CN104585866B - Ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide and preparation method thereof - Google Patents
Ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide and preparation method thereof Download PDFInfo
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- CN104585866B CN104585866B CN201510027854.3A CN201510027854A CN104585866B CN 104585866 B CN104585866 B CN 104585866B CN 201510027854 A CN201510027854 A CN 201510027854A CN 104585866 B CN104585866 B CN 104585866B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Abstract
The invention discloses a kind of ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide, its raw material primarily of following weight portion is made: deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.Electronic cigarette liquid difference of the present invention and conditional electronic atomizing type tobacco juice, without high-temperature heating atomization process, be applicable to the electronic cigarette that ultrasonic atomization mode carries out aspirating; Characteristic tobacco extract and natural bioactive polyoses extract are combined together simultaneously, while making consumer obtain sucking cigarette impression, have adjusted immune function of human body efficiently, have certain health-care efficacy concurrently.
Description
Technical field
The present invention relates to novel electron tobacco juice field, particularly relate to a kind of ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide and preparation method thereof.
Background technology
At present, under the macroeconomic situation that global Tobacco use control continues reinforcement and economic growth continued downturn, World tobacco industry faces a severe challenge.In order to reduce the impact of traditional cigarette on consumer, heating do not burn cigarette, electronic cigarette, buccal cigarette, chew the novel tobacco goods such as cigarette and day by day become the emerging strategic product of tobacco industry, domestic and international tobacco business is by the Major Strategic problem of Development of Novel tobacco product as tobacco business future development.
Electronic cigarette and electronics nicotine delivery device are by Chinese's innovation and creation, but intellectual property is not at tobacco tobacco business.At present, foreign tobacco giant all scolds a huge sum of money to set foot in the research and development that electronic cigarette field carries out Related product.Novel electron tobacco juice is atomized into mist by atomising device by electronic cigarette allows consumer know from experience the sensation of similar smoking.Because of electronic cigarette, to there is not tobacco high temperature pyrolysis domestic, therefore tar content is almost nil, does not have visible flow measurement flue gas, less to surrounding environment influence, gradually by consumer acceptance.Nicotine and flavor component etc. discharge mainly through propane diols and glycerine atomization by current electronic cigarette.But going deep in recent years to the research of electronic cigarette harmfulness, studies have reported that it is similar with traditional cigarette in induced tumor sudden change, some harmful components burst size abroad.Therefore, explore non-heated mode and be atomized, namely ultrasonic atomizatio becomes possibility.
Research confirms, the diseases such as smoking and some respiratory disease, tumour cancer occur relevant.Polysaccharide is extensively present in animal, plant and microorganism wall, toxicity is little, security is high, function is extensive, there is extremely important with special physiologically active, heterogeneity polysaccharide forms proteoglycans by covalent bond and protein and plays biological function, as body lubricating agent, identify the cell of external organization, the basis etc. of blood group substance.In addition, bioactive polysaccharide participates in the immunological regulation of organism, participates in the various activities of life cells, has hypoglycemic, reducing blood lipid, anti-inflammatory, anti-oxidant, anti-ageing, antitumor etc. simultaneously.
Electronic cigarette liquid is the soul that consumer obtains similar impression of smoking, and its quality directly affects the impression of consumer, but existing electronic cigarette liquid is also not overripened, especially almost blank at ultrasonic atomizatio tobacco juice for electronic smoke.In addition, electronic cigarette is due to healthy, environmental protection, and by large-scale popularization, so to particularly important in the one-tenth component selections of Novel electric cigarette formula of liquid, meeting outside smoking requirement, composition matches more healthy better.
Summary of the invention
For the weak point that prior art exists, the object of the present invention is to provide a kind of ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide, this novel electron tobacco juice is applicable to ultrasonic atomizatio mode and aspirates, refine for characteristic tobacco extract and natural bioactive polyoses extract and form, while making consumer obtain sucking cigarette impression, also have adjusted immune function of human body efficiently, there is certain health-care effect.
Object of the present invention is achieved through the following technical solutions:
Be rich in a ultrasonic atomizatio electronic cigarette liquid for bioactive polysaccharide, its raw material primarily of following weight portion is made:
Deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part;
Described natural bioactive polyoses extract be fungi polysaccharide, plant polyose, marine polysaccharide, shitosan one or more.
The present invention's preferred Novel electric cigarette formula of liquid is made up of the raw material of following weight portion:
Deionized water 65 ~ 75 parts, natural bioactive polyoses extract 8 ~ 12 parts, tobacco extract 4 ~ 6 parts, water-soluble flavouring essence for tobacco 2 ~ 4 parts, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.
In order to realize the present invention better, described fungi polysaccharide is one or more mixing of lentinan, flammulina velutipes, GL-B, Cordyceps sinensis polysaccharide, pachymaran, grifola polysaccharide, Blackfungus polyhexose, tremella polysaccharides; Described plant polyose is one or more mixing of tea polysaccharide, red jujube polysaccharide, LBP-X, astragalus polyose, panaxan, Siberian solomonseal rhizome polysaccharide, Radix Et Caulis Acanthopanacis Senticosi polysaccharide, polysaccharides from ginkgo biloba; Described marine polysaccharide is one or both mixing of algal polysaccharides, spirulina polysaccharide; Described shitosan be crab shell element, chitin polysaccharide, bright angle glutelin one or both; Described tobacco extract is one or more mixing of flue-cured tobacco, burley tobaccos and cigar.
Described tobacco extract is the extract in flue-cured tobacco or burley tobaccos or cigar tobacco.
Be rich in a ultrasonic atomizatio electronic cigarette liquid preparation method for bioactive polysaccharide, its preparation method comprises the steps:
Prepared by steps A, raw material:
The extraction of natural bioactive polyoses extract: extract natural bioactive polyoses extract by water distillating method or supercritical extraction method from natural bioactive polysaccharide, described natural bioactive polyoses extract be fungi polysaccharide, plant polyose, marine polysaccharide, shitosan one or more;
The extraction of tobacco extract: extract tobacco extract from tobacco, described tobacco extract is the extract in flue-cured tobacco or burley tobaccos or cigar tobacco;
Step B, prepare novel electron tobacco juice: fully mix according to the raw material of following weight portion and obtain novel electron tobacco juice: deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.
In Novel electric cigarette liquid and preparation method thereof, the present invention can adopt water distillating method and supercritical extraction method two kinds of methods to extract natural bioactive polyoses extract, is: the water distillating method extracting natural bioactive polyoses extract in described steps A is as follows as the concrete technical scheme of the present invention's preferred water distillating method:
First-selection, carries out being mixed to form extract according to mass ratio 1:20 ~ 1:5 by natural bioactive polysaccharide and distilled water; Then adopt ultrasonic wave added Hot water extraction to extract, its ultrasonic time is 10 ~ 40 minutes, while extraction, controls extracting liquid pH value between 7 ~ 9, controls extract temperature at 60 DEG C ~ 100 DEG C;
Namely extract extract after ultrasonic, extraction time is 0.5 ~ 2 hour, and the material of extraction, after separation, purification process, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
The water distillating method extracting natural bioactive polyoses extract further in preferred steps A is as follows:
First-selection, carries out being mixed to form extract according to mass ratio 1:20 ~ 1:5 by natural bioactive polysaccharide and distilled water; Then adopt ultrasonic wave added Hot water extraction to extract, its ultrasonic time is 10 ~ 40 minutes, while extraction, controls extracting liquid pH value between 7 ~ 9, controls extract temperature at 60 DEG C ~ 100 DEG C; Namely extract extract after ultrasonic, extraction time is 0.5 ~ 2 hour, and the material of extraction, after separation, purification process, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
In Novel electric cigarette liquid and preparation method thereof, as the concrete technical scheme of the present invention's preferred water distillating method be: the supercritical extraction method extracting natural bioactive polyoses extract in described steps A is as follows:
Natural bioactive polysaccharide is put into the ethanolic solution that concentration is 1% ~ 20%, and the weight of ethanolic solution is 0.5 ~ 2 times of natural bioactive polysaccharide dry matter weight; Then the ethanolic solution with natural bioactive polysaccharide is carried out supercritical extract process, control extracting pressure is 10 ~ 45MPa, extraction temperature 40 DEG C ~ 85 DEG C, CO
2flow-control is at 10 ~ 30L/h, and extraction time controls at 30 ~ 180 minutes, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
The supercritical extraction method extracting natural bioactive polyoses extract further in preferred steps A is as follows:
Natural bioactive polysaccharide is put into the ethanolic solution that concentration is 1% ~ 20%, and the weight of ethanolic solution is 0.8 ~ 1.8 times of natural bioactive polysaccharide dry matter weight; Then the ethanolic solution with natural bioactive polysaccharide is carried out supercritical extract process, control extracting pressure is 30 ~ 45MPa, extraction temperature 60 DEG C ~ 85 DEG C, CO
2flow-control is at 20 ~ 25L/h, and extraction time controls at 90 ~ 120 minutes, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
The present invention comparatively prior art compares, and has the following advantages and beneficial effect:
(1) novel electron tobacco juice of the present invention is applicable to ultrasonic atomizatio mode and aspirates, characteristic tobacco extract and natural bioactive polyoses extract are refined and are formed, while making consumer obtain sucking cigarette impression, also have and strengthen immunologic function, prevent disease, adjustment human physiological functions, antitumor, radioresistance, anti-oxidant, anti anoxia, antiallergy, anti-inflammatory, reducing blood lipid, reduction blood viscosity, the health-care effect such as hypoglycemic.
(2) the invention provides water distillation or supercritical extract two kinds of technique extracting methods to extract various polysaccharides, the chitosan material in natural bioactive polysaccharide, raw material pure natural, to add without chemistry, leaching process environmental protection and efficiency is higher.
(3) the present invention adopts water to be medium, and ultrasonic atomization mode will be transferred to human body containing nicotine, fragrance matter and natural bioactive polysaccharide.Avoid with propane diols, glycerine for medium, burst size is higher causes potential harmfulness for the formaldehyde etc. that brings of heating atomization mode.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail:
Embodiment
Be rich in a ultrasonic atomizatio electronic cigarette liquid for bioactive polysaccharide, its raw material primarily of following weight portion is made:
Deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part;
Described natural bioactive polyoses extract be fungi polysaccharide, plant polyose, marine polysaccharide, shitosan one or more.
Described water-soluble flavouring essence for tobacco is conventional flavouring essence for tobacco, and it is bought easily in each essence spice for cigarette company, and described flavouring, antioxidant are the conventional cigarette product that market is sold, and are water-soluble.
According to the preferred ultrasonic atomizatio electronic cigarette liquid embodiment of the present invention one be: its raw material primarily of following weight portion is made:
Deionized water 65 ~ 75 parts, natural bioactive polyoses extract 8 ~ 12 parts, tobacco extract 4 ~ 6 parts, water-soluble flavouring essence for tobacco 2 ~ 4 parts, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.
The fungi polysaccharide that the present invention preferably selects is one or more mixing of lentinan, flammulina velutipes, GL-B, Cordyceps sinensis polysaccharide, pachymaran, grifola polysaccharide, Blackfungus polyhexose, tremella polysaccharides.The plant polyose that the present invention preferably selects is one or more mixing of tea polysaccharide, red jujube polysaccharide, LBP-X, astragalus polyose, panaxan, Siberian solomonseal rhizome polysaccharide, Radix Et Caulis Acanthopanacis Senticosi polysaccharide, polysaccharides from ginkgo biloba.The marine polysaccharide that the present invention preferably selects is one or both mixing of algal polysaccharides, spirulina polysaccharide.The shitosan that the present invention preferably selects be crab shell element, chitin polysaccharide, bright angle glutelin one or both.
According to the present invention one preferred embodiment: described tobacco extract is the extract in flue-cured tobacco or burley tobaccos or cigar tobacco.
Be rich in a ultrasonic atomizatio electronic cigarette liquid preparation method for bioactive polysaccharide, its preparation method comprises the steps:
Prepared by steps A, raw material:
The extraction of natural bioactive polyoses extract: extract natural bioactive polyoses extract by water distillating method or supercritical extraction method from natural bioactive polysaccharide, described natural bioactive polyoses extract be fungi polysaccharide, plant polyose, marine polysaccharide, shitosan one or more;
The extraction of tobacco extract: extract tobacco extract from tobacco, described tobacco extract is the extract in flue-cured tobacco or burley tobaccos or cigar tobacco;
Step B, prepare novel electron tobacco juice: fully mix according to the raw material of following weight portion and obtain novel electron tobacco juice: deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.Described water-soluble flavouring essence for tobacco is conventional flavouring essence for tobacco, and it is bought easily in each essence spice for cigarette company, and described thickener, antioxidant are the conventional cigarette product that market is sold, and are water-soluble.
According to the first preferred natural bioactive polyoses extract extracting method in Novel electric cigarette liquid and preparation method thereof of the present invention, the water distillating method extracting natural bioactive polyoses extract in described steps A is as follows:
First-selection, carries out being mixed to form extract according to mass ratio 1:20 ~ 1:5 by natural bioactive polysaccharide and distilled water; Then adopt ultrasonic wave added Hot water extraction to extract, its ultrasonic time is 10 ~ 40 minutes, while extraction, controls extracting liquid pH value between 7 ~ 9, controls extract temperature at 60 DEG C ~ 100 DEG C;
Namely extract extract after ultrasonic, extraction time is 0.5 ~ 2 hour, and the material of extraction, after separation, purification process, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
According to the preferred embodiment of a water distillating method of the present invention, the water distillating method extracting natural bioactive polyoses extract in described steps A is as follows:
First-selection, carries out being mixed to form extract according to mass ratio 1:10 by natural bioactive polysaccharide and distilled water; Then adopt ultrasonic wave added Hot water extraction to extract, its ultrasonic time is 30 minutes, and while extraction, controlling extracting liquid pH value is 8, controls extract temperature at 80 DEG C;
Namely extract extract after ultrasonic, extraction time is 1.5 hours, and the material of extraction, after separation, purification process, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
According to the second preferred natural bioactive polyoses extract extracting method in Novel electric cigarette liquid and preparation method thereof of the present invention, the supercritical extraction method extracting natural bioactive polyoses extract in described steps A is as follows:
Natural bioactive polysaccharide is put into the ethanolic solution that concentration is 1% ~ 20%, and the weight of ethanolic solution is 0.5 ~ 2 times of natural bioactive polysaccharide dry matter weight; Then the ethanolic solution with natural bioactive polysaccharide is carried out supercritical extract process, control extracting pressure is 10 ~ 45MPa, extraction temperature 40 DEG C ~ 85 DEG C, CO
2flow-control is at 10 ~ 30L/h, and extraction time controls at 30 ~ 180 minutes, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
According to the preferred embodiment of a supercritical extraction method of the present invention, the supercritical extraction method extracting natural bioactive polyoses extract in described steps A is as follows:
Natural bioactive polysaccharide is put into the ethanolic solution that concentration is 1% ~ 20%, and the weight of ethanolic solution is 0.8 ~ 1.8 times of natural bioactive polysaccharide dry matter weight; Then the ethanolic solution with natural bioactive polysaccharide is carried out supercritical extract process, control extracting pressure is 30 ~ 45MPa, extraction temperature 60 DEG C ~ 85 DEG C, CO
2flow-control is at 20 ~ 25L/h, and extraction time controls at 90 ~ 120 minutes, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
Matrimony vine is China's tradition rare traditional Chinese medicine, have " red treasured " laudatory title, is rich in plant polyose, protein, vitamins and other nutritious components.LBP-X is a kind of water-soluble polysaccharide extracting from matrimony vine and obtain.Clearly this polysaccharide system proteoglycan, is made up of arabinose, glucose, galactolipin, mannose, wood sugar, rhamnose 6 kinds of monosaccharide components.The main active show after deliberation, LBP-X is fruit of Chinese wolfberry immunity moderation, delaying senility, can improve the symptoms such as the elderly's fatiguability, poor appetite and eye-blurred, and have reducing blood lipid, AFL, the anti-ageing effect of waiting for a long time.Research confirms, algal polysaccharides is embodied in immunoregulation effect: 1. to the adjustment of immunocyte and cell factor.Algal polysaccharides can stimulate the differentiation of various immunocompetent cell (as macrophage, T lymphocyte, bone-marrow-derived lymphocyte etc.), maturation, breeding, makes the immune system of body be restored and strengthen.2. to the effect of complement system.Excess complement activation, not only can consume a large amount of complement components, the anti-infection ability of body is caused to decline, and produce in activation and a large amount of there is bioactive material, cause body that excessive inflammatory reaction occurs and cause the damage of autologous tissue and cell, and sea-tangle water-soluble polysaccharide has certain effect to complement bypass.
There is not high temperature pyrolysis reaction in the ultrasonic atomizatio electronic cigarette liquid that bioactive polysaccharide is rich in the present invention, without the reaction of conditional electronic cigarette 200-300 DEG C of heating atomization, do not adopt with propane diols and glycerine as medium simultaneously, therefore releasing content of coke tar is almost nil, Form aldehyde release is almost nil, meeting while consumer obtains smoking experience, real reduce on self, the impact of other people and environment.Meanwhile, the interpolation of natural bioactive polyoses extract, can activating cell, suppress aging, strengthen immunologic function, prevent disease, adjustment human physiological functions, antitumor, radioresistance, anti-oxidant, anti anoxia, antiallergy, anti-inflammatory etc.In addition, can also reducing blood lipid, reduce blood viscosity, hypoglycemic etc.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. be rich in a ultrasonic atomizatio electronic cigarette liquid for bioactive polysaccharide, it is characterized in that: its raw material primarily of following weight portion is made:
Deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part;
Described natural bioactive polyoses extract be fungi polysaccharide, plant polyose, marine polysaccharide, shitosan one or more.
2. according to the ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide according to claim 1, it is characterized in that: its raw material primarily of following weight portion is made:
Deionized water 65 ~ 75 parts, natural bioactive polyoses extract 8 ~ 12 parts, tobacco extract 4 ~ 6 parts, water-soluble flavouring essence for tobacco 2 ~ 4 parts, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.
3. according to the ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide described in claim 1 or 2, it is characterized in that: described fungi polysaccharide is one or more mixing of lentinan, flammulina velutipes, GL-B, Cordyceps sinensis polysaccharide, pachymaran, grifola polysaccharide, Blackfungus polyhexose, tremella polysaccharides; Described plant polyose is one or more mixing of tea polysaccharide, red jujube polysaccharide, LBP-X, astragalus polyose, panaxan, Siberian solomonseal rhizome polysaccharide, Radix Et Caulis Acanthopanacis Senticosi polysaccharide, polysaccharides from ginkgo biloba; Described marine polysaccharide is one or both mixing of algal polysaccharides, spirulina polysaccharide; Described shitosan be crab shell element, chitin polysaccharide, bright angle glutelin one or both.
4. according to the ultrasonic atomizatio electronic cigarette liquid being rich in bioactive polysaccharide described in claim 1 or 2, it is characterized in that: described tobacco extract is the extract in flue-cured tobacco or burley tobaccos or cigar tobacco.
5. be rich in a ultrasonic atomizatio electronic cigarette liquid preparation method for bioactive polysaccharide, it is characterized in that: its preparation method comprises the steps:
Prepared by steps A, raw material:
The extraction of natural bioactive polyoses extract: extract natural bioactive polyoses extract by water distillating method or supercritical extraction method from natural bioactive polysaccharide, described natural bioactive polyoses extract be fungi polysaccharide, plant polyose, marine polysaccharide, shitosan one or more;
The extraction of tobacco extract: extract tobacco extract from tobacco, described tobacco extract is the extract in flue-cured tobacco or airing cigarette or burley tobaccos or cigar tobacco;
Step B, prepare electronic cigarette liquid: fully mix according to the raw material of following weight portion and obtain electronic cigarette liquid: deionized water 60 ~ 80 parts, natural bioactive polyoses extract 5 ~ 15 parts, tobacco extract 3 ~ 8 parts, water-soluble flavouring essence for tobacco 1 ~ 5 part, flavouring 1 ~ 3 part, antioxidant 1 ~ 3 part.
6., according to the ultrasonic atomizatio electronic cigarette liquid preparation method being rich in bioactive polysaccharide according to claim 5, it is characterized in that: the water distillating method extracting natural bioactive polyoses extract in described steps A is as follows:
First-selection, carries out being mixed to form extract according to mass ratio 1:20 ~ 1:5 by natural bioactive polysaccharide and distilled water; Then adopt ultrasonic wave added Hot water extraction to extract, its ultrasonic time is 10 ~ 40 minutes, while extraction, controls extracting liquid pH value between 7 ~ 9, controls extract temperature at 60 DEG C ~ 100 DEG C;
Namely extract extract after ultrasonic, extraction time is 0.5 ~ 2 hour, and the material of extraction, after separation, purification process, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
7., according to the ultrasonic atomizatio electronic cigarette liquid preparation method being rich in bioactive polysaccharide according to claim 6, it is characterized in that: the water distillating method extracting natural bioactive polyoses extract in described steps A is as follows:
First-selection, carries out being mixed to form extract according to mass ratio 1:10 by natural bioactive polysaccharide and distilled water; Then adopt ultrasonic wave added Hot water extraction to extract, its ultrasonic time is 30 minutes, and while extraction, controlling extracting liquid pH value is 8, controls extract temperature at 80 DEG C;
Namely extract extract after ultrasonic, extraction time is 1.5 hours, and the material of extraction, after separation, purification process, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
8., according to the ultrasonic atomizatio electronic cigarette liquid preparation method being rich in bioactive polysaccharide according to claim 5, it is characterized in that: the supercritical extraction method extracting natural bioactive polyoses extract in described steps A is as follows:
Natural bioactive polysaccharide is put into the ethanolic solution that concentration is 1% ~ 20%, and the weight of ethanolic solution is 0.5 ~ 2 times of natural bioactive polysaccharide dry matter weight; Then the ethanolic solution with natural bioactive polysaccharide is carried out supercritical extract process, control extracting pressure is 10 ~ 45MPa, extraction temperature 40 DEG C ~ 85 DEG C, CO
2flow-control is at 10 ~ 30L/h, and extraction time controls at 30 ~ 180 minutes, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
9., according to the ultrasonic atomizatio electronic cigarette liquid preparation method being rich in bioactive polysaccharide according to claim 8, it is characterized in that: the supercritical extraction method extracting natural bioactive polyoses extract in described steps A is as follows:
Natural bioactive polysaccharide is put into the ethanolic solution that concentration is 1% ~ 20%, and the weight of ethanolic solution is 0.8 ~ 1.8 times of natural bioactive polysaccharide dry matter weight; Then the ethanolic solution with natural bioactive polysaccharide is carried out supercritical extract process, control extracting pressure is 30 ~ 45MPa, extraction temperature 60 DEG C ~ 85 DEG C, CO
2flow-control is at 20 ~ 25L/h, and extraction time controls at 90 ~ 120 minutes, obtains various natural bioactive polyoses extract respectively, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
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| CN106675784A (en) * | 2017-03-13 | 2017-05-17 | 河北中烟工业有限责任公司 | Charging essence for embellishing aroma style cigarettes |
| GB201817860D0 (en) * | 2018-11-01 | 2018-12-19 | Nicoventures Trading Ltd | Aerosolised formulation |
| CN112841709B (en) * | 2021-01-20 | 2022-11-25 | 深圳市艾普生物科技有限公司 | Preparation method and application of nicotine salt |
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