CN104256885A - Tobacco juice solvent for electronic cigarette - Google Patents
Tobacco juice solvent for electronic cigarette Download PDFInfo
- Publication number
- CN104256885A CN104256885A CN201410381331.4A CN201410381331A CN104256885A CN 104256885 A CN104256885 A CN 104256885A CN 201410381331 A CN201410381331 A CN 201410381331A CN 104256885 A CN104256885 A CN 104256885A
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- China
- Prior art keywords
- tobacco juice
- solvent
- electronic cigarette
- electronic
- electronic smoke
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a tobacco juice solvent for an electronic cigarette. The tobacco juice solvent for the electronic cigarette comprises 10wt%-50wt% of butanediol, 5wt%-15wt% of polyethylene glycol, 5wt%-15wt% of triethylene glycol, 1wt%-5wt% of triacetin, 1wt%-5wt% of diacetin, 1wt%-5wt% of sweet taste inhibitor solutions and the balance glycerin, wherein the sweet taste inhibitor solutions are sweet taste inhibitor aqueous solutions or propylene glycol solutions, and the concentration of the sweet taste inhibitor solutions is 5wt%-15wt%. When the electronic cigarette prepared from the tobacco juice solvent is smoked, sweet greasy is avoided, the drying feeling is light, the taste is bitter, and a good application prospect in the development of the tobacco juice solvent of the electronic cigarette is achieved.
Description
Technical field
The invention belongs to electronic cigarette technical field, particularly a kind of tobacco juice for electronic smoke solvent.
Background technology
Electronic cigarette is a kind of important supplementary of traditional cigarette, swift and violent in European & American Market growth in recent years.Electronic cigarette formula of liquid is the core technology of electronic cigarette, and it is dissolved in tobacco juice solvent primarily of nicotine and makes, and also has some other additive.And tobacco juice solvent generally accounts for more than 90% of tobacco juice formula gross mass, the aesthetic quality of solvent formula on electronic cigarette has very important impact.
Existing tobacco juice for electronic smoke solvent, primarily of propane diols and glycerine composition, because the sweet soapy feeling of glycerine is overweight, has had a strong impact on the mouthfeel of electronic cigarette.Now gather as follows with regard to tobacco juice for electronic smoke solvent Patents and solvent composition: patent " a kind of non-combustible electronic spraying cigarette " (application number 03111582.9) of the inventor Han Li application in 2003 of electronic cigarette, disclose a kind of nicotine solution for being atomized, its solvent composition mainly comprises propane diols, glycerine, water and ethanol etc.Repair two patents of invention " a kind of atomized liquid of electronic simulation cigarette " (application number 200910310536.2) and " a kind of electronic simulated cigarette and atomized liquid thereof " (application number 200810090523.4) of fortune application in strong 2008, disclosed atomized liquid, its solvent composition the former mainly comprise polyethylene glycol, propane diols and glycerine, the latter mainly comprises polyethylene glycol, propane diols, glycerine and pure water.The patent of invention " atomized liquid of electronic smoke " (application number 200910104922.6) of China's application in strong 2009, disclose a kind of atomized liquid of electronic smoke, solvent composition mainly contains propane diols, pure water; Another patent of invention " medicinal health type tobacco juice for electronic smoke " of China's application in strong 2009, disclosed a kind of tobacco juice, its solvent composition is also mainly propane diols and pure water.Patent of invention " a kind of preparation method of electronic cigarette liquid " (application number 201110184068.6) of the application in 2011 such as Zheng Junxiang, disclosed electronic cigarette liquid, its solvent is mainly at least one in propane diols and polyethylene glycol, also comprises Tween 80.The patent of invention " a kind of fire-cured tobacco type electronic cigarette tobacco liquid " (application number 201110263484.5) of Yao Ji moral application in 2011, disclosed a kind of electronic cigarette tobacco liquid, the key component of its solvent is glycerine, distilled water, alcohol and propane diols; The patent of invention " a kind of mixed type electronic cigarette tobacco liquid " (application number 201210281706.0) of Yao Ji moral application in 2011, disclosed electronic cigarette tobacco liquid, the main component of its solvent is also glycerine, distilled water, alcohol and propane diols.The patent of invention " a kind of anti-oxidant, softening blood vessel, fresh breath function tobacco juice for electronic smoke " (application number 201210267945.0) of the application in 2012 such as Zhang Zhijun, disclosed electronic cigarette liquid, its solvent forms primarily of propane diols, glycerine and water.The patent of invention " simple and elegant odor type electronic cigarette atomizing tobacco juice and preparation method thereof " (application number 201210457376.6) of the application in 2012 such as Liu Huachen, disclosed a kind of atomization tobacco juice, its solvent composition is mainly propane diols, glycerine, deionized water and alcohol.The patent of invention " a kind of tobacco juice for electronic smoke solvent and tobacco juice for electronic smoke " (application number 201310625207.3) of Liu Qiu application in bright 2013, disclose a kind of tobacco juice for electronic smoke solvent, its main component comprises at least one in propane diols, glycerine, sweet mellow wine, also comprises sorb alcohol and water.The patent of invention " a kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof " (application number 201310677976.8) of the application in 2013 such as Chu Guohai, disclosed tobacco juice for electronic smoke, its solvent forms primarily of deionized water, glycerine and propane diols.The patent of invention " a kind of electronic cigarette atomization tobacco juice and preparation method " (application number 201310686110.3) of the application in 2013 such as soup foundation, disclosed atomization tobacco juice, its solvent is also form primarily of deionized water, glycerine and propane diols.Patent " electronic cigarette oil solvent " (application number 201410028485.5) of the application in 2014 such as Gu Shangkai, disclose a kind of electronic cigarette oil solvent, this solvent joins di-methylcarbinol, triethylene glycol, tetraethylene glycol, five glycol, hexaethylene glycol, seven glycol, eight glycol compositions by 2,2-oxygen.Tobacco juice for electronic smoke solvent composition described in above patent mainly contains propane diols, glycerine, polyethylene glycol, water, alcohol, sweet mellow wine, sorbierite, Tween 80,2,2-oxygen connection di-methylcarbinol, triethylene glycol, tetraethylene glycol, five glycol, hexaethylene glycol, seven glycol, eight glycol etc.
The relevant report that butanediol, glyceryl triacetate, diacetine and sweet taste inhibitor are applied in tobacco juice for electronic smoke solvent is had no in existing tobacco juice for electronic smoke solvent.
Electronic cigarette substituting as conventional cigarette, expects that it can give consumer similar impression on sense organ.The aesthetic quality of tobacco juice for electronic smoke solvent formula on electronic cigarette has very important impact, uses the electronic cigarette that existing tobacco juice for electronic smoke solvent is made, the defect that the sweet soapy feeling of ubiquity is overweight in aspiration procedure and not have in conventional cigarette slightly bitter taste.Therefore, the electronic cigarette adopting existing tobacco juice solvent to make gives the sense organ of consumer and conventional cigarette has very large difference, cannot substitute conventional cigarette to meet the organoleptic requirements of user.
Tobacco juice for electronic smoke solvent of the present invention have employed butanediol innovatively, glyceryl triacetate, diacetine and sweet taste inhibitor, not only solve the heavy problem of the sweet soapy feeling of existing tobacco juice for electronic smoke and make it have the slightly bitter taste of conventional cigarette, the sense organ giving the low sweet soapy feeling of consumer and slightly bitter taste with conventional cigarette is more close, for certain basis has been established in the exploitation of tobacco juice for electronic smoke from now on.
Summary of the invention
The object of the invention is to, for the overweight problem of the ubiquitous sweet soapy feeling of existing tobacco juice for electronic smoke solvent, provide a kind of sweetless greasy tobacco juice for electronic smoke solvent, and this solvent has poor mouthfeel.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is mass percent.
A kind of tobacco juice for electronic smoke solvent, it comprises following component: butanediol 10 ~ 50wt%, polyethylene glycol 5 ~ 15wt%, triethylene glycol 5 ~ 15wt%, glyceryl triacetate 1 ~ 5wt%, diacetine 1 ~ 5wt%, sweet taste inhibitor solution 1 ~ 5wt%, surplus is glycerine; Wherein said sweet taste inhibitor solution is the aqueous solution or the propylene glycol solution of sweet taste inhibitor, and concentration is 5 ~ 15wt%.In a preferred embodiment of the present invention, the concentration of sweet taste inhibitor solution is 10wt%.
Wherein said butanediol is the mixture of one or more in 1,2-butanediol, 1,3-BDO, 2,3-butanediol and BDO, and in a preferred embodiment of the present invention, described butanediol is 1,3-BDO.
In a preferred embodiment of the present invention, described polyethylene glycol is the mixture of one or more in Macrogol 200, PEG400 and Macrogol 600, is more preferably Macrogol 200.
In a preferred embodiment of the present invention; described sweet taste inhibitor is the mixture of one or more in 2-(4-methoxyphenoxy)-propionic acid, 2-(4-methoxyphenoxy)-sodium propionate, 2-(4-methoxyphenoxy)-zinc propionate, 3-(4-methoxybenzoyl base)-propionic acid, gymnemic acid, is wherein more preferably 2-(4-methoxyphenoxy)-sodium propionate.
Tobacco juice for electronic smoke solvent of the present invention have employed butanediol, glyceryl triacetate, diacetine and sweet taste inhibitor innovatively, not only solve the heavy problem of the sweet soapy feeling of existing tobacco juice for electronic smoke and make it have the slightly bitter taste of conventional cigarette, the sense organ giving the low sweet soapy feeling of consumer and slightly bitter taste with conventional cigarette is more close, for certain basis has been established in the exploitation of tobacco juice for electronic smoke from now on.
Compared with prior art, tool of the present invention has the following advantages:
1, tobacco juice for electronic smoke solvent of the present invention is sweetless greasy, substantially improves the mouthfeel of electronic cigarette;
2, tobacco juice for electronic smoke solvent atomization of the present invention is effective, and in electronic cigarette, after application, atomization quantity is larger;
3, during tobacco juice for electronic smoke solvent of the present invention suction, taste is slightly bitter, with the aesthetic quality of traditional cigarette closer to.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is illustrated, it should be noted that embodiment is limited the present invention never in any form.
Embodiment 1-9
In embodiment 1-9, tobacco juice for electronic smoke solvent composition is as shown in table 1.
Wherein "/" represents in the solvent composition of this embodiment not containing corresponding component.
Table 1
Comparative example 1
Electronic cigarette aqueous slkali described in patent " a kind of non-combustible electronic spraying cigarette " (application number 03111582.9), its solution solvent composition comprises following component: propane diols 80wt%, glycerine 8wt%, water 4wt%, alcohol 8wt%.
Comparative example 2
Electronic cigarette atomizing liquid described in patent " a kind of atomized liquid of electronic simulation cigarette " (application number 200910310536.2), its solvent composition can comprise following component: Macrogol 200 55wt%, propane diols 45wt%.
Contrast experiment
Added in identical disposable electric cigarette with identical addition by the tobacco juice for electronic smoke solvent made according to each component proportion in embodiment 1 ~ 9, comparative example 1 ~ 2, and carry out sensory quality assessment, sensory quality assessment the results are shown in Table 3.
Tobacco juice for electronic smoke solvent sensory quality assessment method:
Sensory quality assessment project and scale are arranged: arrange 6 projects, be respectively resistance to suction, amount of smoke, dry sensation, chemical breath, sweet soapy feeling, pleasant impression; Wherein the maximum scale of projects is all 9, and projects are all divided into scoring unit with 1, corresponding to the meaning of each scale value of each assessment item in table 2.
Check problem: provide sample and check table to the expert that smokes panel test, requires that member of smoking smokes panel test to indices according to form requirement.
Result is added up: the smoking result of all members of smoking is all effective, and the individual event smoking result of each member of smoking is asked arithmetic mean of instantaneous value, and result remains to a decimal, and the arithmetic mean of instantaneous value of each individual event is added and, obtain total score, result remains to a decimal, and evaluation result is in table 3.
Table 2
Table 3
As shown in Table 3, compared with two comparative examples, the total score of tobacco juice for electronic smoke solvent of the present invention is all higher, and the sweet soapy feeling that advantage is mainly manifested in tobacco juice for electronic smoke solvent of the present invention is comparatively light, and next shows that amount of smoke is all in larger level.Tobacco juice for electronic smoke solvent of the present invention is because of each component usage ratio difference, and its aesthetic quality is also not quite similar, and as seen from the above table, in embodiment 7, each component ratio structure is more rational, and aesthetic quality's score is the highest.The rareest, tobacco juice for electronic smoke solvent of the present invention has slightly bitter taste, can give consumer the taste perception closer to conventional cigarette, for the development of tobacco juice for electronic smoke solvent is from now on laid a good foundation.
Claims (4)
1. a tobacco juice for electronic smoke solvent, it comprises following component: butanediol 10 ~ 50wt%, polyethylene glycol 5 ~ 15wt%, triethylene glycol 5 ~ 15wt%, glyceryl triacetate 1 ~ 5wt%, diacetine 1 ~ 5wt%, sweet taste inhibitor solution 1 ~ 5wt%, surplus is glycerine; Wherein said sweet taste inhibitor solution is the aqueous solution or the propylene glycol solution of sweet taste inhibitor, and concentration is 5 ~ 15wt%.
2. tobacco juice for electronic smoke solvent according to claim 1, wherein said butanediol is the mixture of one or more in 1,2-butanediol, 1,3-BDO, 2,3-butanediol and BDO.
3. tobacco juice for electronic smoke solvent according to claim 1, wherein said polyethylene glycol is the mixture of one or more in Macrogol 200, PEG400 and Macrogol 600.
4. tobacco juice for electronic smoke solvent according to claim 1, wherein said sweet taste inhibitor is the mixture of one or more in 2-(4-methoxyphenoxy)-propionic acid, 2-(4-methoxyphenoxy)-sodium propionate, 2-(4-methoxyphenoxy)-zinc propionate, 3-(4-methoxybenzoyl base)-propionic acid, gymnemic acid.
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| CN201410381331.4A CN104256885B (en) | 2014-08-05 | 2014-08-05 | A kind of tobacco juice for electronic smoke solvent |
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| CN201410381331.4A CN104256885B (en) | 2014-08-05 | 2014-08-05 | A kind of tobacco juice for electronic smoke solvent |
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| CN104256885A true CN104256885A (en) | 2015-01-07 |
| CN104256885B CN104256885B (en) | 2015-12-30 |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104585866A (en) * | 2015-01-20 | 2015-05-06 | 川渝中烟工业有限责任公司 | Ultrasonic atomized electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof |
| CN104824835A (en) * | 2015-06-05 | 2015-08-12 | 中国烟草总公司郑州烟草研究院 | Application of Kahlua additive in electronic cigarettes |
| CN104824834A (en) * | 2015-05-26 | 2015-08-12 | 郑悦 | Electronic cigarette liquid and preparing method thereof |
| WO2015117243A1 (en) * | 2014-02-07 | 2015-08-13 | Bellerose Samuel | Liquid formulation for e-cigarettes |
| CN104939298A (en) * | 2015-05-21 | 2015-09-30 | 湖南中烟工业有限责任公司 | Atomizing agent for electronic cigarette and electronic cigarette liquid |
| CN106036990A (en) * | 2016-08-03 | 2016-10-26 | 华健 | Mixtanol electronic aerosolization solution |
| CN106983182A (en) * | 2017-06-02 | 2017-07-28 | 北京中教知行互动科技中心 | Fragrant electronic cigarette atomizing liquid of a kind of wine and preparation method thereof |
| CN109475181A (en) * | 2016-07-22 | 2019-03-15 | 日本烟草产业株式会社 | The tobacco filler of non-combustion-type heating smoking article |
| CN110167365A (en) * | 2017-02-03 | 2019-08-23 | 菲利普莫里斯生产公司 | The method and system of the stability of composite before steam for improving electrical steam cigarette device |
| CN110786540A (en) * | 2019-12-05 | 2020-02-14 | 广西中烟工业有限责任公司 | Novel non-glycerin electronic cigarette tobacco tar substrate with uniformly distributed fog particle sizes |
| WO2020141177A1 (en) * | 2018-12-31 | 2020-07-09 | Philip Morris Products S.A. | Liquid nicotine formulation comprising water-immiscible solvents |
| CN112851636A (en) * | 2021-01-20 | 2021-05-28 | 深圳市艾普生物科技有限公司 | Preparation method and application of synthetic nicotine salt |
| CN114158762A (en) * | 2020-09-10 | 2022-03-11 | 湖南中烟工业有限责任公司 | Smoking agent, smoking material and preparation method thereof |
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| CN103808849A (en) * | 2014-03-16 | 2014-05-21 | 国家烟草质量监督检验中心 | Method for measuring content of menthol in electronic cigarette liquid |
| CN103808831A (en) * | 2014-03-16 | 2014-05-21 | 国家烟草质量监督检验中心 | Method for simultaneously determining content of 1,2-propylene glycol, menthol, diethylene glycol, glycerin and triethylene glycol in electronic cigarette juice |
| CN103932404A (en) * | 2014-04-15 | 2014-07-23 | 上海聚华科技股份有限公司 | Electronic cigarette with ultrasonic atomization function and tobacco liquid |
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Patent Citations (4)
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| CN103054172A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from strong-flavor tobacco leaves |
| CN103808849A (en) * | 2014-03-16 | 2014-05-21 | 国家烟草质量监督检验中心 | Method for measuring content of menthol in electronic cigarette liquid |
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Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015117243A1 (en) * | 2014-02-07 | 2015-08-13 | Bellerose Samuel | Liquid formulation for e-cigarettes |
| CN104585866A (en) * | 2015-01-20 | 2015-05-06 | 川渝中烟工业有限责任公司 | Ultrasonic atomized electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof |
| CN104585866B (en) * | 2015-01-20 | 2016-03-30 | 川渝中烟工业有限责任公司 | Ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide and preparation method thereof |
| CN104939298A (en) * | 2015-05-21 | 2015-09-30 | 湖南中烟工业有限责任公司 | Atomizing agent for electronic cigarette and electronic cigarette liquid |
| CN104824834A (en) * | 2015-05-26 | 2015-08-12 | 郑悦 | Electronic cigarette liquid and preparing method thereof |
| CN104824835A (en) * | 2015-06-05 | 2015-08-12 | 中国烟草总公司郑州烟草研究院 | Application of Kahlua additive in electronic cigarettes |
| CN104824835B (en) * | 2015-06-05 | 2017-01-18 | 中国烟草总公司郑州烟草研究院 | Application of Kahlua additive in electronic cigarettes |
| CN109475181B (en) * | 2016-07-22 | 2021-07-20 | 日本烟草产业株式会社 | Tobacco filler for non-combustion heating smoking article |
| CN109475181A (en) * | 2016-07-22 | 2019-03-15 | 日本烟草产业株式会社 | The tobacco filler of non-combustion-type heating smoking article |
| CN106036990A (en) * | 2016-08-03 | 2016-10-26 | 华健 | Mixtanol electronic aerosolization solution |
| CN110167365A (en) * | 2017-02-03 | 2019-08-23 | 菲利普莫里斯生产公司 | The method and system of the stability of composite before steam for improving electrical steam cigarette device |
| CN106983182A (en) * | 2017-06-02 | 2017-07-28 | 北京中教知行互动科技中心 | Fragrant electronic cigarette atomizing liquid of a kind of wine and preparation method thereof |
| WO2020141177A1 (en) * | 2018-12-31 | 2020-07-09 | Philip Morris Products S.A. | Liquid nicotine formulation comprising water-immiscible solvents |
| CN113163847A (en) * | 2018-12-31 | 2021-07-23 | 菲利普莫里斯生产公司 | Liquid nicotine formulation comprising water-immiscible solvent |
| US11992038B2 (en) | 2018-12-31 | 2024-05-28 | Philip Morris Products S.A. | Liquid nicotine formulation comprising partially water-soluble solvent |
| CN110786540A (en) * | 2019-12-05 | 2020-02-14 | 广西中烟工业有限责任公司 | Novel non-glycerin electronic cigarette tobacco tar substrate with uniformly distributed fog particle sizes |
| CN110786540B (en) * | 2019-12-05 | 2022-06-17 | 广西中烟工业有限责任公司 | Novel non-glycerin electronic cigarette tobacco tar substrate with uniformly distributed fog particle sizes |
| CN114158762A (en) * | 2020-09-10 | 2022-03-11 | 湖南中烟工业有限责任公司 | Smoking agent, smoking material and preparation method thereof |
| CN114158762B (en) * | 2020-09-10 | 2023-03-03 | 湖南中烟工业有限责任公司 | Smoking agent, smoking material and preparation method thereof |
| CN112851636A (en) * | 2021-01-20 | 2021-05-28 | 深圳市艾普生物科技有限公司 | Preparation method and application of synthetic nicotine salt |
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