CN105029678A - Tobacco composite additive and application thereof - Google Patents
Tobacco composite additive and application thereof Download PDFInfo
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- CN105029678A CN105029678A CN201510440459.8A CN201510440459A CN105029678A CN 105029678 A CN105029678 A CN 105029678A CN 201510440459 A CN201510440459 A CN 201510440459A CN 105029678 A CN105029678 A CN 105029678A
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- cigarette
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Abstract
The invention provides a tobacco additive for improving the smoking quality of cigarettes and application thereof. The tobacco composite additive is composed of, by mass, 5%-10% of smoking flavor adjusting matter and 90%-95% of combustion adjusting agents. The smoking flavor adjusting matter is combined by sucrose octaacetate and amino acid. The amino acid is formed by combining one or more of asparagine, alanine and proline. The combustion adjusting agents are formed by combining two or more of magnesium lactate, potassium lactate, magnesium acetate and potassium acetate. The tobacco composite additive is applied to cigarette paper or tobacco rods, the fragrance amount and fragrance concentration of the cigarettes can be improved, the smoking fragrance is enriched, foreign smell is reduced, the cigarette combustion speed is adjusted, and the sensory quality of the cigarettes is improved effectively.
Description
Technical field
The present invention relates to Field of Tobacco, more specifically, relate to and a kind ofly improve the tobacco compound additive of cigarette smoking quality and the application in tobacco thereof.
Background technology
Tar is owing to producing after the material burn incompletely in tobacco leaf.Bitting midges mainly comes from cigarette and burns and sucks some chemical analysis in the tar and flue gas produced in process, as harmful substances such as CO, hydrogen cyanide, crotonaldehyde, BaP, dibenzanthracene, nitrosamines material and some nitrogen heterocyclics, therefore, reduce the harm key of smoking to health to be to reduce the harmful substance contents in flue gas.
China's cigarette is based on traditional flue-cured tobacco, and the sugar content of flue-cured tobacco is higher, and the tar content reducing cigarette product is the important content of tobacco research.Along with to the growing interest of cigarette consumption person to health, the research and development of low-coke tar cigarette product are the inexorable trends of tobacco business development.Reducing cigarette tar and reducing method generally can be divided into Physical and chemical method, and Physical is mainly realized by the dilution rate or filtering rod that improve cigarette; Chemical method mainly adds chemicals and carries out chemistry and fall Jiao in tobacco or in cigarette material, its effect comprises the effects such as absorption, combustion-supporting and catalysis, while reduction tar, and the also corresponding reduction of the aroma substance in flue gas, thus the pumped mass of reduction cigarette.
Because in low-coke tar cigarette, the content of T/N is lower, cause cigarette fragrance thin out, excitant increases, and flue gas is roughening.Compensating aroma problem oneself seem comparatively outstanding, especially for all the more so the tobacco business that China's Virginian-type cigarette accounts for more than 95%.Cigarette being carried out to the tobacco additive agent of compensating aroma, by adding this tobacco additive agent in pipe tobacco, cigarette paper, tobacco sheets by paper making method or other auxiliary material, effectively can compensate the loss of aroma of low-coke tar cigarette, and then improve the pumped mass of cigarette.Additive cigarette being carried out to compensating aroma requires higher, should free from extraneous odour, can play again and cover the effect that xylon gas, enrichment cigarette are fragrant, coordinate flue gas acid-base balance.
Perfuming cigarette needs blending researcher to know attribute and the compatibility each other of each perfume material, and long-term smell of powder accumulation of smokeing panel test.For a long time, additive of tobacco product field is mainly studied on the pipe tobacco that concentrates in cigarette product, very few to the research of cigarette paper perfuming aspect.
Summary of the invention
The object of the present invention is to provide a kind of tobacco additive agent improving cigarette smoking quality, its effective coordination flue gas acid-base balance, covers xylon gas, reduces and stimulates, and increases aroma quality and perfume quantity, improves cigarette smoking quality.
In order to realize foregoing invention object, the technical solution used in the present invention is:
One grows tobacco compound additive, and the component calculated by following mass percent forms: 5% ~ 10% inhales taste Auto-regulator and 90% ~ 95% combustionregulator; Described suction taste Auto-regulator is sucrose octaacetate and combination of amino acids, and described amino acid is selected from one or more the combination in asparagine, alanine, proline; Described combustionregulator is two or more combination in magnesium lactate, potassium lactate, magnesium acetate, potassium acetate.
Suction taste Auto-regulator of the present invention is two or more combination in sucrose octaacetate, asparagine, alanine, proline, described suction taste Auto-regulator is a kind of Studies of The Aromatic Substances of diving, itself does not have fragrance or little on fragrance impact, but pyrolysis important flavor matter can be produced in the process of burning, as flavor matters such as Pyrazine, Fructus Hordei Germinatus phenols, and the fragrance fragment of cigarette odor-absorbing can be improved, it has some special aroma, can coordinate with cigarette perfume, enriches odor characteristic to a certain extent and comprehensively improves cigarette smoking quality.
Combustionregulator of the present invention is two or more combination in magnesium lactate, potassium lactate, magnesium acetate, potassium acetate.Described combustionregulator effectively can regulate the burn rate of cigarette, and then changes the content of cigarette smoke chemical substance, thus affects the aesthetic quality of cigarette.
Preferably, described suction taste Auto-regulator is one or more the combination in sucrose octaacetate and asparagine, alanine, proline.
More preferably, in described suction taste Auto-regulator, the mass percent of described sucrose octaacetate is 50 ~ 60%.
Preferably, the component calculated by following mass percent forms: 5% inhales taste Auto-regulator and 95% combustionregulator.
Tobacco compound additive of the present invention has wide range of applications, and both can be applicable on cigarette paper, also can be applicable in cigarette shreds or tobacco sheets by paper making method.
Another object of the present invention is applied in cigarette paper and cigarette shreds by tobacco compound additive.
Being applied as in cigarette paper: according to the existing production equipment of cigarette paper, production technology is carried out with slurry, copy paper.In cigarette paper coating Process of Applying Glue, this tobacco compound additive is mixed with the aqueous solution that mass percentage concentration is 30% ~ 50%, this aqueous solution is coated on cigarette paper, the mode that addition manner chooses coating or dipping according to product type carries out single or double applying glue, and then requires that drying rear point is cut to cigarette paper according to papermaking common process.
Described tobacco compound additive accounts for 0.5% ~ 5.0% of cigarette paper dry weight, and preferably, the quality of described tobacco compound additive is 0.8% ~ 2.5% of cigarette paper dry weight.
In the application preparing cigarette shreds, the ratio of described tobacco compound additive in cigarette shreds is 0.5% ~ 8.0% of cigarette shreds dry weight.Preferably, the ratio of described tobacco compound additive in cigarette shreds is 1.0% ~ 3.0% of cigarette shreds dry weight.
Tobacco compound additive of the present invention is applied in the pumped mass that cigarette paper and cigarette shreds effectively can promote cigarette, carry out sensory evaluating smoking's result to the cigarette that with the addition of tobacco compound additive of the present invention to show, compared with control sample, cigarette smoking style is unchanged, perfume quantity obviously increases, and the fine and smooth soft degree of flue gas increases, and assorted gas diminishes, stimulation degree reduces, and oral cavity comfort level significantly improves.
Carry out thermal cracking analysis to the cigarette paper adding tobacco compound additive of the present invention, result shows, the major cleavage products under condition of different temperatures is aldehyde ketone, furans, condensed-nuclei aromatics compounds.Compared with contrast sample, the harmful substances such as the crotonaldehyde of cigarette paper at high temperature cracking prepared by the method for the invention, aldehydes, benzene class, indenes class and condensed-nuclei aromatics class reduce, and ketone, furans, phenols increase, and the flavor matter such as furfuryl alcohol, lactone content increases.
Compared with prior art, the invention has the beneficial effects as follows:
Tobacco compound additive of the present invention, by reasonably combined suction taste Auto-regulator and combustionregulator, can effective coordination flue gas acid-base balance, cover xylon gas, reduce and stimulate, increase aroma quality and perfume quantity, improve cigarette smoking quality.Described tobacco compound additive is applied in cigarette paper or cigarette shreds, perfume quantity and the fragrance level of cigarette can be promoted, enrich cigarette perfume (or spice), reduce assorted gas, regulate cigarette burn rate, effectively promote the aesthetic quality of cigarette.
Detailed description of the invention
Further describe the present invention by following specific embodiment, should be appreciated that specific embodiment described herein only for explaining the present invention, being not intended to limit the present invention, in the scope that can limit in right of the present invention, carry out various change.
In embodiment and comparative example, pipe tobacco homogeneous phase used is all the classical pipe tobacco of double happiness, purchased from Guangdong China Tobacco Industry Co., Ltd.It should be added that, for the sensory evaluation of cigarette, pipe tobacco is main contributor, and compound additive on the basis of the contribution to pipe tobacco, can bring lifting.Therefore, there is not comparative sense in the sensory evaluation between different pipe tobaccos.
comparative example
Get 1000kg paper pulp (containing filler), after stirring, obtain cigarette paper finished product according to cigarette paper conventional production process, cigarette paper is quantitatively 30.1g/m
2, air permeance for cigarette paper is 51.3CU.
embodiment 1
Get 1000kg paper pulp (containing filler), after stirring, conveniently technique carries out copy paper with slurry.In cigarette paper size application stage, get sucrose octaacetate 0.5kg, asparagine 0.3kg, proline 0.2kg, magnesium lactate 2kg, potassium lactate 5kg, potassium acetate 2kg, be dissolved in 100kg distilled water, after stirring, form settled solution, adopt coating method to carry out one side applying glue interpolation.Dry after applying glue, obtain cigarette paper finished product according to cigarette paper conventional production process, cigarette paper is quantitatively 30.2g/m
2, air permeance for cigarette paper is 50.6CU.
embodiment 2
Preparation method is identical with embodiment 1, the component of additive is as different from Example 1: sucrose octaacetate 0.5kg, asparagine 0.3kg, alanine 0.2kg, magnesium lactate 2.5kg, potassium lactate 5kg, potassium acetate 1.5kg, the technical parameter of obtained cigarette paper is in table 1.
embodiment 3
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose octaacetate 0.6kg, asparagine 0.2kg, alanine 0.2kg, magnesium lactate 3kg, potassium lactate 6kg, the technical parameter of obtained cigarette paper is in table 1.
embodiment 4
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose octaacetate 0.5kg, asparagine 0.25kg, alanine 0.25kg, potassium acetate 5kg, magnesium acetate 4kg.The technical parameter of obtained cigarette paper is in table 1.
embodiment 5
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose octaacetate 0.2kg, asparagine 0.1kg, proline 0.2kg, potassium lactate 6.5kg, magnesium lactate 2.5kg.The technical parameter of obtained cigarette paper is in table 1.
embodiment 6
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose octaacetate 0.3kg, asparagine 0.1kg, proline 0.1kg, potassium lactate 5.5kg, magnesium lactate 2.5kg, potassium acetate 1.0k.The technical parameter of obtained cigarette paper is in table 1.
embodiment 7
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose octaacetate 0.5kg, asparagine 0.3kg, proline 0.3kg, magnesium lactate 2kg, potassium lactate 5kg, potassium acetate 2kg.The technical parameter of obtained cigarette paper is in table 1.
embodiment 8
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose octaacetate 0.7kg, asparagine 0.5kg, alanine 0.3kg, potassium acetate 5kg, magnesium acetate 4kg.The technical parameter of obtained cigarette paper is in table 1.
comparative example 1
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: sucrose 0.5kg, asparagine 0.2kg, niacinamide 0.1kg, proline 0.2kg, magnesium lactate 2kg, potassium lactate 5kg, potassium acetate 2kg.The technical parameter of obtained cigarette paper is in table 1.
comparative example 2
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: glucose ester 0.5kg, asparagine 0.2kg, niacinamide 0.1kg, proline 0.2kg, magnesium lactate 2kg, potassium lactate 5kg, potassium acetate 2kg.The technical parameter of obtained cigarette paper is in table 1.
comparative example 3
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: vitamin B6 0.2kg, nicotinic acid 0.1kg, proline 0.2kg, potassium citrate 6.5kg, potassium acetate 2.5kg.The technical parameter of obtained cigarette paper is in table 1.
comparative example 4
Preparation method is identical with embodiment 1, and the component of additive is as different from Example 1: nicotinic acid 0.15kg, proline 0.25kg, potassium lactate 6.5kg, potassium acetate 2.5kg.The technical parameter of obtained cigarette paper is in table 1.
Get the cigarette paper prepared by above-described embodiment and comparative example and do not add the cigarette paper of additive of the present invention for contrast sample, the technical parameter of each cigarette paper is in table 1.When pipe tobacco is identical with other cigarette material, cigarette paper is made the cigarette finished product of same size.
Table 1 cigarette paper technical parameter and cigarette specification
Method of smokeing panel test, with reference to the evaluation method of tobacco business standard YC/T138-1998 " tobacco and tobacco product sensory evaluation method ", is carried out sensory evaluating smoking to above-mentioned cigarette, be the results are shown in Table 2.As known from Table 2, compared with control sample, cigarette style characteristic is unchanged, and perfume quantity obviously increases, and the fine and smooth soft degree of flue gas increases, and assorted gas diminishes, and stimulate degree to reduce, oral cavity comfort level significantly improves, and cigarette sense organ integrate score promotes obviously.
Table 2 cigarette sensory evaluating smoking score
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without the need to also giving all embodiments.All any amendments done within the spirit and principles in the present invention, equivalent to replace and improvement etc., within the protection domain that all should be included in the claims in the present invention.
Claims (9)
1. one to grow tobacco compound additive, it is characterized in that, the component calculated by following mass percent forms: 5% ~ 10% inhales taste Auto-regulator and 90% ~ 95% combustionregulator; Described suction taste Auto-regulator is sucrose octaacetate and combination of amino acids, and described amino acid is selected from one or more the combination in asparagine, alanine, proline; Described combustionregulator is one or more combinations in magnesium lactate, potassium lactate, magnesium acetate, potassium acetate.
2. tobacco compound additive according to claim 1, is characterized in that, in described suction taste Auto-regulator, the mass percent of described sucrose octaacetate is 50 ~ 60%.
3. tobacco compound additive according to claim 1, is characterized in that, the component calculated by following mass percent forms: 5% inhales taste Auto-regulator and 95% combustionregulator.
4. the tobacco compound additive described in any one of claim 1 ~ 3 is preparing the application in cigarette paper.
5. application according to claim 4, is characterized in that, the ratio of described tobacco compound additive in cigarette paper is 0.5% ~ 5.0% of cigarette paper dry weight.
6. application according to claim 5, is characterized in that, the ratio of described tobacco compound additive in cigarette paper is 0.8% ~ 2.5% of cigarette paper dry weight.
7. the tobacco compound additive described in any one of claim 1 ~ 3 is preparing the application in cigarette shreds.
8. application according to claim 7, is characterized in that, the ratio of described tobacco compound additive in cigarette shreds is 0.5% ~ 8.0% of cigarette shreds dry weight.
9. application according to claim 8, is characterized in that, the ratio of described tobacco compound additive in cigarette shreds is 1.0% ~ 3.0% of cigarette shreds dry weight.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106858709A (en) * | 2017-04-17 | 2017-06-20 | 中国烟草总公司郑州烟草研究院 | A kind of amino acid ion liquid of selectivity reducing cigarette crotonaldehyde in mainstream smoke and its application |
CN110934320A (en) * | 2020-01-20 | 2020-03-31 | 中国烟草总公司郑州烟草研究院 | Preparation and application of additive capable of reducing wood gas and irritation of cut stems |
CN111194941A (en) * | 2020-01-14 | 2020-05-26 | 深圳新火瑞升技术有限公司 | Application of heating aid in heating non-combustion smoking material and product |
CN114634890A (en) * | 2022-03-22 | 2022-06-17 | 云南中烟工业有限责任公司 | Azospirillum azotobacter, and separation method and application thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106858709A (en) * | 2017-04-17 | 2017-06-20 | 中国烟草总公司郑州烟草研究院 | A kind of amino acid ion liquid of selectivity reducing cigarette crotonaldehyde in mainstream smoke and its application |
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CN111194941B (en) * | 2020-01-14 | 2022-06-28 | 深圳新火瑞升技术有限公司 | Application of heating aid in heating non-combustion smoking material and product |
CN110934320A (en) * | 2020-01-20 | 2020-03-31 | 中国烟草总公司郑州烟草研究院 | Preparation and application of additive capable of reducing wood gas and irritation of cut stems |
CN110934320B (en) * | 2020-01-20 | 2021-12-24 | 中国烟草总公司郑州烟草研究院 | Preparation and application of additive capable of reducing wood gas and irritation of cut stems |
CN114634890A (en) * | 2022-03-22 | 2022-06-17 | 云南中烟工业有限责任公司 | Azospirillum azotobacter, and separation method and application thereof |
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