CN111329098B - Fumigating and flavoring method and application thereof in tobacco - Google Patents
Fumigating and flavoring method and application thereof in tobacco Download PDFInfo
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- CN111329098B CN111329098B CN202010194229.9A CN202010194229A CN111329098B CN 111329098 B CN111329098 B CN 111329098B CN 202010194229 A CN202010194229 A CN 202010194229A CN 111329098 B CN111329098 B CN 111329098B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring
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- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a fumigating and flavoring method, which comprises the steps of taking natural spice plants and tobacco leaves as main materials, adding functional auxiliary materials, fumigating for 5-48 hours in a closed container at 50-150 ℃, cooling at room temperature, and standing for 24 hours to obtain the fumigated natural spice plants and the fumigated tobacco leaves. The invention also discloses the application of the fumigated tobacco leaves or/and fumigated natural spice plants obtained by the fumigation and flavoring method in cigarettes.
Description
Technical Field
The invention belongs to the technical field of cigarette flavoring, and particularly relates to a fumigation flavoring method and application thereof in improving the smoking quality of cigarettes.
Background
People pay more and more attention to natural substances while developing and changing society and science and technology, and the valuable resource of nature is applied to the cigarette production process to improve the smoking quality of cigarettes, so that the method is a hot spot in the research and development of the tobacco industry at present. Therefore, the technology and the product which are low in cost, simple and convenient to operate in the preparation method, natural, non-toxic and harmless, can effectively enrich the cigarette fragrance and improve the comfort, soft feeling and fineness of smoke are found, and are one of the key problems to be solved in the tobacco industry at present. The low coking is the inevitable trend of the development of the tobacco industry, the smoking taste of the cigarettes is reduced due to the low coking, and the insufficient aroma gradually becomes the prominent problem of the tobacco development. How to overcome the key technology influencing the aroma quality and the aroma quantity of cigarettes becomes the core for improving the competitiveness of cigarette production.
In the prior art, the spice is often directly added into the cigarette, and although the direct adding method is simple in operation, the smoking quality of the tobacco is not obviously improved. The invention adopts the fumigation flavoring method for the first time to improve the smoking quality of the cigarettes.
Disclosure of Invention
The invention aims to provide a fumigation and fragrance blending method and application thereof in improving the smoking quality of cigarettes aiming at the defects of the prior art, so as to enrich the cigarette fragrance of the cigarettes, increase the cigarette fragrance amount, improve the softness, fineness and comfort of the smoke, and enable the smoke to have layering and sweet aftertaste.
The purpose of the invention is realized by the following technical scheme.
All percentages used in the present invention are mass percentages unless otherwise indicated.
The invention discloses a fumigating and flavoring method, which comprises the steps of taking natural spice plants and tobacco leaves as main materials, adding functional auxiliary materials, fumigating for 5-48 h in a closed container at 50-150 ℃, cooling at room temperature, and standing for about 24h to obtain the fumigated natural spice plants and the fumigated tobacco leaves.
Preferably, the weight parts of the raw materials are as follows: 20-50 parts of tobacco leaves, 10-50 parts of natural spice plants and 1-5 parts of functional auxiliary materials.
Preferably, the functional auxiliary materials comprise organic acid salt, amino acid and natural moisturizing factor; the weight parts of the components are as follows: 1-20 parts of natural moisturizing factors, 10-50 parts of organic acid salts and 1-30 parts of amino acids;
preferably, the preparation method of the functional auxiliary material comprises the following steps: dissolving organic acid salt at 40-60 ℃, adding propylene glycol in a mass ratio of 1:1, adding natural moisturizing factors and amino acid, and mixing at 50-70 ℃ for 0.5h to obtain the functional auxiliary material.
Preferably, the organic acid salt is one or more of sodium potassium citrate, sodium potassium tartrate, acetate, lactate or fumarate; the amino acid is one or more of aspartic acid, threonine, glutamic acid, glycine, alanine, valine, isoleucine, proline, phenylalanine, histidine or serine; the natural moisturizing factor is one or more of hyaluronic acid, aloe gel or luffa water.
Preferably, the natural spice plant is one or more of lavender, dendrobium, ganoderma lucidum, Yunnan black tea, Pu' er tea, yerba mate, kudzu root, liquorice, frangipani, hops, honeysuckle, sterculia lychnophora, dandelion, rose, iris tectorum, mimosa, asian mint, peppermint, shiitake, helichrysum, jasmine, citronella, labdanum, vanilla, valerian, vanilla, rosemary, spearmint, raspberry, geranium, ganoderma, cinnamon, tree moss, ganoderma, pine cone, coffee, maca, fenugreek, chicory, malt, ophiopogon root, termitomyces albuminosus, violet leaf, ylang-ylang.
The second aspect of the invention discloses the use of the fumigated tobacco leaves or/and fumigated natural spice plants obtained by the fumigation method in cigarettes; the use of the fumigated tobacco leaves alone, the fumigated natural spice plants, or the fumigated tobacco leaves and the fumigated natural spice plants in cigarettes simultaneously.
Preferably, the fumigated natural spice plants are subjected to spice extraction to obtain spice extracting solution, and the spice extracting solution is used in cigarettes; the pure spice in the common spice extracting solution is 1-10 wt%, the spice extracting solution is sprayed on tobacco shreds, and the pure spice generally accounts for 0.01-1% of the weight of the common tobacco shreds; more preferably, the pure spice accounts for 0.08-0.5% of the weight of the common cut tobacco.
Compared with the prior art, the invention has the following advantages:
1. after the tobacco leaves are fumigated and flavored, lipid cigarette aroma substances such as ethyl hexanoate, diethyl succinate, ethyl maltol and the like which are not contained in the tobacco leaves appear; compared with the common cigarette, the cigarette has rich fragrance, the cigarette fragrance amount is increased, the fragrance is more fragrant, the smoke is soft, the fineness is improved, the cigarette fragrance is elegant, and the aftertaste is clean and comfortable; the suction comfort is improved significantly.
2. The extract of the natural spice plants after fumigation is used in cigarettes, so that the cigarette fragrance of the cigarettes is enriched, the cigarette fragrance amount is increased, the softness, the fineness and the comfort of the smoke are improved, the smoke has the effects of layering and sweet aftertaste, the harmony with cigarette products and the mellow feeling of the whole fragrance can be obviously increased, a good rich fragrance effect is provided for the cigarettes, and the effects of improving or enriching the fragrance of the cigarettes and increasing the fullness and the fineness of the cigarette fragrance are achieved.
3. The fumigated natural spice plant and the tobacco leaves fumigated by different spices are simultaneously used in cigarettes, so that the tobacco fragrance of different cigarettes can be enriched.
4. The fumigating and blending method of the invention uses natural perfume plants and tobacco leaves as raw materials, and is supplemented with organic acid salt, amino acid and natural moisturizing factor functional auxiliary material formula to carry out common closed fumigating and blending, so that natural fragrance components can be preserved to the maximum extent, and simultaneously, mutual fusion and permeation of fragrance are achieved through thermal action. According to the fumigation flavor blending condition, the Maillard reaction occurs under the synergistic effect of the functional auxiliary material formula, rich aroma components are obtained to the maximum extent through fumigation flavor blending, the cigarette flavor can be remarkably enriched, the aroma of the cigarette is improved, the smoke is coordinated, the sweet and moist feeling is increased, and the cigarette has a good application effect; compared with the method of directly adding corresponding perfume into common tobacco shreds, the method has obvious fragrance, aroma and sweet feeling.
5. The fumigation flavoring method uses common raw materials, has the advantages of sufficient raw material sources, low cost, no toxicity and harm, simple preparation process flow and convenient operation. The fumigated tobacco leaves or the fumigated natural spice plant extract is used in cigarettes without changing the existing cigarette production process.
Detailed Description
The present invention will be described in further detail with reference to the following specific examples, which are not intended to limit the scope of the present invention.
Example 1
Taking 3 parts of aloe gel, 5 parts of potassium sodium citrate and 3 parts of aspartic acid, dissolving the potassium sodium citrate with ultrapure water, heating and stirring uniformly at 50 ℃, adding propylene glycol according to the mass ratio of 1:1, then sequentially adding the aloe gel and the aspartic acid, and continuously heating and stirring for 0.5h at 50 ℃ to obtain the required functional auxiliary material.
50 parts of tobacco leaves, 20 parts of Pu' er tea and 3 parts of functional auxiliary materials are fumigated in a closed container at 120 ℃ for 10 hours, cooled at room temperature and then placed for 24 hours, and then taken out for later use.
Performing microwave-assisted steam distillation on the fumigated Pu 'er tea, performing microwave-assisted steam distillation by taking a mixed solution of ethanol and water (the volume ratio is 1:1) as an extraction solvent according to the mass ratio of the raw materials to the solvent of 1:10, performing microwave power of 550W, radiating for 15min, and cooling at room temperature to obtain the fumigated Pu' er tea extract.
Example 2
The fumigated tobacco leaves in the embodiment 1 are added into a tobacco shred formula according to the mass ratio of 2%, and then are rolled into cigarettes through the processes of shredding, perfuming and wrapping according to the conventional cigarette process, wherein the cigarettes are respectively named as No. 1 cigarettes. On the same production line, a control cigarette 1 is rolled according to the same cigarette process, and the control cigarette 1 is a cigarette added with non-fumigated tobacco leaves. And then regulating the moisture content of the cigarette sample to 12% according to the national standard GB/T16447-1996 atmospheric environment for regulating and testing tobacco and tobacco products, and performing sensory cigarette smoking evaluation by a smoking evaluation expert group according to the regulation of GB 5606.4-1996 cigarette sensory technical requirements. The results of the smoke panel are shown in Table 1.
0.2g of the fumigated Pu 'er tea extract prepared in the example 1 is uniformly mixed with feed liquid containing conventional spices and the fumigated Pu' er tea extract respectively, and then the mixture is uniformly sprayed on 100g of tobacco leaves respectively by using a high-pressure nozzle, wherein the spraying process is carried out in the tobacco shred feeding process, and then the tobacco shreds are rolled into cigarettes by the processes of shredding, perfuming and rolling according to the conventional cigarette process, and the cigarettes are respectively named as No. a cigarettes. On the same production line, rolling a control cigarette according to the same cigarette process, wherein the control cigarette a is a cigarette added with the same proportion of the Pu' er tea extract which is not fumigated. And then regulating the moisture content of the cigarette sample to 12% according to the national standard GB/T16447-1996 atmospheric environment for regulating and testing tobacco and tobacco products, and performing sensory cigarette smoking evaluation by a smoking evaluation expert group according to the regulation of GB 5606.4-1996 cigarette sensory technical requirements. The results of the smoke panel are shown in Table 1.
The fumigated tobacco leaves and the fumigated Pu 'er tea extracting solution prepared in the embodiment 1 are simultaneously applied to cigarettes, and the fumigated tobacco leaves and the fumigated Pu' er tea extracting solution 0.2g in mass ratio are added into 100g of tobacco shreds; then adding 0.2g of common tobacco leaves and Pu' er tea extract into 100g of tobacco shreds, and then rolling into cigarettes according to the conventional cigarette process through the processes of shredding, perfuming and wrapping, wherein the cigarettes are named as No. A cigarettes. On the same production line, a control cigarette is rolled according to the same cigarette process, and the control cigarette A is a cigarette added with the same proportion of the non-fumigated Pu' er tea extract and the same proportion of the functional auxiliary materials. And then regulating the moisture content of the cigarette sample to 12% according to the national standard GB/T16447-1996 atmospheric environment for regulating and testing tobacco and tobacco products, and performing sensory cigarette smoking evaluation by a smoking evaluation expert group according to the regulation of GB 5606.4-1996 cigarette sensory technical requirements. The results of the smoke panel are shown in Table 1.
Example 3
Taking 7 parts of hyaluronic acid, 10 parts of potassium lactate and 8 parts of proline, dissolving the potassium lactate with ultrapure water, heating and stirring uniformly at 60 ℃, adding propylene glycol according to the mass ratio of 1:1, then sequentially adding the hyaluronic acid and the proline, and continuously heating and stirring for 0.5h at 70 ℃ to obtain the required functional auxiliary material.
Fumigating 40 parts of tobacco leaves, 10 parts of peppermint, 15 parts of coffee and 2 parts of functional auxiliary materials in a self-made closed container at the temperature of 60 ℃ for 48 hours, cooling at room temperature, standing for 24 hours and taking out for later use.
Performing microwave-assisted steam distillation on the fumigated peppermint and coffee, performing microwave-assisted steam distillation on a mixed solution of ethanol and water (the volume ratio is 1:1) serving as an extraction solvent according to the mass ratio of the raw materials to the solvent of 1:30, performing microwave power of 650W, performing radiation for 30min, and cooling at room temperature to obtain the fumigated peppermint + coffee extract.
Example 4
The fumigated tobacco leaves obtained in the embodiment 3 are added into tobacco shreds in a mass ratio of 5%, and then the tobacco shreds are rolled into cigarettes through the processes of shred preparation, flavoring and wrapping according to the conventional cigarette process, wherein the cigarettes are respectively named as No. 2 cigarettes. On the same production line, a control cigarette 2 is rolled according to the same cigarette process, and the control cigarette 2 is a cigarette added with the non-fumigated tobacco leaves in the same proportion. And then regulating the moisture content of the cigarette sample to 12% according to the national standard GB/T16447-1996 atmospheric environment for regulating and testing tobacco and tobacco products, and performing sensory cigarette smoking evaluation by a smoking evaluation expert group according to the regulation of GB 5606.4-1996 cigarette sensory technical requirements. The results of the smoke panel are shown in Table 1.
0.5g of the fumigating peppermint and coffee extract prepared in the example 3 is uniformly sprayed on 100g of tobacco leaves by a high-pressure nozzle, the spraying process is carried out in the tobacco shred feeding process, and then the tobacco leaves are rolled into cigarettes by the processes of shredding, flavoring and rolling according to the conventional cigarette process, and the cigarettes are respectively named as No. b cigarettes. And (3) rolling a control cigarette b on the same production line according to the same cigarette process, wherein the control cigarette b is a normal cigarette added with the unvaporized peppermint and coffee extract in the same proportion. And then regulating the moisture content of the cigarette sample to 12% according to the national standard GB/T16447-1996 atmospheric environment for regulating and testing tobacco and tobacco products, and performing sensory cigarette smoking evaluation by a smoking evaluation expert group according to the regulation of GB 5606.4-1996 cigarette sensory technical requirements. The results of the smoke panel are shown in Table 1.
The fumigation tobacco leaf prepared in the example 3 and the fumigation Pu 'er tea extract prepared in the example 1 are simultaneously applied to cigarettes, the fumigation tobacco leaf and the fumigation Pu' er tea extract with the mass ratio of 5% are uniformly sprayed on 100g of tobacco shreds by a high-pressure nozzle, and then the tobacco shreds are rolled into cigarettes by the processes of shredding, perfuming and rolling according to the conventional cigarette process, wherein the cigarettes are respectively named as No. B cigarettes. On the same production line, a control cigarette B is rolled according to the same cigarette process, and the control cigarette B is a cigarette added with non-fumigated tobacco leaves, non-fumigated peppermint + coffee extract and functional auxiliary materials in the same proportion as in example 1. And then regulating the moisture content of the cigarette sample to 12% according to the national standard GB/T16447-1996 atmospheric environment for regulating and testing tobacco and tobacco products, and performing sensory cigarette smoking evaluation by a smoking evaluation expert group according to the regulation of GB 5606.4-1996 cigarette sensory technical requirements. The results of the smoke panel are shown in Table 1.
TABLE 1 cigarette sensory quality evaluation results
TABLE 2 sensory evaluation scoring table
As can be seen from tables 1 and 2, compared with the control cigarette added with the non-fumigated tobacco leaves and the non-fumigated extracting solution, the fumigated tobacco leaves and the fumigated spice plant extracting solution obtained in embodiments 1 to 4 have no influence on the original style of the cigarette, but can further enrich the cigarette aroma, increase the aroma amount and fullness of the cigarette aroma, make the cigarette aroma more mellow and fine, increase the sweet feeling of the smoke, and improve the sensory comfort of the cigarette. Improves and enhances the sensory quality of the cigarette to a certain extent.
TABLE 3 suction evaluation Table
The results of the smoke panel tests in table 3 show that the comfort of the cigarettes prepared in examples 1 to 4, which contain the fumigated tobacco leaves and the fumigated spice plant extract of the present invention, is about 0.6 point higher on average, the smoke characteristic is about 0.6 point higher on average, the sweetness in the taste style is about 0.36 point higher on average, and the sourness is about 0.28 point higher on average, compared with the control cigarettes containing the fumigated tobacco leaves and the fumigated spice plant extract. Therefore, the fumigated tobacco leaves and the fumigated spice plant extract can be added into cigarettes to obviously increase the aroma amount and fullness of cigarette fragrance, make the cigarette fragrance more mellow and finer, enrich the smoke taste of the cigarettes, reduce the smoke irritation of the cigarettes and improve the throat comfort of users, and particularly, the cigarettes No. B have very good effect.
TABLE 4 results of routine flue gas analysis
As can be seen from Table 4, compared with the control cigarette, the main stream smoke of the cigarette added with the fumigated tobacco leaves and the fumigated spice plant extract has obviously reduced tar content, which is averagely reduced by more than 0.80 mg/cigarette; meanwhile, the moisture of the smoke is obviously increased by about 0.4 mg/cigarette on average.
TABLE 5 comparison of aroma Components
As can be seen from table 5, compared with the control tobacco leaves without fumigation, the main aroma components of the tobacco leaves added with the fumigation agent of the present invention are mainly esters, alcohols, ketones and phenols, and the content thereof is significantly increased. After fumigation and flavoring, lipid cigarette aroma substances such as ethyl hexanoate, diethyl succinate, ethyl maltol and the like which are not contained in the tobacco leaves appear, and the tobacco leaves have sweet taste, fruit aroma or wine aroma, can enrich the aroma of the cigarette aroma, inhibit irritation and improve the smoking taste of the cigarettes; ethyl palmitate, cembratriene diol, menthol and the like have the fragrance characteristics of burnt fragrance, sweet fragrance, flower fragrance, fruit fragrance, milk fragrance and the like, the richness and the layering sense of the cigarette fragrance are increased, and the characteristic style of the cigarette is further enhanced.
Claims (7)
1. A fumigating and flavoring method is characterized in that natural spice plants and tobacco leaves are used as main materials, functional auxiliary materials are added, fumigation is carried out in a closed container for 5-48 h at the temperature of 50-150 ℃, and the mixture is cooled at room temperature and then placed to obtain fumigated natural spice plants and fumigated tobacco leaves; the functional auxiliary materials comprise organic acid salt, amino acid and natural moisturizing factors, and the functional auxiliary materials comprise the following components in parts by weight: 1-20 parts of natural moisturizing factors, 10-50 parts of organic acid salts and 1-30 parts of amino acids; the organic acid salt is one or more of potassium sodium citrate, potassium sodium tartrate, acetate, lactate or fumarate; the amino acid is one or more of aspartic acid, threonine, glutamic acid, glycine, alanine, valine, isoleucine, proline, phenylalanine, histidine or serine; the natural moisturizing factor is one or more of hyaluronic acid, aloe gel or luffa water.
2. The fumigating and blending method of claim 1, wherein the raw materials comprise, by weight: 20-50 parts of tobacco leaves, 10-50 parts of natural spice plants and 1-5 parts of functional auxiliary materials.
3. The fumigating and blending method of claim 1, wherein the preparation method of the functional auxiliary materials comprises the following steps: dissolving organic acid salt at 40-60 ℃, adding propylene glycol in a mass ratio of 1:1, adding natural moisturizing factors and amino acid, and mixing at 50-70 ℃ for 0.5h to obtain the functional auxiliary material.
4. The fumigation flavouring method of claim 1, wherein said natural flavouring plant is one or more of lavender, dendrobium, ganoderma lucidum, black tea of yunnan, pu' er tea, yerba mate, pueraria root, licorice, frangipani, hops, honeysuckle, sterculia lychnophora, dandelion, rose, iris, mimosa, asian mint, peppermint, shiitake, helichrysum, jasmine, citronella, labra, vanilla, valerian, vanilla, rosemary, spearmint, raspberry, geranium, ganoderma, cinnamon, tree moss, ganoderma, pine cone, coffee, maca, fenugreek, chicory, malt, ophiopogon root, termitomyces, violet leaf, ylang-ylang.
5. Use of the fumigated tobacco leaves or/and fumigated natural spice plants obtained by the fumigation method according to claim 1 in cigarettes.
6. The use according to claim 5, wherein the fumigated natural spice plants are subjected to spice extraction to obtain spice extract, and the spice extract is used in cigarettes.
7. The use according to claim 6, characterized in that the extraction step of the perfume extract is: taking a mixed solution of ethanol and water as an extractant, performing microwave-assisted steam distillation on the fumigated natural perfume plants according to the mass ratio of the fumigated natural perfume plants to the extractant of 1: 5-1: 30, and then freezing, separating and concentrating to obtain a perfume extracting solution; wherein the microwave power is 250-800W, and the radiation time is 5-60 min.
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|---|---|---|---|---|
| CN102934838A (en) * | 2012-11-30 | 2013-02-20 | 姜波 | Chinese herbal incense with tobacco aroma through baking fumigation |
| CN103099310A (en) * | 2013-02-04 | 2013-05-15 | 红云红河烟草(集团)有限责任公司 | Tobacco moistening agent and application thereof |
| CN105307515A (en) * | 2013-06-19 | 2016-02-03 | 日本烟草产业株式会社 | Process for producing raw tobacco material |
| CN106387990A (en) * | 2016-11-22 | 2017-02-15 | 中国烟草总公司郑州烟草研究院 | High-nicotine tobacco extract and application thereof |
| CN110522065A (en) * | 2018-05-25 | 2019-12-03 | 红塔烟草(集团)有限责任公司 | A kind of flue-cured tobacco method improving quality of tobacco using tealeaves |
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2020
- 2020-03-19 CN CN202010194229.9A patent/CN111329098B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102934838A (en) * | 2012-11-30 | 2013-02-20 | 姜波 | Chinese herbal incense with tobacco aroma through baking fumigation |
| CN103099310A (en) * | 2013-02-04 | 2013-05-15 | 红云红河烟草(集团)有限责任公司 | Tobacco moistening agent and application thereof |
| CN105307515A (en) * | 2013-06-19 | 2016-02-03 | 日本烟草产业株式会社 | Process for producing raw tobacco material |
| CN106387990A (en) * | 2016-11-22 | 2017-02-15 | 中国烟草总公司郑州烟草研究院 | High-nicotine tobacco extract and application thereof |
| CN110522065A (en) * | 2018-05-25 | 2019-12-03 | 红塔烟草(集团)有限责任公司 | A kind of flue-cured tobacco method improving quality of tobacco using tealeaves |
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