CN103054187B - Spice composite particle filter stick and preparation method thereof - Google Patents
Spice composite particle filter stick and preparation method thereof Download PDFInfo
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- CN103054187B CN103054187B CN201210577572.7A CN201210577572A CN103054187B CN 103054187 B CN103054187 B CN 103054187B CN 201210577572 A CN201210577572 A CN 201210577572A CN 103054187 B CN103054187 B CN 103054187B
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Abstract
The invention relates to the technical field of filter sticks and discloses a spice composite particle filter stick. The spice composite particle filter stick comprises a cellulose acetate fiber substrate and molding paper wrapped outside the cellulose acetate fiber substrate, and treated piquancy solid particles are compounded on cellulose acetate fibers. The piquancy solid particles are compounded in the cellulose acetate fibers of the filter sticks, suction resistance produced by the filter sticks is applicable, miscellaneous gas and irritation of smoke can be removed, and taste suction is improved. Cigarette smoke brings spice of the piquancy solid particles out to some extent, abundant and full degree of the smoke is improved, cigarette aroma is strengthened, and simultaneously abundant taste sense experience is produced in the oral cavity.
Description
Technical field
The present invention relates to production of cigarettes technical field, more specifically, relate to a kind of spice composite particles filter stick and preparation method thereof.
Background technology
Generally speaking, carcinogenic composition in cigarette smoke is present in tar more, the number of tar content is also used as the index of cigarette harmfulness size, along with improving constantly of living standard, the continuous lifting of health of people consciousness, " reducing tar and reducing harm " of cigarette becomes the focus of smoker's concern and the study hotspot of the art.
Filter stick plays a part very important in the design of Tar, and the filter tip of cigarette can be held back the granule phase substance matter in flue gas effectively, reduces the tar content that human body is taken in.Cellulose acetate filter rod, as a chief component of cigarette material, has obtained general application.In order to strengthen the absorption property of cellulose acetate filter rod, in filter stick, add complex solid particle.The complex solid particle adding in filter stick is at present mainly the inorganic substances such as active carbon, or the tobacco particle such as offal, expanded cabo, expanded cut tobacco, play and increase the effect such as the adsorption function of filter stick, reduction tar, the direction of research and technological means are all by strengthening filtration and the absorption to main flume.
But according to cigarette blending circle viewpoint, the fragrance matter of cigarette is also in tar, and the content that reduces tar and nicotine just means the taste that reduces tobacco.Can say, the fragrance that how not only reduces tar content in cigarette simultaneously but also do not lose cigarette makes tobacco manufacturing enterprise spend all considering.
And meanwhile, realizing at filter tip the tar content reducing in cigarette does not lose again on the basis of cigarette fragrance simultaneously, further ensure that cigarette product fragrance meets the needs of consumer to strange product, allowing produce the rich and varied sense of taste in cigarette smoke smoker oral cavity and experience, is another important research content of developing new product.
Pungent material mainly refers to plant drying powder or the essential oil with excitant taste that in foodstuff flavouring blending, use.Mankind's ancient times just start using some have irritating pungent plant as medicine for diet, their essential oil content is higher, has strong to be taste, to be fragrant effect, can not only promote appetite, improves flavour of food products, and also has sterilization and anticorrosion function.Present pungent material not only has pulverous but also has goods of essential oil or oleoresin form.
In cigarette filter rod, do not add at present any research report of pungent material particle.
Summary of the invention
The technical problem to be solved in the present invention is the deficiency that overcomes existing filter stick technology, a kind of new composite particles filter stick is provided, effectively realize the tar content reducing in cigarette, be again cigarette flavouring simultaneously, and further provide abundant cigarette product fragrance to meet the pursuit of consumer to cigarette flavor.
Another technical problem that will solve of the present invention is to provide the preparation method of described filter stick.
Goal of the invention of the present invention is achieved by the following technical programs:
A kind of spice composite particles filter stick is provided, comprises acetate fiber base material and be wrapped in the forming paper outside acetate fiber base material, by mass, acetate fiber base material comprises 90～99% acetate fiber and 1～10% treated pungent material solid particle; Described treated pungent material solid particle is scattered on acetate fiber;
Described treated pungent material solid particle is to obtain through constant temperature and humidity balance to constant moisture content after food flavor and pungent material solid particle are mixed in proportion; The consumption of described food flavor is 0.01%～0.1% of pungent material mass of solid particles;
Described pungent material is one or more mixtures of capsicum, ginger, pepper, turmeric, hot red pepper, Chinese prickly ash, chilly or cumin, and the granularity of described pungent material solid particle is 30～200 orders.
Preferably, by mass, acetate fiber base material comprises 95% acetate fiber and 5% treated pungent material solid particle.
Preferably, the consumption of described food flavor is 0.05% of pungent material mass of solid particles.
The preferred peppermint oil of described food flavor, ennel oil or horseradish, more preferably adopt mixture that peppermint oil and ennel oil is mixed to get for 1:1～2 in mass ratio as food flavor of the present invention.The present invention sums up and finds through a large amount of experimental studies, uses peppermint oil and fennel seeds pungent material solid particle to be had to the effect of Titian, lures that the fragrance release of pungent material solid particle is more fully more fragrant sooner into, and the smoke characteristic producing with cigarette burning complements each other.
The granularity of described pungent material solid particle is 20～200 orders, preferably 30～80 orders, and size is suitable adding in filter stick just in time, not only can not stop up the passage of filter stick, affects filter efficiency, nor can be taken out of filter stick by flue gas.Most preferably be 40 orders, on above-mentioned beneficial effect basis, can from filter stick, see intuitively, give brand-new food particle visual effect and the experience of cigarette consumption person.
Preferably, described constant moisture content is 8%～10%.
The present invention provides a kind of preparation method of pungent material composite particles filter stick simultaneously, comprises the following steps:
S1. pungent material particle is pulverized, sieved, obtain pungent material solid particle;
S2. food flavor and pungent material solid particle are mixed to the pungent material solid particle that obtains perfuming;
The pungent material solid particle of the perfuming S3. S2 being obtained is placed into climatic chamber, and balance is to constant moisture content;
S4. S3 gained pungent material solid particle is dispersed on acetate fiber, obtaining load has the cellulose acetate filter rod base material of the pungent material solid particle of perfuming;
S5. by forming paper, cellulose acetate filter rod base material is wrapped up, prepare composite particles filter stick.
Constant moisture content described in S3 is preferably 10%.Equilibration time is preferably 48 hours.
Described in S3, the temperature of Balance Treatment is 22 DEG C.
Beneficial effect of the present invention:
Along with the continuous pursuit of consumer to healthy living, Tar becomes the study hotspot of the art, and cigarette product is constantly focused on reducing tar and reducing harm.But apodeictic, simple simple reducing tar and reducing harm technical scheme makes fragrance and the jealous also loss thereupon of cigarette smoke, and the consumer who makes some like dense smoke feels dissatisfied.The present invention uses the pungent Material Additions such as capsicum, Chinese prickly ash, pepper, horseradish in filter stick, can increase the saturation degree of cigarette smoke.But add and in the design theory of this irritating material, with the art, cigarette is constantly reduced to irritating technical research trend and run counter to, need to sum up accurate adding proportion and processing mode, to obtain the harmony of saturated smoke perfume and flue gas harmony.
Process is to the composition characteristic research of spicy substance and constantly Experimental Comparison analysis, and the present invention sums up and draws, use capsicum, ginger, pepper, turmeric, hot red pepper, Chinese prickly ash, chilly or cumin combination reasonably treatment process can obtain beyond thought beneficial effect.
The present invention creatively adopts reasonable pungent particle after treatment to make an addition in the acetate fiber base material of filter stick, first the present invention has studied optimum particle size range 20～200 orders that pungent particle is combined with acetate fiber, in described particle size range, solve and added the relation between particle, filtering rod, filter efficiency, pungent particle and acetate fiber are brought into play the synergy of absorption well, absorption affinity is high, be conducive to the absorption to tar and other harmful substances, effectively realize the tar content reducing in cigarette; Under described particle size range condition, the present invention is through constantly analyzing contrast and experimental study, further sum up perfuming and the moisture equilibration technical scheme of pungent particle, the pungent particle of processing through the present invention makes an addition in filter stick, cigarette is in the time of suction, the flue gas producing extracts the pungent fragrant pungency component band of treated pungent particle, in enriching cigarette note, in oral cavity, producing the rich and varied sense of taste experiences, the excitant producing is liked within the degree of accepting consumer, has significant stimulating effect.
Under the adding technique scheme providing in invention, the resistance to suction that filter stick produces is suitable, can remove better assorted gas and excitant in flue gas, improve the fine and smooth degree of flue gas, there is improved action to inhaling taste, significantly increase cigarette flavor richness and saturation degree, modified smoke behavior and concentration, can improve the shortcoming of falling burnt cigarette flavor after treatment, concentration deficiency simultaneously.
Brief description of the drawings
Fig. 1 is the binary composite particles filter stick of embodiment 3.
Detailed description of the invention
Further describe the present invention below in conjunction with specific embodiment.
Embodiment 1
S1. granulation: by capsicum, ginger, pepper crushed after being dried, excessively mix according to the mass ratio of 1:0.5:1 after 20 mesh sieves respectively, obtain spice (pungent) solid particle;
S2. disperse: 10% the ratio that accounts for acetate fiber quality according to S1 gained solid particle by solid particle be dispersed in common after shredding cigarette for acetate tow (commercial) upper, obtain containing composite particles tow;
S5. moulding: adopt composite particles filter stick formation paper that solid particle tow parcel is prepared into composite particles filter stick.
Adopt GB/T19609-2004(to adopt conventional analysis, smoking machine is measured tar) method carries out flue gas analysis to filter stick and shows, the cigarette that employing contains spice (pungent) solid particle filter stick, compare the cigarette of common cigarette acetate tow filter stick, the tar content 5%(that can effectively reduce in flue gas is that 10mg tar reduces 0.5mg).The filter stick that the present embodiment provides, foodstuff solid particle and acetate tow are brought into play collaborative suction-operated, are conducive to the absorption to tar and other harmful substances.Note: filter stick need be made complete cigarette just can carry out tar mensuration.
Employing equal length (120mm) contains spice (pungent) solid particle filter stick and common cigarette acetate tow filter stick carries out filtering rod test through resistance to suction tester (Suo Ding D49+D49X8 type SODIM testboard), assay method is with reference to existing routine, in the time that the flow steady air flow that is 17.5ml/s is flowed through filter stick, the pressure differential at filter stick two ends is filtering rod.
After tested: common filter stick pressure drop 3080Pa, spice (pungent) solid particle 2995Pa.
Adopt the present embodiment spice (pungent) solid particle to be compound in the acetate fiber of filter stick, compare common cellulose acetate filter rod, the resistance to suction that the present embodiment filter stick produces is more suitable, and pungent class note is outstanding, improve the fragrance degree of saturation of flue gas, have improved action to inhaling taste.
The present embodiment is used the cigarette that contains foodstuff solid particle filter stick and common cigarette the cigarette of acetate tow filter stick, transfers to 10 professional members of smoking to smoke panel test, and smoking result is in shown in table 1 and table 2:
Table 1
| Cigarette sample | Sensory evaluation |
| Common fiber tow filter rods | Cigarette perfume (or spice) is main, and perfume quantity is general, and assorted gas slightly appears, and flue gas is more coarse, slightly stimulates |
| Spice particle filter stick | Perfume quantity and richness increase, and assorted gas is covered to effect, and there is stronger pungent material aftertaste in oral cavity, stimulates slightly and increases |
Table 2
In cigarette filter rod acetate fiber, add simply the pungent particle of pungent perfume (or spice), the granularity of particle is suitable, cigarette smoke extracts the pungent band of foodstuff solid particle to a certain extent, in enriching cigarette note, can modify smoke behavior, in oral cavity, produce the distinctive excitant of capsicum, there is certain stimulating effect, and aftertaste sense is rich and varied, but the harmony of entirety does not have remarkable improvement, it is slightly poor that excitant is also compared the common filter stick of ratio, estimates that the excitant non-consumer of the present embodiment cigarette is liked in the degree of accepting.
Embodiment 2
S1. granulation: by capsicum, ginger, pepper crushed after being dried, excessively mix according to the mass ratio of 1:0.5:1 after 20 mesh sieves respectively, obtain spice (pungent) solid particle;
S2. perfuming processing: with 0.1% the ratio that accounts for spice (pungent) mass of solid particles, food flavor peppermint oil is added in described solid particle, mix;
S3. balance: solid particle after treatment S2 is placed into climatic chamber equilibrium water conten 48 hours, makes its moisture content be about 10%;
S4 disperses: 5% the ratio that accounts for acetate fiber quality according to the described solid particle after equilibrium water conten by solid particle be dispersed in common after shredding cigarette for acetate tow (commercial) upper, obtain containing composite particles tow;
S5 moulding: adopt composite particles filter stick formation paper that solid particle tow parcel is prepared into composite particles filter stick.
Adopt GB/T19609-2004(to adopt conventional analysis, smoking machine is measured tar) method carries out flue gas analysis to filter stick and shows, the cigarette that employing contains spice (pungent) solid particle filter stick, compare the cigarette of common cigarette acetate tow filter stick, the tar content 5%(that can effectively reduce in flue gas is that 10mg tar reduces 0.5mg).The filter stick that the present embodiment provides, spice (pungent) solid particle and acetate tow are brought into play collaborative suction-operated, are conducive to the absorption to tar and other harmful substances.Note: filter stick need be made complete cigarette just can carry out tar mensuration.
Employing equal length (120mm) contains foodstuff solid particle filter stick and common cigarette acetate tow filter stick carries out filtering rod test through resistance to suction tester (Suo Ding D49+D49X8 type SODIM testboard), assay method is with reference to existing routine, in the time that the flow steady air flow that is 17.5ml/s is flowed through filter stick, the pressure differential at filter stick two ends is filtering rod.
After tested: common filter stick pressure drop 3080Pa, spice (pungent) solid particle composite filter 2995Pa.
The present embodiment is compound to these solid particles in the acetate fiber base material of filter stick, compare common cellulose acetate filter rod, the resistance to suction that the present embodiment filter stick produces is suitable, note abundance and saturation degree obviously strengthen, pungent class note is outstanding, can cover preferably the assorted gas in flue gas, improve the fine and smooth degree of flue gas, have improved action to inhaling taste.
The present embodiment will contain the cigarette of spice (pungent) solid particle filter stick and the cigarette of common cigarette acetate tow filter stick, transfer to 10 professional members of smoking to smoke panel test, and smoking result is in shown in table 3 and table 4:
Table 3
| Cigarette sample | Sensory evaluation |
| Common fiber tow filter rods | Cigarette perfume (or spice) is main, and perfume quantity is general, and assorted gas slightly appears, and flue gas is more coarse, slightly stimulates |
| Spice particle filter stick | Perfume quantity, richness and saturation degree obviously increase, and flue gas is finer and smoother soft, and assorted gas is covered to effect, and there is stronger pungent material aftertaste in oral cavity, and excitant is faint |
Table 4
The cigarette that contains capsicum, ginger, pepper particle filter stick, flue gas is finer and smoother soft, illustrates that adding particle has played modification smoke behavior, covers the effect of assorted gas, meanwhile, cigarette note is abundant, and the saturation degree of fragrance increases, and produces the distinctive sense of taste of spicy substance and impact in oral cavity, aftertaste sense is rich and varied, so member of smoking does not provide the scoring of bad excitant, provides on the contrary good excitant mark, illustrate that filter stick of the present invention takes like a shot for consumer.
Embodiment 3
S1. granulation: pulverized 40 mesh sieves after Chinese prickly ash, hot red pepper are mixed according to the mass ratio of 1:1, and obtained pungent solid particle;
S2. perfuming processing: 1% the ratio with pungent mass of solid particles adds food flavor in S1 gained solid particle, mixes; Food flavor is the mixture that peppermint oil and ennel oil are mixed to get for 1:1 in mass ratio;
S3. balance: S2 gained solid particle is placed into climatic chamber equilibrium water conten 48 hours, makes its moisture content be about 10%;
S4. disperse: the ratio that accounts for acetate fiber quality 5% according to the described solid particle after equilibrium water conten by solid particle be dispersed in common after shredding cigarette for acetate tow (commercial) upper, obtain containing composite particles tow;
S5. moulding: adopt composite particles filter stick formation paper that solid particle tow parcel is prepared into composite particles filter stick.
Adopt GB/T19609-2004(to adopt conventional analysis, smoking machine is measured tar) method carries out flue gas analysis to filter stick and shows, the cigarette that employing contains pungent solid particle filter stick, compare the cigarette of common cigarette acetate tow filter stick, the tar content 3%(that can effectively reduce in flue gas is that 10mg tar reduces 0.3mg).The filter stick that the present embodiment provides, pungent solid particle and acetate tow are brought into play collaborative suction-operated, are conducive to the absorption to tar and other harmful substances.Note: filter stick need be made complete cigarette just can carry out tar mensuration.
Employing equal length 120mm contains pungent solid particle filter stick and common cigarette acetate tow filter stick carries out filtering rod test through resistance to suction tester (Suo Ding D49+D49X8 type SODIM testboard), assay method is with reference to existing routine, in the time that the flow steady air flow that is 17.5ml/s is flowed through filter stick, the pressure differential at filter stick two ends is filtering rod.
After tested: common filter stick pressure drop 3080Pa, pungent solid particle composite filter 3012Pa.
The present embodiment is compound to pungent solid particle in the acetate fiber base material of filter stick, compare common cellulose acetate filter rod, the resistance to suction that the present embodiment filter stick produces is suitable, pungent class note obviously promotes, can remove preferably the assorted gas in flue gas, improve the soft degree of flue gas, increase the light spicy taste perception in oral cavity, use peppermint oil and fennel seeds pungent material solid particle to be had to the effect of Titian, the fragrance release of luring pungent material solid particle into is more fully more fragrant sooner, and the smoke characteristic producing with cigarette burning complements each other.
The present embodiment is used the cigarette that contains pungent solid particle filter stick and common cigarette the cigarette of acetate tow filter stick, transfers to 10 professional members of smoking to smoke panel test, and smoking result is in shown in table 5 and table 6:
Table 5
| Cigarette sample | Sensory evaluation |
| Common fiber tow filter rods | Cigarette perfume (or spice) is main, and perfume quantity is general, and assorted gas slightly appears, and flue gas is more coarse, slightly stimulates |
| Spice particle filter stick | Perfume quantity and saturation degree obviously increase, and flue gas is finer and smoother soft, and assorted gas is covered to effect, and there is stronger pungent material aftertaste in oral cavity, does not realize excitant, the strong scent experience of enriching |
Table 6
The cigarette that contains Chinese prickly ash, hot red pepper particle filter stick, flue gas is finer and smoother soft, illustrate that adding particle has played modification smoke behavior, covers the effect of assorted gas, meanwhile, cigarette note is abundant, the saturation degree of fragrance increases, and produces the distinctive sense of taste of spicy substance and impact in oral cavity, and aftertaste sense is rich and varied, member of smoking provides good excitant mark, illustrates that filter stick of the present invention takes like a shot for consumer.
Embodiment 4
S1. granulation: being crushed to granularity after Chinese prickly ash, hot red pepper are mixed according to the mass ratio of 1:1 is 40 orders, obtains pungent solid particle;
S2. perfuming processing: by peppermint oil, ennel oil in mass ratio 1:2 be mixed into food flavor,, mix toward adding essence in pungent solid particle described in S1 in 0.05% ratio of gross mass;
S3. balance: solid particle described in S2 is placed into climatic chamber equilibrium water conten 48 hours, makes its moisture content be about 10%;
S4. disperse: 5% the ratio that accounts for acetate fiber quality according to solid particle after equilibrium water conten by solid particle be dispersed in common after shredding cigarette for acetate tow (commercial) upper, obtain containing composite particles tow;
S5. moulding: adopt composite particles filter stick formation paper that solid particle tow parcel is prepared into composite particles filter stick.
Adopt GB/T19609-2004(to adopt conventional analysis, smoking machine is measured tar) method carries out flue gas analysis to filter stick and shows, the cigarette that employing contains foodstuff solid particle filter stick, compare the cigarette of common cigarette acetate tow filter stick, the tar content 3%(that can effectively reduce in flue gas is that 10mg tar reduces 0.3mg).The filter stick that the present embodiment provides, pungent solid particle and acetate tow are brought into play collaborative suction-operated, are conducive to the absorption to tar and other harmful substances.Note: filter stick need be made complete cigarette just can carry out tar mensuration.
Employing equal length 120mm contains pungent solid particle filter stick and common cigarette acetate tow filter stick carries out filtering rod test through resistance to suction tester (Suo Ding D49+D49X8 type SODIM testboard), assay method is with reference to existing routine, in the time that the flow steady air flow that is 17.5ml/s is flowed through filter stick, the pressure differential at filter stick two ends is filtering rod.
After tested: common filter stick pressure drop 3080Pa, pungent solid particle composite filter 3012Pa.
The present embodiment is compound to these solid particles in the acetate fiber base material of filter stick, compare common cellulose acetate filter rod, the resistance to suction that the present embodiment filter stick produces is suitable, pungent class note obviously promotes, can remove preferably the assorted gas in flue gas, improve the degree of saturation of flue gas, increase the taste perception of pungent perfume (or spice).
The present embodiment is used the cigarette that contains pungent solid particle filter stick and common cigarette the cigarette of acetate tow filter stick, transfers to 10 professional members of smoking to smoke panel test, and smoking result is in shown in table 7 and table 8:
Table 7
| Cigarette sample | Sensory evaluation |
| Common fiber tow filter rods | Cigarette perfume (or spice) is main, and perfume quantity is general, and assorted gas slightly appears, and flue gas is more coarse, slightly stimulates |
| Spice particle filter stick | Perfume quantity and saturation degree obviously increase, and flue gas is finer and smoother soft, and assorted gas is covered to effect, and there are stronger pungent and fennel aftertaste in oral cavity, does not realize excitant, the strong scent experience of enriching |
Table 8
The present embodiment and common tow are prepared into binary composite particles filter stick (binary filter stick) according to the length ratio of 1:1, the structural representation of binary filter stick is shown in shown in accompanying drawing 1, wherein 1 is composite particles filter stick, 2 is foodstuff composite particles, and 3 is composite particles filter stick formation paper, and 4 is common fiber tow filter rods, 5 is common fiber tow filter rods forming paper, 6 is composite filter forming paper, and 7 suck end for cigarette, and 8 is cigarette pipe tobacco end.With the cellulose acetate filter rod contrast of same length, after tipping cigarette shreds section, the contrast test of smokeing panel test is as shown in table 9:
Table 9
Claims (8)
1. a spice composite particles filter stick, comprise acetate fiber base material and be wrapped in the forming paper outside acetate fiber base material, it is characterized in that, by mass, acetate fiber base material comprises 90～99% acetate fiber and 1～10% treated pungent material solid particle; Described treated pungent material solid particle is scattered on acetate fiber;
Described treated pungent material solid particle is to obtain through constant temperature and humidity balance to constant moisture content after food flavor and pungent material solid particle are mixed in proportion; The consumption of described food flavor is 0.01%～0.1% of pungent material mass of solid particles;
Described pungent material is Chinese prickly ash and hot red pepper, and the granularity of described pungent material solid particle is 20～200 orders,
Described food flavor is peppermint oil and ennel oil.
2. spice composite particles filter stick according to claim 1, is characterized in that, by mass, acetate fiber base material comprises 95% acetate fiber and 5% treated pungent material solid particle.
3. spice composite particles filter stick according to claim 1, is characterized in that, the consumption of described food flavor is 0.05% of pungent material mass of solid particles.
4. spice composite particles filter stick according to claim 1, is characterized in that, the granularity of described pungent material solid particle is 30～80 orders.
5. spice composite particles filter stick according to claim 4, is characterized in that, the granularity of described pungent material solid particle is 40 orders.
6. according to a preparation method for the spice composite particles filter stick described in claim 1 to 5 any one, it is characterized in that, comprise the following steps:
S1. pungent material raw material is pulverized, sieved and obtain pungent material solid particle;
S2. food flavor and pungent material solid particle are mixed in proportion;
S3. pungent material solid particle S2 being obtained is placed into climatic chamber, and balance is to constant moisture content;
S4. S3 gained pungent material solid particle is dispersed on acetate fiber, obtains acetate fiber base material;
S5. by forming paper, acetate fiber base material is wrapped up, prepare composite particles filter stick.
7. preparation method according to claim 6, is characterized in that, described constant moisture content is 10%.
8. preparation method according to claim 6, is characterized in that, the time of described balance is 48 hours.
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103393220A (en) * | 2013-08-14 | 2013-11-20 | 中国烟草总公司郑州烟草研究院 | Preparation and application of Chinese herbal cigarette filter additive carrier material |
| CN104824844A (en) * | 2015-04-10 | 2015-08-12 | 云南瑞升烟草技术（集团）有限公司 | Cigarette filter rod-used filamentous plant filter material |
| CN107699155A (en) * | 2017-10-17 | 2018-02-16 | 湖北中烟工业有限责任公司 | A kind of cumin fragrance cigarette connects mouth glue and preparation method thereof |
| CN108552586A (en) * | 2018-04-30 | 2018-09-21 | 南通烟滤嘴有限责任公司 | Bulky grain ternary or multi-element composite filter stick |
| CN113679092B (en) * | 2021-09-08 | 2023-04-07 | 湖北中烟工业有限责任公司 | Preparation method of cigarette spice capable of reducing harmful substances in smoke |
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| CN1200901A (en) * | 1998-02-26 | 1998-12-09 | 郭上前 | Cigarette with Chinese prickly ash |
| CN101433373A (en) * | 2008-12-12 | 2009-05-20 | 广东中烟工业有限责任公司 | Granule and preparation method thereof |
| CN102090718A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, relieving cough and refreshing |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10051884B2 (en) * | 2010-03-26 | 2018-08-21 | Philip Morris Usa Inc. | Controlled release mentholated tobacco beads |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1200901A (en) * | 1998-02-26 | 1998-12-09 | 郭上前 | Cigarette with Chinese prickly ash |
| CN101433373A (en) * | 2008-12-12 | 2009-05-20 | 广东中烟工业有限责任公司 | Granule and preparation method thereof |
| CN102090718A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, relieving cough and refreshing |
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