CN112956730A - CBD-containing mint electronic atomized liquid and preparation method thereof - Google Patents
CBD-containing mint electronic atomized liquid and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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Abstract
The application relates to the technical field of electronic atomized liquid, and particularly discloses mint electronic atomized liquid containing CBD and a preparation method thereof. The mint electronic atomized liquid is prepared from the following raw materials of spearmint essence, peppermint essence, ice mint essence, watermelon essence, orange essence, cooling agent, spearmint oil, peppermint oil, ethyl acetate, ethanol, deionized water, pure fragrant ethyl maltol, vanillin, sweetening agent, menthol, levo carvone, menthyl lactate, CBD oil, propylene glycol and vegetable glycerol. The mint electronic atomized liquid has the advantages of good reduction feeling, pure mint flavor, comfortable and natural cool flavor, moderate cool degree, good smoke amount, natural and comfortable aftertaste and good smoking taste, and the CBD is grafted into the mint electronic atomized liquid, so that the fragrance, the comfort degree and the like of the mint electronic atomized liquid are not influenced, the health effect of the mint electronic atomized liquid is increased, and the mint electronic atomized liquid has wide application prospect.
Description
Technical Field
The application relates to the technical field of electronic atomized liquid, in particular to mint electronic atomized liquid containing CBD and a preparation method thereof.
Background
The electronic cigarette is an electronic product simulating a cigarette, and has the same appearance, smoke and feeling as the cigarette. Because the electronic cigarette does not contain harmful substances such as tar, carbon monoxide and the like and has little harm to the body of a consumer, the electronic cigarette has already gained market acceptance and is accepted by wide consumers, and the demand of the electronic cigarette is continuously increased. With the development of society and the progress of science and technology, people continuously improve the health consciousness and also put forward higher requirements on the electronic cigarette.
The electronic atomization liquid is used as an important raw material of the electronic cigarette, and has direct feeling and experience for consumers. Mint is always a popular spice, gives a cool feeling, and has the fragrance which is well complemented with the fragrance in the electronic atomized liquid and is popular with consumers. In the related technology, generally, vacuum freeze-dried mint particles are directly added into raw materials, and although the mint electronic atomized liquid has mint fragrance, the mint electronic atomized liquid is not rich, soft and natural in fragrance and easy to generate bitter taste, and cannot meet market demands.
Disclosure of Invention
In order to improve the smoking taste of the mint electronic atomized liquid and increase the application of CBD, the application provides the mint electronic atomized liquid containing CBD and a preparation method thereof.
In a first aspect, the application provides an electronic peppermint atomized liquid containing CBD, which adopts the following technical scheme:
the CBD-containing mint electronic atomized liquid is prepared from the following raw materials, by weight, 8-12 parts of spearmint essence, 1-1.4 parts of peppermint essence, 2.5-6.5 parts of peppermint essence, 0.1-0.7 part of watermelon essence, 0.2-0.7 part of orange essence, 14-20 parts of cooling agent, 0.1-0.4 part of spearmint oil, 0.1-0.35 part of peppermint oil, 0.05-0.2 part of ethyl acetate, 0.3-0.7 part of ethanol, 0.05-0.2 part of deionized water, 4-7 parts of pure fragrant ethyl maltol, 1-5 parts of vanillin, 1-5 parts of sweetening agent, 10-14 parts of menthol, 0.1-0.5 part of levo carvone, 0.05-0.5 part of menthyl lactate, 4-6 parts of CBD oil, 10-19 parts of propylene glycol and 20-23 parts of vegetable glycerol.
By adopting the technical scheme, the spearmint essence, the peppermint essence, the ice mint essence, the watermelon essence and the orange essence have different fragrances and tastes, and the reduction feeling of the electronic peppermint atomized liquid is improved through the synergistic effect among the spearmint essence, the peppermint essence, the ice mint essence, the watermelon essence and the orange essence. The vanillin has vanilla bean fragrance and strong milk fragrance, can play a role in enhancing and fixing fragrance, the menthyl lactate has light cool mint gas, meanwhile, the durability of the fragrance of the mint electronic atomized liquid is improved, the pure fragrant ethyl maltol is a fragrance synergist, has good improving and enhancing effects, and the taste and the aftertaste of the mint electronic atomized liquid are improved by combining the synergistic effect of the vanillin and the menthyl lactate. The spearmint oil has the fresh, sweet and slightly cool fragrance of spearmint, the levocarvone has light fragrance, and the levocarvone also has certain antibacterial property on pathogenic fungi, so that the storage time of the mint electronic atomized liquid is effectively prolonged.
The peppermint oil has refreshing effect, and also has natural exciting effect, and can promote breath circulation and improve brain. The menthol has the effects of cooling, refreshing and moistening the throat, but the menthol also has bitter taste, and the cooling agent has strong cool feeling and no bitter taste, and can effectively cover the bitter taste of the menthol by combining the sweetening agent, the vegetable glycerin and the pure fragrant ethyl maltol and enable the electronic mint atomized liquid to have good sweet taste. The propylene glycol has no obvious smell, but has the advantages of smooth tobacco oil and wide solubility, but the smoke amount is less, and the vegetable glycerin is added, so that the smoke amount can be effectively increased, the sweet taste is also realized, the sweet taste of the mint electronic atomized liquid is increased, and the mouthfeel of the mint electronic atomized liquid is improved.
The CBD oil is cannabidiol which is a pure natural component extracted from cannabis sativa, the cannabidiol has the functions of blocking the adverse effect of certain polyphenols on the nervous system of a human body, blocking breast cancer metastasis, treating epilepsy, resisting rheumatoid arthritis, resisting insomnia and other physiological activities, has a good effect on treating multiple sclerosis, has the effect of inhibiting cannabinoid receptors, has certain effects on anxiety, schizophrenia, epilepsy and the like, and can improve the skin, kill cancer cells, resist tumors, regulate metabolism and the like.
In this application, through adding CBD, not only increased the healthy efficiency of peppermint electronic atomization liquid to combine the synergism between peppermint oil and the raw materials, do not influence the fragrant smell, comfort level etc. of peppermint electronic atomization liquid, with CBD grafting to electronic atomization liquid, obtained the peppermint electronic atomization liquid new product that contains CBD, not only increased CBD's application, make peppermint electronic atomization liquid have healthy composition moreover, thereby make peppermint electronic atomization liquid have wide application prospect.
In the application, through the synergistic effect between the raw materials, the mint electronic atomized liquid has the advantages of being fresh, fragrant and sweet, uniform and transparent, and also has the advantages of being good in reduction sense, pure in mint flavor, comfortable and natural in cool flavor, moderate in cool degree, good in smoke amount, natural and comfortable in aftertaste and good in smoking taste, and the market demand is met.
Optionally, the cooling agent is prepared from the following raw materials, by weight, 9-11 parts of spearmint essence, 1.1-1.3 parts of peppermint essence, 3-5 parts of peppermint essence, 0.3-0.55 part of watermelon essence, 0.4-0.6 part of orange essence, 16-18 parts of cooling agent, 0.2-0.3 part of spearmint oil, 0.2-0.3 part of peppermint oil, 0.1-0.15 part of ethyl acetate, 0.4-0.6 part of ethanol, 0.1-0.15 part of deionized water, 5-6 parts of pure fragrant ethyl maltol, 2.5-4 parts of vanillin, 2.5-4.5 parts of sweetening agent, 11-13 parts of menthol, 0.2-0.4 part of levorotation carvone, 0.1-0.3 part of menthyl lactate, 4.5-5.5 parts of CBD oil, 13-16 parts of propylene glycol and 21-22 parts of vegetable glycerol.
Optionally, the mint flavor composition comprises, by weight, 10 parts of spearmint flavor, 1.2 parts of peppermint flavor, 4 parts of peppermint flavor, 0.45 part of watermelon flavor, 0.55 part of orange flavor, 17 parts of cooling agent, 0.25 part of spearmint oil, 0.25 part of peppermint oil, 0.1 part of ethyl acetate, 0.5 part of ethanol, 0.1 part of deionized water, 5.5 parts of pure fragrant ethyl maltol, 3.5 parts of vanillin, 3.5 parts of sweetening agent, 12 parts of menthol, 0.3 part of laevorotation carvone, 0.2 part of menthyl lactate, 5 parts of CBD oil, 13.6 parts of propylene glycol and 22 parts of vegetable glycerol.
By adopting the technical scheme, the proportion of the mint electronic atomized liquid is further limited, and the performance of the mint electronic atomized liquid is improved.
Optionally, the CBD oil is levocannabidiol extracted from plants.
By adopting the technical scheme, the intersolubility of the raw materials of the CBD oil is increased, and the stability of the CBD oil in the mint electronic atomized liquid raw materials is also improved.
Optionally, the sweetener is a sucralose sweetener.
By adopting the technical scheme, the sucralose sweetening agent is prepared by taking sucrose as a raw material, not only has sweet taste, but also has the advantages of large sweetness, natural and pure and lasting sweet taste and good thermal stability, simultaneously has a calorific value close to zero, does not cause obesity, can be used by diabetes patients, and has the advantage of safety. The sucralose sweetening agent is added into the mint electronic atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the sweet taste of the mint electronic atomized liquid is improved.
Optionally, the cooling agent is a mixture of a cooling agent WS-3 and a cooling agent WS-23, and the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 is (8-10) to (7-9).
By adopting the technical scheme, the cooling agent WS-3 is N-ethyl-5-methyl-2- (1-methylethyl) ring, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent WS-3 not only has light mint fragrance, but also has strong cooling feeling, and more importantly, the cooling agent WS-23 does not have bitter feeling of menthol and irritant side effect. Through the synergistic effect of the cooling agent WS-3, the cooling agent WS-23 and the menthol, the mint aroma and the cooling feeling can be effectively increased.
Optionally, the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 is 9: 8.
By adopting the technical scheme, the proportion of the cooling agent WS-3 to the cooling agent WS-23 is further limited, and the performance of the mint electronic atomized liquid is improved.
In a second aspect, the application provides a preparation method of an electronic peppermint atomized liquid containing CBD, which adopts the following technical scheme:
a preparation method of CBD-containing mint electronic atomized liquid comprises the following steps:
adding peppermint essence, ice mint essence, watermelon essence and orange essence into spearmint essence at room temperature, and stirring for 10-20min to obtain premix a;
adding spearmint oil, peppermint oil, ethyl acetate, pure fragrant ethyl maltol, vanillin, levo-carvone and menthyl lactate into menthol at room temperature, and stirring for 10-20min to obtain premix b;
adding propylene glycol into vegetable glycerol at the temperature of 45-55 ℃, stirring for 10-20min, then adding a cooling agent, a sweetening agent, a premix a and a premix b, stirring for 10-20min, then dropwise adding CBD oil under the condition of continuous stirring, after the CBD oil is dropwise added for 5-10min, blowing inert gas at the flow rate of 10-20mL/min, continuously stirring for 40-60min, and cooling to obtain a semi-finished product;
adding ethanol into the semi-finished product at room temperature, stirring for 10-20min, dropwise adding deionized water, stirring for 20-30min after dropwise adding deionized water is completed within 5-10min, standing for 2-3h, filtering to remove impurities, and standing for 1-2h to obtain the electronic peppermint atomized liquid.
By adopting the technical scheme, the raw materials are mixed step by step, and the inert gas is introduced into the mixed materials of the vegetable glycerol, the propylene glycol, the cooling agent, the sweetening agent, the premix a, the premix b and the CBD oil, so that the disturbance of the raw materials can be effectively increased, the raw materials are fully fused, part of the inert gas remained in the raw materials is reduced, and the oxygen is reduced to enter the raw materials. Adding ethanol at room temperature to reduce ethanol volatilization, adding deionized water dropwise to mix ethanol and raw materials, standing, filtering, and standing to reduce bubbles in the electronic peppermint atomized liquid.
Meanwhile, the materials are mixed in a heating mode, the temperature is controlled to be 45-55 ℃, so that the raw materials are fully dissolved, the mixing is more uniform, the material mixing efficiency is improved, and the fragrance loss or change caused by overhigh temperature is reduced.
Optionally, the filtering and impurity removing are performed by using a filter screen, and the aperture of the filter screen is 1000-2000 meshes.
Through adopting above-mentioned technical scheme, filter the impurity in the peppermint electronic atomization liquid, reduce the influence of impurity to peppermint electronic atomization liquid.
Optionally, the inert gas is nitrogen.
By adopting the technical scheme, the nitrogen has the advantages of simple and safe use and low cost, and the production cost of the mint electronic atomized liquid is reduced.
In summary, the present application has the following beneficial effects:
1. the mint electronic atomized liquid containing the CBD has the advantages of being fresh, sweet, uniform and transparent through the synergistic effect of the raw materials, good in restoration feeling, pure in mint flavor, comfortable and natural in cool flavor, moderate in cool degree, good in smoke amount, natural and comfortable in aftertaste and good in smoking taste, and meets market demands. Meanwhile, the CBD is grafted into the electronic atomized liquid by combining the synergistic effect of the CBDs, so that the health effect of the mint electronic atomized liquid is increased, the fragrance, the comfort degree and the like of the mint electronic atomized liquid are not influenced, the application of the CBD is increased, the mint electronic atomized liquid has healthy components, and the mint electronic atomized liquid has wide application prospect.
2. According to the preparation method of the CBD-containing electronic mint atomized liquid, the inert gas is introduced, so that the disturbance of the raw materials can be effectively increased, the raw materials are fully fused, part of the inert gas remained in the raw materials is reduced, and the oxygen is reduced to enter the raw materials. Meanwhile, the materials are mixed in a heating mode, the temperature is controlled to be 45-55 ℃, so that the raw materials are fully dissolved, the mixing is more uniform, the material mixing efficiency is improved, and the fragrance loss or change caused by overhigh temperature is reduced.
Detailed Description
The present application will be described in further detail with reference to examples.
Raw materials
The spearmint flavor is selected from Guangzhou Hengyu science and technology limited; the peppermint essence and the ice peppermint essence are selected from morning fragrance essence and spice Limited company in Shenzhen city; the watermelon essence is selected from Guangzhou Hengyu science and technology limited; the orange essence is selected from Guangzhou Hengyu science and technology limited; the cooling agent WS-3 and the cooling agent WS-23 are selected from Xian Taima bioengineering company, Inc.; spearmint oil is selected from the trillion perfume oils ltd, ge am; peppermint oil is selected from Nanjing Ponno Biotech limited; the pure fragrant ethyl maltol is selected from Cian Henjida Biotech limited; the vanillin is selected from the group consisting of Gianer trillion perfume oil Co; the sweetener is selected from the group consisting of Jicheng Jiekang sucralose manufacturing Co., Ltd; the Mentholum is selected from Yulongxiang biotechnology Co Ltd; the L-carvone is selected from Saian Jia Boying Biotech limited; menthyl lactate is selected from the trillion perfume oils, Inc. of Jian; the CBD oil is extracted from plants and is selected from Yunan Han union pharmaceutical Co., Ltd; the vegetable glycerin is selected from Guangzhou Convergence chemical Co.
Examples
TABLE 1 example the content (unit: g) of each raw material in the peppermint electronic atomized liquid
| Raw materials | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 |
| Green mint essence | 8 | 9 | 10 | 11 | 12 |
| Peppermint essence | 1.4 | 1.3 | 1.2 | 1.1 | 1 |
| Ice mint essence | 5 | 6.5 | 4 | 3 | 2.5 |
| Watermelon essence | 0.7 | 0.1 | 0.45 | 0.55 | 0.3 |
| Orange essence | 0.65 | 0.7 | 0.55 | 0.4 | 0.2 |
| Cooling agent | 14 | 18 | 17 | 16 | 20 |
| Spearmint oil | 0.3 | 0.2 | 0.25 | 0.1 | 0.4 |
| Peppermint oil | 0.2 | 0.1 | 0.25 | 0.35 | 0.3 |
| Ethyl acetate | 0.1 | 0.2 | 0.1 | 0.05 | 0.15 |
| Ethanol | 0.7 | 0.6 | 0.5 | 0.3 | 0.4 |
| Deionized water | 0.05 | 0.1 | 0.1 | 0.1 | 0.15 |
| Pure fragrant ethyl maltol | 7 | 4 | 5.5 | 5.1 | 6 |
| Vanillin | 1 | 4 | 3.5 | 5 | 2.5 |
| Sweetening agent | 4.5 | 5 | 3.5 | 1 | 2.5 |
| Menthol crystal | 11 | 10 | 12 | 13 | 14 |
| L-carvone | 0.1 | 0.2 | 0.3 | 0.4 | 0.5 |
| Menthyl lactate | 0.3 | 0.5 | 0.2 | 0.05 | 0.1 |
| CBD oil | 6 | 5.5 | 5 | 4.5 | 4 |
| Propylene glycol | 19 | 13 | 13.6 | 16 | 10 |
| Vegetable glycerin | 20 | 21 | 22 | 22 | 23 |
| Total up to | 100 | 100 | 100 | 100 | 100 |
Example 1
An electronic atomized liquid containing CBD from herba Menthae is shown in Table 1.
Wherein the cooling agent is a mixture of a cooling agent WS-3 and a cooling agent WS-23, and the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 is 8: 7.
A preparation method of CBD-containing mint electronic atomized liquid comprises the following steps:
adding the peppermint essence, the ice mint essence, the watermelon essence and the orange essence into the spearmint essence at room temperature, and stirring for 20min to obtain premix a.
Adding spearmint oil, peppermint oil, ethyl acetate, pure fragrant ethyl maltol, vanillin, levo-carvone and menthyl lactate into menthol at room temperature, and stirring for 20min to obtain premix b.
Adding propylene glycol into vegetable glycerol at the temperature of 45 ℃, stirring for 10min, then adding a cooling agent, a sweetening agent, a premix a and a premix b, stirring for 20min, then dropwise adding CBD oil under the condition of continuous stirring, after the CBD oil is dropwise added for 5min, blowing nitrogen gas at the flow rate of 20mL/min, continuously stirring for 40min, and cooling to obtain a semi-finished product.
Adding ethanol into the semi-finished product at room temperature, stirring for 10min, dropwise adding deionized water, stirring for 30min after 5min, standing for 2h, filtering with a filter screen to remove impurities, wherein the aperture of the filter screen is 1000 meshes, and standing for 1h to obtain the electronic peppermint atomized liquid.
Examples 2 to 5
An electronic peppermint atomized liquid containing CBD, which is characterized in that the difference between examples 2-5 and example 1 is that the raw material proportion is different, and the raw material proportion is shown in Table 1.
Example 6
The difference between the mint electronic atomized liquid containing CBD and the embodiment 3 is that the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 in the raw materials of the mint electronic atomized liquid is 9: 8.
Example 7
The difference between the mint electronic atomized liquid containing CBD and the embodiment 3 is that the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 in the raw materials of the mint electronic atomized liquid is 10: 9.
Example 8
An electronic atomized mint liquid containing CBD, which is different from the electronic atomized mint liquid in example 6 in the preparation method.
A preparation method of CBD-containing mint electronic atomized liquid comprises the following steps:
adding the peppermint essence, the ice mint essence, the watermelon essence and the orange essence into the spearmint essence at room temperature, and stirring for 15min to obtain premix a.
Adding spearmint oil, peppermint oil, ethyl acetate, pure fragrant ethyl maltol, vanillin, levo-carvone and menthyl lactate into menthol at room temperature, and stirring for 15min to obtain premix b.
Adding propylene glycol into vegetable glycerol at the temperature of 50 ℃, stirring for 15min, then adding a cooling agent, a sweetening agent, a premix a and a premix b, stirring for 15min, then dropwise adding CBD oil under the condition of continuous stirring, after the CBD oil is dropwise added for 8min, blowing nitrogen gas at the flow rate of 15mL/min, continuously stirring for 45min, and cooling to obtain a semi-finished product.
Adding ethanol into the semi-finished product at room temperature, stirring for 15min, dropwise adding deionized water, stirring for 25min after the deionized water is added for 8min, standing for 2.5h, filtering with a filter screen to remove impurities, wherein the aperture of the filter screen is 1340 meshes, and standing for 1.5h to obtain the mint electronic atomized liquid.
Example 9
An electronic atomized mint liquid containing CBD, which is different from the electronic atomized mint liquid in example 6 in the preparation method.
A preparation method of CBD-containing mint electronic atomized liquid comprises the following steps:
adding the peppermint essence, the ice mint essence, the watermelon essence and the orange essence into the spearmint essence at room temperature, and stirring for 10min to obtain premix a.
Adding spearmint oil, peppermint oil, ethyl acetate, pure fragrant ethyl maltol, vanillin, levo-carvone and menthyl lactate into menthol at room temperature, and stirring for 10min to obtain premix b.
Adding propylene glycol into vegetable glycerol at the temperature of 55 ℃, stirring for 20min, then adding a cooling agent, a sweetening agent, a premix a and a premix b, stirring for 10min, then dropwise adding CBD oil under the condition of continuous stirring, after the CBD oil is completely dropwise added for 10min, blowing nitrogen gas at the flow rate of 10mL/min, continuously stirring for 60min, and cooling to obtain a semi-finished product.
Adding ethanol into the semi-finished product at room temperature, stirring for 20min, dropwise adding deionized water, stirring for 20min after the deionized water is added for 10min, standing for 3h, filtering with a filter screen to remove impurities, wherein the aperture of the filter screen is 2000 meshes, and standing for 2h to obtain the mint electronic atomized liquid.
Comparative example
Comparative example 1
The difference between the CBD-containing electronic mint atomized liquid and the embodiment 6 is that green mint essence, savory mint essence, ice mint essence, watermelon essence and orange essence are replaced by the same amount of vacuum freeze-dried mint particles in the raw materials of the electronic mint atomized liquid.
Comparative example 2
An electronic peppermint atomized liquid containing CBD is different from the electronic peppermint atomized liquid in example 6 in that the CBD oil is replaced by the same amount of propylene glycol in the raw materials of the electronic peppermint atomized liquid.
Comparative example 3
The difference between the mint electronic atomized liquid containing CBD and the embodiment 6 is that the raw material of the mint electronic atomized liquid is equal to propylene glycol instead of ethyl acetate, ethanol and deionized water.
Comparative example 4
An electronic peppermint atomized liquid containing CBD is different from the electronic peppermint atomized liquid in the preparation method of the electronic peppermint atomized liquid in example 6.
A preparation method of CBD-containing mint electronic atomized liquid comprises the following steps:
adding propylene glycol, a cooling agent, a sweetening agent, spearmint essence, peppermint essence, ice mint essence, watermelon essence, orange essence, menthol, spearmint oil, peppermint oil, ethyl acetate, ethanol, deionized water, pure fragrant ethyl maltol, vanillin, levorotation carvone, menthyl lactate and CBD oil into vegetable glycerin at the temperature of 65 ℃, stirring for 60min, standing for 3h, then filtering by using a filter screen to remove impurities, wherein the aperture of the filter screen is 1000 meshes, and standing for 1h to obtain the mint electronic atomized liquid.
Performance test
Samples were prepared from the mint electronic atomized liquids obtained in examples 1 to 9 and comparative examples 1 to 4, and the following performance tests were carried out, and the test results are shown in table 2.
Wherein, the content of the methanol in the sample is detected according to GB/T7917.4-1987 methanol Standard test method for sanitary chemistry of cosmetics.
According to GB/T5009.49-2008 'analytical method of fermented wine and its compound wine sanitation standard', the formaldehyde content in the sample is detected.
According to GB5009.74-2014 'heavy metal limit test in food safety national standard food additives', the content of heavy metals in a sample is detected.
The phthalate content of the samples was determined according to GB5009.271-2016 phthalate determination in national food safety Standard.
The total number of colonies in the sample was determined according to GB4789.2-2016 (national food safety Standard food microbiology test for Total colony count assay).
TABLE 2 test results
As can be seen from the table 2, the mint electronic atomized liquid has lower methanol content, formaldehyde content, heavy metal content and phthalate content, and simultaneously has lower total number of bacterial colonies, thereby meeting the market demand.
130 male smokers, who were aged 25 to 35 years and randomly divided into 13 groups of 10 persons, were selected for preparing samples of the mint electronic atomized liquids obtained in examples 1 to 9 and comparative examples 1 to 4, and the fragrance and appearance were evaluated. Then, each group of smokers took the sample with the electronic cigarette, and evaluated the refreshing feeling, the sweet taste, the reducing feeling, the smoke amount, the unpleasant taste, and the aftertaste of the sample after use, and the evaluation results are shown in table 3.
TABLE 3 test results
As can be seen from table 3, the mint electronic atomized liquid of the present application, through the synergistic effect between the raw materials, has the advantages of fresh, sweet, uniform and transparent, and also has the advantages of good reduction feeling, pure mint flavor, comfortable and natural cool flavor, moderate cool degree, good smoke amount, natural and comfortable aftertaste, and good smoking taste, and meets the market demand.
By comparing the example 6 with the comparative example 1, it can be seen that the spearmint essence, the peppermint essence, the ice mint essence, the watermelon essence and the orange essence are added into the raw materials, and the electronic mint atomized liquid has good reduction feeling and aftertaste through the synergistic effect of the spearmint essence, the peppermint essence, the watermelon essence and the orange essence, and the influence of the foreign flavor is reduced.
Through comparing the embodiment 6 with the comparative example 2, it can be seen that the CBD oil is added into the raw materials, and the synergistic effect between the CBD and the raw materials is utilized, so that the health efficacy of the mint electronic atomized liquid is increased, and the fragrance, the comfort and the like of the mint electronic atomized liquid are not influenced.
By comparing example 6 with comparative example 3, it can be seen that the addition of ethyl acetate, ethanol, and deionized water to the raw materials can increase the aroma, appearance, cooling, and sweetness of the mint electronic atomized liquid.
By comparing example 6 with comparative example 4, it can be seen that the preparation method of the present application can increase the aroma, appearance, cooling feeling, and sweet taste of the mint electronic atomized liquid.
The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.
Claims (10)
1. The CBD-containing mint electronic atomized liquid is characterized in that: the mint essence cooling tea is prepared from the following raw materials, by weight, 8-12 parts of green mint essence, 1-1.4 parts of peppermint essence, 2.5-6.5 parts of mint essence, 0.1-0.7 part of watermelon essence, 0.2-0.7 part of orange essence, 14-20 parts of cooling agent, 0.1-0.4 part of spearmint oil, 0.1-0.35 part of peppermint oil, 0.05-0.2 part of ethyl acetate, 0.3-0.7 part of ethanol, 0.05-0.15 part of deionized water, 4-7 parts of pure fragrant ethyl maltol, 1-5 parts of vanillin, 1-5 parts of sweetening agent, 10-14 parts of menthol, 0.1-0.5 part of levocarvone, 0.05-0.5 part of menthyl lactate, 4-6 parts of CBD oil, 10-19 parts of propylene glycol and 20-23 parts of glycerol.
2. The CBD-containing mint electronic atomized liquid as claimed in claim 1, wherein: the mint essence cooling beverage is prepared from the following raw materials, by weight, 9-11 parts of spearmint essence, 1.1-1.3 parts of peppermint essence, 3-5 parts of peppermint essence, 0.3-0.55 part of watermelon essence, 0.4-0.6 part of orange essence, 16-18 parts of cooling agent, 0.2-0.3 part of spearmint oil, 0.2-0.3 part of peppermint oil, 0.1-0.15 part of ethyl acetate, 0.4-0.6 part of ethanol, 0.05-0.1 part of deionized water, 5-6 parts of pure fragrant ethyl maltol, 2.5-4 parts of vanillin, 2.5-4.5 parts of sweetening agent, 11-13 parts of menthol, 0.2-0.4 part of levorotation carvone, 0.1-0.3 part of menthyl lactate, 4.5-5.5 parts of CBD oil, 13-16 parts of propylene glycol and 21-22 parts of vegetable glycerol.
3. The CBD-containing mint electronic atomized liquid as claimed in claim 1, wherein: the mint essence ice cream is prepared from the following raw materials, by weight, 10 parts of green mint essence, 1.2 parts of peppermint essence, 4 parts of mint ice essence, 0.45 part of watermelon essence, 0.55 part of orange essence, 17 parts of cooling agent, 0.25 part of spearmint oil, 0.25 part of peppermint oil, 0.1 part of ethyl acetate, 0.5 part of ethanol, 0.1 part of deionized water, 5.5 parts of pure fragrant ethyl maltol, 3.5 parts of vanillin, 3.5 parts of sweetening agent, 12 parts of menthol, 0.3 part of levorotation carvone, 0.2 part of menthyl lactate, 5 parts of CBD oil, 13.6 parts of propylene glycol and 22 parts of vegetable glycerol.
4. The CBD-containing mint electronic atomized liquid as claimed in claim 1, wherein: the CBD oil is L-cannabidiol extracted from plants.
5. The CBD-containing mint electronic atomized liquid as claimed in claim 1, wherein: the sweetener is a sucralose sweetener.
6. The CBD-containing mint electronic atomized liquid as claimed in claim 1, wherein: the cooling agent is a mixture of a cooling agent WS-3 and a cooling agent WS-23, and the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 is (8-10) to (7-9).
7. The CBD-containing mint electronic atomized liquid as claimed in claim 6, wherein: the weight ratio of the cooling agent WS-3 to the cooling agent WS-23 is 9: 8.
8. A method of preparing an electronic atomized liquid of mint containing CBD according to any one of claims 1 to 7, wherein: the method comprises the following steps:
adding peppermint essence, ice mint essence, watermelon essence and orange essence into spearmint essence at room temperature, and stirring for 10-20min to obtain premix a;
adding spearmint oil, peppermint oil, ethyl acetate, pure fragrant ethyl maltol, vanillin, levo-carvone and menthyl lactate into menthol at room temperature, and stirring for 10-20min to obtain premix b;
adding propylene glycol into vegetable glycerol at the temperature of 45-55 ℃, stirring for 10-20min, then adding a cooling agent, a sweetening agent, a premix a and a premix b, stirring for 10-20min, then dropwise adding CBD oil under the condition of continuous stirring, after the CBD oil is dropwise added for 5-10min, blowing inert gas at the flow rate of 10-20mL/min, continuously stirring for 40-60min, and cooling to obtain a semi-finished product;
adding ethanol into the semi-finished product at room temperature, stirring for 10-20min, dropwise adding deionized water, stirring for 20-30min after dropwise adding deionized water is completed within 5-10min, standing for 2-3h, filtering to remove impurities, and standing for 1-2h to obtain the electronic peppermint atomized liquid.
9. The method for preparing the CBD-containing mint electronic atomized liquid as claimed in claim 8, wherein the CBD-containing mint electronic atomized liquid comprises the following steps: the filtration and impurity removal are carried out by adopting a filter screen, and the aperture of the filter screen is 1000-2000 meshes.
10. The method for preparing the CBD-containing mint electronic atomized liquid as claimed in claim 8, wherein the CBD-containing mint electronic atomized liquid comprises the following steps: the inert gas is nitrogen.
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| CN113749278A (en) * | 2021-09-16 | 2021-12-07 | 深圳市真味生物科技有限公司 | Lily-flavored electronic atomized liquid and preparation method thereof |
| CN115005490A (en) * | 2022-06-28 | 2022-09-06 | 深圳梵活生命科学股份有限公司 | Electronic mint tobacco atomized liquid without nicotine and preparation method thereof |
| CN115141680A (en) * | 2022-07-04 | 2022-10-04 | 深圳梵活生命科学股份有限公司 | Grapefruit essence composition special for electronic atomized liquid and preparation method thereof |
| CN115322832A (en) * | 2022-09-14 | 2022-11-11 | 湖北中烟工业有限责任公司 | Cool flavor, tobacco sheet and non-combustible cigarette |
| CN115363241A (en) * | 2022-09-07 | 2022-11-22 | 深圳市亚美健康科技有限公司 | Atomized liquid for refreshing and restoring consciousness and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113749278A (en) * | 2021-09-16 | 2021-12-07 | 深圳市真味生物科技有限公司 | Lily-flavored electronic atomized liquid and preparation method thereof |
| CN113749278B (en) * | 2021-09-16 | 2023-09-12 | 深圳市真味生物科技有限公司 | Lily-flavored electronic atomized liquid and preparation method thereof |
| CN115005490A (en) * | 2022-06-28 | 2022-09-06 | 深圳梵活生命科学股份有限公司 | Electronic mint tobacco atomized liquid without nicotine and preparation method thereof |
| CN115141680A (en) * | 2022-07-04 | 2022-10-04 | 深圳梵活生命科学股份有限公司 | Grapefruit essence composition special for electronic atomized liquid and preparation method thereof |
| CN115363241A (en) * | 2022-09-07 | 2022-11-22 | 深圳市亚美健康科技有限公司 | Atomized liquid for refreshing and restoring consciousness and preparation method thereof |
| CN115322832A (en) * | 2022-09-14 | 2022-11-11 | 湖北中烟工业有限责任公司 | Cool flavor, tobacco sheet and non-combustible cigarette |
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