CN106047483B - A kind of pungent fragrant odor type flavouring essence for tobacco and its concocting method based on fragrance threshold value - Google Patents
A kind of pungent fragrant odor type flavouring essence for tobacco and its concocting method based on fragrance threshold value Download PDFInfo
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- 239000003205 fragrance Substances 0.000 title claims abstract description 64
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 50
- 241000208125 Nicotiana Species 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 17
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 73
- 239000002304 perfume Substances 0.000 claims abstract description 24
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims abstract description 22
- RUMOYJJNUMEFDD-UHFFFAOYSA-N perillyl aldehyde Chemical compound CC(=C)C1CCC(C=O)=CC1 RUMOYJJNUMEFDD-UHFFFAOYSA-N 0.000 claims abstract description 18
- WBYWAXJHAXSJNI-VOTSOKGWSA-M .beta-Phenylacrylic acid Natural products [O-]C(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-M 0.000 claims abstract description 13
- WBYWAXJHAXSJNI-SREVYHEPSA-N Cinnamic acid Chemical compound OC(=O)\C=C/C1=CC=CC=C1 WBYWAXJHAXSJNI-SREVYHEPSA-N 0.000 claims abstract description 13
- 229930016911 cinnamic acid Natural products 0.000 claims abstract description 13
- 235000013985 cinnamic acid Nutrition 0.000 claims abstract description 13
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 claims abstract description 13
- 150000001299 aldehydes Chemical class 0.000 claims abstract description 12
- QOTQFLOTGBBMEX-UHFFFAOYSA-N alpha-angelica lactone Chemical compound CC1=CCC(=O)O1 QOTQFLOTGBBMEX-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000002904 solvent Substances 0.000 claims abstract description 12
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 claims abstract description 11
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000005770 Eugenol Substances 0.000 claims abstract description 11
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims abstract description 11
- AXMVYSVVTMKQSL-UHFFFAOYSA-N UNPD142122 Natural products OC1=CC=C(C=CC=O)C=C1O AXMVYSVVTMKQSL-UHFFFAOYSA-N 0.000 claims abstract description 11
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229940117916 cinnamic aldehyde Drugs 0.000 claims abstract description 11
- 229960002217 eugenol Drugs 0.000 claims abstract description 11
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 claims abstract description 11
- 230000001953 sensory effect Effects 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 230000000694 effects Effects 0.000 claims description 37
- 239000000463 material Substances 0.000 claims description 37
- 239000000796 flavoring agent Substances 0.000 claims description 15
- 235000019634 flavors Nutrition 0.000 claims description 15
- 235000006990 Pimenta dioica Nutrition 0.000 claims description 9
- 240000008474 Pimenta dioica Species 0.000 claims description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 238000012216 screening Methods 0.000 claims description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 244000061176 Nicotiana tabacum Species 0.000 claims description 4
- 210000000697 sensory organ Anatomy 0.000 claims description 4
- NTPLXRHDUXRPNE-UHFFFAOYSA-N 4-methoxyacetophenone Chemical compound COC1=CC=C(C(C)=O)C=C1 NTPLXRHDUXRPNE-UHFFFAOYSA-N 0.000 claims description 3
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims description 3
- WTWBUQJHJGUZCY-UHFFFAOYSA-N cuminaldehyde Chemical compound CC(C)C1=CC=C(C=O)C=C1 WTWBUQJHJGUZCY-UHFFFAOYSA-N 0.000 claims description 3
- 239000001069 triethyl citrate Substances 0.000 claims description 3
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 claims description 3
- 235000013769 triethyl citrate Nutrition 0.000 claims description 3
- 239000000654 additive Substances 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 2
- 125000003158 alcohol group Chemical group 0.000 claims 1
- 125000005456 glyceride group Chemical group 0.000 claims 1
- 239000000052 vinegar Substances 0.000 claims 1
- 235000021419 vinegar Nutrition 0.000 claims 1
- 238000011156 evaluation Methods 0.000 abstract description 7
- 239000012496 blank sample Substances 0.000 abstract description 3
- 239000000523 sample Substances 0.000 abstract description 3
- 238000012360 testing method Methods 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 description 12
- 239000007789 gas Substances 0.000 description 6
- 235000013599 spices Nutrition 0.000 description 6
- 235000009508 confectionery Nutrition 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 description 2
- XARVANDLQOZMMJ-CHHVJCJISA-N 2-[(z)-[1-(2-amino-1,3-thiazol-4-yl)-2-oxo-2-(2-oxoethylamino)ethylidene]amino]oxy-2-methylpropanoic acid Chemical compound OC(=O)C(C)(C)O\N=C(/C(=O)NCC=O)C1=CSC(N)=N1 XARVANDLQOZMMJ-CHHVJCJISA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Confectionery (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The pungent fragrant odor type flavouring essence for tobacco and its concocting method that the present invention relates to a kind of based on fragrance threshold value, are composed of the following weight percentages of raw materials: perfume base 1-25%, solvent 75-99%；Wherein, the parts by weight group prejudice of perfume base each component is as follows: 0.1-10 parts of anisic aldehyde, 0.05-5 parts of eugenol, 0.1-5 parts of cinnamic acid, 0.1-5 parts of 2- hexenoic aldehyde, 0.02-3 parts of perillaldehyde, 0.1-10 parts of cinnamic aldehyde, 0.1-5 parts of alpha-angelica lactone.The pungent fragrant odor type flavouring essence for tobacco of the present invention is added in pipe tobacco, cigarette product is made using this field routine techniques, sensory evaluation test result shows: comparing with the blank sample for being not added with the pungent fragrant odor type flavouring essence for tobacco of the present invention, cigarette sample aroma quality after addition improves, pungent fragrance breath is obvious, and pleasant impression is improved, mask miscellaneous gas.
Description
Technical field
The invention belongs to essence technical fields, and in particular to a kind of pungent fragrant odor type flavouring essence for tobacco based on fragrance threshold value and its
Concocting method.
Background technique
With the continuous improvement of our people's living standard, consumer to the sucking quality of cigarette and safety also increasingly
Concern.State Tobacco Monopoly Bureau proposes according to the variation of cigarette market and the development trend of domestic and international tobacco business " with harm reduction
Tar reduction engineering is served as theme, and is attached most importance to developing Chinese-style cigarette, General Promotion Chinese tobacco scientific and technological level " developing direction.With
The development of lowering harm and decreasing coking engineering, tar reduction and the fragrant technology of guarantor have become the key for restricting cigarette development, especially in current tar content
In the case where having had very big decline, further significantly tar reduction, difficulty will be got over again while keeping cigarette odor-absorbing
Come bigger.How while reducing cigarette tar content, makes cigarette fragrance remain to be received by consumer, have become cigarette
The main attack project of industry, and influence the key factor that cigarette product tar in China's reduces.
Flavors and fragrances can not only assign the unique taste of cigarette and style, but also can cover cigarette disadvantage, improve cigarette
Fragrance and jealous, promotion cigarette physical property.With national " blending engineering " implementation, flavors and fragrances is in Chinese-style cigarette core
Heart technology formed in effect it is more and more important, especially in terms of constructing cigarette category differentiation.This category difference causes
People when aspirating kinds of cigarettes brand bring unique style and features and product individuality, become consumer and rely selection consumption
Crucial foundation.
Spicy fragrance is a kind of very important note in Virginian-type cigarette aromatic style.Develop the cigarette with typical case Xin Xiang
With essence, and it is applied to cigarette, can not only effectively highlights the pungent fragrant aromatic style of cigarette, and cigarette production can be significantly improved
Product quality.However, fragrant odor type flavouring essence for tobacco pungent so far and its concocting method are there is not yet correlative study is reported.
Currently, cigarette blending relies primarily on the experience and talent of perfumer, lacks theoretical direction and data supporting.In cigarette
Threshold value refer to the minimum concentration value that fragrance matter is experienced in cigarette smoke by the sense organ of people.Different cigarettes is fragrant
Material deposits difference to the threshold value of cigarette, and this otherness has important practical significance to cigarette blending.Threshold value is smaller
Fragrance, to show cigarette odor characteristic of the same race effect it is stronger, contribution it is bigger, vice versa.The cigarette that cigarette blending obtains is used
Essence is a kind of complicated flavor system being made of Multiple components, constitute the content of each cigarette monomer perfume of the system with
The ratio between threshold value can be described as activity threshold of the fragrance in system, and the active threshold according to different tobacco aromaticss in system
It is worth size, can determine whether different tobacco aromaticss to the function and effect and percentage contribution of fragrance complex system.It can thus be seen that according to
Threshold value size, in conjunction with economic cost factor, the activity threshold of each constituent, has in rational allocation target flavor systems
Pointedly carry out cigarette blending, the utilization rate of tobacco aromaticss can be effectively improved, enhances the high efficiency of cigarette blending.
Therefore, it is necessary to by the threshold value for using for reference tobacco aromaticss, with the work of each constituent in target flavor systems
Property threshold value be measurement index, design pungent fragrant flavor essence concocting method, and carry out cigarette blending according to this method, it is excellent to obtain performance
Pungent fragrant odor type flavouring essence for tobacco more.
Summary of the invention
Present invention aims to overcome that lacking the defect of theoretical direction and data supporting in cigarette fragrance process, pass through reference
Tobacco aromaticss threshold value, and fragrance Costco Wholesale is combined, carry out cigarette flavoring essence allotment, obtains the novel pungent fragrant odor type cigarette of one kind and use
Essence, which can not only effectively highlight the pungent fragrant aromatic style of cigarette, and can significantly improve cigarette product quality.
To achieve the above object, the present invention adopts the following technical scheme:
A kind of pungent fragrant odor type flavouring essence for tobacco concocting method based on fragrance threshold value, includes the following steps:
(1) flavor deployment principle determines
Material screening and ratio Controlling principle based on fragrance threshold value are determined first:
1. small (the threshold value < 3.0 × 10 of preferred threshold value-6 Ng/ branch) fragrance as material of main part, material of main part
The sum of activity threshold account for the 60-90% of all spices activity threshold summation.Big the spice phase ratio, threshold value with threshold value
Small fragrance is bigger to the contribution for improving cigarette quality, highlights cigarette and bakes fragrant and sweet better effect, therefore the perfume (or spice) small with threshold value
Material is used as main body fragrance, uses more as far as possible in allotment, the sum of activity threshold of these fragrance is made to account for the active threshold of all spices
The sum of value (gross activity threshold value) 60-90%；
2. by larger (threshold value >=3.0 × 10 of threshold value-6 Ng/ branch) but price lower (300 yuan/kg of price <) perfume (or spice)
Material is used as auxiliary material, and the sum of activity threshold of auxiliary material accounts for the 10-30% of all spices activity threshold summation.Due to threshold value
Lesser main body fragrance also needs other to bake fragrant and sweet fragrance auxiliary, therefore, when larger and close in threshold value, in conjunction with its it is economical at
Sheet, the preferably lower fragrance of price, make the sum of activity threshold of these fragrance account for gross activity threshold value 10-30%；
3. (threshold value >=3.0 × 10 big for threshold value-6 Ng/ branch) and price it is higher (price >=300 yuan/kg)
Fragrance, then it is few as far as possible with or without but capable of being obviously improved except the fragrance of cigarette sensory quality effect, make the work of these fragrance
The sum of property threshold value accounts for gross activity threshold value 0-10%.
(2) material is collected and is investigated
Collecting has common tobacco aromaticss acetanisole, cinnamic acid, alpha-angelica lactone, the 4- methyl for mentioning Yang Xinxiang
Cinnamic acid, cumal, 2- hexenoic aldehyde, perillaldehyde, anisic aldehyde, cinnamic aldehyde and eugenol etc., and each tobacco aromaticss are investigated in cigarette
In threshold value and price..
(3) material screening and flavor deployment
Material screening is carried out according to the flavor deployment principle that step (1) determines:
1. the threshold value of anisic aldehyde and eugenol is smaller, and respectively less than 3.0 × 10-6 Ng/ branch, pretend based on material；
2. other fragrance threshold values are larger, it is all larger than 3.0 × 10-6 Ng/ branch, but wherein 2- hexenoic aldehyde, cinnamic aldehyde, purple
Soviet Union aldehyde, cinnamic acid price be respectively less than 300 yuan/kg, economic cost is low, pretends as auxiliary material；
3. remaining fragrance threshold value is all larger than 3.0 × 10-6 Ng/ is propped up and price is all larger than 300 yuan/kg, therefore is being formulated
In it is few as far as possible use, wherein alpha-angelica lactone can be obviously improved cigarette sensory quality, therefore also selection enters composition.
In the present invention, (Chen Zhifei, Yang Jing, Ma Yuping wait tobacco to the evaluation reference literature of each tobacco aromaticss threshold value
The foundation of fragrance threshold value sensory evaluation method and application [J] tobacco science and technology, 2016,49(4): method in 30-36) into
Row.
After determining material of main part and auxiliary material, the ratio of each perfume monomer is adjusted first, and acquisition smells perfume compared with harmony
Initial formulation formula is finely adjusted then using blank cigarette as carrier, spicy fragrance can be highlighted by being finally obtained one kind
The novel pungent fragrant odor type flavouring essence for tobacco of cigarette product quality can be improved again.That is, a kind of pungent fragrant odor type cigarette based on fragrance threshold value is used
Essence is composed of the following weight percentages of raw materials: perfume base 1-25%, solvent 75-99%；Wherein, the weight of perfume base each component
Amount part composition see the table below:
。
Specifically, the solvent is one in alcohol, propylene glycol, triacetyl glycerine, water, triethyl citrate and glycerol
Kind or two or more mixtures.
Application of the above-mentioned pungent fragrant odor type flavouring essence for tobacco in cigarette, wherein the pungent fragrant odor type flavouring essence for tobacco is in cigarette
Additive amount be preferably 0.06wt%.
Compared to the prior art, beneficial effects of the present invention:
1) present invention innovatively introduces fragrance threshold value in cigarette fragrance process and has in conjunction with economic cost factor
Pointedly carry out cigarette blending, obtain the pungent fragrant flavouring essence for tobacco of superior performance, effectively enhance the high efficiency of cigarette blending,
The utilization rate of tobacco aromaticss is improved, cigarette blending economic cost is reduced.Meanwhile it overcoming previous cigarette blending and purely relying on warp
The defect tested provides a new approaches for Modern cigarette industry blending.
2) the pungent fragrant odor type flavouring essence for tobacco of the present invention is added in pipe tobacco, cigarette is made using this field routine techniques and is produced
Product, sensory evaluation test result show: comparing with the blank sample for being not added with the pungent fragrant odor type flavouring essence for tobacco of the present invention, the volume after addition
Cigarette sample aroma quality improves, and pungent fragrance breath is obvious, and improves pleasant impression, masks miscellaneous gas.
Specific embodiment
Technical solution of the present invention is further discussed in detail with reference to embodiments, but protection scope of the present invention
It is not limited thereto.
A kind of pungent fragrant odor type flavouring essence for tobacco concocting method based on fragrance threshold value, includes the following steps:
(1) flavor deployment principle determines
Material screening and ratio Controlling principle based on fragrance threshold value are determined first:
1. small (the threshold value < 3.0 × 10 of preferred threshold value-6 Ng/ branch) fragrance as material of main part, material of main part
The sum of activity threshold account for the 60-90% of all spices activity threshold summation.Big the spice phase ratio, threshold value with threshold value
Small fragrance is bigger to the contribution for improving cigarette quality, highlights cigarette and bakes fragrant and sweet better effect, therefore the perfume (or spice) small with threshold value
Material is used as main body fragrance, uses more as far as possible in allotment, the sum of activity threshold of these fragrance is made to account for the active threshold of all spices
The sum of value (gross activity threshold value) 60-90%；
2. by larger (threshold value >=3.0 × 10 of threshold value-6 Ng/ branch) but price lower (300 yuan/kg of price <) perfume (or spice)
Material is used as auxiliary material, and the sum of activity threshold of auxiliary material accounts for the 10-30% of all spices activity threshold summation.Due to threshold value
Lesser main body fragrance also needs other to bake fragrant and sweet fragrance auxiliary, therefore, when larger and close in threshold value, in conjunction with its it is economical at
Sheet, the preferably lower fragrance of price, make the sum of activity threshold of these fragrance account for gross activity threshold value 10-30%；
3. (threshold value >=3.0 × 10 big for threshold value-6 Ng/ branch) and price it is higher (price >=300 yuan/kg)
Fragrance, then it is few as far as possible with or without but capable of being obviously improved except the fragrance of cigarette sensory quality effect, make the work of these fragrance
The sum of property threshold value accounts for gross activity threshold value 0-10%.
(2) material is collected and is investigated
Collecting has common tobacco aromaticss acetanisole, cinnamic acid, alpha-angelica lactone, the 4- methyl for mentioning Yang Xinxiang
Cinnamic acid, cumal, 2- hexenoic aldehyde, perillaldehyde, anisic aldehyde, cinnamic aldehyde and eugenol etc., and each tobacco aromaticss are investigated in cigarette
In threshold value and price..
(3) material screening and flavor deployment
Material screening is carried out according to the flavor deployment principle that step (1) determines:
1. the threshold value of anisic aldehyde and eugenol is smaller, and respectively less than 3.0 × 10-6 Ng/ branch, pretend based on material；
2. other fragrance threshold values are larger, it is all larger than 3.0 × 10-6 Ng/ branch, but wherein 2- hexenoic aldehyde, cinnamic aldehyde, purple
Soviet Union aldehyde, cinnamic acid price be respectively less than 300 yuan/kg, economic cost is low, pretends as auxiliary material；
3. remaining fragrance threshold value is all larger than 3.0 × 10-6 Ng/ is propped up and price is all larger than 300 yuan/kg, therefore is being formulated
In it is few as far as possible use, wherein alpha-angelica lactone can be obviously improved cigarette sensory quality, therefore also selection enters composition.
Embodiment 1-3
Each raw material weight proportioning of soup processed of the pungent fragrant odor type flavouring essence for tobacco of embodiment 1 to 3 is as shown in table 1 to table 3.Wherein, real
Applying solvent in example 1 is alcohol, and solvent is propylene glycol in embodiment 2, and solvent is triethyl citrate in embodiment 3.
The raw material proportioning of pungent perfume odor type flavouring essence for tobacco described in 1 embodiment 1 of table
| Raw material | Quality (g) | Activity threshold accounting (%) |
| Anisic aldehyde | 0.2 | 34 |
| Eugenol | 0.3 | 34 |
| Cinnamic acid | 0.5 | 3 |
| 2- hexenoic aldehyde | 1.4 | 2 |
| Perillaldehyde | 3 | 17 |
| Cinnamic aldehyde | 1.6 | 7 |
| Alpha-angelica lactone | 1 | 3 |
| Solvent | 92.0 | - |
The raw material proportioning of pungent perfume odor type flavouring essence for tobacco described in 2 embodiment 2 of table
| Raw material | Quality (g) | Activity threshold accounting (%) |
| Anisic aldehyde | 0.4 | 48 |
| Eugenol | 0.3 | 24 |
| Cinnamic acid | 1.0 | 5 |
| 2- hexenoic aldehyde | 2 | 3 |
| Perillaldehyde | 3 | 12 |
| Cinnamic aldehyde | 0.8 | 3 |
| Alpha-angelica lactone | 2 | 5 |
| Solvent | 90.5 | - |
The raw material proportioning of pungent perfume odor type flavouring essence for tobacco described in 3 embodiment 3 of table
| Raw material | Quality (g) | Activity threshold accounting (%) |
| Anisic aldehyde | 0.2 | 24 |
| Eugenol | 0.6 | 47 |
| Cinnamic acid | 1.5 | 7 |
| 2- hexenoic aldehyde | 4 | 5 |
| Perillaldehyde | 1.2 | 5 |
| Cinnamic aldehyde | 2.4 | 7 |
| Alpha-angelica lactone | 2 | 5 |
| Solvent | 88.1 | - |
The preparation method of pungent perfume odor type flavouring essence for tobacco described in above-described embodiment 1-3, specifically: each component is taken in proportion simultaneously
Mix obtain perfume base, perfume base is added in solvent, stirring to be completely dissolved to get.
The pungent fragrant odor type flavouring essence for tobacco that embodiment 1-3 is deployed is added in pipe tobacco in the ratio of 0.06wt%, using this
Cigarette product is made in field routine techniques.Then it is carried out according to " YC/T 415-2011 tobacco is in product sensory evaluation method "
Sensory evaluation.As a result as shown in table 4 and 5.
4 sense organ evaluating meter of table
| Number | Sensory evaluation |
| Blank | Aroma quality is medium, and perfume quantity is less, flue gas slightly bitter taste, slightly miscellaneous gas |
| Embodiment 1 | Aroma quality improves, and perfume quantity is more sufficient, and slightly pungent fragrance breath, irritation mitigates, and pleasant impression is relatively clean comfortable |
| Embodiment 2 | Aroma quality is good, and perfume quantity is more sufficient, and pungent fragrance breath is obvious, and micro- to have miscellaneous gas, pleasant impression is completely comfortable |
| Embodiment 3 | Aroma quality improves, and perfume quantity is more sufficient, and pungent fragrance breath is denseer, micro- to have miscellaneous gas, and pleasant impression is relatively clean comfortable |
5 sense organ evaluating meter of table (national standard marking)
| Group | Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous gas (12) | Irritation (20) | Pleasant impression (25) | It is total |
| Blank | 5.00 | 29.00 | 5.00 | 10.50 | 17.00 | 22.00 | 88.50 |
| Embodiment 1 | 5.00 | 29.05 | 5.00 | 10.63 | 17.19 | 22.28 | 89.15 |
| Embodiment 2 | 5.00 | 29.13 | 5.00 | 10.72 | 17.34 | 22.19 | 89.38 |
| Embodiment 3 | 5.00 | 29.22 | 5.00 | 10.81 | 17.65 | 22.11 | 89.79 |
The result shows that: it is compared with blank sample, the aroma quality that the cigarette sample of pungent fragrant odor type flavouring essence for tobacco is added improves, Xin Xiang
Note significantly improves, while can improve pleasant impression, covers miscellaneous gas, and spicy fragrance score value improves 0.5 point or more.
Claims (5)
1. a kind of pungent fragrant odor type flavouring essence for tobacco based on fragrance threshold value, which is characterized in that by the raw material group of following weight percentage
At: perfume base 1-25%, solvent 75-99%；Wherein, the parts by weight composition of perfume base each component see the table below:
。
2. pungent fragrant odor type flavouring essence for tobacco as described in claim 1, which is characterized in that the solvent is alcohol, propylene glycol, three vinegar
The mixture of one or more of acid glyceride, water, triethyl citrate and glycerol.
3. application of the pungent fragrant odor type flavouring essence for tobacco as claimed in claim 1 or 2 in cigarette.
4. application of the pungent fragrant odor type flavouring essence for tobacco in cigarette as claimed in claim 3, which is characterized in that the pungent fragrant odor type cigarette
It is 0.06wt% with additive amount of the essence in cigarette.
5. the concocting method of pungent perfume odor type flavouring essence for tobacco described in a kind of claim 1, which is characterized in that include the following steps:
(1) flavor deployment principle determines
Material screening and ratio Controlling principle based on fragrance threshold value are determined first:
1. preferred threshold value < 3.0 × 10-6As material of main part, the sum of activity threshold of material of main part accounts for the fragrance of ng/ branch
The 60-90% of all spices activity threshold summation；
2. by threshold value >=3.0 × 10-6The fragrance of ng/ branch but 300 yuan/kg of price < as auxiliary material, auxiliary material
The sum of activity threshold accounts for the 10-30% of all spices activity threshold summation；
3. for threshold value >=3.0 × 10-6Ng/ branch and price >=300 yuan/kg fragrance are then few with or without but capable of being promoted
Except the fragrance of cigarette sensory quality effect, the sum of activity threshold of these fragrance is made to account for all spices activity threshold summation
0-10%；
(2) material is collected and is investigated
Collecting has common tobacco aromaticss acetanisole, cinnamic acid, alpha-angelica lactone, the 4- methyl cinnamyl for mentioning Yang Xinxiang
Acid, cumal, 2- hexenoic aldehyde, perillaldehyde, anisic aldehyde, cinnamic aldehyde and eugenol, and each common tobacco aromaticss are investigated in cigarette
Threshold value and price；
(3) material screening and flavor deployment
Material screening is carried out according to the flavor deployment principle that step (1) determines:
1. the threshold value of anisic aldehyde and eugenol is respectively less than 3.0 × 10-6Ng/ branch, pretend based on material；
2. the threshold value of 2- hexenoic aldehyde, cinnamic aldehyde, perillaldehyde, cinnamic acid is all larger than 3.0 × 10-6Ng/ is propped up but price is respectively less than 300
Member/kg is pretended as auxiliary material；
3. alpha-angelica lactone threshold value is greater than 3.0 × 10-6Ng/ is propped up and price is greater than 300 yuan/kg, but can promote cigarette sense organ
Quality, therefore also selection alpha-angelica lactone enters composition.
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| CN106590914B (en) * | 2016-11-30 | 2020-06-23 | 湖北中烟工业有限责任公司 | Natural spicy essence and preparation method and application thereof |
| CN109135922B (en) * | 2018-07-25 | 2021-12-17 | 河南中烟工业有限责任公司 | Recombinant maple essence based on aroma threshold, reconstruction method thereof and application of recombinant maple essence in cigarettes |
| CN112457914A (en) * | 2020-10-27 | 2021-03-09 | 四川三联新材料有限公司 | Spicy base for improving smoking comfort of heated cigarettes and application thereof |
| CN115468873A (en) * | 2022-08-05 | 2022-12-13 | 张家口卷烟厂有限责任公司 | Method for rapidly and accurately detecting essence and spice through portable densimeter |
| CN116463171B (en) * | 2023-04-27 | 2024-04-12 | 广州科百欣香料有限公司 | Essence for enhancing cigarette aroma and preparation method and application thereof |
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