CN109135922A - A kind of recombination maple maple flavour, its reconstructing method and application in cigarette based on Low Flavour Threshold - Google Patents
A kind of recombination maple maple flavour, its reconstructing method and application in cigarette based on Low Flavour Threshold Download PDFInfo
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- CN109135922A CN109135922A CN201810824737.3A CN201810824737A CN109135922A CN 109135922 A CN109135922 A CN 109135922A CN 201810824737 A CN201810824737 A CN 201810824737A CN 109135922 A CN109135922 A CN 109135922A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/36—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring
- A24B15/40—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms
- A24B15/403—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0092—Heterocyclic compounds containing only N as heteroatom
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention relates to a kind of recombination maple maple flavour based on Low Flavour Threshold; it is characterized in that; the recombination maple maple flavour is made of flavor component, carbohydrate and solvent; wherein; maple maple flavour is recombinated in terms of 100%, each component includes methyl cyclopentenyl ketone, 2 acetyl furans, 5 hydroxymethyl furfural, furfural, acetyl pyrrole, 2.6- dimethyl pyrazine, dorinone, linalool, fenugreck lactone, alpha-angelica lactone, Ergol, vanillic aldehyde, n-nonanoic acid, citric acid, fumaric acid in flavor component；The weight proportion of each component in carbohydrate are as follows: sucrose 0~1%, fructose 2~2.6%, glucose 10~16%, maltose 20~32%；Surplus is solvent.The recombination maple maple flavour is applied in cigarette, can obviously increase cigarette flavor amount and flue gas concentration, promote aroma quality, improves comfort, and without negative effects such as burnt bitter breath, sweet senses.
Description
Technical field
The invention belongs to flavouring essence for tobacco technical fields, and in particular to a kind of recombination maple maple flavour based on Low Flavour Threshold, its
Reconstructing method and the application in cigarette.
Background technique
In recent years, with the rapid development of social economy with the rapid raising of living standards of the people, the majority of consumers are increasingly
Pay attention to personal health, low tar, less harmful etc., which require, to be proposed to tobacco consumption product inherent quality quality.And tobacco business is response
Consumer demand, deepen continuously propulsion " reducing tar and reducing harm " engineering, but how while reducing coke tar in cigarette, reduction cigarette endangers
The high fragrance of cigarette, high-comfort contour metric attribute is kept to have become the key for restricting Chinese-style cigarette development, especially current
In the case that tar content has had very big decline, further significantly tar reduction again, difficulty while keeping cigarette odor-absorbing
It will be increasing.
Flavors and fragrances is improving cigarette flavor amount, is improving cigarette flavor quality side as one of cigarette product core technology
Face plays important supporting role, therefore is all the time also Chinese-style cigarette focus of attention.Maple extract is maple maple wood molasses
A kind of traditional tobacco additive, is mainly used for blended type cigarette all the time obtained by extracting through organic solvent, rolls up increasing
While cigarette perfume tolerance and flue gas concentration, promotion aroma quality, improvement comfort, the bitter breath of strong coke, sweet sense etc. are also brought
Negative effect and affect its practical application in Chinese-style cigarette.Importantly, maple extract is grown by its originating species
The influence of the growing environments factor such as environment temperature, moisture, soil, illumination leads to different year, different sources even different batches
Between product quality fluctuation is big, stability is poor, meanwhile, various processes difference also results in maple extract product five in the market
Hua Bamen, poor quality constrain its application in Chinese-style cigarette away from big.Therefore, exploitation is without negative effect and product matter
The project that stable maple extract product has become tobacco enterprise and food service industry concern is measured, and in maple extract key component
System separates on analysis foundation, obtains novel maple maple flavour by fragrance model reconstruction technology and is undoubtedly feasible technological approaches.
Fragrance energy value (OAV) is the concentration for constituting a certain monomer perfume of complicated fragrance system and the ratio of its Low Flavour Threshold
Value, and the OAV size according to different tobacco aromaticss in system, can determine whether different tobacco aromaticss to fragrance system percentage contribution
Difference, OAV bigger fragrance is bigger to the contribution of fragrance system, and vice versa.This contribution otherness is to improving fragrance model weight
Structure technology has important practical significance.
Therefore, the present invention is on maple extract key component separation analysis foundation, from OAV and economic cost the two dimensions
It sets out, carries out maple extract model reconstruction, obtain a kind of recombination maple maple flavour of superior performance, not only eliminate maple extract
The middle unfavorable ingredient for generating the negative effects such as burnt bitter breath, sweet sense, overcomes traditional maple extract stable product quality difference
Inherent shortcoming, and effectively improve fragrance utilization rate and blending high efficiency.
Summary of the invention
Present invention aims to overcome that prior art defect, provides a kind of recombination maple maple flavour based on Low Flavour Threshold, it should
Flavouring essence for tobacco can obviously increase cigarette flavor amount and flue gas concentration, promote aroma quality, improve comfort, and without burnt bitter breath, sweet tea
The negative effects such as soapy feeling.
The reconstructing method for the recombination maple maple flavour that the present invention also provides above-mentioned based on Low Flavour Threshold and its in cigarette
Using.
To achieve the above object, the present invention adopts the following technical scheme:
A kind of reconstructing method of the recombination maple maple flavour based on Low Flavour Threshold, specifically comprises the following steps:
1) maple maple flavour ingredient divides:
According to maple extract composition analysis result, 26 kinds of ingredients that content is greater than 0.4mg/kg are filtered out, are drafted as maple maple
Essence initial formulation, and 26 kinds of ingredients are divided into 22 kinds of volatile fragrant components and 4 kinds of non-volatile carbohydrate contents, it is specifically shown in
The following table 1；
1 maple maple flavour ingredient of table divides
2) flavor component note is sorted out:
With reference to " tobacco perfume material " (Xie Jianping, Chemical Industry Press, 2009, ISBN:9787122055125), " eat
Fragrance handbook " (Sun Baoguo, Liu Yuping, Sinopec publishing house, 2004, ISBN:9787801645906), respectively according to burnt sweet tea
Fragrant, baking perfume, fruity, 6 kinds of fragrance of a flower, milk and sour notes, 22 kinds of volatile fragrant components are sorted out, categorization results are shown in
Table 2；
2 volatile fragrant components note of table divides
3) the fragrance energy value OAV of flavor component is calculated:
According to the content and its Low Flavour Threshold of flavor component, obtained by the ratio calculation of levels and its Low Flavour Threshold
Fragrance energy value of the diverse fragrant flavour ingredient in maple extract system, is shown in Table 3；
The fragrance energy value of flavor component in 3 maple extract of table
4) maple maple flavour ingredient is recombinated
According to the fragrance energy value OAV of flavor component in maple extract, in same note, go in the fragrant and sweet note of coke dropping
The flavor component of OAV≤0.005；Remove the flavor component for baking OAV≤0.01 in note；Remove floral notes, fruity note
With the flavor component of OAV≤10.0 in sour note；Simultaneously the entire essence of horn of plenty bake fragrant and sweet note, improve cigarette taste relax
Adaptive adds additional alpha-angelica lactone, citric acid and fumaric acid；And on the basis of each flavor component content in proportion on float downward
The amount of employing finally complements to 100% with solvent to optimize to formula.
Finally determining recombination maple maple flavour is made of flavor component, carbohydrate and solvent, wherein recombination maple maple flavour with
The weight proportion of 100% meter, flavor component and carbohydrate see the table below, and surplus is solvent；
.The solvent is the mixture of propylene glycol, water or propylene glycol and water arbitrary proportion.
Application of the recombination maple maple flavour in cigarette based on Low Flavour Threshold that the present invention also provides above-mentioned.
Innovative point of the present invention is to develop the maple extract of a kind of no negative effect and stable product quality, with can be effective
Promote fragrance utilization rate and blending high efficiency.The present invention is on maple extract key component separation analysis foundation, from OAV and economy
Two dimensions of cost are set out, and the recombination maple maple flavour that maple extract model reconstruction obtains a kind of superior performance, the recombination maple are carried out
Maple flavour is applied in cigarette, can obviously increase cigarette flavor amount and flue gas concentration, promote aroma quality, improves comfort, and nothing
The negative effects such as burnt hardship breath, sweet sense.
Specific embodiment
Technical solution of the present invention is further discussed in detail with reference to embodiments, but protection scope of the present invention
It is not limited thereto.
Embodiment 1 to 3
Each raw material weight proportioning of soup processed of the recombination maple maple perfume of embodiment 1 to 3 is shown in Table 4.Wherein, solvent is third in embodiment 1
Glycol, solvent is the propylene glycol of volume ratio 1:1 and the mixed liquor of water in embodiment 2 and 3.
Each raw material weight proportioning of soup processed of the recombination maple maple flavour of 4 embodiment of table 1 to 3
The preparation method of maple maple flavour is recombinated described in above-described embodiment 1-3, specifically: each raw material component is taken in proportion, is added
Enter into solvent, stirring to be completely dissolved to get.
The reconstructing method of the above-mentioned recombination maple maple flavour based on Low Flavour Threshold, specifically comprises the following steps:
1) maple maple flavour ingredient divides:
According to maple extract composition analysis result, 26 kinds of ingredients that content is greater than 0.4mg/kg are filtered out, are drafted as maple maple
Essence initial formulation, and 26 kinds of ingredients are divided into 22 kinds of volatile fragrant components and 4 kinds of non-volatile carbohydrate contents, it is specifically shown in
The following table 5；
5 maple maple flavour ingredient of table divides
2) flavor component note is sorted out:
With reference to " tobacco perfume material " (Xie Jianping, Chemical Industry Press, 2009, ISBN:9787122055125), " eat
Fragrance handbook " (Sun Baoguo, Liu Yuping, Sinopec publishing house, 2004, ISBN:9787801645906), respectively according to burnt sweet tea
Fragrant, baking perfume, fruity, 6 kinds of fragrance of a flower, milk and sour notes, 22 kinds of volatile fragrant components are sorted out, categorization results are shown in
Table 6；
6 volatile fragrant components note of table divides
3) the fragrance energy value OAV of flavor component is calculated:
According to the content and its Low Flavour Threshold of flavor component, diverse fragrant flavour ingredient is calculated in maple extract system
Fragrance energy value, is shown in Table 7；
The fragrance energy value of flavor component in 7 maple extract of table
4) maple maple flavour ingredient is recombinated
According to the fragrance energy value OAV of flavor component in maple extract, in same note, go in the fragrant and sweet note of coke dropping
The flavor component of OAV≤0.005；Remove the flavor component for baking OAV≤0.01 in note；Remove floral notes, fruity note
With the flavor component of OAV≤10.0 in sour note；Simultaneously the entire essence of horn of plenty bake fragrant and sweet note, improve cigarette taste relax
Adaptive adds additional alpha-angelica lactone, citric acid and fumaric acid；And on the basis of each flavor component content in proportion on float downward
The amount of employing finally complements to 100% with solvent to optimize to formula.
Cigarette application test
The recombination maple maple flavour of embodiment 1-3 allotment preparation is added in pipe tobacco in the ratio of 0.06wt%, while with
The pipe tobacco of recombination maple maple flavour is not added as blank control group, cigarette product, equilibrium water are made using conventional method in that art
Divide (humidity 60% ± 2%, 25 ± 1 DEG C of temperature) for 24 hours, then according to " YC/T 415-2011 tobacco is in product sensory evaluation side
Method " sensory evaluation is carried out, as a result as shown in Table 8 and 9.
8 sense organ evaluating meter of table
| Group | Sensory evaluation |
| Blank group | Aroma quality is medium, and perfume quantity is less, and flue gas irritation is larger, slightly miscellaneous gas |
| Embodiment 1 | Aroma quality is preferable, and perfume quantity is more sufficient, slightly irritation, and pleasant impression is cleaner |
| Embodiment 2 | Aroma quality is good, and perfume quantity is sufficient, and irritation mitigates, and pleasant impression is completely comfortable |
| Embodiment 3 | Aroma quality improves, and perfume quantity is more sufficient, micro- to have miscellaneous gas, and pleasant impression is relatively comfortable |
9 sense organ evaluating meter of table (national standard marking)
Table 8 and 9 the result shows that: compared with blank sample, add the present invention recombination maple maple flavour cigarette sample fragrance
Qualitative change is good, and perfume quantity significantly improves, and flue gas pleasant impression is improved, and masks miscellaneous gas；Maple maple flavour is recombinated simultaneously to also ensure that
Stable product quality, this can greatly expand its application in Chinese-style cigarette.
Claims (4)
1. a kind of recombination maple maple flavour based on Low Flavour Threshold, which is characterized in that the recombination maple maple flavour is by flavor component, carbohydrate
It is formed with solvent, wherein in terms of 100%, the weight proportion of flavor component and carbohydrate see the table below recombination maple maple flavour, and surplus is molten
Agent；
2. the recombination maple maple flavour based on Low Flavour Threshold as described in claim 1, which is characterized in that the solvent be propylene glycol,
The mixture of water or propylene glycol and water arbitrary proportion.
3. a kind of reconstructing method of the recombination maple maple flavour described in claim 1 based on Low Flavour Threshold, which is characterized in that including such as
Lower step:
1) maple maple flavour ingredient divides:
According to maple extract composition analysis result, 26 kinds of ingredients that content is greater than 0.4mg/kg are filtered out, are drafted as maple maple flavour
Initial formulation, and 26 kinds of ingredients are divided into 22 kinds of volatile fragrant components and 4 kinds of non-volatile carbohydrate contents, specifically it see the table below
1；
1 maple maple flavour ingredient of table divides
2) flavor component note is sorted out:
With reference to " tobacco perfume material ", " flavorant handbook ", respectively according to burnt fragrant and sweet, baking perfume, fruity, the fragrance of a flower, milk and acid
Fragrant 6 kinds of notes, 22 kinds of volatile fragrant components are sorted out, categorization results are shown in Table 2；
2 volatile fragrant components note of table divides
3) the fragrance energy value OAV of flavor component is calculated:
According to the content and Low Flavour Threshold of flavor component, it is living that fragrance of the diverse fragrant flavour ingredient in maple extract system is calculated
Force value is shown in Table 3；
The fragrance energy value of flavor component in 3 maple extract of table
4) maple maple flavour ingredient is recombinated
According to the fragrance energy value OAV of flavor component in maple extract, in same note, go OAV in the fragrant and sweet note of coke dropping≤
0.005 flavor component；Remove the flavor component for baking OAV≤0.01 in note；Remove floral notes, fruity note and sour
The flavor component of OAV≤10.0 in note；Simultaneously the entire essence of horn of plenty bake fragrant and sweet note, improve cigarette taste comfort,
Add additional alpha-angelica lactone, citric acid and fumaric acid；And the use that floats up and down in proportion on the basis of each flavor component content
Amount finally complements to 100% with solvent to optimize to formula.
4. application of the recombination maple maple flavour in cigarette described in claim 1 based on Low Flavour Threshold.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810824737.3A CN109135922B (en) | 2018-07-25 | 2018-07-25 | Recombinant maple essence based on aroma threshold, reconstruction method thereof and application of recombinant maple essence in cigarettes |
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| CN201810824737.3A CN109135922B (en) | 2018-07-25 | 2018-07-25 | Recombinant maple essence based on aroma threshold, reconstruction method thereof and application of recombinant maple essence in cigarettes |
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| CN109135922A true CN109135922A (en) | 2019-01-04 |
| CN109135922B CN109135922B (en) | 2021-12-17 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112226280A (en) * | 2020-10-09 | 2021-01-15 | 湖北中烟工业有限责任公司 | Spice based on key aroma components of osmanthus fragrans and application of spice in cigarettes |
| CN116103088A (en) * | 2023-03-21 | 2023-05-12 | 江苏中烟工业有限责任公司 | Incense base module formula component for improving internal quality of fine cigarettes and application |
| CN116333818A (en) * | 2023-03-29 | 2023-06-27 | 河南中烟工业有限责任公司 | Tobacco essence for highlighting Chinese style cigarette sweet taste characteristics, blending method and application |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112226280A (en) * | 2020-10-09 | 2021-01-15 | 湖北中烟工业有限责任公司 | Spice based on key aroma components of osmanthus fragrans and application of spice in cigarettes |
| CN116103088A (en) * | 2023-03-21 | 2023-05-12 | 江苏中烟工业有限责任公司 | Incense base module formula component for improving internal quality of fine cigarettes and application |
| CN116333818A (en) * | 2023-03-29 | 2023-06-27 | 河南中烟工业有限责任公司 | Tobacco essence for highlighting Chinese style cigarette sweet taste characteristics, blending method and application |
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| Publication number | Publication date |
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| CN109135922B (en) | 2021-12-17 |
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