CN105907458A - Health-caring sesame oil suitable for people having hypertension, hyperglycemia and hyperlipidemia and preparation method of same - Google Patents

Health-caring sesame oil suitable for people having hypertension, hyperglycemia and hyperlipidemia and preparation method of same Download PDF

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Publication number
CN105907458A
CN105907458A CN201610251455.XA CN201610251455A CN105907458A CN 105907458 A CN105907458 A CN 105907458A CN 201610251455 A CN201610251455 A CN 201610251455A CN 105907458 A CN105907458 A CN 105907458A
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parts
radix
health
sesame oil
semen
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王浩
王健
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ANHUI HUAAN FOOD Co Ltd
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ANHUI HUAAN FOOD Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/13Coniferophyta (gymnosperms)
    • A61K36/15Pinaceae (Pine family), e.g. pine or cedar
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/25Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
    • A61K36/258Panax (ginseng)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/36Caryophyllaceae (Pink family), e.g. babysbreath or soapwort
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/537Salvia (sage)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/62Nymphaeaceae (Water-lily family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/736Prunus, e.g. plum, cherry, peach, apricot or almond
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/738Rosa (rose)
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/10Refining fats or fatty oils by adsorption

Abstract

The invention discloses health-caring sesame oil suitable for people having hypertension, hyperglycemia and hyperlipidemia. The sesame oil is prepared from the raw materials including, by weight, 1500-1800 parts of black sesame, 60-80 parts of flaxseeds, 30-40 parts of pine nuts, 20-30 parts of salvia miltiorrhiza, 20-30 parts of panax notoginseng, 20-30 parts of American ginseng, 10-20 parts of peach kernels, 10-20 parts of roxburgh rose, 10-20 parts of purslane, 10-20 parts of radix stellariae, 15-25 parts of lotus leaves and 20-30 parts of pollen pini. The invention also discloses a preparation method of the health-caring sesame oil. The sesame oil has significant effects of preventing and improving hypertension, diabetes and hyperlipidemia, improves the life quality of patients suffered from the hypertension, hyperglycemia and hyperlipidemia, and has excellent social and economical benefits.

Description

Health-care sesame oil that a kind of three-hypers crowd is suitable for and preparation method thereof
Technical field
The present invention relates to Health-care sesame oil technical field, be specifically related to what a kind of three-hypers crowd was suitable for Health-care sesame oil and preparation method thereof.
Background technology
Recently as the change of the raising of people's living standard, mode of operation and dietary structure, The symptoms such as " three-hypers disease " hypertension, hyperglycemia, hyperlipidemia improve day by day, and these symptoms are to people Healthy bring serious potential collision hazard, had a strong impact on daily life and body The heart is healthy, as nursed one's health not in time, it would be possible to can cause fatal disease.At present for above-mentioned Symptom specific aim medicine is the most, if any Western medicine and Chinese medicine, these medicines have difference to eliminating disease Medical functions, mostly as eliminating surface symptoms, and the efficacy of a drug is excessive, needs the long period Treatment, medicine time is long, causes a certain degree of damage not only for liver, and right Taste will also result in stimulation in various degree, affects the health of the mankind.Therefore early prevention is the heaviest Want, relevant with people's life style at ordinary times with a lot of risk factors of " three-hypers disease ", therefore support It is particularly important for becoming good dietary habit, and edible oil is to ensure that the basis of good diet, Select the edible oil with special health-care effect, prevention " three-hypers disease " is had particularly important work With.Oleum sesami is a kind of edible oil common in daily life, and its aromatic flavor, abnormal smells from the patient are unique, The nutritional labelings such as vitamin, linoleic acid and mineral containing multiple preciousness, have slow down aging, The effect such as blood fat-reducing blood pressure-decreasing, loosening bowel to relieve constipation, great edibility, but existing Oleum sesami raw material Showing slightly single on composition, health value is the highest.Natural Chinese medicines raw material is added in preparation process, Increase its health-care effect, thus improve edibility, have broad application prospects.
Summary of the invention
It is an object of the invention to provide Health-care sesame oil and preparation thereof that a kind of three-hypers crowd is suitable for Method.
For realizing object above, the present invention is achieved by the following technical programs:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: black Semen Sesami 1500-1800 part, flaxseed 60-80 part, Semen Pini 30-40 part, Radix Salviae Miltiorrhizae 20-30 part, Radix Notoginseng 20-30 part, Radix Panacis Quinquefolii 20-30 part, Semen Persicae 10-20 part, Fructus Rosae Normalis 10-20 part, Dens Equi Herba Amaranthi tricoloris 10-20 part, Radix Stellariae 10-20 part, Folium Nelumbinis 15-25 part, Pollen Pini 20-30 part.
Preferably, it is made up of the raw material of following weight portion: Semen Sesami Nigrum 1650-1750 part, flaxseed 65-75 part, Semen Pini 33-36 part, Radix Salviae Miltiorrhizae 20-24 part, Radix Notoginseng 25-29 part, Radix Panacis Quinquefolii 20-24 Part, Semen Persicae 13-16 part, Fructus Rosae Normalis 10-13 part, Herba Portulacae 15-18 part, Radix Stellariae 15-20 part, Folium Nelumbinis 19-23 part, Pollen Pini 25-30 part.
Preferably, it is made up of the raw material of following weight portion: Semen Sesami Nigrum 1700 parts, flaxseed 70 Part, 35 parts of Semen Pini, Radix Salviae Miltiorrhizae 21 parts, Radix Notoginseng 26 parts, Radix Panacis Quinquefolii 20 parts, 15 parts of Semen Persicae, Fructus Rosae Normalis 12 parts, Herba Portulacae 16 parts, Radix Stellariae 17 parts, 22 parts of Folium Nelumbinis, Pollen Pini 28 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 6-8 times 75% second After alcohol-water solution soaks 2-4h, it is heated to reflux 2-3h, filters, obtain extract, reduce pressure, distill Obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 40-60 mesh sieve, obtain mixed Compound;
3) by step 2) in mixture join in extraction kettle, add 1.5-2.5 times of material body Long-pending extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out Asia and face Boundary extracts, and extracting pressure is 7-10MPa, extraction temperature 30-35 DEG C, cycling extraction 3-5 time, 15-25min, CO every time2Flow velocity is 60-80L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, In the separation liquid obtained, add adsorbent remove impurity, be cooled to 0 DEG C, remove wax, filter to obtain product.
Preferably, described step 1) in be heated to reflux temperature and be 60-65 DEG C.
Preferably, described step 4) in the temperature of separating still be 15-20 DEG C, pressure is 0.5-1Mpa.
In the present invention, effect of each raw material is as follows:
Oleum sesami aromatic flavor, abnormal smells from the patient are unique, vitamin containing multiple preciousness, linoleic acid and The nutritional labelings such as mineral, have the effects such as slow down aging, blood fat-reducing blood pressure-decreasing, loosening bowel to relieve constipation, great Edibility.
Flaxseed is the seed of flax family (Linaceae) linum, and linum is one of big oil crop of China five, linum Oil is a kind of high-quality edible oil, rich in alpha-linolenic acid, linoleic acid, oleic acid, Palmic acid, tristearin The various unsaturated fatty acids such as acid, wherein linolenic acid content is up to 48%, is the highest in vegetable oil , alpha-linolenic acid can be directly translated into DHA and EPA in human body, and these materials are that human body must The unsaturated fatty acid needed, is also bathypelagic fish main body of oil, it is possible to restoration updating cranial nerve The unsaturated fatty acid chain of cell membrane, play brain-strengthening, nootropics, blood fat reducing, antiplatelet aggregation, Expansion small artery and antithrombotic etc..
The nutritive value of Semen Pini is the highest, in every hectogram stuffed pork breast with pine kernels, containing 16.7 grams of protein, fat Fat 63.5 grams, carbohydrate 9.8 grams and mineral calcium 78 milligrams, 236 milligrams of phosphorus, ferrum The nutrient substance such as 6.7 milligrams and unsaturated fatty acid.The most sub-oil of fat constituent in Semen Pini The unsaturated fatty acids such as acid, linoleic acid, and content of vitamin E is up to 30%, has well Vessel softening and the atherosclerotic effect of preventing and treating;Pine nut, can loosening bowel to relieve constipation rich in fatty oil Cathartic and do not hinder healthy energy;Additionally, phosphorus and Fe content in Semen Pini are the abundantest, this is to brain Good benefiting action is had with nerve.
Radix Salviae Miltiorrhizae integrate nourish blood, invigorate blood circulation, blood stasis dispelling, pain relieving, tissue regeneration promoting blood, effect is notable and property Taste is gentle, has benefit to have scattered, has no side effect, and Radix Salviae Miltiorrhizae is the good medicine of heart tonifying, is of great benefit to blood vessel, Can coronary artery dilating, expand peripheral blood vessel, improve microcirculation, and it is to antithrombus formation Powerful mean, also have promote tissue reparation and regeneration, improve liver microcirculation.
Radix Notoginseng has promoting blood circulation to remove blood stasis effect, has regulation blood pressure, antiplatelet aggregation, antithrombotic shape Become, coronary artery dilating, increase coronary flow, improve cardiac muscle blood oxygen supply, suppress myocardial contraction Power, decreased heart rate, reduce peripheral vascular resistance, reduce myocardial oxygen consumption, anti-atherogenic is hard The effect changed, is proven, and uncomfortable in chest, angina cordis that Radix Notoginseng is caused by coronary heart disease in treatment have Satisfied curative effect is the most notable to the function reducing cholesterol and blood fat.Its effect is peculiar bright It is called " Radix Stephaniae Sinicae (Radix Stephaniae Dielsianae) " for pharmacy man Li Shizhen (1518-1593 A.D.).
Radix Panacis Quinquefolii can with arrhythmia, resist myocardial ischemia, anti-cardiac muscle oxidation, strengthening cardiac muscle receive Contracting ability, patients with coronary heart disease Symptoms is deficiency of both QI and YIN, palpitation and short breath can long-term taking the West Ginseng, it addition, Radix Panacis Quinquefolii can reduce blood coagulability, suppression platelet aggregation, anti-tremulous pulse medicated porridge Sample hardens and promotes Growth of red blood cells, increases hematochrome, and Radix Panacis Quinquefolii also has regulation blood pressure and blood glucose Effect.
Semen Persicae sugariness is bitter, containing substantial amounts of Semen Persicae glycosides, volatile oil, Semen Persicae enzyme, fatty oil etc. Various nutrient elements, has removing blood stasis blood stasis expelling, moisturizes effect of intestinal, it is possible to vasodilator, increases stock Blood flow volume, reduces vascular resistance, directly helps expansion blood vessel wall, additionally, Semen Persicae also has Suppression blood coagulation and haemolysis, it is possible to help improve blood circulation.
Fructus Rosae Normalis is the fruit of Rosaceae perennial machaka rosa roxburghii, has clearing away heat and promoting production of body fluid, stomach invigorating The effect helped digestion, rich in sugar, vitamin, carotene, organic acid and 20 several amino acids, More than 10 plant the trace element useful to human body, and superoxide dismutase (being called for short SOD), SOD is internationally recognized to have anti-ageing, the active substance of protective effect on cancer risk, also has antiviral, anti- The effect of radiation, prevents and treats aspect at cardiovascular, digestive system and various tumor disease, applies ten Divide extensively.
Herba Portulacae contains abundant L-norepinephrine, dopamine and DOPA isoreactivity material, Norepinephrine can excite blood vessel beta-receptor, makes vasoconstriction, strengthens myocardial function, and goes back Carbohydrate metabolism in insulin secretion, regulation human body can be promoted, there is reduction blood sugar concentration, keep blood The effect that sugar is stable;Containing abundant omega-fatty acid, have very well reducing cardiovascular diseases Effect Herba Portulacae in potassium content reach 1.7%, it is possible to decrease blood pressure, decreased heart rate, there is protection Action of the heart.
Radix Stellariae is China's parts of generic medicinal plants, can reduce serum ornitrol concentration, and can make actively Arteries and veins lipoids content reduces;Saponin may act on plasma lipoprotein, stop cholesteric esterification and It is in the deposition of blood vessel wall, it is also possible to stop cholesterol from intestinal absorption etc..Radix Stellariae can be empty clearly Heat, dispelling fever with infantile malnutrition, the best antibacterial action.
Folium Nelumbinis color is dark green, gas fragrance, containing abundant chemical substance, such as beta-carotene, Huang Ketone, volatile oil, soaps, steroidal, vitamin C, multiple alkaloid, nelumboside, Quercetin, Isoquercitrin and tartaric acid, citric acid, malic acid, oxalic acid, polysaccharide etc., have heat clearing away solution Poison, sending up the lucid YANG, the effect of cooling blood for hemostasis, recent studies confirms, Folium Nelumbinis has good fall blood Sugar, blood fat reducing, protection immune organ, the effect of enhancing immunization.
Pollen Pini refers to the pine genus plant stamens such as Pinus massoniana Lamb, Pinus tabuliformis, Pinus koraiensis, Pinus armandi Franch-P. Komavovii Lavl. and Pinus sylvestnis var. mongolica Litv. Produced dry pollen, has the biggest medical value, except containing protein, fat, saccharide Outside etc. general nutrient substance, possibly together with multivitamin, trace element, flavone, enzyme, fat Acid and coenzyme etc. more than 200 plant nutritional labeling and bioactive substances, comprehensive nutrition and equalize, tool There is the effect of QI invigorating of dispeling the wind, and nervous system can also be adjusted, reduce internal lactate level, alleviate Spirit and operating pressure, physical strength reinforcing, energy, make fatigue comprehensively be recovered, and improves people Body autoimmunity.
The method have the benefit that the present invention use subcritical abstraction technology extraction carry oil oil yield high and Do not destroy active component in raw material, with Oleum sesami as carrier, add flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, The raw material such as Radix Notoginseng, Fructus Rosae Normalis refines jointly, and the mutual compatibility of each composition strengthens, and is of high nutritive value, energy Effectively reduce blood fat, cholesterol, reduce blood viscosity, vessel softening, just promoting insulin Often secrete, prevent and treat arteriosclerosis, hence for preventing and improving hypertension, diabetes, high blood Fat has remarkable result, improves the quality of life of " three high " patient, has well society and warp Ji benefit.
Detailed description of the invention
For making the purpose of the embodiment of the present invention, technical scheme and advantage clearer, below will knot Close the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely retouched State, it is clear that described embodiment is a part of embodiment of the present invention rather than whole realities Execute example.Based on the embodiment in the present invention, those of ordinary skill in the art are not making creation The every other embodiment obtained under property work premise, broadly falls into the scope of protection of the invention.
Embodiment 1:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: Fructificatio Amaurodermatis Rudae Fiber crops 1700 parts, flaxseed 70 parts, 35 parts of Semen Pini, Radix Salviae Miltiorrhizae 21 parts, Radix Notoginseng 26 parts, the West Join 20 parts, 15 parts of Semen Persicae, Fructus Rosae Normalis 12 parts, Herba Portulacae 16 parts, Radix Stellariae 17 parts, Folium Nelumbinis 22 parts, Pollen Pini 28 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 7 times 75% ethanol After aqueous solution soaking 3h, it is heated to 65 DEG C of backflow 3h, filters, obtain extract, reduce pressure, steam Evaporate to obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 50 mesh sieves, obtain mixing Thing;
3) by step 2) in mixture join in extraction kettle, add 2 times of volume of material Extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out subcritical extraction Taking, extracting pressure is 8MPa, extraction temperature 30 DEG C, cycling extraction 4 times, each 20min, CO2Flow velocity is 70L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, Temperature from still is 20 DEG C, and pressure is 0.8Mpa, adds adsorbent and remove in the separation liquid obtained Miscellaneous, it is cooled to 0 DEG C, removes wax, filter to obtain product.
Embodiment 2:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: Fructificatio Amaurodermatis Rudae Fiber crops 1750 parts, flaxseed 73 parts, 34 parts of Semen Pini, Radix Salviae Miltiorrhizae 22 parts, Radix Notoginseng 28 parts, the West Join 21 parts, 14 parts of Semen Persicae, Fructus Rosae Normalis 10 parts, Herba Portulacae 17 parts, Radix Stellariae 16 parts, Folium Nelumbinis 21 parts, Pollen Pini 27 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 6 times 75% ethanol After aqueous solution soaking 2h, it is heated to 65 DEG C of backflow 3h, filters, obtain extract, reduce pressure, steam Evaporate to obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 40 mesh sieves, obtain mixing Thing;
3) by step 2) in mixture join in extraction kettle, add 1.8 times of volume of material Extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out subcritical extraction Taking, extracting pressure is 7MPa, extraction temperature 35 DEG C, cycling extraction 3 times, each 25min, CO2Flow velocity is 65L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, Temperature from still is 15 DEG C, and pressure is 0.5Mpa, adds adsorbent and remove in the separation liquid obtained Miscellaneous, it is cooled to 0 DEG C, removes wax, filter to obtain product.
Embodiment 3:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: Fructificatio Amaurodermatis Rudae Fiber crops 1650 parts, flaxseed 75 parts, 33 parts of Semen Pini, Radix Salviae Miltiorrhizae 24 parts, Radix Notoginseng 25 parts, the West Join 24 parts, 13 parts of Semen Persicae, Fructus Rosae Normalis 13 parts, Herba Portulacae 15 parts, Radix Stellariae 20 parts, Folium Nelumbinis 19 parts, Pollen Pini 30 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 8 times 75% ethanol After aqueous solution soaking 2.5h, it is heated to 60 DEG C of backflow 2.5h, filters, obtain extract, reduce pressure, Distill to obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 60 mesh sieves, obtain mixing Thing;
3) by step 2) in mixture join in extraction kettle, add 2.5 times of volume of material Extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out subcritical extraction Taking, extracting pressure is 10MPa, extraction temperature 30 DEG C, cycling extraction 4 times, each 15min, CO2Flow velocity is 75L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, Temperature from still is 18 DEG C, and pressure is 0.7Mpa, adds adsorbent and remove in the separation liquid obtained Miscellaneous, it is cooled to 0 DEG C, removes wax, filter to obtain product.
Embodiment 4:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: Fructificatio Amaurodermatis Rudae Fiber crops 1750 parts, flaxseed 65 parts, 36 parts of Semen Pini, Radix Salviae Miltiorrhizae 20 parts, Radix Notoginseng 29 parts, the West Join 20 parts, 16 parts of Semen Persicae, Fructus Rosae Normalis 10 parts, Herba Portulacae 18 parts, Radix Stellariae 15 parts, Folium Nelumbinis 23 parts, Pollen Pini 25 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 7 times 75% ethanol After aqueous solution soaking 4h, it is heated to 60 DEG C of backflow 2h, filters, obtain extract, reduce pressure, steam Evaporate to obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 40 mesh sieves, obtain mixing Thing;
3) by step 2) in mixture join in extraction kettle, add 2.3 times of volume of material Extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out subcritical extraction Taking, extracting pressure is 7MPa, extraction temperature 30 DEG C, cycling extraction 5 times, each 20min, CO2Flow velocity is 80L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, Temperature from still is 15 DEG C, and pressure is 1Mpa, adds adsorbent remove impurity in the separation liquid obtained, It is cooled to 0 DEG C, removes wax, filter to obtain product.
Embodiment 5:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: black Semen Sesami 1500 parts, flaxseed 80 parts, 30 parts of Semen Pini, Radix Salviae Miltiorrhizae 30 parts, Radix Notoginseng 20 parts, west Radix Panacis Quinquefolii 30 parts, 10 parts of Semen Persicae, Fructus Rosae Normalis 20 parts, Herba Portulacae 10 parts, Radix Stellariae 20 parts, lotus 15 parts of leaf, Pollen Pini 30 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 8 times 75% ethanol After aqueous solution soaking 2h, it is heated to 65 DEG C of backflow 3h, filters, obtain extract, reduce pressure, steam Evaporate to obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 50 mesh sieves, obtain mixing Thing;
3) by step 2) in mixture join in extraction kettle, add 1.5 times of volume of material Extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out subcritical extraction Taking, extracting pressure is 10MPa, extraction temperature 35 DEG C, cycling extraction 3 times, each 25min, CO2Flow velocity is 75L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, Temperature from still is 20 DEG C, and pressure is 0.8Mpa, adds adsorbent and remove in the separation liquid obtained Miscellaneous, it is cooled to 0 DEG C, removes wax, filter to obtain product.
Embodiment 6:
The Health-care sesame oil that a kind of three-hypers crowd is suitable for, is made up of the raw material of following weight portion: black Semen Sesami 1800 parts, flaxseed 60 parts, 40 parts of Semen Pini, Radix Salviae Miltiorrhizae 20 parts, Radix Notoginseng 30 parts, west Radix Panacis Quinquefolii 20 parts, 20 parts of Semen Persicae, Fructus Rosae Normalis 10 parts, Herba Portulacae 20 parts, Radix Stellariae 10 parts, lotus 25 parts of leaf, Pollen Pini 20 parts.
The preparation method of the Health-care sesame oil that three-hypers crowd is suitable for, including following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 7 times 75% ethanol After aqueous solution soaking 3h, it is heated to 62 DEG C of backflow 2.5h, filters, obtain extract, reduce pressure, steam Evaporate to obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 40 mesh sieves, obtain mixing Thing;
3) by step 2) in mixture join in extraction kettle, add 2 times of volume of material Extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out subcritical extraction Taking, extracting pressure is 8.5MPa, extraction temperature 32 DEG C, cycling extraction 3 times, each 20min, CO2Flow velocity is 65L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, Temperature from still is 18 DEG C, and pressure is 0.9Mpa, adds adsorbent and remove in the separation liquid obtained Miscellaneous, it is cooled to 0 DEG C, removes wax, filter to obtain product.
Through the detection of Health-care sesame oil effect and clinical case are found, in embodiment 1 Health-care sesame oil effect is optimal.
Clinical case: select 250 ages the eater in 30-70 year, 53 years old mean age, Wherein subhealth state personnel 40, simple hyperlipemic patients 30 example, simple hypertension 30 example, Simple hyperglycemic patients 30 example, complicated hypertension hyperglycemic patients 30 example, complicated hypertension is high Blood fat patient 30 example, merges hyperglycemia hyperlipemic patients 30 example, hyperlipidemia and hypertension hyperglycemia All there is patient 30 example.The food of the edible oil culinary art of the edible embodiment of the present invention 1 preparation, sub-strong Kang personnel follow up a case by regular visits to 1 year make moderate progress without three-hypers symptom, health status;Other edible for patients 6 After Yue, weak on his pins, dizziness headache that patient causes because of three-hypers, the conjunctival congestion, uncomfortable in chest nervous of blushing All make moderate progress etc. symptom, after adhering to edible 1 year, suffer from the patients' blood of hypertension the most all Less than 140/90mmHg, effective percentage reaches more than 86.7%, suffers from the patient of hyperlipidemia, cholesterol With triglyceride substantially all in normal level, effective percentage is all more than 83.3%;Suffers from hyperglycemia Patient's fasting glucose be substantially at 3.9~6.1mmol/L, effective percentage more than 76.7%, with Track is investigated 1 year and is kept stable.
It should be noted that in this article, the relational terms of such as first and second or the like is only Only it is used for separating an entity or operation with another entity or operating space, and not necessarily Require or imply and there is the relation of any this reality or suitable between these entities or operation Sequence.And, term " includes ", " comprising " or its any other variant are intended to nonexcludability Comprise, so that include the process of a series of key element, method, article or equipment not only Including those key elements, but also include other key elements being not expressly set out, or also include The key element intrinsic for this process, method, article or equipment.There is no more restriction In the case of, statement " including ... " key element limited, it is not excluded that including described wanting Process, method, article or the equipment of element there is also other identical element.
Above example only in order to technical scheme to be described, is not intended to limit;Although With reference to previous embodiment, the present invention is described in detail, those of ordinary skill in the art It is understood that the technical scheme described in foregoing embodiments still can be modified by it, Or wherein portion of techniques feature is carried out equivalent;And these amendments or replacement, not The essence making appropriate technical solution departs from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (6)

1. the Health-care sesame oil that a three-hypers crowd is suitable for, it is characterised in that by following weight portion Raw material make: Semen Sesami Nigrum 1500-1800 part, flaxseed 60-80 part, Semen Pini 30-40 part, Radix Salviae Miltiorrhizae 20-30 part, Radix Notoginseng 20-30 part, Radix Panacis Quinquefolii 20-30 part, Semen Persicae 10-20 part, Fructus Rosae Normalis 10-20 part, Herba Portulacae 10-20 part, Radix Stellariae 10-20 part, Folium Nelumbinis 15-25 part, Pollen Pini 20-30 part.
2. the Health-care sesame oil that three-hypers crowd as claimed in claim 1 is suitable for, it is characterised in that It is made up of the raw material of following weight portion: Semen Sesami Nigrum 1650-1750 part, flaxseed 65-75 part, pine Sub-33-36 part, Radix Salviae Miltiorrhizae 20-24 part, Radix Notoginseng 25-29 part, Radix Panacis Quinquefolii 20-24 part, Semen Persicae 13-16 Part, Fructus Rosae Normalis 10-13 part, Herba Portulacae 15-18 part, Radix Stellariae 15-20 part, Folium Nelumbinis 19-23 part, Pollen Pini 25-30 part.
3. the Health-care sesame oil that three-hypers crowd as claimed in claim 2 is suitable for, it is characterised in that Be made up of the raw material of following weight portion: Semen Sesami Nigrum 1700 parts, flaxseed 70 parts, 35 parts of Semen Pini, Radix Salviae Miltiorrhizae 21 parts, Radix Notoginseng 26 parts, Radix Panacis Quinquefolii 20 parts, 15 parts of Semen Persicae, Fructus Rosae Normalis 12 parts, Dens Equi Herba Amaranthi tricoloris 16 parts, Radix Stellariae 17 parts, 22 parts of Folium Nelumbinis, Pollen Pini 28 parts.
4. the preparation of the Health-care sesame oil that the three-hypers crowd as described in claim 1-3 is arbitrary is suitable for Method, it is characterised in that include following methods:
1) weigh Pollen Pini, breaking cellular wall, be dried, add Pollen Pini quality 6-8 times 75% second After alcohol-water solution soaks 2-4h, it is heated to reflux 2-3h, filters, obtain extract, reduce pressure, distill Obtain concentrated solution, standby;
2) weigh respectively Semen Sesami Nigrum, flaxseed, Semen Pini, Radix Salviae Miltiorrhizae, Radix Notoginseng, Radix Panacis Quinquefolii, Semen Persicae, Fructus Rosae Normalis, Herba Portulacae, Radix Stellariae, Folium Nelumbinis, mix homogeneously, pulverize, cross 40-60 mesh sieve, obtain mixed Compound;
3) by step 2) in mixture join in extraction kettle, add 1.5-2.5 times of material body Long-pending extractant CO2, and add appropriate entrainer, and airtight, stirring mixing, carry out Asia and face Boundary extracts, and extracting pressure is 7-10MPa, extraction temperature 30-35 DEG C, cycling extraction 3-5 time, 15-25min, CO every time2Flow velocity is 60-80L/h, extraction, obtains extract;
4) by step 1) concentrated solution and step 3) transfer to separating still separates together with extract, In the separation liquid obtained, add adsorbent remove impurity, be cooled to 0 DEG C, remove wax, filter to obtain product.
5. the preparation method of the Health-care sesame oil that three-hypers crowd as claimed in claim 4 is suitable for, It is characterized in that, described step 1) in be heated to reflux temperature and be 60-65 DEG C.
6. the preparation method of the Health-care sesame oil that three-hypers crowd as claimed in claim 4 is suitable for, It is characterized in that, described step 4) in the temperature of separating still be 15-20 DEG C, pressure is 0.5-1Mpa.
CN201610251455.XA 2016-04-20 2016-04-20 Health-caring sesame oil suitable for people having hypertension, hyperglycemia and hyperlipidemia and preparation method of same Pending CN105907458A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106942396A (en) * 2017-04-27 2017-07-14 安徽华宇调味食品有限公司 A kind of processing method of Boxthorn Seed Oil/seedless roxburgh rose compound health sesame oil
CN108142581A (en) * 2017-12-13 2018-06-12 安徽省颍上县大河湾粮油食品有限公司 A kind of reducing blood lipid sesame oil
CN108450567A (en) * 2018-04-20 2018-08-28 管天球 A kind of preparation method of preventing hypertension tea oil
CN109666536A (en) * 2018-11-29 2019-04-23 河北中科汉禧生物科技有限公司 The extracting method of omega-fatty acid

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CN103636816A (en) * 2013-12-06 2014-03-19 太和县庄老汉杂粮有限公司 Sesame oil with functions of blood pressure lowering and health caring
CN104041602A (en) * 2014-05-12 2014-09-17 安徽省甘泉养蜂专业合作社 Hyperlipidemia hypertension prevention health care sesame oil and preparation method thereof
CN105267247A (en) * 2014-07-18 2016-01-27 中国科学院大连化学物理研究所 Application of bee pollen extract in preparation of blood pressure-lowering or liver-protecting medicines and health-care products

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Publication number Priority date Publication date Assignee Title
CN103636816A (en) * 2013-12-06 2014-03-19 太和县庄老汉杂粮有限公司 Sesame oil with functions of blood pressure lowering and health caring
CN104041602A (en) * 2014-05-12 2014-09-17 安徽省甘泉养蜂专业合作社 Hyperlipidemia hypertension prevention health care sesame oil and preparation method thereof
CN105267247A (en) * 2014-07-18 2016-01-27 中国科学院大连化学物理研究所 Application of bee pollen extract in preparation of blood pressure-lowering or liver-protecting medicines and health-care products

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106942396A (en) * 2017-04-27 2017-07-14 安徽华宇调味食品有限公司 A kind of processing method of Boxthorn Seed Oil/seedless roxburgh rose compound health sesame oil
CN108142581A (en) * 2017-12-13 2018-06-12 安徽省颍上县大河湾粮油食品有限公司 A kind of reducing blood lipid sesame oil
CN108450567A (en) * 2018-04-20 2018-08-28 管天球 A kind of preparation method of preventing hypertension tea oil
CN109666536A (en) * 2018-11-29 2019-04-23 河北中科汉禧生物科技有限公司 The extracting method of omega-fatty acid

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Application publication date: 20160831