CN110226775A - It is a kind of to add in the flavoring tow stick and preparation method thereof heated in the cigarette filter rod that do not burn - Google Patents

It is a kind of to add in the flavoring tow stick and preparation method thereof heated in the cigarette filter rod that do not burn Download PDF

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Publication number
CN110226775A
CN110226775A CN201910600458.3A CN201910600458A CN110226775A CN 110226775 A CN110226775 A CN 110226775A CN 201910600458 A CN201910600458 A CN 201910600458A CN 110226775 A CN110226775 A CN 110226775A
Authority
CN
China
Prior art keywords
flavoring
tow stick
tow
stick
pelelith
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910600458.3A
Other languages
Chinese (zh)
Inventor
洪玮
苏加坤
蔡继宝
邓宇
朱春晖
徐达
郭磊
罗娟敏
索卫国
张晓旭
倪悦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Jiangxi Industrial Co Ltd
Original Assignee
China Tobacco Jiangxi Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Jiangxi Industrial Co Ltd filed Critical China Tobacco Jiangxi Industrial Co Ltd
Priority to CN201910600458.3A priority Critical patent/CN110226775A/en
Publication of CN110226775A publication Critical patent/CN110226775A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/04Cigars; Cigarettes with mouthpieces or filter-tips
    • A24D1/042Cigars; Cigarettes with mouthpieces or filter-tips with mouthpieces
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • A24D3/048Tobacco smoke filters characterised by their shape or structure containing additives
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/08Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
    • A24D3/10Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives

Abstract

It is a kind of to add in the flavoring tow stick heated in tobacco plug of not burning, it is characterized in that designing one section of tow stick close to tobacco end, the tow stick is between tobacco segment and temperature descending section, utilize pelelith large specific surface area, the characteristic of porous excellent adsorption, it is adsorbed essence spice for cigarette and is loaded in the tow stick, technical solution of the present invention discharge essence when suction can constantly, improve the bad generation for inhaling taste of flue gas, the higher flavors and fragrances of boiling point can be added, it assigns low temperature smoke of tobacco and more makes fragrant and sweet profit, saturation is abundant, lasting fragrance, and flavoring tow stick preparation process is simple, qualification rate is high, production cost is low, stability is good.

Description

It is a kind of to add in flavoring tow stick and its preparation heated in the cigarette filter rod that do not burn Method
Technical field
The present invention relates to novel tobacco technical fields, specifically, being a kind of add in heating the cigarette filter rod that do not burn Flavoring tow stick.
Background technique
As health is increasingly paid attention in the continuous reinforcement and people of national governments' tobacco control dynamics, recent domestic is each Large enterprises develop the novel tobacco products of various substitution traditional cigarettes, especially to meet the consumption demand of variation one after another Heat the cigarette that do not burn.As heat not burning type cigarette have be not involved in burning, without tar, suction taste sweet tea unlike as electronics tobacco tar Greasy unique advantage, it is deep to be liked by some consumers.However, heating do not burn cigarette audience predominantly do things creatively, The young and middle-aged consumer for having certain demand rich to cigarette style passes through three-dimensional blending therefore exploitation heating is not burnt when cigarette Technology increases suction interest, strengthens cigarette style characteristics important in inhibiting.There is research to make an addition to fragrance in smoked sheet, due to Smoked sheet temperature reaches 200~400 DEG C when heating, and essence is easy to happen chemical reaction and generates the bad suction taste of peculiar smell generation, and fragrance Discharge it is too fast, cause suction when front and back section inhale taste difference it is excessive.There is research to be placed in fragrance by way of fragrant line or quick-fried pearl close In the filter tip of lip end, since temperature is too low, it is unsuitable for the addition of higher fragrance, it is rich bad.
Summary of the invention
The present invention adsorbs essence spice for cigarette using pelelith, and loads on one section of addition between tobacco segment and temperature descending section Tow stick in, can make suction when essence constantly discharge, improve flue gas it is bad inhale taste generation, the higher perfume (or spice) of boiling point can be added Smart fragrance assigns low temperature smoke of tobacco and more makes fragrant and sweet profit, is saturated abundant, lasting fragrance, and flavoring tow stick preparation process Simply, qualification rate is high, production cost is low, stability is good.
The present invention is achieved by the following technical programs:
The present invention provides a kind of additions not to burn the flavoring tow stick in cigarette filter rod in heating, and the cigarette is from filter tip Section is loaded with enrichment essence in the tow stick to the right by filter segment, four Duan Zucheng of temperature descending section, tow stick section and tobacco segment The pelelith of fragrance.
It adds the present invention also provides a kind of in the preparation method for heating the flavoring tow stick in the cigarette filter rod that do not burn, Be characterized in that the following steps are included:
1) selection: specific surface area is selected to be greater than 20m2The pelelith of/g is as substrate, and sieving, choosing mesh number is 10~35 Pelelith 9~15;
Preferably, the pelelith specific surface area of the selection is 25m2/ g or so, mesh number are 18~20, and grain diameter is 0.5~2mm, it is furthermore preferred that pelelith grain diameter is 1mm or so.
2) attached perfume (or spice): making essence spice for cigarette uniform adsorption in the porous channel of pelelith particle, and it is fragrant that enrichment essence is made The pelelith particle of material;
Preferably, the attached fragrant rate control of the pelelith particle is 20~35%, attached perfume weight 2mg.Wherein, attached fragrant rate Weight before=(weight before the attached perfume of weight-after attached perfume)/attached perfume.
3) flavoring tow stick forms: the tow stick of one segment length about 1~3cm of preparation or so, and pelelith particle is uniform Distribution be added in the tow stick form to get.
Preferably, in the preparation of the tow stick, tow stick length about 2cm or so is produced, adds 9~12 peleliths Particle is uniformly distributed wherein.
Preferably, the tow stick of stating is cellulose acetate filter rod.
Essence spice for cigarette of the present invention preferably is selected from ethylmaltol, the different Fu Er ketone of oxidation, β-damascone, huge One of three ketenes of beans, jujube tincture, ethyl acetate, vanillic aldehyde, citric acid are a variety of.
Due to heating the special construction of cigarette that do not burn, about 200~400 DEG C of the temperature of tobacco segment, passing through temperature descending section After cooling, about 30~50 DEG C of the temperature of nearly lip end filter segment, traditionally flavors and fragrances or addition exist in tobacco segment or addition In the filter tip of nearly lip end, but there is its disadvantage.It has no and has been reported that by essence addition, the present invention is in tobacco segment and cooling in tobacco front end One section of flavoring tow stick is added between section, due to without special cooling device, this section of temperature control about 100~ 200 DEG C, the pelelith that tow stick section at such a temperature is loaded with absorption flavors and fragrances has following clear superiority:
1. if directly contacting the heating rod of high temperature or the annular of high temperature due to tobacco segment flavors and fragrances is placed in tobacco segment Heated wall, essence are prone to cracking and generate bad suction taste, and to will lead to essence release too fast for excessively high temperature, so that suction Shi Qianhou sections of suction taste differences are excessive.If flavors and fragrances is enriched in pelelith and is loaded in tow stick section, not due to tow stick Heating device is contacted, while flavors and fragrances is not susceptible to cracking under moderate moisture, also can get the volatilization sustained release of essence.
If 2. flavors and fragrances is placed in nearly lip end filter segment, since filter segment temperature is lower, the slightly higher flavors and fragrances of boiling point It is difficult to discharge, and the rate of transform is lower.The flavoring tow stick that the present invention adds can load the higher flavors and fragrances of boiling point, to mention The high various selective of essence, meets the rich of flue gas, simultaneously as pelelith particle, far from lip end, particle is not easy Suck human body.
In conclusion the present invention is not burnt the one section of special flavoring tow stick tool added in cigarette filter rod in traditional heating There is above-mentioned more and practical value, there are no disclosed report and application in similar product.The present invention for the first time will Flavors and fragrances is added between the tobacco segment and temperature descending section of moderate temperature, and the flavoring model comparision is special, has novelty, more existing There is perfuming method to have improved multinomial effect, there is centainly perspective and very wide in heating cigarette field of not burning Application prospect.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Main portions explanation:
1- filter segment;
2-- temperature descending section;
3- tow stick section;
4- pelelith particle;
5- tobacco segment.
Specific embodiment
The present invention is described in further detail combined with specific embodiments below.But this should not be interpreted as in the present invention The range for stating theme is only limitted to embodiment below, all that model of the invention is belonged to based on the technology that the content of present invention is realized It encloses.
In order to prove flavoring mode of the invention better than traditional flavoring mode, in embodiment selected flavors and fragrances be plus Commonly used by the hot cigarette that do not burn, boiling point distribution is at 30~300 DEG C.
Embodiment 1
The cigarette containing flavoring tow stick is prepared by the following method, comprising the following steps:
1) selection: selection specific surface area is 30~35m2/ g, mesh number are 14~18, and grain diameter is 0.8mm or so volcano 9, stone are used as substrate;
2) attached perfume (or spice): take ethylmaltol, the different Fu Er ketone of oxidation, β-damascone, ethyl acetate, vanillic aldehyde by 20:3: The weight ratio of 2:2:30 is uniformly mixed, and pelelith particle is added, and impregnating 48h adsorbs fragrance, and spiced pelelith is made, attached Fragrant weight 2mg, attached perfume rate 22.6%;
3) Flavoring filter section forms: the cellulose acetate filter rod that one segment length of preparation is 3cm, and by 9 attached fragrant peleliths Grain, which is uniformly distributed to be added in the tow stick, to be formed;
4) cigarette forming: being made heating using the flavoring tow stick and do not burn cigarette finished product, the cigarette from filter segment to the right By filter segment, four Duan Zucheng of temperature descending section, tow stick section and tobacco segment.
Embodiment 2
The cigarette containing flavoring tow stick is prepared by the following method, comprising the following steps:
1) selection: selection specific surface area is 20~25m2/ g, mesh number are 18~20, and grain diameter is 1mm or so pelelith 12 are used as substrate;
2) attached perfume (or spice): take ethylmaltol, the different Fu Er ketone of oxidation, β-damascone, jujube tincture, citric acid by 20:3:2:2: 15 weight ratio is uniformly mixed, and pelelith particle is added, and impregnating 48h adsorbs fragrance, and spiced pelelith, attached fragrant weight is made Measure 2mg, attached perfume rate 22.3%;
3) Flavoring filter section forms: the cellulose acetate filter rod that one segment length of preparation is 1cm, and by 12 attached fragrant peleliths Grain, which is uniformly distributed to be added in the tow stick, to be formed;
4) cigarette forming: being made heating using the Flavoring filter and do not burn cigarette finished product, the cigarette from filter segment to the right by Filter segment, four Duan Zucheng of temperature descending section, tow stick section and tobacco segment.
Embodiment 3
The cigarette containing flavoring tow stick is prepared by the following method, comprising the following steps:
1) selection: selection specific surface area is 20~25m2/ g, mesh number are 18~20, and grain diameter is the volcano of 1mm or so 12, stone are used as substrate;
2) attached perfume (or spice): take ethylmaltol, Megastigmatrienone, β-damascone, ethyl acetate in 20:3:5:2 ratio It is uniformly mixed, pelelith particle is added, impregnating 48h adsorbs fragrance, and spiced pelelith, attached perfume weight 2mg, attached perfume (or spice) is made Rate 26.4%;
3) flavoring tow stick section forms: the cellulose acetate filter rod that one segment length of preparation is 2cm, and by 12 attached fragrant peleliths Particle is uniformly distributed to be added in the tow stick and form;
4) cigarette forming: being made heating using the flavoring tow stick and do not burn cigarette finished product, the cigarette from filter segment to the right By filter segment, four Duan Zucheng of temperature descending section, tow stick section and tobacco segment.
Embodiment 4
The cigarette containing flavoring tow stick is prepared by the following method, comprising the following steps:
1) selecting specific surface area is 20~25m2/ g, mesh number are 18~20, and grain diameter is pelelith 12 of 1mm or so As substrate.
2) it attached perfume (or spice): takes ethylmaltol, the different Fu Er ketone of oxidation, vanillic aldehyde to be uniformly mixed in the ratio of 15:5:20, fire is added Mountain stone particle, impregnating 48h adsorbs fragrance, and spiced pelelith, attached perfume weight 2.2mg, attached perfume rate 24.6% is made;
3) flavoring tow stick section forms: the cellulose acetate filter rod that one segment length of preparation is 2cm, and by 12 attached fragrant peleliths Particle is uniformly distributed to be added in the tow stick and form;
4) cigarette forming: being made heating using the flavoring tow stick and do not burn cigarette finished product, the cigarette from filter segment to the right By filter segment, four Duan Zucheng of temperature descending section, tow stick section and tobacco segment.
Comparative example 1
Cigarette is prepared by the following method, comprising the following steps:
1) selecting specific surface area is 20~25m2/ g, mesh number are 18~20, and grain diameter is pelelith 12 of 1mm or so As substrate.
2) it attached perfume (or spice): takes ethylmaltol, the different Fu Er ketone of oxidation, vanillic aldehyde to be uniformly mixed in the ratio of 15:5:20, fire is added Mountain stone particle, impregnating 48h adsorbs fragrance, and spiced pelelith, attached perfume weight 1.8mg, attached perfume rate 20.6% is made;
3) flavoring tow stick section forms: the cellulose acetate filter rod that one segment length of preparation is 2cm, and by 12 attached fragrant peleliths Particle is uniformly distributed to be added in the tow stick and form;
4) cigarette forming: being made heating using the flavoring tow stick and do not burn cigarette finished product, the cigarette from filter segment to the right By three Duan Zucheng of filter segment, tow stick section and tobacco segment.
By the heating being prepared according to Examples 1 to 4 and comparative example 1 do not burn cigarette carry out sensory effects evaluation.
Evaluation method: being smoked panel test by a five people groups, heating do not burn cigarette sensory effects evaluation mainly for Its aroma quality, perfume quantity, sweet sense, the sense of miscellaneous thorn and five indexs of fragrance stability score respectively, then calculate total score and ask flat Mean value, point system are shown in Table 1, and evaluation result is shown in Table 2.
1 standards of grading of table
2 evaluation result of table
Above-described embodiment is only more excellent embodiment of the invention, is implemented according to the technical essence of the invention to above Any simple modification and alternate variation that example is made, belong to technical solution of the present invention range.

Claims (6)

1. a kind of addition is not burnt the flavoring tow stick in cigarette filter rod in heating, it is characterised in that the cigarette from filter segment to The right side is loaded with enrichment flavors and fragrances in the tow stick by filter segment, four Duan Zucheng of temperature descending section, tow stick section and tobacco segment Pelelith.
2. according to claim 1 add in the preparation method for heating the flavoring tow stick in the cigarette filter rod that do not burn, It is characterized in that the described method comprises the following steps:
1) selection: specific surface area is selected to be greater than 20m2The pelelith of/g is as substrate, and by sieving, choosing mesh number is 10~35 Pelelith 9~15;
2) attached perfume (or spice): making essence spice for cigarette uniform adsorption in the porous channel of pelelith particle, and enrichment flavors and fragrances is made Pelelith particle;
3) flavoring tow stick forms: the tow stick of one segment length about 1~3cm of preparation or so, and pelelith particle is added to this In tow stick form to get.
3. it is not burnt the preparation method of the flavoring tow stick in cigarette filter rod according to addition described in claims 2 in heating, It is characterized in that the tow stick is cellulose acetate filter rod.
4. according to claim 2 add in the preparation method for heating the flavoring tow stick in the cigarette filter rod that do not burn, It is characterized in that the granular size that pelelith described in the step 1) is chosen is 0.5~2mm.
5. according to claim 2 add in the preparation method for heating the flavoring tow stick in the cigarette filter rod that do not burn, It is characterized in that essence spice for cigarette used in pelelith is selected from ethylmaltol, the different Fu Er ketone of oxidation, β-damascone, huge One of three ketenes of beans, jujube tincture, ethyl acetate, vanillic aldehyde, citric acid are a variety of.
6. according to claim 2 add in the preparation method for heating the flavoring tow stick in the cigarette filter rod that do not burn, It is characterized in that in the step 3) that tow stick length is 1~3cm, the attached fragrant rate of pelelith particle is controlled 20~35%.
CN201910600458.3A 2019-07-04 2019-07-04 It is a kind of to add in the flavoring tow stick and preparation method thereof heated in the cigarette filter rod that do not burn Pending CN110226775A (en)

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Cited By (5)

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CN110537728A (en) * 2019-09-25 2019-12-06 杨成云 Polylactic acid tow forming filter tip stick fragrance sheet and forming equipment and process
CN112205666A (en) * 2020-11-19 2021-01-12 云南纯旭生物科技有限公司 A cigarette containing Arecae semen component and capable of being heated without burning
CN113088389A (en) * 2021-04-08 2021-07-09 武汉黄鹤楼香精香料有限公司 Water-soluble dropping pill prepared from porous material and preparation method thereof
CN113455699A (en) * 2021-07-12 2021-10-01 河南中烟工业有限责任公司 Heating cigarette with uniform fragrance release amount by mouth
CN114606061A (en) * 2022-04-24 2022-06-10 云南养瑞科技集团有限公司 Sustained-release gel material and preparation method and application thereof

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110537728A (en) * 2019-09-25 2019-12-06 杨成云 Polylactic acid tow forming filter tip stick fragrance sheet and forming equipment and process
CN110537728B (en) * 2019-09-25 2024-03-01 杨成云 Polylactic acid tow forming filter rod fragrant sheet, forming equipment and process
CN112205666A (en) * 2020-11-19 2021-01-12 云南纯旭生物科技有限公司 A cigarette containing Arecae semen component and capable of being heated without burning
CN113088389A (en) * 2021-04-08 2021-07-09 武汉黄鹤楼香精香料有限公司 Water-soluble dropping pill prepared from porous material and preparation method thereof
CN113455699A (en) * 2021-07-12 2021-10-01 河南中烟工业有限责任公司 Heating cigarette with uniform fragrance release amount by mouth
CN114606061A (en) * 2022-04-24 2022-06-10 云南养瑞科技集团有限公司 Sustained-release gel material and preparation method and application thereof
CN114606061B (en) * 2022-04-24 2023-07-25 云南养瑞科技集团有限公司 Sustained-release gel material and preparation method and application thereof

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Application publication date: 20190913