CN103622157B - Ternary tobacco fiber paper filter stick containing herbaceous plants and manufacturing method thereof - Google Patents
Ternary tobacco fiber paper filter stick containing herbaceous plants and manufacturing method thereof Download PDFInfo
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- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
本发明涉及烟草滤棒技术领域,公开了一种复合草本植物的三元烟草纤维纸质滤棒,所述滤棒由滤芯和包裹滤芯的成型纸组成,所述滤芯包括两段烟草纤维纸质滤芯和设置于两段烟草纤维纸质滤芯之间的中药材滤芯,所述的烟草纤维纸质滤芯由纸质纤维卷制而成,所述的中药材滤芯由中药材颗粒压制而成。本发明所述的纸质滤棒比醋酸纤维滤棒有更强的去除焦油和尼古丁的能力,原料来源于烟草或天然植物,消费者看到的滤棒的颜色与香烟烟丝一致,具有强烈的烟草天然材料质感,合理地中药材添加方案为卷烟的烟气增加了丰富的滋味,为滤棒技术领域指引了新的研究方向。
The invention relates to the technical field of tobacco filter sticks, and discloses a ternary tobacco fiber paper filter stick with composite herbal plants. The filter element and the Chinese medicinal material filter element arranged between the two sections of tobacco fiber paper filter elements, the tobacco fiber paper filter element is rolled from paper fibers, and the Chinese medicinal material filter element is made of pressed Chinese medicinal material particles. The paper filter rod of the present invention has a stronger ability to remove tar and nicotine than the cellulose acetate filter rod. The raw material comes from tobacco or natural plants. The color of the filter rod seen by consumers is consistent with that of cigarette shreds, and has a strong The texture of natural tobacco materials and the reasonable addition of Chinese herbal medicines add a rich taste to the smoke of cigarettes, and guide a new research direction for the field of filter rod technology.
Description
技术领域technical field
本发明涉及卷烟滤棒技术领域,更具体地说,涉及一种复合草本植物的三元烟草纤维纸质滤棒及其制备方法。The invention relates to the technical field of cigarette filter sticks, and more specifically relates to a three-element tobacco fiber paper filter stick with composite herbs and a preparation method thereof.
背景技术Background technique
卷烟烟气中包含有微粒,通常称之为焦油。焦油中含有大量的化学成分,有4000至5000种,都是烟草不完全燃烧的产物。除了焦油外,卷烟烟雾中还包含有其他物质,如“蒸汽”或“气体”相,也包括挥发性的烟草燃烧物质,如乙醛以及其它低分子重量成分。卷烟烟雾中的其他相,如“半挥发性”相,其中包括许多燃烧物质,与微粒和蒸汽相等同。Cigarette smoke contains particles, commonly known as tar. Tar contains a large number of chemical components, 4000 to 5000 kinds, all of which are products of incomplete combustion of tobacco. In addition to tar, cigarette smoke contains other substances, such as the "steam" or "gas" phase, which also includes volatile tobacco combustion substances such as acetaldehyde and other low molecular weight components. Other phases in cigarette smoke, such as the "semi-volatile" phase, which includes many combustion substances, are equivalent to particulate and vapor phases.
卷烟滤棒能够过滤烟雾成分。卷烟的滤棒是由滤芯和成型纸组成的。现有滤棒的滤芯一般都是采用醋酸纤维或聚丙烯纤维组成。由于这些含有纤维的滤芯直接与人体的嘴唇相接触,最近有媒体报道,纤维特别是聚丙烯纤维可能会随着卷烟的抽吸进入人体,并对人体健康造成损害。滤嘴是卷烟的重要组成部分,利用卷烟滤嘴里的吸附材料及其添加剂可以过滤掉烟支主流烟气里的有害物质。目前,滤嘴滤材主要有三种类型:醋酸纤维、聚丙烯纤维和纸。纸质滤嘴因对烟气截留效率较高,且较之丢弃的醋酸纤维滤嘴和聚丙烯纤维滤嘴更易降解而备受关注。Cigarette filter rods can filter smoke components. Cigarette filter rods are composed of filter elements and molding paper. The filter element of existing filter rod all is to adopt acetate fiber or polypropylene fiber to form generally. Because these fiber-containing filter elements are in direct contact with the lips of the human body, recently there have been media reports that fibers, especially polypropylene fibers, may enter the human body along with the smoking of cigarettes and cause damage to human health. The filter tip is an important part of the cigarette, and the harmful substances in the mainstream smoke of the cigarette can be filtered out by using the absorbent material and its additives in the cigarette filter tip. At present, there are three main types of filter media: acetate fiber, polypropylene fiber and paper. Paper filters have attracted much attention due to their higher smoke retention efficiency and easier degradation than discarded acetate and polypropylene filters.
目前现有技术中也有一些植物纤维烟用滤棒的报道,如(专利号200910185294)报道了一种植物纤维烟用滤棒及其制备方法。但该专利滤棒由稻草纤维、麦草纤维、烟草秸秆纤维和大豆秸秆纤维直接构成,主要是利用植物秸杆降低卷烟成本,减少使用后的滤嘴和丝束生产过程对环境的污染,此外并并不能提供更多符合卷烟滤棒要求的功能。At present, there are some reports of plant fiber tobacco filter sticks in the prior art, for example (Patent No. 200910185294) reports a plant fiber tobacco filter stick and its preparation method. However, the patented filter rod is directly composed of rice straw fiber, wheat straw fiber, tobacco straw fiber and soybean straw fiber. Can not provide more functions that meet the requirements of the cigarette filter rod.
由绉丝纸制成的卷烟过滤嘴首次在20世纪20年代引进欧洲卷烟市场,纸质的滤嘴比醋酸纤维有更强的去除焦油和尼古丁的能力,但消费者一直不能接受,直到20世纪50年代,随着醋酸纤维的开发,过滤嘴卷烟才开始得到消费者的广泛认可,主要原因是纸张有“纸张的味道”,消费者往往不喜欢这一点。而且纸张较软,在吸烟的过程中污染严重,因此不宜直接作为过滤嘴使用。目前,醋酸纤维制成的过滤嘴是被广泛应用的一种。随着消费者对于健康的不断追求,以醋酸纤维为主的经由化学物质制备得到的滤嘴因为非天然性特点逐渐受到抵触。但目前还没有找到完全替代醋酸纤维的新材料。Cigarette filters made of crepe paper were first introduced to the European cigarette market in the 1920s. Paper filters have a stronger ability to remove tar and nicotine than acetate fibers, but consumers have not accepted them until the 1950s. With the development of acetate in the 1990s, filter cigarettes only began to gain widespread acceptance among consumers, mainly because the paper had a "paper smell," which consumers often disliked. Moreover, the paper is relatively soft, and the pollution is serious during the smoking process, so it is not suitable to be directly used as a filter tip. At present, the filter tip made of acetate fiber is widely used. With the continuous pursuit of health by consumers, the filters made of cellulose acetate and prepared from chemical substances are gradually being resisted because of their unnatural characteristics. But there is no new material that can completely replace cellulose acetate.
现有技术采用干法纸作为制备卷烟滤嘴棒滤材的技术也得到了开发,大都采用木浆纤维为主要纤维材料,或辅以一定比例的复合纤维、热熔纤维或生态纤维以达到各自的目标。如中国专利(CN180167B)“干法纸卷烟滤棒及其制备方法”,其在木浆纤维中添加了5%~65%的热熔性皮芯纤维;再如中国专利申请(CN101171981A)“二元复合卷烟过滤嘴棒”采用膨化干法纸制备得到的材料作为靠近烟丝的一元滤嘴的滤芯,该材料由纯木浆或50%~95%木浆和5%~50%复合纤维直接组成;还有中国专利申请(CN101624756A)“生物降解型香烟过滤嘴用非织造布及其制备方法”采用了木浆纤维、高熔点聚乳酸纤维、低熔点聚乳酸纤维和水溶性胶。也有人直接将烟草纤维通过风机输送至成型工段铺网成型,在成型网带上形成蓬松均匀的纤维网,再经施胶、预热、辊压、固化和成型制成卷烟滤材纸,并在成型过程中添加天然药草废弃原料。这些干法纸用的纤维涉及了木浆纤维、复合纤维、热熔性皮芯纤维、聚乳酸纤维等纤维类型,这些纤维尽管可用于制作滤嘴的滤材,但过滤烟气的同时使得烟香损失较多,且带入一定的木质杂气,在抽吸时对卷烟吸味和吃味有一定的负面影响,不能保证卷烟品质,更重要的是这些现有材料的颜色和品质与天然烟草的感觉相差甚远,不能迎合卷烟消费者对天然烟草感觉的追求。The prior art adopts air-laid paper as the technology of preparing cigarette filter rod filter material and has also been developed, most of which adopt wood pulp fiber as the main fiber material, or supplemented by a certain proportion of composite fiber, hot-melt fiber or ecological fiber to achieve their respective The goal. Such as the Chinese patent (CN180167B) "dry paper cigarette filter rod and its preparation method", which adds 5% to 65% of heat-melting sheath-core fiber in the wood pulp fiber; another example of the Chinese patent application (CN101171981A) Elementary composite cigarette filter rod” uses the material prepared by puffed dry-laid paper as the filter element of the elemental filter near the shredded tobacco. The material is directly composed of pure wood pulp or 50% to 95% wood pulp and 5% to 50% composite fiber; There is also a Chinese patent application (CN101624756A) "Nonwoven fabric for biodegradable cigarette filter and its preparation method" which uses wood pulp fiber, high melting point polylactic acid fiber, low melting point polylactic acid fiber and water-soluble glue. There are also people who directly transport the tobacco fibers to the forming section through the blower to form a fluffy and uniform fiber web on the forming belt, and then through sizing, preheating, rolling, curing and forming to make cigarette filter paper, and Natural herb waste raw materials are added during the molding process. The fibers used for these airlaid papers involve fiber types such as wood pulp fibers, composite fibers, hot-melt sheath-core fibers, and polylactic acid fibers. Although these fibers can be used to make filter materials for filter tips, they filter smoke while making smoke There is a lot of loss of aroma, and a certain amount of woody gas is brought in, which has a certain negative impact on the taste and taste of cigarettes during smoking, and cannot guarantee the quality of cigarettes. What is more important is that the color and quality of these existing materials are consistent with natural The feeling of tobacco is very different, and it cannot cater to the pursuit of cigarette consumers for the feeling of natural tobacco.
在近期的研究中,也有人将烟草纤维应用于干法制纸中,将烟草纤维通过风机输送至成型工段铺网成型,在成型网带上形成蓬松均匀的纤维网。再经施胶、预热、辊压、固化和成型制成卷烟滤材纸,并在成型过程中添加天然药草废弃原料。但是它的技术方案还是通过简单烟草纤维铺设而成,而且使用各种胶体粘合而成,所以它去除杂气的效果不佳,而且使用的胶体过多会给香烟烟嘴带来异味,另外,并不能解决减少烟草废弃料的问题,而且在生产过程中额外添加烟草纤维,反而提高了整只香烟的烟草使用量。In recent research, some people have also applied tobacco fiber in dry-laid papermaking, and the tobacco fiber is transported to the forming section by a fan for laying and forming, and a fluffy and uniform fiber web is formed on the forming belt. Then through sizing, preheating, rolling, curing and molding to make cigarette filter paper, and add natural herb waste raw materials in the molding process. However, its technical solution is still made by laying simple tobacco fibers, and it is bonded with various colloids, so it is not effective in removing miscellaneous gases, and using too much colloid will bring peculiar smell to the cigarette holder. In addition, It does not solve the problem of reducing tobacco waste, and adding additional tobacco fibers in the production process increases the tobacco consumption of the whole cigarette.
另外,现有的卷烟生产企业在生产中,产生很多废料,如废弃烟叶、烟末、碎片、烟梗等,目前对这些废料的利用主要是因为降焦的目的将这些废料再加工后加入卷烟的烟丝中替代少部分烟丝,但是众所周知,这些材料在烟丝中的添加量受到非常大的限制,不能完全解决烟草生产企业废料处置的问题和变废为宝的力度。In addition, the existing cigarette manufacturers produce a lot of waste during production, such as discarded tobacco leaves, tobacco powder, debris, tobacco stems, etc. The current utilization of these wastes is mainly for the purpose of reducing coke and adding these wastes to cigarettes after reprocessing However, as we all know, the amount of these materials added to cut tobacco is very limited, which cannot completely solve the problem of waste disposal in tobacco production enterprises and the efforts to turn waste into treasure.
目前还没有找到可完全替代醋酸纤维、给消费者天然烟草感觉的新的纸质滤嘴材料。At present, there is no new paper filter material that can completely replace cellulose acetate and give consumers a natural tobacco feeling.
发明内容Contents of the invention
本发明要解决的技术问题是克服现有滤棒技术的不足,提供一种复合草本植物的三元烟草纤维纸质滤棒。本发明设计三段滤芯结构的滤棒,基于烟草纤维纸质滤棒良好的过滤、吸附功能,降低卷烟烟气中的焦油含量,并通过烟气将草本植物的有效成分带出,补充降焦给烟气香韵和吃味带来的不足,保证卷烟中药材的药香吃味。The technical problem to be solved by the present invention is to overcome the deficiency of the existing filter stick technology and provide a ternary tobacco fiber paper filter stick with composite herbs. The present invention designs a filter rod with a three-stage filter element structure, based on the good filtration and adsorption functions of the tobacco fiber paper filter rod, reduces the tar content in cigarette smoke, and takes out the active ingredients of herbal plants through the smoke to supplement tar reduction Insufficient to the aroma and taste of the smoke, to ensure the aroma and taste of the medicinal materials in the cigarette.
本发明另一要解决的技术问题是提供所述滤棒的制备方法。Another technical problem to be solved by the present invention is to provide a preparation method of the filter stick.
本发明的目的通过以下技术方案予以实现:The purpose of the present invention is achieved through the following technical solutions:
提供一种复合草本植物的三元烟草纤维纸质滤棒,包括滤芯和包裹滤芯的成型纸,所述滤芯由两段烟草纤维纸质滤芯和设置于两段烟草纤维纸质滤芯之间的中药材滤芯组成;所述的烟草纤维纸质滤芯由纸质纤维辊压、卷制而成;A ternary tobacco fiber paper filter rod with composite herbal plants is provided, including a filter element and a molding paper wrapping the filter element, the filter element is composed of two sections of tobacco fiber paper filter elements and a traditional Chinese medicine arranged between the two sections of tobacco fiber paper filter elements The tobacco fiber paper filter element is formed by rolling and rolling the paper fiber;
所述纸质纤维是采用烟草原料和长纤维原料分别磨浆得到烟草纤维浆和长纤维浆,将烟草纤维浆和长纤维浆进行配浆、抄片、压榨、干燥制成纤维纸基,纤维纸基经涂布、干燥即得;The paper fiber is obtained by grinding tobacco raw material and long fiber raw material respectively to obtain tobacco fiber pulp and long fiber pulp, and then the tobacco fiber pulp and long fiber pulp are mixed, sheeted, pressed, and dried to form a fiber paper base. The paper base is obtained by coating and drying;
所述中药材为人参、虫草、燕窝、铁皮枫斗、藏红花或绞股蓝中的一种或几种。优选人参、虫草或绞股蓝中的一种或几种。The Chinese medicinal materials are one or more of ginseng, cordyceps, bird's nest, Tiepifengdou, saffron or gynostemma. One or more of ginseng, cordyceps or gynostemma is preferred.
所述中药材颗粒为粒度为8目~50目的粉末或者厚度≦0.1mm的薄片。The Chinese herbal medicine granules are powders with a particle size of 8 mesh to 50 mesh or flakes with a thickness≦0.1mm.
所述两段烟草纤维纸质滤芯和设置于两段烟草纤维纸质滤芯之间的中药材滤芯的长度比例为1:0.1~1。The length ratio of the two sections of tobacco fiber paper filter elements to the Chinese herbal medicine filter element arranged between the two sections of tobacco fiber paper filter elements is 1:0.1-1.
所述的长纤维原料为烟梗、烟秸秆、藤蔓、甘草、棉纤维和竹纤维中的一种或几种;所述的烟草纤维原料为烟叶、烟梗、烟末或烟碎片中的一种或几种。The long fiber raw material is one or more of tobacco stems, tobacco stalks, vines, licorice, cotton fiber and bamboo fiber; the tobacco fiber raw material is one of tobacco leaves, tobacco stems, tobacco powder or tobacco fragments species or several.
所述烟草纤维浆和长纤维浆进行配浆的质量比例为1:0.5~3。The mass ratio of the tobacco fiber pulp and the long fiber pulp is 1:0.5-3.
本发明同时提供了所述的复合草本植物的三元烟草纤维纸质滤棒的制备方法,包括以下步骤:The present invention simultaneously provides the preparation method of the ternary tobacco fiber paper filter rod of the composite herb plant, comprising the following steps:
S1.制备烟草纤维纸质基材;S1. Prepare tobacco fiber paper substrate;
S2.制备中药材滤芯:将中药材颗粒用成型纸包裹或将中药材颗粒洒于烟草纤维纸质基材经辊压、卷制得到中药材颗粒滤芯;S2. Prepare the Chinese herbal medicine filter element: wrap the Chinese herbal medicine granules with molding paper or sprinkle the Chinese herbal medicine granules on the tobacco fiber paper base material, roll and roll to obtain the Chinese herbal medicine granule filter element;
S3.将烟草纤维纸质基材经辊压,卷制,切段,得烟草纤维纸质滤芯;将中药材颗粒滤芯设置于两段烟草纤维纸质滤芯之间;在三段滤芯外包裹成型纸即得复合草本植物的三元烟草纤维纸质滤棒。S3. The tobacco fiber paper base material is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the Chinese herbal medicine particle filter element is arranged between two sections of tobacco fiber paper filter elements; wrapped and formed outside the three-section filter element The paper is a ternary tobacco fiber paper filter rod of composite herbal plants.
优选地,S3是将烟草纤维纸质基材经辊压,卷制,切段,得烟草纤维纸质滤芯,应用于卷烟的烟丝端;将烟草纤维纸质基材经辊压,卷制,压制沟槽,切段,得带有沟槽的烟草纤维纸质滤芯,应用于卷烟的嘴唇接触端;将中药材颗粒滤芯设置于烟丝端和嘴唇接触端的烟草纤维纸质滤芯之间;在三段滤芯外包裹成型纸即得。Preferably, in S3, the tobacco fiber paper substrate is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element, which is applied to the shredded tobacco end of the cigarette; the tobacco fiber paper substrate is rolled, rolled, Press the grooves, cut into sections, and obtain a tobacco fiber paper filter element with grooves, which is applied to the lip contact end of the cigarette; the Chinese herbal medicine particle filter element is arranged between the shredded tobacco end and the tobacco fiber paper filter element at the lip contact end; Wrap the section filter element with molding paper.
优选地,S1包括以下步骤:Preferably, S1 includes the following steps:
S11.将烟草纤维原料和长纤维原料浸提处理,分别得到烟草纤维原料的提取液、烟草纤维原料固体渣、长纤维原料提取液和长纤维原料固体渣;S11. extracting the tobacco fiber raw material and the long fiber raw material to obtain respectively the extract of the tobacco fiber raw material, the solid slag of the tobacco fiber raw material, the extract of the long fiber raw material and the solid slag of the long fiber raw material;
S12.将烟草纤维原料固体渣和长纤维原料固体渣分别磨浆,得到烟草纤维浆和长纤维浆;S12. Refining the tobacco fiber raw material solid slag and the long fiber raw material solid slag respectively to obtain tobacco fiber pulp and long fiber pulp;
S13.将烟草纤维浆和长纤维原料浆按比例混合后抄片,经压榨,干燥,制成烟草纤维纸基;S13. After mixing the tobacco fiber pulp and the long fiber raw material pulp in proportion, sheeting is made, squeezed, and dried to make a tobacco fiber paper base;
S14.将步骤S1得到的烟草纤维原料提取液涂到S13所得的烟草纤维纸基上,干燥,得到烟草纤维纸质基材。S14. Apply the tobacco fiber raw material extract obtained in step S1 to the tobacco fiber paper base obtained in S13, and dry to obtain a tobacco fiber paper base.
所述长纤维浆的原料为烟梗、烟秸秆、烟茎、藤蔓、甘草、棉纤维、木质纤维或竹纤维中的一种或几种。优选使用烟梗、烟秸秆制备得到的长纤维,因其本身来自于烟草,对卷烟香气会有提升作用,和烟丝的一致性会更加地强。作为另一优选,本发明所述长纤维的原料可以选择竹纤维,因其来源广泛,成本适中,纤维结构与烟草原料制备得到的(短)纤维相得益彰,保证了纸质滤棒材料的抗张指数、抗张强度、撕裂指数、松厚度、紧度等性能优良,保证很好地烟气截留效率和卷烟烟气的香味。本发明可以采用常规购买的长纤维浆。所述的烟草原料包括烟梗、烟叶及碎片、烟末中的一种或几种,这几种纤维主要来源于烟草产生企业生产过程中的废弃原料,这些废弃原料需要耗费生产企业的人力、物力、财力和空间来堆置或和处置,用于制备滤棒,可以让废弃原料得到更加充分地利用。The raw material of the long-fiber pulp is one or more of tobacco stems, tobacco stalks, tobacco stems, vines, licorice, cotton fibers, wood fibers or bamboo fibers. It is preferable to use long fibers prepared from tobacco stems and tobacco stalks, because they are derived from tobacco, which can improve the aroma of cigarettes and have a stronger consistency with shredded tobacco. As another preference, bamboo fiber can be selected as the raw material of the long fiber of the present invention, because of its wide source, moderate cost, fiber structure and (short) fiber prepared from tobacco raw materials complement each other, ensuring the tensile strength of the paper filter rod material Index, tensile strength, tear index, bulk, tightness and other properties are excellent, ensuring good smoke retention efficiency and cigarette smoke flavor. The present invention can use conventionally purchased long fiber pulp. The tobacco raw materials include one or more of tobacco stems, tobacco leaves and chips, and tobacco powder. These fibers are mainly derived from waste materials in the production process of tobacco production enterprises. These waste materials need to consume manpower, Material resources, financial resources and space are used to stack or dispose of filter rods, so that waste materials can be more fully utilized.
优选地,所述烟草纤维浆和长纤维浆进行配浆的质量比例为1:0.5~3。更优选为1:1~2。Preferably, the mass ratio of the tobacco fiber pulp and the long fiber pulp is 1:0.5-3. More preferably, it is 1:1-2.
S2所述将中药材粉碎过8目~50目筛;或者将中药材切成厚度≦0.1mm的薄片。As described in S2, crush the Chinese herbal medicine through a sieve of 8 mesh to 50 mesh; or cut the Chinese herbal medicine into thin slices with a thickness ≤ 0.1 mm.
S11所述浸提处理的温度为60~90℃,持续60~100分钟,反复1~3次。The temperature of the leaching treatment in S11 is 60-90°C, lasts for 60-100 minutes, and repeats 1-3 times.
本发明有益效果如下:The beneficial effects of the present invention are as follows:
1、本发明提供了一种新的三元复合烟草纤维纸质滤棒,本发明设计三段滤芯结构的滤棒,为依次相连接的烟草纤维纸质滤芯、草本植物颗粒滤芯、烟草纤维纸质滤芯,基于烟草纤维纸质滤棒,本发明彻底改变了现有的滤棒材料设计思想,真正将天然烟草纤维材料的质感和优良的滤棒功能完美结合,本发明纸质滤棒具有较高的吸附性及相对吸收性,相比现有的醋酸纤维或聚丙烯纤维纤维材料,纸质的滤棒比醋酸纤维有更强的去除焦油和尼古丁的能力,可以吸附更多的卷烟主流烟气气溶胶,从而提高滤棒的过滤效率,保证了优良的降焦和减害功能,草本植物颗粒的有效成分被烟气带出,补充降焦给烟气香韵和吃味带来的损失,实验证明,本发明滤棒中草本植物成分与烟气中的致香成分相辅相成,改善卷烟烟气润湿性,赋予卷烟甜润的口感,提高卷烟吸食时的舒适度,为卷烟提供保润回甘、提升烟气香气丰富度的有益效果。1. The present invention provides a new ternary composite tobacco fiber paper filter rod. The present invention designs a filter rod with three sections of filter core structure, which are successively connected tobacco fiber paper filter cores, herb particle filter cores, and tobacco fiber paper Based on the tobacco fiber paper filter rod, the present invention has completely changed the design idea of the existing filter rod material, and truly perfectly combines the texture of the natural tobacco fiber material with the excellent filter rod function. The paper filter rod of the present invention has a relatively high High adsorption and relative absorption. Compared with the existing acetate fiber or polypropylene fiber material, the paper filter stick has a stronger ability to remove tar and nicotine than acetate fiber, and can absorb more cigarette mainstream smoke Aerosol, thereby improving the filtration efficiency of the filter rod, ensuring excellent coke reduction and harm reduction functions, the active ingredients of herbal plant particles are carried out by the smoke, supplementing the loss of coke reduction to the aroma and taste of the smoke , experiments have proved that the herbal plant components in the filter rod of the present invention and the aroma components in the smoke complement each other, improve the wettability of cigarette smoke, endow cigarettes with a sweet taste, improve the comfort of cigarettes when smoking, and provide cigarettes with moisture retention. Sweetness, the beneficial effect of enhancing the richness of smoke aroma.
2、本发明滤棒使用的原料全部来源于天然植物,纸质的滤嘴摈除了消费者不喜欢的“纸张的味道”和“化纤的味道”,滤棒颜色外观与卷烟烟丝相近,具有强烈的烟草天然材料质感,配以中药材的香味和精油成分,带给消费者全新的天然、保健的感官冲击。实现滤棒技术可视化、可触摸化,产品具有浓厚的中国特色,引发消费者兴趣,易于口碑相传,对卷烟产品的销售具有较强的市场触动性,为卷烟技术领域指引了新的研究方向。2. The raw materials used in the filter stick of the present invention are all derived from natural plants. The paper filter tip eliminates the "taste of paper" and "taste of chemical fiber" that consumers do not like. The texture of natural tobacco materials, together with the fragrance of Chinese medicinal materials and essential oil components, brings consumers a new natural and healthy sensory impact. Realize the visualization and touchability of filter rod technology, the product has strong Chinese characteristics, arouses consumers' interest, is easy to spread by word of mouth, has a strong market impact on the sales of cigarette products, and guides a new research direction for the field of cigarette technology.
3、本发明滤棒材料具有优良的承载能力,其更适合承载各种烟用添加剂。3. The filter rod material of the present invention has excellent load-carrying capacity, and is more suitable for carrying various cigarette additives.
4、采用合适的短纤维浆和长纤维浆的比例,采用造纸法制备得到纸质烟草纤维纸质滤芯,不但有效提高了滤棒的过滤效率,降低卷烟的焦油及有害物质,而且大大的提高了吸烟者对滤棒纸质和天然烟草感官体验的需求,在吸食香烟时得到更好的接触感受。4. Using a suitable ratio of short fiber pulp and long fiber pulp, the paper tobacco fiber paper filter element is prepared by papermaking method, which not only effectively improves the filtration efficiency of the filter rod, reduces the tar and harmful substances of cigarettes, but also greatly improves the It meets the needs of smokers for the sensory experience of filter rod paper and natural tobacco, and obtains a better contact feeling when smoking cigarettes.
5、本发明滤棒的制备方法简单,易于推广。5. The preparation method of the filter rod of the present invention is simple and easy to popularize.
附图说明Description of drawings
图1烟草纤维纸质滤棒材料实物图。Fig. 1 The actual picture of the tobacco fiber paper filter rod material.
图2烟草纤维纸质滤棒电子显微镜图。Fig. 2 Electron microscope image of tobacco fiber paper filter rod.
图3复合草本植物的三元纸质滤棒结构示意图。Fig. 3 Schematic diagram of the structure of the ternary paper filter rod of the composite herbal plant.
其中,1为烟草纤维纸质滤芯,2为中药材滤芯,3为成型纸。Among them, 1 is a tobacco fiber paper filter element, 2 is a Chinese herbal medicine filter element, and 3 is a molding paper.
图4带沟槽设计复合草本植物的三元纸质滤棒结构示意图。其中,1为烟草纤维纸质滤芯,2为保润植物滤芯,3为成型纸,4为带有沟槽的烟草纤维纸质滤芯,5为沟槽。Fig. 4 Schematic diagram of the structure of a ternary paper filter rod with a grooved design composite herb plant. Among them, 1 is a tobacco fiber paper filter element, 2 is a moisturizing plant filter element, 3 is a molding paper, 4 is a tobacco fiber paper filter element with grooves, and 5 is a groove.
具体实施方式Detailed ways
下面结合附图和具体实施例进一步详细说明本发明。人参、虫草、燕窝、铁皮枫斗、藏红花或绞股蓝均为市购中药材。The present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments. Ginseng, Cordyceps, Bird's Nest, Tiepi Fengdou, Saffron or Gynostemma are all commercial Chinese herbal medicines.
实施例1Example 1
S1用烟叶、烟梗和甘草制备烟草纤维滤芯S1 prepares tobacco fiber filter element with tobacco leaves, tobacco stems and licorice
(1)提取烟叶和烟梗(1) Extracting tobacco leaves and tobacco stems
S11.将烟草原料浸提处理,得到烟草原料的提取液、烟草原料的固体渣;S11. extracting the tobacco raw material to obtain an extract of the tobacco raw material and a solid slag of the tobacco raw material;
本实施例按料液质量比为1:7分别将烟梗和水,提取温度为60℃,提取时间为100分钟,反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1:10分别将烟叶和水,提取温度为80℃,提取时间为60分钟,反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
S12.将烟草原料的固体渣磨浆,得到烟草纤维浆;市购木质纤维浆本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。S12. Refining the solid slag of tobacco raw materials to obtain tobacco fiber pulp; commercially available lignocellulosic pulp. The refining process in this embodiment refers to the refining process in the existing tobacco sheet.
将甘草用适量水浸泡(浸泡时间不做严格限定,通常为60分钟左右)后磨浆得甘草长纤维浆;Soak the licorice with an appropriate amount of water (soaking time is not strictly limited, usually about 60 minutes), and then refine to obtain licorice long-fiber pulp;
S13.将烟草纤维浆和甘草长纤维浆按质量比为1:0.5的比例配抄,抄片获得烟草纤维纸基,在压力为0.4MPa压力下压榨5分钟,然后置于温度为105℃下干燥1小时。S13. Blend tobacco fiber pulp and licorice long fiber pulp at a mass ratio of 1:0.5, and sheet to obtain tobacco fiber paper base, press at a pressure of 0.4MPa for 5 minutes, and then place at a temperature of 105°C Let dry for 1 hour.
S14.将S11所得的烟梗提取液和烟叶提取液重新涂布到S13所得烟草纤维纸基上,自然干燥,得到烟草纤维纸质基材。S14. Recoat the tobacco stem extract and tobacco leaf extract obtained in S11 on the tobacco fiber paper substrate obtained in S13, and dry naturally to obtain a tobacco fiber paper substrate.
S2.制备藏红花颗粒滤芯:将藏红花粉碎过20目筛,干燥后包裹成型纸即得;S2. Prepare the saffron particle filter element: crush the saffron through a 20-mesh sieve, wrap it with molding paper after drying;
S3.将烟草纤维纸质基材经辊压,卷制,切段,得烟草纤维纸质滤芯;将藏红花颗粒滤芯设置于两段烟草纤维纸质滤芯之间;在三段滤芯外包裹水松纸即得含草本植物的三元纸质滤棒。三段滤芯的长度比例为1:1:1。S3. The tobacco fiber paper base material is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the saffron particle filter element is arranged between the two sections of the tobacco fiber paper filter element; the three sections of the filter element are wrapped with cork The paper is a ternary paper filter stick containing herbs. The length ratio of the three-section filter element is 1:1:1.
滤棒的结构如附图3所示,其中,1为两段烟草纤维纸质滤芯,2为中药材滤芯,3为成型纸。下述实施例结构同本实施例。The structure of the filter rod is as shown in accompanying drawing 3, wherein, 1 is two sections of tobacco fiber paper filter cores, 2 is Chinese herbal medicine filter cores, and 3 is molding paper. The structure of the following embodiments is the same as this embodiment.
实施例2Example 2
S1.用烟末、烟碎片和烟秸秆制备带沟槽烟草纤维滤棒S1. Preparation of grooved tobacco fiber filter rods from tobacco powder, tobacco fragments and tobacco stalks
S11.将原料浸提处理,得到原料的提取液、原料的固体渣;S11. extracting the raw material to obtain the extract of the raw material and the solid slag of the raw material;
本实施例按料液质量比为1:7分别将烟梗和水,提取温度为60℃,提取时间为100分钟,反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1:10分别将烟叶和水,提取温度为80℃,提取时间为60分钟,反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
按料液质量比为1:10分别将烟碎片和水,提取温度为75℃,提取时间为60分钟。处理后得到的烟碎片提取液和烟碎片固体渣。According to the mass ratio of solid to liquid of 1:10, the smoke fragments and water were separated, the extraction temperature was 75°C, and the extraction time was 60 minutes. The smoke chip extract and the smoke chip solid slag obtained after treatment.
S12.将烟叶固体渣和烟碎片固体渣按照1:1的质量比例混合后磨浆,得到烟草纤维浆;S12. mixing the solid slag of tobacco leaves and the solid slag of tobacco chips according to the mass ratio of 1:1, and refining to obtain tobacco fiber pulp;
另取干燥的烟秸秆用适量水浸泡(浸泡时间不做严格限定,通常为60分钟左右)后磨浆得烟秸秆长纤维浆;本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。Separately take dry tobacco stalks and soak them in an appropriate amount of water (soaking time is not strictly limited, usually about 60 minutes) and refine them to obtain tobacco stalk long-fiber pulp; the refining process in this example refers to the refining process in the existing tobacco sheet .
S13.将烟草纤维浆和烟秸秆长纤维浆按质量比为1:3的比例配抄,抄片获得烟草纤维纸基,在压力为0.4MPa压力下压榨5分钟,然后置于温度为105℃下干燥1小时。S13. Blend tobacco fiber pulp and tobacco stalk long-fiber pulp at a mass ratio of 1:3, and sheet to obtain tobacco fiber paper base, press at a pressure of 0.4MPa for 5 minutes, and then place at a temperature of 105°C Dry for 1 hour.
S14.将步骤S11得到的烟草纤维原料的提取液涂步到S13干燥后的烟草纤维纸基上,然后干燥,得到烟草纤维纸质基材;见附图1可见,烟草纤维纸质基材的颜色和质感与烟丝十分相近。S14. apply the extract solution of the tobacco fiber raw material obtained in step S11 to the tobacco fiber paper base after drying in S13, and then dry to obtain the tobacco fiber paper base material; see accompanying drawing 1 as seen, the tobacco fiber paper base material The color and texture are very similar to shredded tobacco.
S2.制备虫草颗粒滤芯:将虫草粉碎过15目筛,干燥后包裹成型纸即得;S2. Prepare the Cordyceps granule filter element: crush the Cordyceps and pass through a 15-mesh sieve, and wrap it with molding paper after drying;
S3.将烟草纤维纸质基材经辊压,卷制,切段,得烟草纤维纸质滤芯,应用于卷烟的烟丝端;将烟草纤维纸质基材经辊压,卷制,压制沟槽,切段,得带有沟槽的烟草纤维纸质滤芯,应用于卷烟的嘴唇接触端;将虫草颗粒滤芯设置于烟丝端和嘴唇接触端的烟草纤维纸质滤芯之间;在三段滤芯外包裹成型纸即得。滤棒的结构示意图将附图4所示。S3. Rolling, rolling, and cutting the tobacco fiber paper base material to obtain a tobacco fiber paper filter element, which is applied to the shredded tobacco end of the cigarette; rolling, rolling, and pressing the tobacco fiber paper base material into grooves , cut into sections to obtain a tobacco fiber paper filter element with grooves, which is applied to the lip contact end of the cigarette; the Cordyceps particle filter element is arranged between the shredded tobacco end and the tobacco fiber paper filter element at the lip contact end; Shaped paper is ready. The structural schematic diagram of the filter rod will be shown in accompanying drawing 4.
实施例3Example 3
S1.用烟末、烟碎片和烟茎制备带沟槽烟草纤维滤棒S1. Preparation of grooved tobacco fiber filter rods from tobacco dust, tobacco fragments and tobacco stems
S11.将原料浸提处理,得到原料的提取液、原料的固体渣;S11. extracting the raw material to obtain the extract of the raw material and the solid slag of the raw material;
本实施例按料液质量比为1:7分别将烟梗和水,提取温度为60℃,提取时间为100分钟,反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1:10分别将烟叶和水,提取温度为80℃,提取时间为60分钟,反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
按料液质量比为1:10分别将烟碎片和水,提取温度为75℃,提取时间为60分钟。处理后得到的烟碎片提取液和烟碎片固体渣。According to the mass ratio of solid to liquid of 1:10, the smoke fragments and water were separated, the extraction temperature was 75°C, and the extraction time was 60 minutes. The smoke chip extract and the smoke chip solid slag obtained after treatment.
S12.将烟叶固体渣和烟碎片固体渣按照1:1的质量比例混合后磨浆,得到烟草纤维浆;S12. mixing the solid slag of tobacco leaves and the solid slag of tobacco chips according to the mass ratio of 1:1, and refining to obtain tobacco fiber pulp;
另取干燥的烟茎用适量水浸泡(浸泡时间不做严格限定,通常为60分钟左右)后磨浆得烟茎长纤维浆;Another dried tobacco stem is soaked in an appropriate amount of water (soaking time is not strictly limited, usually about 60 minutes), and then refined to obtain tobacco stem long-fiber pulp;
本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。The refining process in this embodiment refers to the refining process in the existing tobacco sheet.
S13.将烟草纤维浆和烟茎长纤维浆按质量比为1:1的比例配抄,抄片获得烟草纤维纸基,在压力为0.4MPa压力下压榨5分钟,然后置于温度为105℃下干燥1小时。S13. Blend tobacco fiber pulp and tobacco stem long fiber pulp in a ratio of 1:1 by mass, and make sheet to obtain tobacco fiber paper base, press at a pressure of 0.4MPa for 5 minutes, and then place at a temperature of 105°C Dry for 1 hour.
S14.将步骤S11得到的烟草纤维原料的提取液涂步到S13干燥后的烟草纤维纸基上,然后干燥,得到烟草纤维纸质基材;见附图1可见,烟草纤维纸质基材的颜色和质感与烟丝十分相近。S14. apply the extract solution of the tobacco fiber raw material obtained in step S11 to the tobacco fiber paper base after drying in S13, and then dry to obtain the tobacco fiber paper base material; see accompanying drawing 1 as seen, the tobacco fiber paper base material The color and texture are very similar to shredded tobacco.
S2.制备绞股蓝颗粒滤芯:将藏红花粉碎过30目筛,干燥后洒于烟草纸质纤维上,辊压,卷制包裹成型纸即得;S2. Prepare the Gynostemma granule filter element: crush the saffron through a 30-mesh sieve, sprinkle it on the tobacco paper fiber after drying, roll it, and wrap it into a wrapping paper to obtain the product;
S3.将烟草纤维纸质基材经辊压,卷制,切段,得烟草纤维纸质滤芯;将绞股蓝颗粒滤芯设置于两段烟草纤维纸质滤芯之间;在三段滤芯外包裹水松纸即得复合草本植物的三元纸质滤棒。S3. The tobacco fiber paper base material is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the Gynostemma gynostemma particle filter element is arranged between the two sections of tobacco fiber paper filter elements; Paper is a ternary paper filter stick of compound herbs.
实施例4Example 4
S1.用烟末和木纤维浆制备烟草纤维滤棒S1. Preparation of tobacco fiber filter rods with tobacco dust and wood fiber pulp
S11.将烟草原料浸提处理,得到烟草原料的提取液、烟草原料的固体渣;S11. extracting the tobacco raw material to obtain an extract of the tobacco raw material and a solid slag of the tobacco raw material;
本实施例按料液质量比为1:7分别将烟梗和水,提取温度为60℃,提取时间为100分钟,反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1:10分别将烟叶和水,提取温度为80℃,提取时间为60分钟,反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
S12.将烟草原料的固体渣别磨浆,得到烟草纤维浆;市购木纤维浆,本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。S12. Separately refine the solid slag of the tobacco raw material to obtain tobacco fiber pulp; commercially available wood fiber pulp, the refining process in this embodiment refers to the refining process in the existing tobacco sheet.
S13.将烟草纤维浆和竹纤维浆(市购)按质量比为1:2的比例配抄,抄片获得烟草纤维纸基,在压力为0.4MPa压力下压榨5分钟,然后置于温度为105℃下干燥1小时。S13. Blending tobacco fiber pulp and bamboo fiber pulp (commercially available) at a mass ratio of 1:2, sheeting to obtain a tobacco fiber paper base, pressing for 5 minutes under a pressure of 0.4 MPa, and then placing it at a temperature of Dry at 105°C for 1 hour.
S14.将步骤S1得到的烟草纤维原料的提取液涂步到S3干燥后的烟草纤维纸基上,然后干燥,得到烟草纤维纸质基材;S14. Apply the extract of the tobacco fiber raw material obtained in step S1 to the tobacco fiber paper base dried in S3, and then dry to obtain the tobacco fiber paper base material;
S2.制备人参颗粒滤芯:将人参切薄片,薄片厚度为0.1毫米左右,用成型纸包裹即得;S2. Prepare the ginseng particle filter element: cut the ginseng into thin slices, the thickness of which is about 0.1 mm, and wrap it with molding paper;
S3.将烟草纤维纸质基材经辊压,卷制,切段,得烟草纤维纸质滤芯;将人参颗粒滤芯设置于两段烟草纤维纸质滤芯之间;在三段滤芯外包裹水松纸即得复合草本植物的三元纸质滤棒。S3. The tobacco fiber paper base material is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the ginseng particle filter element is arranged between two sections of tobacco fiber paper filter elements; and the three sections of filter element are wrapped with cork Paper is a ternary paper filter stick of compound herbs.
实施例5应用检测Example 5 Application Detection
1、物理性能根据Y/CT152-2001进行测定实施例1、2、3、4所得滤棒的物理性能,结果如表1所述。1. Physical properties The physical properties of the filter rods obtained in Examples 1, 2, 3, and 4 were measured according to Y/CT152-2001, and the results are as described in Table 1.
表1纤维材料物理性能Table 1 Physical properties of fiber materials
2、卷烟感官评价结果2. Results of sensory evaluation of cigarettes
以采用醋酸纤维滤棒的卷烟为对照样,与采用本发明所得烟草纤维纸质滤棒的卷烟样品为试验样,进行卷烟感官评吸,结果见表2所示,感官评吸的分数由7名专业评吸员各自打分后,取平均分后所得(每个项目满分为10分,小数点后保留一位小数,趋势越好,分数越高)。Taking the cigarette that adopts the cellulose acetate filter rod as the control sample, and the cigarette sample that adopts the tobacco fiber paper filter rod obtained by the present invention as the test sample, carry out the cigarette sensory evaluation and smoking, the results are shown in Table 2, and the scores of the sensory evaluation and smoking are divided by 7 The average score is obtained after each professional reviewer scores each item (the full score for each item is 10 points, and one decimal place is reserved after the decimal point. The better the trend, the higher the score).
表2感官评价结果Table 2 Sensory evaluation results
本发明实施例1至4滤棒的试验样产品烟气软绵、细腻,流速较慢,绵长感明显增加;香气协调性好,杂气小,烟气润感显著增加,口腔回甘明显,整体舒适度明显提升;其中实施例3和实施例4试验样烟气明显有甘醇的回味,十分自然爽口。The smoke of the test sample products of the filter rods of Examples 1 to 4 of the present invention is soft and delicate, the flow rate is relatively slow, and the lingering feeling is obviously increased; the aroma coordination is good, the miscellaneous gas is small, the smoke moistness is significantly increased, and the oral cavity is obviously sweet. The overall comfort level is significantly improved; among them, the smoke of the test samples of Example 3 and Example 4 obviously has a mellow aftertaste, which is very natural and refreshing.
3、卷烟烟气七种有害成分化学分析3. Chemical analysis of seven harmful components in cigarette smoke
以采用醋酸纤维滤棒的卷烟为对照样,与采用本发明实施例3所得烟草纤维纸质滤棒的卷烟样品为试验样,根据卷烟危害性评价指数,对样品燃吸产生的烟气成分进行化学检测,以7种主要的有害物质作为检测指标,卷烟危害性指数见表3所示,结果显示,本发明实施例样品的危害性指数与正常样相比,降低了16.17%。Taking the cigarette that adopts the cellulose acetate filter rod as the control sample, and the cigarette sample that adopts the tobacco fiber paper filter rod obtained in Example 3 of the present invention as the test sample, according to the cigarette hazard evaluation index, the smoke components generated by the burning of the sample are analyzed. For chemical detection, 7 main harmful substances are used as detection indicators. The hazard index of cigarettes is shown in Table 3. The results show that the hazard index of the sample of the embodiment of the present invention is reduced by 16.17% compared with the normal sample.
表3卷烟危害性评价结果Table 3 Results of cigarette hazard evaluation
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