CN102488320A - Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding - Google Patents
Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding Download PDFInfo
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- CN102488320A CN102488320A CN201110405187XA CN201110405187A CN102488320A CN 102488320 A CN102488320 A CN 102488320A CN 201110405187X A CN201110405187X A CN 201110405187XA CN 201110405187 A CN201110405187 A CN 201110405187A CN 102488320 A CN102488320 A CN 102488320A
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- essential oil
- paper mulberry
- mulberry fruit
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Abstract
The invention discloses application of paper mulberry fruit essential oil in a cigarette flavoring and material feeding. The paper mulberry fruit essential oil is extracted and prepared by the following steps of: cleaning paper mulberry fruit, mashing, and transferring pulp obtained after mashing to a flask; adding a solvent A to the flask, and distilling and leaching in a water bath; and cooling leaching liquid, filtering with gauze, extracting the filtrate at reduced pressure, and concentrating the filtrate to obtain the paper mulberry fruit essential oil. A solvent B is added to the paper mulberry fruit essential oil in a volume ratio of 1:1 to obtain diluted liquid, and the diluted liquid accounting for 0.05-0.5% the total weight of tobacco shreds is added to the tobacco shreds during the flavoring and material feeding process. The application of paper mulberry fruit essential oil in cigarette flavoring and material feeding disclosed by the invention has the advantages that: the smoking quality of the cigarette is improved, the smoking aroma quality is improved, cigarette aroma is enriched, and the original tobacco aroma is in harmony with the paper mulberry fruit essential oil; the paper mulberry fruit is from natural plant, is free of chemical pollution, and is simple in extraction method, convenient for operation and low in production cost; and the application of the paper mulberry fruit does not change the traditional cigarette processing process and has practical production significance and value.
Description
Technical field
The present invention relates to the application in the reinforced field of a kind of perfuming cigarette, especially relate to the application of a kind of Chinese holly tree fruit essential oil in perfuming cigarette is reinforced.
Background technology
Chinese holly tree (Broussonetia papyrifera (Linn.) Vent) has another name called Chu Shu, ancient slurry tree, deer subtree, tissue paper tree etc., and for the Moraceae Chinese holly belongs to perennial deciduous tree or shrub, dioecism is distributed in China and removes the north, northeast, the northern most of areas in northwest.The paper mulberry fruit is a collective fruits, both can eat raw, can make wine again, and the ripening fruits title " Paper mulberry Fruit " that is used as medicine is common Chinese medicine, has the kidney tonifying clearing liver, and the effect of the diuresis that makes eye bright is used for soreness and weakness of waist and knees, the consumptive disease hectic fever due to yin, and dizzy blurred vision, order is given birth to screen film, oedema turgor.Domestic research of setting fruit about Chinese holly is not found in the Application in Tobacco precedent mainly at aspects such as chemical constituents determination and nutritious and healthy drinks.
Along with growing interest and attention to smoking and health problem; Low burnt low harm cigarette has been represented the developing direction of Chinese cigarette; And the low harm of domestic all kinds of low Jiao cigarette product; Also have quality defect in various degree, as fragrance thinly owe plentiful, odor characteristic is not obvious, flue gas concentration is not enough, flue gas drying, sweet degree is not enough, comfort level is relatively poor etc.Characteristics such as natural perfume material has the complicacy of composition, numerous types, fragrance is abundant, lasting is lasting are sought effective flavor component from natural plants, become the inexorable trend of cigarette development.
Summary of the invention
The technical problem that the present invention will solve is to provide the application of a kind of Chinese holly tree fruit essential oil in perfuming cigarette is reinforced, with Chinese holly set the fruit essential oil be applied to tobacco flavoring reinforced in, can improve cigarette flavor matter, perfume quantity after the application; Enrich cigarette flavor; Make the cigarette smoke exquisiteness, pass through and send out, cover assorted gas, stimulate slightly and reduce; Good with flue gas harmony, pleasant impression is comfortable, it is sweet to promote the production of body fluid.
For solving the problems of the technologies described above, the application of a kind of Chinese holly tree of the present invention fruit essential oil in perfuming cigarette is reinforced comprises the steps:
1) extracts paper mulberry fruit essential oil
Chinese holly set blend after fruit is cleaned, the slurries after blending are transferred in the flask; In flask, add solvent orange 2 A, 50 ℃ of water-bath distillation lixiviates; Filtered through gauze is used in leaching liquor cooling back, the filtrate decompression extracting, will filtrate concentrates, and gets Chinese holly tree fruit essential oil;
2) add pipe tobacco
Be in Chinese holly tree fruit essential oil to add solvent B dilution at 1: 1 by volume, this dilution added in the pipe tobacco in the flavoring and casing process according to 0.05%～0.5% of pipe tobacco gross weight.
Further, the clean employing described in the step 1) is pure water.
Further, the described solvent orange 2 A of step 1) is an absolute ethyl alcohol.
Further, the ratio of slurries described in the step 1) and solvent orange 2 A is 1: 7.2g/mL.
Further, the condition of water-bath distillation described in the step 1) is: bath temperature is 90 ℃, and distillation time is 5h.
Further, the concentrated employing Rotary Evaporators in the step 1); The concentrate quality is 2.96 times of corresponding fruit quality.
Further, the solvent B step 2) is that ethanol, propane diols or ethanol and propane diols volume ratio are 1: 1 mixed solution.
The present invention has following beneficial effect:
1, application of the present invention can improve the sucking quality of cigarette, improves perfume quantity, fragrance matter, have promote the production of body fluid, sweet effect, pleasant impression is comfortable, covers assorted gas, stimulates slightly to reduce, and is better with this fragrant hamony of tobacco, and good effect is also played in flue gas drying sense etc.
2, paper mulberry fruit essential oil derives from natural plants, does not have the Pollution by Chemicals problem, its low preparation cost, and its application do not change existing cigarette processing technology, has actual production meaning and value.
The specific embodiment
Below in conjunction with specific embodiment the present invention is for further processing, but the present invention is not limited to following examples.
Embodiment 1:
The application of a kind of Chinese holly tree fruit essential oil in perfuming cigarette is reinforced comprises the steps:
1) extracts paper mulberry fruit essential oil
Clean with pure water gathering red ripe Chinese holly tree fruit, get the 50g fruit after leaving standstill, blend homogenate with juice extractor (Czech Braun, model 4184); Homogenate is transferred in the 500mL flask, adds the 360mL absolute ethyl alcohol, distill 5h in 90 ℃ the water-bath; Cooled leaching liquor is removed slag with filtered through gauze, decompress filter, filtrating is with Rotary Evaporators (Switzerland B ü CHI; R-210A) concentrate, get 148g salmon pink solution, be Chinese holly tree fruit essential oil;
2) add pipe tobacco
Configuration ethanol and propane diols volume ratio are 1: 1 mixed solution, are by volume in Chinese holly tree fruit essential oil to add this mixed solution at 1: 1 to dilute, and according to 0.05% of pipe tobacco gross weight this dilution are added in the pipe tobacco.
Embodiment 2:
Repeat embodiment 1, its difference only is in Chinese holly tree fruit essential oil, to add ethanol in 1: 1 by volume, obtains dilute solution, according to 0.25% of pipe tobacco gross weight this dilute solution is added in the pipe tobacco.
Embodiment 3:
Repeat embodiment 1, its difference only is in Chinese holly tree fruit essential oil, to add propane diols in 1: 1 by volume, obtains dilute solution, according to 0.5% of pipe tobacco gross weight this dilute solution is added in the pipe tobacco.
The applicant uses middle-grade cigarette as blank, Chinese holly is set the fruit essential oil in the flavoring and casing process, put on middle-grade cigarette shreds, and Chinese holly tree fruit essential oil consumption is the 0.05%-0.5% of pipe tobacco weight; The cigarette and the blank cigarette that apply Chinese holly tree fruit essential oil comment the judging panel of qualification to smoke panel test through having tobacco business state, and smoking result is seen table 1.
Table 1 adds Chinese holly tree fruit essential oil and blank cigarette contrast smoking result
Can know that by table 1 when the mass fraction that accounts for pipe tobacco when the Chinese holly tree fruit essential oil that adds was 0.25%, various effects were best, and no matter aspect fragrance, pleasant impression, assorted gas, excitant, harmony, all be better than the control group that does not add Chinese holly tree fruit essential oil.
Obviously, the above embodiment of the present invention only be for clearly the present invention is described and is done for example, and be not to be qualification to embodiment of the present invention.For the those of ordinary skill in affiliated field, on the basis of above-mentioned explanation, can also make other multi-form variation or change.Here can't give exhaustive to all embodiments.Everyly belong to the row that conspicuous variation that technical scheme of the present invention extends out or change still are in protection scope of the present invention.
Claims (7)
1. the application of paper mulberry fruit essential oil in perfuming cigarette is reinforced is characterized in that, comprises following concrete steps:
1) extracts paper mulberry fruit essential oil
Chinese holly set blend after fruit is cleaned, the slurries after blending are transferred in the flask; In flask, add solvent orange 2 A, 50 ℃ of water-bath distillation lixiviates; Filtered through gauze is used in leaching liquor cooling back, the filtrate decompression extracting, will filtrate concentrates, and gets Chinese holly tree fruit essential oil;
2) add pipe tobacco
Be in Chinese holly tree fruit essential oil to add solvent B dilution at 1: 1 by volume, this dilution added in the pipe tobacco in the flavoring and casing process according to 0.05%～0.5% of pipe tobacco gross weight.
2. application according to claim 1 is characterized in that, the clean employing described in the step 1) be pure water.
3. application according to claim 1 is characterized in that, the described solvent orange 2 A of step 1) is an absolute ethyl alcohol.
4. application according to claim 1 is characterized in that, the ratio of slurries described in the step 1) and solvent orange 2 A is 1: 7.2g/mL.
5. application according to claim 1 is characterized in that, the condition of water-bath distillation described in the step 1) is: bath temperature is 90 ℃, and distillation time is 5h.
6. application according to claim 1 is characterized in that, the concentrated employing Rotary Evaporators in the step 1); The concentrate quality is 2.96 times of corresponding fruit quality.
7. application according to claim 1 is characterized in that step 2) described in solvent B be that ethanol, propane diols or ethanol and propane diols volume ratio are 1: 1 mixed solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110405187.XA CN102488320B (en) | 2011-12-08 | 2011-12-08 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110405187.XA CN102488320B (en) | 2011-12-08 | 2011-12-08 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
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| Publication Number | Publication Date |
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| CN102488320A true CN102488320A (en) | 2012-06-13 |
| CN102488320B CN102488320B (en) | 2015-04-15 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201110405187.XA Active CN102488320B (en) | 2011-12-08 | 2011-12-08 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104862079A (en) * | 2015-05-27 | 2015-08-26 | 天水师范学院 | Method for extracting essential oil from trigonella foenum-graecum leaves |
| CN112042996A (en) * | 2020-10-15 | 2020-12-08 | 江苏中烟工业有限责任公司 | Application of artemisia selengensis essential oil in cigarette flavoring and casing |
| CN112107023A (en) * | 2020-09-17 | 2020-12-22 | 江苏中烟工业有限责任公司 | Application of ampelopsis grossedentata leaf extract in cigarette flavoring |
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| CN1605618A (en) * | 2004-09-07 | 2005-04-13 | 中国科学院武汉植物园 | Preparation and purification method for plant linoleic acid |
| CN1973701A (en) * | 2006-12-27 | 2007-06-06 | 广东中烟工业公司 | Additive for lowering the stimulation of cigarette smoke |
| CN1990001A (en) * | 2005-12-29 | 2007-07-04 | 贵州三农楮桃产业开发有限公司 | Process for extracting total saponin from papermulberry fruit |
| CN102133334A (en) * | 2011-03-08 | 2011-07-27 | 山东大学威海分校 | Preparation method of compound fructus broussonetiae preparation and application thereof |
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| CN1605618A (en) * | 2004-09-07 | 2005-04-13 | 中国科学院武汉植物园 | Preparation and purification method for plant linoleic acid |
| CN1990001A (en) * | 2005-12-29 | 2007-07-04 | 贵州三农楮桃产业开发有限公司 | Process for extracting total saponin from papermulberry fruit |
| CN1973701A (en) * | 2006-12-27 | 2007-06-06 | 广东中烟工业公司 | Additive for lowering the stimulation of cigarette smoke |
| CN102133334A (en) * | 2011-03-08 | 2011-07-27 | 山东大学威海分校 | Preparation method of compound fructus broussonetiae preparation and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104862079A (en) * | 2015-05-27 | 2015-08-26 | 天水师范学院 | Method for extracting essential oil from trigonella foenum-graecum leaves |
| CN104862079B (en) * | 2015-05-27 | 2017-10-27 | 天水师范学院 | A kind of method for extracting faenum graecum blade essential oil |
| CN112107023A (en) * | 2020-09-17 | 2020-12-22 | 江苏中烟工业有限责任公司 | Application of ampelopsis grossedentata leaf extract in cigarette flavoring |
| CN112042996A (en) * | 2020-10-15 | 2020-12-08 | 江苏中烟工业有限责任公司 | Application of artemisia selengensis essential oil in cigarette flavoring and casing |
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| Publication number | Publication date |
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| CN102488320B (en) | 2015-04-15 |
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