CN112042996A - Application of artemisia selengensis essential oil in cigarette flavoring and casing - Google Patents
Application of artemisia selengensis essential oil in cigarette flavoring and casing Download PDFInfo
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- CN112042996A CN112042996A CN202011101660.0A CN202011101660A CN112042996A CN 112042996 A CN112042996 A CN 112042996A CN 202011101660 A CN202011101660 A CN 202011101660A CN 112042996 A CN112042996 A CN 112042996A
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- essential oil
- artemisia selengensis
- flavoring
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the technical field of cigarette flavoring and feeding, and particularly discloses application of artemisia selengensis essential oil in cigarette flavoring and feeding. The artemisia selengensis essential oil is extracted according to the following steps: cleaning artemisia selengensis, airing, removing 20-30% of water, and crushing to obtain slurry; adding a solvent A into the slurry, and distilling in a water bath to obtain a leaching solution; cooling the leaching solution, filtering with gauze to remove residue, extracting under reduced pressure, and concentrating the filtrate to obtain Artemisia selengensis essential oil. Adding a solvent B into the artemisia selengensis essential oil according to the volume ratio of 1:1 to obtain a diluent, and adding the diluent into the cut tobacco in the flavoring and feeding process according to 0.05-0.2% of the total weight of the cut tobacco. The invention can improve the aroma quality of the cigarette, enrich the aroma, be compatible with the original aroma of the tobacco, soften and refine the smoke and reduce the stimulation; the artemisia selengensis essential oil is derived from natural plants and has good safety; the extraction is simple and the cost is low; and the application does not change the existing cigarette processing technology, and has practical production significance and value.
Description
Technical Field
The invention belongs to the technical field of cigarette flavoring and feeding, and particularly relates to application of artemisia selengensis essential oil in cigarette flavoring and feeding.
Background
With the increasing attention and importance to the health of cigarette consumers, low-tar cigarette products become the development direction of Chinese cigarettes, and various domestic low-tar and low-harm cigarette products can generate quality defects of different degrees, such as thin and less full aroma, low aroma concentration, dry smoke, poor comfort and the like, while the tar content is reduced. The natural spice has the characteristics of complex composition, various types, rich fragrance, lasting fragrance and the like, and the effective fragrance components are searched from natural plants, which becomes a necessary trend for the development of cigarettes.
Artemisia selengensis is a plant of Artemisia of Compositae, also called Artemisia betel, Artemisia angustifolia, Artemisia sphaerocephala and the like, is a perennial herbaceous plant, and is distributed in original Asia, northeast China, North China and middle south China on barren beach and barren land. The artemisia selengensis not only has high edible value, but also has high nutritional value, contains a plurality of vitamins and a plurality of mineral elements such as calcium, phosphorus, iron, zinc and the like, has cool property, and has the effects of clearing heat and removing toxicity, cooling and refreshing, suppressing liver fire, dispelling wind-damp, diminishing inflammation, relieving cough and the like. The artemisia selengensis contains various fragrant substances (such as flavonoids, caryophyllene, borneol and the like), so that the artemisia selengensis has unique faint scent flavor. Domestic research on artemisia selengensis mainly applied to aspects of food health care, medicinal value and the like, and no application precedent in tobacco is found.
Disclosure of Invention
In order to solve the problems, the invention provides the application of the artemisia selengensis essential oil in the cigarette flavoring and casing, the artemisia selengensis essential oil is applied in the tobacco flavoring and casing, after the application, the aroma note of the cigarette can be enriched, the aroma amount can be improved, the smoke of the cigarette is fine and smooth and can be diffused, the miscellaneous gas can be covered, the irritation can be reduced, the harmony with the cigarette aroma is good, the aftertaste is comfortable, and the body fluid is sweet and moist.
In order to achieve the purpose, the invention adopts the following specific technical scheme:
the application of artemisia selengensis essential oil in cigarette flavoring and casing comprises the following steps:
s1, extracting artemisia selengensis essential oil
Cleaning artemisia selengensis, airing, removing 20-30% of water, and crushing to obtain slurry; adding a solvent A into the slurry, and distilling and extracting in a water bath to obtain a leaching solution; filtering the leaching solution with gauze to remove residues, vacuum filtering, and concentrating the filtrate to obtain Artemisia selengensis essential oil;
s2, adding tobacco shreds
Adding a solvent B into the artemisia selengensis essential oil according to the volume ratio of 1:1 to obtain a diluent, and adding the diluent into tobacco shreds according to 0.05-0.2% of the total weight of the tobacco shreds (wherein the solvent A and the solvent B are solvents which can dissolve the artemisia selengensis essential oil, have good volatility and low toxicity, such as ethanol, ethyl acetate and the like).
Preferably, in step S1, the artemisia selengensis is washed with purified water.
Preferably, in step S1, the solvent a is absolute ethanol.
Preferably, in step S1, the mass-to-volume ratio of the slurry to the solvent a is 1 (6-10).
Preferably, in step S1, the conditions of the water bath distillation are as follows: the water bath temperature is 85-95 ℃, and the distillation time is 5.5-7.5 h.
Preferably, in step S1, the filtrate is concentrated using a rotary evaporator.
Preferably, in step S2, the solvent B is ethanol, propylene glycol or a 1:1 ethanol-propylene glycol mixed solution.
Preferably, in step S1, the solvent a is added to the slurry and then the ultrasound is turned on, the solvent a is added in at least two batches, and the ultrasound extraction is performed for 1-3 hours. The ultrasonic extraction is combined with batch feeding, so that the mixing effect of the solvent A and the slurry can be improved, and various aroma substances in the slurry can be fully released.
Preferably, in step S2, the method for adding the diluent into the cut tobacco in the flavoring process is as follows: and putting the cut tobacco into a roller, atomizing the diluent through a nozzle, spraying the atomized diluent onto the surface of the cut tobacco, and controlling negative pressure in the roller. Increasing the contact area of the diluent and the cut tobacco by atomizing the diluent; the pressure in the roller is controlled to be negative pressure, so that the diluent can be quickly permeated into the cut tobacco, and the volatilization loss is avoided; the tobacco shreds flow by the rotation of the roller, so that the dispersion of the diluent is accelerated, and meanwhile, the tobacco shreds keep certain looseness, and the agglomeration in a negative pressure environment is avoided; therefore, the method for adding the artemisia selengensis essential oil into the tobacco shreds has the advantages of fast penetration and good uniformity.
The invention has the following beneficial effects:
1. the reagent used in the invention has low toxicity and good safety, and the fragrance of the extract cannot be destroyed, and various fragrant substances of the artemisia selengensis can be effectively extracted according to the method of the invention to obtain the artemisia selengensis essential oil applicable to tobacco; the artemisia selengensis essential oil disclosed by the invention is added into tobacco shreds, so that the smoking quality of cigarettes can be effectively improved, the fragrance of the cigarettes is enriched, the fragrance amount is improved, the smoke of the cigarettes is fine and smooth and permeable, miscellaneous gases are covered, the irritation is reduced, the harmony with the fragrance of the cigarettes is good, the aftertaste is comfortable, and the tobacco shreds are sweet and moist.
2. The artemisia selengensis essential oil is derived from natural plants, so that the problem of chemical pollution is solved, and the safety is good; the preparation cost is low, the extraction method is simple and feasible, and the method is suitable for industrial large-scale mass production; and the application does not change the existing cigarette processing technology, and has practical production significance and value.
Detailed Description
In order to more clearly and completely describe the technical scheme of the invention, the technical scheme of the invention is further described in detail by combining the specific examples, and it should be understood that the specific examples described herein are only used for explaining the invention, are not used for limiting the invention, and can be variously changed within the scope defined by the claims of the invention.
Example 1
The application of artemisia selengensis essential oil in cigarette flavoring and casing comprises the following steps:
s1, extracting artemisia selengensis essential oil
Cleaning artemisia selengensis with purified water, airing, removing 20-30% of water, and crushing and homogenizing by a juicer (Czech Braun, model 4184) to obtain slurry; transferring the serous fluid to a 500mL flask, adding absolute ethyl alcohol into the flask according to the mass-volume ratio of the serous fluid to the absolute ethyl alcohol of 1:6.9, and distilling and extracting for 6 hours in a water bath kettle at 90 ℃ to obtain a leaching solution; filtering the leaching solution with gauze, removing residue, vacuum filtering, and concentrating the filtrate with rotary evaporator (Switzerland Buchi, R-210A) to obtain Artemisia selengensis essential oil;
s2, adding tobacco shreds
Preparing a mixed solution of ethanol and propylene glycol in a volume ratio of 1:1, adding the prepared ethanol-propylene glycol mixed solution into artemisia selengensis essential oil in a volume ratio of 1:1 to obtain a diluent, and uniformly spraying the diluent on the cut tobacco in the flavoring and feeding processes according to 0.05%, 0.1% and 0.2% of the total weight of the cut tobacco respectively.
Example 2
Example 1 was repeated with the only difference that: in step S2, ethanol is added to artemisia selengensis essential oil according to a volume ratio of 1:1 to obtain a diluted solution, and the diluted solution is uniformly sprayed on the cut tobacco in the flavoring and feeding processes according to 0.05%, 0.1% and 0.2% of the total weight of the cut tobacco respectively.
Example 3
Example 1 was repeated with the only difference that: in step S2, propylene glycol is added to artemisia selengensis essential oil according to a volume ratio of 1:1 to obtain a diluted solution, and the diluted solution is uniformly sprayed on the cut tobacco in the flavoring and feeding processes according to 0.05%, 0.1% and 0.2% of the total weight of the cut tobacco respectively.
And (3) performance testing: taking a medium-grade cigarette as a blank control, applying the artemisia selengensis essential oil to medium-grade cigarette tobacco shreds in the perfuming and feeding processes according to the embodiments 1-3, wherein the using amount of the artemisia selengensis essential oil is 0.05-0.2% of the weight of the tobacco shreds; the cigarettes and blank cigarettes added with the artemisia selengensis essential oil are subjected to smoking evaluation by a judge with national evaluation qualification in the tobacco industry, the smoking evaluation method and the standard reference GB5606.4-2005 (part 4 of cigarettes: sensory technical requirements), and the smoking evaluation results are shown in Table 1.
Table 1 cigarette added with artemisia selengensis essential oil and blank cigarette comparative smoking evaluation results
As can be seen from table 1, the smoking quality of the cigarettes added with artemisia selengensis essential oil is obviously better than that of the control group cigarettes without artemisia selengensis essential oil; compared among the examples 1-3, when the usage amount of the artemisia selengensis essential oil in tobacco shreds is not changed, only the diluent solvents (ethanol, propylene glycol and ethanol-propylene glycol mixed solution) of the artemisia selengensis essential oil are changed, the smoking result is consistent, and the three diluent solvents have no obvious difference; in each of examples 1 to 3, when the added artemisia selengensis essential oil accounts for 0.1% of the mass of the cut tobacco, the effect is the best, and the fragrance, aftertaste, miscellaneous odor, irritation and harmony are better than those of a control group without the artemisia selengensis essential oil.
Example 4
Example 1 was repeated with the only difference that: in the embodiment, a water bath distillation pretreatment step is added, namely in step S1, before adding absolute ethyl alcohol into the slurry, the ultrasonic treatment is started, the absolute ethyl alcohol is divided into two batches according to the mass ratio of 1:1, the two batches are added into the slurry at an interval of 30min, the ultrasonic treatment is carried out for 1.5h, and then the water bath distillation and the subsequent steps are carried out. The pretreatment step can fully release various aroma substances in the pulp, and reduce the consumption of the raw material of the artemisia selengensis.
Example 5
Example 1 was repeated with the only difference that: the embodiment provides an optimized method for adding diluent into tobacco shreds, which is short in time consumption and good in artemisia selengensis essential oil permeability, and comprises the following specific processes: moisture regaining treatment is carried out on the tobacco shreds, and the moisture is controlled to be 10-15%; then the cut tobacco is placed in a rotary roller, the diluent is atomized by a nozzle and then sprayed to the surface of the cut tobacco, and negative pressure is controlled in the roller.
It should be understood that the above-mentioned embodiments of the present invention are only examples for clearly illustrating the present invention, and are not intended to limit the embodiments of the present invention, and it will be obvious to those skilled in the art that other variations or modifications may be made on the basis of the above description, and all embodiments may not be exhaustive, and all obvious variations or modifications may be included within the scope of the present invention.
Claims (9)
1. The application of artemisia selengensis essential oil in cigarette flavoring and casing is characterized in that: the method comprises the following steps:
s1, extracting artemisia selengensis essential oil
Cleaning artemisia selengensis, airing, removing 20-30% of water, and crushing to obtain slurry; adding a solvent A into the slurry, and distilling and extracting in a water bath to obtain a leaching solution; filtering the leaching solution with gauze to remove residues, vacuum filtering, and concentrating the filtrate to obtain Artemisia selengensis essential oil;
s2, adding tobacco shreds
Adding a solvent B into the artemisia selengensis essential oil according to the volume ratio of 1:1 to obtain a diluent, and adding the diluent into the cut tobacco in the flavoring and feeding process according to 0.05-0.2% of the total weight of the cut tobacco.
2. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S1, Artemisia selengensis is washed with purified water.
3. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S1, the solvent a is absolute ethanol.
4. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S1, the mass-to-volume ratio of the slurry to the solvent A is 1 (6-10).
5. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S1, the conditions of the water bath distillation are as follows: the water bath temperature is 85-95 ℃, and the distillation time is 5.5-7.5 h.
6. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S1, the filtrate was concentrated using a rotary evaporator.
7. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S2, the solvent B is ethanol, propylene glycol or a mixed solution of ethanol and propylene glycol in a volume ratio of 1: 1.
8. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S1, before adding the solvent A into the slurry, the ultrasonic extraction is started, the solvent A is added into the slurry in at least two batches, and the ultrasonic extraction is carried out for 1-3 h.
9. The use of artemisia selengensis essential oil in cigarette flavoring and casing according to claim 1, wherein the essential oil comprises the following components in percentage by weight: in step S2, the method for adding the diluent into the cut tobacco in the flavoring and charging process is as follows: and putting the cut tobacco into a roller, atomizing the diluent through a nozzle, spraying the atomized diluent onto the surface of the cut tobacco, and controlling negative pressure in the roller.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011101660.0A CN112042996A (en) | 2020-10-15 | 2020-10-15 | Application of artemisia selengensis essential oil in cigarette flavoring and casing |
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| CN202011101660.0A CN112042996A (en) | 2020-10-15 | 2020-10-15 | Application of artemisia selengensis essential oil in cigarette flavoring and casing |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488320A (en) * | 2011-12-08 | 2012-06-13 | 江苏中烟工业有限责任公司 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
| CN108546594A (en) * | 2018-04-12 | 2018-09-18 | 江西中烟工业有限责任公司 | A kind of preparation method and application of mud wormwood artemisia tobacco aromaticss |
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2020
- 2020-10-15 CN CN202011101660.0A patent/CN112042996A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488320A (en) * | 2011-12-08 | 2012-06-13 | 江苏中烟工业有限责任公司 | Application of paper mulberry fruit essential oil in cigarette flavoring and material feeding |
| CN108546594A (en) * | 2018-04-12 | 2018-09-18 | 江西中烟工业有限责任公司 | A kind of preparation method and application of mud wormwood artemisia tobacco aromaticss |
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Address after: No. 406-3, Zhongshan North Road, Nanjing, Jiangsu 210019 Applicant after: CHINA TOBACCO JIANGSU INDUSTRIAL Co.,Ltd. Address before: Bell tower of technical center, No.29 Xinglong Street, Jianye District, Nanjing City, Jiangsu Province Applicant before: CHINA TOBACCO JIANGSU INDUSTRIAL Co.,Ltd. |
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Application publication date: 20201208 |