CN101928637B - Mixed tincture for cigarettes and preparation method and application thereof in tobacco essence - Google Patents
Mixed tincture for cigarettes and preparation method and application thereof in tobacco essence Download PDFInfo
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- CN101928637B CN101928637B CN 200910062788 CN200910062788A CN101928637B CN 101928637 B CN101928637 B CN 101928637B CN 200910062788 CN200910062788 CN 200910062788 CN 200910062788 A CN200910062788 A CN 200910062788A CN 101928637 B CN101928637 B CN 101928637B
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- Prior art keywords
- mixed
- tincture
- cigarette
- mixed tincture
- cigarettes
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- 229940098465 tincture Drugs 0.000 title claims abstract description 42
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 38
- 241000208125 Nicotiana Species 0.000 title claims abstract description 18
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title abstract description 6
- 241000735527 Eupatorium Species 0.000 claims abstract description 10
- 239000000706 filtrate Substances 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 241000125205 Anethum Species 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 238000010298 pulverizing process Methods 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 9
- 239000003205 fragrance Substances 0.000 abstract description 8
- 239000000779 smoke Substances 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 230000000996 additive effect Effects 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract 2
- 241001127714 Amomum Species 0.000 abstract 1
- 240000000662 Anethum graveolens Species 0.000 abstract 1
- 235000013399 edible fruits Nutrition 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000002304 perfume Substances 0.000 description 8
- 239000000796 flavoring agent Substances 0.000 description 6
- 235000013599 spices Nutrition 0.000 description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 239000003546 flue gas Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- 239000007921 spray Substances 0.000 description 3
- 238000005352 clarification Methods 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Abstract
The invention discloses a mixed tincture for cigarettes and preparation and application thereof in a tobacco essence. The mixed tincture for the cigarettes is obtained by the steps of: uniformly mixing tsaoko amomum fruit, dill and fortune eupatorium herb in a weight ratio of 1:4-6:2-3; grinding the mixture; extracting the mixture with 50 to 60 percent solution of ethanol; and filtering the extracted product to obtain filtrate, namely, the mixed tincture for the cigarettes. The mixed tincture serving as an essence additive of the tobacco essence has the advantages of remarkable effect, capability of increasing smoke concentration, rich cigarette fragrance, addition of special fragrance, soft smoke, high fragrance quality, improved mouth-feel, high stability and the like.
Description
Technical field
The invention belongs to the essence spice for cigarette field, specifically a kind of cigarette mixed tincture and preparation and application in tobacco essence.
Background technology
Cigarette additive comprises medicinal extract, extract, tincture, fruit juice extract etc.The essence and flavoring agent such as medicinal extract, extract mostly is the refluxing extraction gained, some volatile fragrance matters or destroyed or with solvent loss, this is unhelpful for the improvement on the cigarette smoke odor characteristic in concentration process.And tincture has overcome destruction or the loss of volatile fragrance matter in the said process, and, technique large with its output is simple, low cost and other advantages and enjoy favor.At present, be applied to yet there are no in the cigarette flavors report take the mixing natural material as the main mixed tincture that makes.Therefore inventing a kind of cigarette is highly profitable with mixed tincture.
Summary of the invention
Purpose of the present invention is exactly the defective for prior art, a kind of cigarette mixed tincture and preparation method is provided, and is applied in the essence spice for cigarette to improve flavor quality of cigarette.
Technical solution of the present invention is by following realization: it be with tsaoko, dill, eupatorium by weight 1: 4-6: 2-3 mixes rear pulverizing, and with the lixiviate of 50-60% ethanolic solution, the complete rear filtration of lixiviate obtains filtrate, is the cigarette mixed tincture.
The preferred technical scheme of the present invention is that the weight ratio of tsaoko, dill, eupatorium is 1: 4-6: 2-3, and with 50% ethanolic solution lixiviate, wherein extraction time is 15 days, ethanolic solution is 10: 1 with the total amount ratio of mixed material.
Can improve flavor quality of cigarette in the pipe tobacco with mixed tincture adding cigarette of the present invention, the weight that is added into the mixed tincture in the pipe tobacco accounts for 0.05% of pipe tobacco weight.
Smoking result shows that mixed tincture of the present invention enriches cigarette perfume (or spice) increasing flue gas concentration, increases special note, and soft flue gas promotes fragrance matter, improve the aspect such as mouthfeel and have good effect, and stability better.
The present invention is that a new application has been opened up in the application of natural perfume material.Mixed tincture can be mentioned the increase flue gas concentration as essence spice for cigarette, enriches cigarette perfume (or spice), increases special note, and soft flue gas promotes the effect of fragrance matter, is a kind of good natural perfume material.
The specific embodiment
The present invention is described further below by embodiment.
The preparation of embodiment 1 mixed tincture
Tsaoko, dill, eupatorium are mixed rear pulverizing by weight 1: 6: 3, cross 20 mesh sieves.With 50% ethanolic solution lixiviate, ethanolic solution is 10: 1 with the total amount ratio of mixed material, and lixiviate 15 days is filtered to clarification, namely gets mixed tincture.
Embodiment 2
Tsaoko, dill, eupatorium are mixed rear pulverizing by weight 1: 4: 2, cross 20 mesh sieves.With 60% ethanolic solution lixiviate, ethanolic solution is 10: 1 with the total amount ratio of mixed material, and lixiviate 15 days is filtered to clarification, namely gets mixed tincture.
Reinforced the smokeing panel test of embodiment 3 mixed tinctures
Take by weighing 0.02g (feeding quantity is 0.05%) mixed tincture, add distilled water to 2.2g, behind the mixing, spray equably with micro sprayer and to be added to (5 yuan of blank) on the 40g pipe tobacco.The pipe tobacco that will feed in raw material is packed in the sealing bag, place 75 ℃ of constant temperature 30min in the baking oven, then it is suitable to moisture to shake rapidly pipe tobacco, roll into cigarette, put into constant temperature (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) more than the case inner equilibrium 48h, the group of please smokeing panel test (11 people) smokes panel test.Contrast adds the cigarette that the pipe tobacco (5 yuan of blank) of identical distilled water rolls for spray only.
Embodiment 3 mixed tincture quality stability are estimated
Cigarette after reinforced is placed under (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) condition, and the group of smokeing panel test (11 people) carries out reexamining of continuous three weeks to it, to investigate its quality stability.
Contrast test:
Determining of extract alcohol content
After getting tsaoko, dill, eupatorium (1: 6: 3) and pulverizing (crossing 20 mesh sieves), respectively with 50%, 70% alcohol in 1: 8 ratio lixiviate 15 days, take a sample and smoke panel test.The result shows that 50% alcohol lixiviate mixed tincture is better than 70% alcohol lixiviate mixed tincture, and the aspects such as 50% alcohol lixiviate mixed tincture excitant, mouthfeel, perfume quantity all are better than 70% alcohol lixiviate mixed tincture, so extraction solvent is decided to be 50% alcohol.
Determining of extract solid-to-liquid ratio
After getting tsaoko, dill, eupatorium (1: 6: 3) and pulverizing (crossing 20 mesh sieves), the alcohol with 50% is taken a sample and is smoked panel test in 1: 5,1: 8,1: 10 ratio lixiviate 15 days.
1.4 determining of mixed tincture extraction time
After getting tsaoko, dill, eupatorium (1: 6: 3) and pulverizing (crossing 20 mesh sieves), the alcoholic solution with 50% is in 1: 10 ratio lixiviate, takes a sample respectively at 15d, 20d, 25d and smokes panel test.
Its smoking result sees Table 1:
The table 1 mixed tincture table of smokeing panel test
Based on the above results as can be known, determine that its optimised process is: natural perfume material is pulverized (crossing 20 mesh sieves), uses 50% alcohol, and material ratio is 1: 10, lixiviate 15d best results.It can soft flue gas in cigarette, increase cigarette flavor, improve the effects such as cigarette flavor matter.
The reinforced effect of smokeing panel test
Mixed tincture spray is added on 5 yuan of blank pipe tobaccos, rolled cigarette is distributed to 11 people's the group of smokeing panel test, take 5 yuan of blank pipe tobaccos as contrast, its smoking result sees Table 2:
The reinforced effect of smokeing panel test of table 2 mixed tincture
As known from Table 2, to smell perfume (or spice) more special because of mixed tincture, so when feeding quantity reached 0.1%, the fragrant harmony of cigarette was just slightly poor, external fragrance also begins to appear, so best feeding quantity is 0.05%.
Mixed tincture quality stability is estimated
Because natural perfume material is subjected to the influence of environmental factor and external condition larger, in order to investigate its quality stability, we place under (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) condition by the cigarette after reinforced (0.05%), the group (11 people) of please smokeing panel test carries out reexamining of continuous three weeks to it, to investigate its quality stability.Its three all smoking result sees Table 3.
Table 3 mixed tincture quality stability evaluation table
As known from Table 3, through the effect assessment in continuous three weeks, its effect of smokeing panel test does not change, and slightly increase improving mouthfeel effect, but variation not quite, and hence one can see that, and mixed tincture quality stability is better.
Claims (4)
1. cigarette mixed tincture, it be with tsaoko, dill, eupatorium by weight 1: 4-6: 2-3 mixes rear pulverizing, and with the lixiviate of 50-60% ethanolic solution, the complete rear filtration of lixiviate obtains filtrate, is the cigarette mixed tincture.
2. a kind of cigarette mixed tincture according to claim 1, wherein extraction time is 15 days, ethanolic solution is 10: 1 with the total amount ratio of mixed material.
3. a kind of cigarette mixed tincture according to claim 1, the concentration that it is characterized in that ethanolic solution is 50%.
4. the cigarette application of mixed tincture in the pipe tobacco of cigarette, it be with tsaoko, dill, eupatorium by weight 1: 4-6: 2-3 mixes rear pulverizing, with the lixiviate of 50-60% ethanolic solution, the complete rear filtration of lixiviate obtains filtrate, be the cigarette mixed tincture, mixed tincture is added in the pipe tobacco of cigarette, the weight that is added into the mixed tincture in the pipe tobacco accounts for 0.05% of pipe tobacco weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910062788 CN101928637B (en) | 2009-06-23 | 2009-06-23 | Mixed tincture for cigarettes and preparation method and application thereof in tobacco essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910062788 CN101928637B (en) | 2009-06-23 | 2009-06-23 | Mixed tincture for cigarettes and preparation method and application thereof in tobacco essence |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101928637A CN101928637A (en) | 2010-12-29 |
| CN101928637B true CN101928637B (en) | 2013-03-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 200910062788 Expired - Fee Related CN101928637B (en) | 2009-06-23 | 2009-06-23 | Mixed tincture for cigarettes and preparation method and application thereof in tobacco essence |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102653703B (en) * | 2011-03-01 | 2013-07-17 | 湖北中烟工业有限责任公司 | Top dressing flavor for improving influence of Chinese herbal medicine extract on cigarette taste |
| CN104479867A (en) * | 2014-11-28 | 2015-04-01 | 湖北中烟工业有限责任公司 | Microcapsule purification method and application of dill oil for cigarettes |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4502494A (en) * | 1982-07-08 | 1985-03-05 | International Flavors & Fragrances Inc. | Norbornyl esters and uses thereof in augmenting or enhancing the _organoleptic properties of a consumable material and process for _preparing same |
| CN1103563A (en) * | 1993-12-08 | 1995-06-14 | 王冰 | Non-tobacco health cigarette |
| WO2004052128A2 (en) * | 2002-12-11 | 2004-06-24 | British American Tobacco (Investments) Limited | Improvements relating to smoking articles |
| CN1935045A (en) * | 2006-10-10 | 2007-03-28 | 王冰 | Non-tobacco cigarette |
| CN101116533A (en) * | 2007-09-04 | 2008-02-06 | 川渝中烟工业公司 | Process for reducing mixed cigarette smoke by using Chinese herbal medicine |
-
2009
- 2009-06-23 CN CN 200910062788 patent/CN101928637B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4502494A (en) * | 1982-07-08 | 1985-03-05 | International Flavors & Fragrances Inc. | Norbornyl esters and uses thereof in augmenting or enhancing the _organoleptic properties of a consumable material and process for _preparing same |
| CN1103563A (en) * | 1993-12-08 | 1995-06-14 | 王冰 | Non-tobacco health cigarette |
| WO2004052128A2 (en) * | 2002-12-11 | 2004-06-24 | British American Tobacco (Investments) Limited | Improvements relating to smoking articles |
| CN1935045A (en) * | 2006-10-10 | 2007-03-28 | 王冰 | Non-tobacco cigarette |
| CN101116533A (en) * | 2007-09-04 | 2008-02-06 | 川渝中烟工业公司 | Process for reducing mixed cigarette smoke by using Chinese herbal medicine |
Non-Patent Citations (1)
| Title |
|---|
| 范传书.手工雪茄烟的配方及制做工艺.《烟草科技》.1987,(第1期),第29-32页. * |
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| Publication number | Publication date |
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| CN101928637A (en) | 2010-12-29 |
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