of promotion, improves memory, suppresses the effects such as (having treatment breast carcinoma, the effect of carcinoma of prostate) of fragrant pure enzyme, and multiple efficacies such as also having slow down aging is taken in the effect that has the alzheimer disease of preventing and treating simultaneously for a long time.Can processing raw material as drugs and health care products.The present invention has easy to implement, and implementation cost is low, the characteristics that implementation result is good
The specific embodiment
Embodiments of the invention.Extract the method for Saponin, make by following step.
After a, Fructus Broussonetiae drying are pulverized, cross 50 mesh sieves, get Papermulberry Fruit, get the A product.
B, Papermulberry Fruit is isolated paper mulberry peach oil by mechanical expression; Or Papermulberry Fruit dropped into CO
2In the supercritical extraction unit, controlled pressure extracts under the temperature 40-50 ℃ of condition at 10mpa-20mpa.Extract, isolate paper mulberry peach oil; Remaining mixture is the B product.
C, with the B product, with 95% edible ethanol through the refining extraction of apparatus,Soxhlet's, the C product.
The saponin content height that adopts method of the present invention to extract, after tested, the Fructus Broussonetiae total saponin content of C product is 51.8%.
Claims (4)
1. from Fructus Broussonetiae, extract the method for total Saponin, it is characterized in that: make by following step;
A, the Fructus Broussonetiae drying pulverized after, cross the 40-60 mesh sieve, the Papermulberry Fruit that obtains is the A product;
B, the A product are isolated paper mulberry peach oil by mechanical expression; Or, paper mulberry peach oil extract and separate is gone out in the A product input carbon dioxide supercritical fluid extraction device; Remaining mixture is the B product;
C, with the B product with the refining extraction of organic solvent, the total Saponin of Fructus Broussonetiae.
2. the method for extracting total Saponin from Fructus Broussonetiae according to claim 1 is characterized in that: step b is, isolates paper mulberry peach oil with the A product by the mechanical expression method; Or the A product are dropped in the carbon dioxide supercritical fluid extraction device, controlled pressure extracts under 5mpa-30mpa, temperature 40-50 ℃ condition, goes out the paper mulberry peach is separating of oil; Remaining mixture is the B product.
3. the method for extracting total Saponin from Fructus Broussonetiae according to claim 1 and 2 is characterized in that: step C is, the B product are made with extra care extraction with ethanol through apparatus,Soxhlet's, gets the total Saponin of Fructus Broussonetiae.
4. the method for extracting total Saponin from Fructus Broussonetiae according to claim 3 is characterized in that: step C is, the B product are made with extra care extraction with 95% edible ethanol through apparatus,Soxhlet's, gets the total Saponin of Fructus Broussonetiae.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2005102008916A CN1990001B (en) | 2005-12-29 | 2005-12-29 | Process for extracting total saponin from papermulberry fruit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2005102008916A CN1990001B (en) | 2005-12-29 | 2005-12-29 | Process for extracting total saponin from papermulberry fruit |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1990001A true CN1990001A (en) | 2007-07-04 |
| CN1990001B CN1990001B (en) | 2011-05-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2005102008916A Expired - Fee Related CN1990001B (en) | 2005-12-29 | 2005-12-29 | Process for extracting total saponin from papermulberry fruit |
Country Status (1)
| Country | Link |
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| CN (1) | CN1990001B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488320A (en) * | 2011-12-08 | 2012-06-13 | 江苏中烟工业有限责任公司 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
| CN103859297A (en) * | 2014-04-07 | 2014-06-18 | 丁丹丹 | Noodle processing method with low fracture rate |
| CN103858950A (en) * | 2014-04-07 | 2014-06-18 | 丁丹丹 | Method for extracting saponin in fructus broussonetiae and application |
-
2005
- 2005-12-29 CN CN2005102008916A patent/CN1990001B/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488320A (en) * | 2011-12-08 | 2012-06-13 | 江苏中烟工业有限责任公司 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
| CN103859297A (en) * | 2014-04-07 | 2014-06-18 | 丁丹丹 | Noodle processing method with low fracture rate |
| CN103858950A (en) * | 2014-04-07 | 2014-06-18 | 丁丹丹 | Method for extracting saponin in fructus broussonetiae and application |
| CN103859297B (en) * | 2014-04-07 | 2015-04-01 | 丁丹丹 | Noodle processing method with low fracture rate |
| CN103858950B (en) * | 2014-04-07 | 2015-11-11 | 丁丹丹 | The extracting method of saponin and application in a kind of Paper mulberry Fruit |
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| Publication number | Publication date |
|---|---|
| CN1990001B (en) | 2011-05-18 |
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Granted publication date: 20110518 Termination date: 20151229 |
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