CN104585873B - Electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof - Google Patents
Electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof Download PDFInfo
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- CN104585873B CN104585873B CN201510028019.1A CN201510028019A CN104585873B CN 104585873 B CN104585873 B CN 104585873B CN 201510028019 A CN201510028019 A CN 201510028019A CN 104585873 B CN104585873 B CN 104585873B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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Abstract
The invention discloses an electronic cigarette liquid rich in biological active polysaccharide and a preparation method of the electronic cigarette liquid. The electronic cigarette liquid is mainly formed by the following raw materials in parts by weight: 50-70 parts of propylene glycol, 5-15 parts of glycerin, 5-10 parts of deionized water, 5-15 parts of natural biological active polysaccharide extracts, 3-10 parts of tobacco extracts, 1-5 parts of tobacco flavor, 1-3 parts of thickener and 1-3 parts of antioxidant. The electronic cigarette liquid disclosed by the invention is suitable for being smoked in an electronic atomizing way and is formed by refining the tobacco extracts and the natural biological active polysaccharide extracts, an immune function of a human body is also widely regulated while the feeling of smoking a cigarette is obtained by a consumer, and a certain healthcare function is obtained.
Description
Technical field
The present invention relates to tobacco juice for electronic smoke field, more particularly, to a kind of electronic cigarette rich in bioactive polysaccharide
Liquid and preparation method thereof.
Background technology
Smoking and healthy problem global medical and health circle focus of attention always.At present, in global tobacco control
System is persistently strengthened under the macroeconomic situation with economic growth continued downturn, and World tobacco industry faces a severe challenge.
In order to reduce the impact to consumer for the traditional cigarette, the smoke-free tobacco product with buccal cigarette as representative, heating
Do not burn cigarette and electronic cigarette becomes the main flow of novel tobacco product.
Electronic cigarette is electronics nicotine delivery device, is by Chinese's innovation and creation.At present, foreign tobacco is huge
Head all scolds a huge sum of money to set foot in the research and development that electronic cigarette field carries out Related product.Electronic cigarette passes through atomising device by electronics
Cigarette tobacco juice is atomized into mist allows consumer know from experience the sensation of similar smoking.Because electronic cigarette does not have tobacco high temperature
Thermal cracking is domestic, therefore tar content is almost nil, does not have visible flow measurement flue gas, less to surrounding environment influence,
Gradually approved by consumer.Nicotine is mainly become with fragrance with glycerine atomization by electronic cigarette by propane diols at present
Grade and discharge, also some electronic cigarettes are to be discharged nicotine and flavor component etc. by ultrasonic atomizatio water
Come.
Research confirmation, smoking and respiratory system chronic inflammatory reaction, chronic obstructive disease of lung, lung cancer etc.
Disease occurs related.Bioactive polysaccharide refers to be present in biology in vivo, can promote or strengthen body health,
There is control cell differentiation, adjust the old and feeble class non-specificity spectrum immunomodulator of cell growth, can swash
Immunocyte alive, improves body's immunity and does not have toxic and side effect to normal cell.Over nearly 20 years, due to
The developing rapidly of the subjects such as glycobiology, Natural Medicine Chemistry, carbohydrate chemistry, people are to polysaccharide and its compound
Active function have more and more deep understanding.Bioactive polysaccharide: can be decomposed by the enzyme in human body and absorb
And play its physiological regulatory action；Some polysaccharide dissolve in acid solution, form positively charged cation collection
Group, is positively charged edibility fiber only at present；There is good compatibility to human body cell, will not
Produce rejection；It is natural cellulose, nontoxic；Heavy metal can be chelated, as internal heavy metal
The eliminant of ion.Additionally, bioactive polysaccharide has the biological action highly beneficial to human body
Activating cell, suppression are aging；Strengthen immunologic function；Prevention disease, promotes disease recovery from illness；Adjust human body life
Reason function；Antitumor；Radioresistance, anti-oxidant；Anti anoxia；Antiallergy；Anti-inflammatory；Reducing blood lipid, reduction
Blood viscosity, hypoglycemic etc..
Tobacco juice for electronic smoke is the soul that consumer obtains similar impression of smoking, and its quality directly affects consumer's
Impression, but existing tobacco juice for electronic smoke is not also overripened, the taste research especially when electronic cigarette aspirates
On there is larger technological gap, electronic cigarette due to health, environmental protection, by large-scale popularization, so to electronic cigarette
Particularly important in the one-tenth component selections of tobacco juice formula, meeting outside smoking requirement, composition matches more healthy better.
Content of the invention
Part in view of the shortcomings of the prior art, it is an object of the invention to provide a kind of be rich in biologically active
The tobacco juice for electronic smoke of polysaccharide, this tobacco juice for electronic smoke is applied to atomizing type and is aspirated, and has Luzhou-flavor, clear
The characteristic tobacco extract such as odor type or flat-flavor is refined with natural bioactive polyoses extract and forms, and order disappears
Expense person obtains while sucking cigarette and experience, and also extensively efficiently have adjusted the various functions of human immune system,
There is certain health-care effect.
The purpose of the present invention is achieved through the following technical solutions:
A kind of tobacco juice for electronic smoke rich in bioactive polysaccharide, it is mainly made up of the raw material of following weight portion:
50～70 parts of propane diols, 5～15 parts of glycerine, 5～10 parts of deionized water, natural bioactive is many
5～15 parts of sugar extract, 3～10 parts of tobacco extract, 1～5 part of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant；
Described natural bioactive polyoses extract is fungi polysaccharide, plant polyose, marine polysaccharide, shell
One or more of glycan.
Currently preferred electronic cigarette formula of liquid is made up of the raw material of following weight portion:
55～65 parts of propane diols, 6～12 parts of glycerine, 6～9 parts of deionized water, natural bioactive is many
6～12 parts of sugar extract, 4～8 parts of tobacco extract, 2～5 parts of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant.
In order to the present invention is better achieved, described fungi polysaccharide is lentinan, flammulina velutipes, glossy ganoderma are many
Sugar, Cordyceps sinensis polysaccharide, pachymaran, grifola polysaccharide, Blackfungus polyhexose, mix one or more of tremella polysaccharides
Close；Described plant polyose is tea polysaccharide, red jujube polysaccharide, LBP-X, astragalus polyose, panaxan, Huang
Smart polysaccharide, Radix Et Caulis Acanthopanacis Senticosi polysaccharide, one or more mixing of polysaccharides from ginkgo biloba；Described marine polysaccharide is marine alga
Polysaccharide, one or two mixing of spirulina polysaccharide；Described shitosan is crab shell element or chitin polysaccharide, bright
Angle glutelin one or two.
Described tobacco extract is the extract in flue-cured tobacco or airing cigarette or burley tobaccos or cigar tobacco.
A kind of electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide, its preparation method comprises the steps:
Step a, raw material preparation:
The extraction of natural bioactive polyoses extract: by water distillating method or supercritical extraction method from sky
So extract natural bioactive polyoses extract in bioactive polysaccharide, described natural bioactive polysaccharide carries
Take thing to be fungi polysaccharide, one or more of plant polyose, marine polysaccharide, shitosan；
The extraction of tobacco extract: extract tobacco extract from tobacco, described tobacco extract is flue-cured tobacco
Or the extract in airing cigarette or burley tobaccos or cigar tobacco；
Step b, prepare tobacco juice for electronic smoke: the raw material according to following weight portion is sufficiently mixed and obtains electronic cigarette
Liquid: 50～70 parts of propane diols, 5～15 parts of glycerine, 5～10 parts of deionized water, natural bioactive is many
5～15 parts of sugar extract, 3～10 parts of tobacco extract, 1～5 part of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant.
In electronic cigarette liquid and preparation method thereof, the present invention can adopt water distillating method and supercritical extraction method
Two methods extract natural bioactive polyoses extract, as the concrete skill of currently preferred water distillating method
Art scheme is: the water distillating method extracting natural bioactive polyoses extract in described step a is as follows:
First-selection, natural bioactive polysaccharide and distilled water are mixed to form than 1:20～1:5 according to thing liquid
Extract；Then extracted using ultrasonic wave added Hot water extraction, its ultrasonic time is 10～40 minutes,
While extracting, control extract ph value between 7～9, control and extract liquid temp at 60 DEG C～100 DEG C；
Ultrasonic finish after extract is extracted, extraction time is 0.5～2 hour, the material of extraction is separated,
After purification process, respectively obtain various natural bioactive polyoses extracts, finally many to natural bioactive
Sugar extract carries out vacuum drying treatment.
The water distillating method extracting natural bioactive polyoses extract in further preferred step a is as follows:
First-selection, natural bioactive polysaccharide and distilled water are mixed to form than 1:20～1:5 according to thing liquid
Extract；Then extracted using ultrasonic wave added Hot water extraction, its ultrasonic time is 10～40 minutes,
While extracting, control extract ph value between 7～9, control and extract liquid temp at 60 DEG C～100 DEG C；
Ultrasonic finish after i.e. to extract extract, extraction time be 0.5～2 hour, the material of extraction is separated, pure
After change is processed, respectively obtain various natural bioactive polyoses extracts, finally to natural bioactive polysaccharide
Extract carries out vacuum drying treatment.
In electronic cigarette liquid and preparation method thereof, as currently preferred water distillating method concrete technical scheme it is:
The supercritical extraction method extracting natural bioactive polyoses extract in described step a is as follows:
Natural bioactive polysaccharide is put in the ethanol solution that concentration is 20%～100%, the weight of ethanol solution
It is 0.5～2 times of natural bioactive polysaccharide dry matter weight；Then by with natural bioactive polysaccharide
Ethanol solution carries out supercritical extract process, and control extracting pressure is 10～45mpa, and 40 DEG C of extraction temperature～
85 DEG C, co2Flow controls in 10～30l/h, and extraction time controlled at 30～180 minutes, respectively obtains each
Plant natural bioactive polyoses extract, finally natural bioactive polyoses extract is carried out at vacuum drying
Reason.
The supercritical extraction method of natural bioactive polyoses extract is extracted such as in further preferred step a
Under:
Natural bioactive polysaccharide is put in the ethanol solution that concentration is 40%～90%, the weight of ethanol solution
It is 0.8～1.8 times of natural bioactive polysaccharide dry matter weight；Then will be with natural bioactive polysaccharide
Ethanol solution carry out supercritical extract process, control extracting pressure be 30～45mpa, 60 DEG C of extraction temperature～
85 DEG C, co2Flow controls in 20～25l/h, and extraction time controlled at 90～120 minutes, respectively obtains each
Plant natural bioactive polyoses extract, finally natural bioactive polyoses extract is carried out at vacuum drying
Reason.
The present invention compared with the prior art, has advantages below and a beneficial effect:
(1) tobacco juice for electronic smoke of the present invention is applied to atomizing type and is aspirated, and has Luzhou-flavor, delicate fragrance type
Or the characteristic tobacco extract such as flat-flavor is refined with natural bioactive polyoses extract and forms, make consumer
While acquisition is sucked cigarette and experienced, also there is enhancing immunologic function, prevention disease, adjust Human Physiology machine
, antitumor, radioresistance, anti-oxidant, anti anoxia, antiallergy, anti-inflammatory, reducing blood lipid, blood can be reduced
Stickiness, the health-care effect such as hypoglycemic.
(2) the invention provides water distillation or two kinds of technique extracting methods of supercritical extract are extracting natural biological
Various polysaccharides in active polysaccharide, chitosan material, raw material is pure natural, no chemistry adds, extraction process
Environmental protection and efficiency is higher.
Specific embodiment
With reference to embodiment, the present invention is described in further detail:
Embodiment
A kind of tobacco juice for electronic smoke rich in bioactive polysaccharide, it is mainly made up of the raw material of following weight portion:
50～70 parts of propane diols, 5～15 parts of glycerine, 5～10 parts of deionized water, natural bioactive is many
5～15 parts of sugar extract, 3～10 parts of tobacco extract, 1～5 part of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant；
Described natural bioactive polyoses extract is fungi polysaccharide, plant polyose, marine polysaccharide, shell
One or more of glycan.
Described flavouring essence for tobacco is conventional flavouring essence for tobacco, and it is very convenient in each essence spice for cigarette company
Ground is bought, and described thickener, antioxidant are the conventional cigarette product sell on market.
According to one preferred tobacco juice for electronic smoke embodiment of the present invention it is: it is mainly former by following weight portion
Material is made:
55～65 parts of propane diols, 6～12 parts of glycerine, 6～9 parts of deionized water, natural bioactive is many
6～12 parts of sugar extract, 4～8 parts of tobacco extract, 2～5 parts of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant.
The fungi polysaccharide of the present invention preferably selection is lentinan, flammulina velutipes, GL-B, Chinese caterpillar fungus are many
Sugar, pachymaran, grifola polysaccharide, Blackfungus polyhexose, one or more mixing of tremella polysaccharides.The present invention
Preferably selection plant polyose be tea polysaccharide, red jujube polysaccharide, LBP-X, astragalus polyose, panaxan,
Siberian solomonseal rhizome polysaccharide, Radix Et Caulis Acanthopanacis Senticosi polysaccharide, one or more mixing of polysaccharides from ginkgo biloba.The ocean of the present invention preferably selection
Biological polyoses are algal polysaccharides, one or two mixing of spirulina polysaccharide.The shell of the present invention preferably selection gathers
Sugar for crab shell element or chitin polysaccharide, bright angle glutelin one or two.
According to one preferred embodiment of the invention it is: described tobacco extract is flue-cured tobacco or airing cigarette or white
Extract in rib cigarette or cigar tobacco.
A kind of electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide, its preparation method comprises the steps:
Step a, raw material preparation:
The extraction of natural bioactive polyoses extract: by water distillating method or supercritical extraction method from sky
So extract natural bioactive polyoses extract in bioactive polysaccharide, described natural bioactive polysaccharide carries
Take thing to be fungi polysaccharide, one or more of plant polyose, marine polysaccharide, shitosan；
The extraction of tobacco extract: extract tobacco extract from tobacco, described tobacco extract is flue-cured tobacco
Or the extract in airing cigarette or burley tobaccos or cigar tobacco；
Step b, prepare tobacco juice for electronic smoke: the raw material according to following weight portion is sufficiently mixed and obtains electronic cigarette
Liquid: 50～70 parts of propane diols, 5～15 parts of glycerine, 5～10 parts of deionized water, natural bioactive is many
5～15 parts of sugar extract, 3～10 parts of tobacco extract, 1～5 part of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant.Described flavouring essence for tobacco is conventional flavouring essence for tobacco, and it is in each essence spice for cigarette
Company easily buys, and described thickener, antioxidant are the conventional cigarette sold on market and produce
Product.
Carried according to the first preferred natural bioactive polyoses extract in electronic cigarette liquid and preparation method thereof of the present invention
Take method, the water distillating method extracting natural bioactive polyoses extract in described step a is as follows:
First-selection, natural bioactive polysaccharide and distilled water are mixed to form than 1:20～1:5 according to thing liquid
Extract；Then extracted using ultrasonic wave added Hot water extraction, its ultrasonic time is 10～40 minutes,
While extracting, control extract ph value between 7～9, control and extract liquid temp at 60 DEG C～100 DEG C；
Ultrasonic finish after extract is extracted, extraction time is 0.5～2 hour, the material of extraction is separated,
After purification process, respectively obtain various natural bioactive polyoses extracts, finally many to natural bioactive
Sugar extract carries out vacuum drying treatment.
The preferred embodiment of a water distillating method according to the present invention, extracts natural biological in described step a
The water distillating method of polysaccharide extraction thing is as follows:
First-selection, natural bioactive polysaccharide is carried out being mixed to form extract than 1:10 according to thing liquid with distilled water；
Then extracted using ultrasonic wave added Hot water extraction, its ultrasonic time is 30 minutes, while extracting,
Control extract ph value between 8, control and extract liquid temp at 80 DEG C；
Ultrasonic finish after extract is extracted, extraction time is 1.5 hours, the material of extraction is separated,
After purification process, respectively obtain various natural bioactive polyoses extracts, finally many to natural bioactive
Sugar extract carries out vacuum drying treatment.
Carried according to the second preferred natural bioactive polyoses extract in electronic cigarette liquid and preparation method thereof of the present invention
Take method, the supercritical extraction method extracting natural bioactive polyoses extract in described step a is as follows:
Natural bioactive polysaccharide is put in the ethanol solution that concentration is 20%～100%, the weight of ethanol solution
It is 0.5～2 times of natural bioactive polysaccharide dry matter weight；Then by with natural bioactive polysaccharide
Ethanol solution carries out supercritical extract process, and control extracting pressure is 10～45mpa, and 40 DEG C of extraction temperature～
85 DEG C, co2Flow controls in 10～30l/h, and extraction time controlled at 30～180 minutes, respectively obtains each
Plant natural bioactive polyoses extract, finally natural bioactive polyoses extract is carried out at vacuum drying
Reason.
The preferred embodiment of a supercritical extraction method according to the present invention, extracts sky in described step a
So the supercritical extraction method of bioactive polysaccharide extract is as follows:
Natural bioactive polysaccharide is put in the ethanol solution that concentration is 40%～90%, the weight of ethanol solution
It is 0.8～1.8 times of natural bioactive polysaccharide dry matter weight；Then will be with natural bioactive polysaccharide
Ethanol solution carry out supercritical extract process, control extracting pressure be 30～45mpa, 60 DEG C of extraction temperature～
85 DEG C, co2Flow controls in 20～25l/h, and extraction time controlled at 90～120 minutes, respectively obtains each
Plant natural bioactive polyoses extract, finally natural bioactive polyoses extract is carried out at vacuum drying
Reason.
Immunological regulation is one of primary bioactivity of active polysaccharides from plants, and numerous studies show, plant polyose
There is suppression tumour growth, immune cell activated, improve the effect of body's immunity.Lentinan is injected
In clinical practice, research confirms that lentinan can improve alimentary canal to the ancillary drug of liquid antineoplaston the most
Tumor patient postoperative cd3, cd4 positive cell number rises, and cd8 positive cell number declines, cd4/cd8 ratio
Raise, improve the survival rate of patient's half a year and 1 year half.The activity of nk cell can be strengthened, thus reaching simultaneously
To the effect of killing tumor cell transplanting transfer, concrete bibliographic reference Wang Su, Zhou Zhenying, Pan Liangxi's et al.
" impact to chemotherapy cancer patient nk activity for the domestic lentinan ".Research confirm (with specific reference to Sun Guiju,
Wang Shaokang, Zhang Yong etc. " LBP-X, Tea Polysaccharides mixture are to patients with type Ⅰ DM rat hypoglycemic activity
And the impact to diabetic complication index of correlation ". food research and development .2003；24(2):75-78)
LBP-X and Tea Polysaccharides mixture have enhancement mode diabetic animal models insulin sensitivity, increase
Liver glycogen reserves, reduction blood sugar level, improve sod level in serum, thus preventing diabetic complication.
In chen hx and zhang m, " the components and antioxidant activity of of xie
Polysaccharide conjugate from green tea " report a kind of green tea that is isolatable from periodical
Difference polysaccharide conjugates are inhibited to hydroxy radical, peroxylradicals and lipid peroxidation.Additionally,
Spirulina polysaccharide has capability of resistance to radiation, and panaxan, LBP-X have antimutagenic effect, and black fungus is many
Sugar has removing superoxide anion, the anti-oxidant and mitochondrial function of protection.
There is not high temperature pyrolysis reaction, therefore tar in the tobacco juice for electronic smoke that the present invention is rich in bioactive polysaccharide
Burst size is almost nil, meet consumer obtain smoking experience while, reduce to itself, other people and ring
The impact in border.Meanwhile, the interpolation of natural bioactive polyoses extract, can with activating cell, suppression aging,
Strengthen immunologic function, prevention disease, adjust human physiological functions, antitumor, radioresistance, anti-oxidant, anti-
Anoxic, antiallergy, anti-inflammatory etc..Further, it is also possible to reducing blood lipid, reduce blood viscosity, hypoglycemic etc..
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all at this
Any modification, equivalent and improvement made within bright spirit and principle etc., should be included in the present invention
Protection domain within.
Claims (8)
1. a kind of tobacco juice for electronic smoke rich in bioactive polysaccharide it is characterised in that: it is mainly by following weight
The raw material of part is made:
50～70 parts of propane diols, 5～15 parts of glycerine, 5～10 parts of deionized water, natural bioactive is many
5～15 parts of sugar extract, 3～10 parts of tobacco extract, 1～5 part of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant；
Described natural bioactive polyoses extract is fungi polysaccharide, plant polyose, marine polysaccharide, shell
One or more of glycan；
Described fungi polysaccharide be lentinan, flammulina velutipes, GL-B, Cordyceps sinensis polysaccharide, pachymaran,
Grifola polysaccharide, Blackfungus polyhexose, one or more mixing of tremella polysaccharides；Described plant polyose be tea polysaccharide,
Red jujube polysaccharide, LBP-X, astragalus polyose, panaxan, Siberian solomonseal rhizome polysaccharide, Radix Et Caulis Acanthopanacis Senticosi polysaccharide, ginkgo are many
One or more mixing of sugar；Described marine polysaccharide is algal polysaccharides, one kind of spirulina polysaccharide or two
Plant mixing；Described shitosan be crab shell element or chitin polysaccharide, bright angle glutelin one or two.
2. according to the tobacco juice for electronic smoke rich in bioactive polysaccharide described in claim 1 it is characterised in that:
It is mainly made up of the raw material of following weight portion:
55～65 parts of propane diols, 6～12 parts of glycerine, 6～9 parts of deionized water, natural bioactive is many
6～12 parts of sugar extract, 4～8 parts of tobacco extract, 2～5 parts of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant.
3., according to the tobacco juice for electronic smoke rich in bioactive polysaccharide described in claim 1 or 2, its feature exists
In: described tobacco extract is the extract in flue-cured tobacco or airing cigarette or burley tobaccos or cigar tobacco.
4. a kind of electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide it is characterised in that: its preparation side
Method comprises the steps:
Step a, raw material preparation:
The extraction of natural bioactive polyoses extract: by water distillating method or supercritical extraction method from sky
So extract natural bioactive polyoses extract in bioactive polysaccharide, described natural bioactive polysaccharide carries
Take thing to be fungi polysaccharide, one or more of plant polyose, marine polysaccharide, shitosan；
The extraction of tobacco extract: extract tobacco extract from tobacco, described tobacco extract is flue-cured tobacco
Or the extract in airing cigarette or burley tobaccos or cigar tobacco；
Step b, prepare tobacco juice for electronic smoke: the raw material according to following weight portion is sufficiently mixed and obtains electronic cigarette
Liquid: 50～70 parts of propane diols, 5～15 parts of glycerine, 5～10 parts of deionized water, natural bioactive is many
5～15 parts of sugar extract, 3～10 parts of tobacco extract, 1～5 part of flavouring essence for tobacco, 1～3 part of thickener,
1～3 part of antioxidant.
5., according to the electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide described in claim 4, it is special
Levy and be: the water distillating method extracting natural bioactive polyoses extract in described step a is as follows:
First-selection, natural bioactive polysaccharide and distilled water are mixed to form than 1:20～1:5 according to thing liquid
Extract；Then extracted using ultrasonic wave added Hot water extraction, its ultrasonic time is 10～40 minutes,
While extracting, control extract ph value between 7～9, control and extract liquid temp at 60 DEG C～100 DEG C；
Ultrasonic finish after i.e. to extract adopt Hot water extraction extract, extraction time be 0.5～2 hour, carry
The material taking is separated, after purification process, obtain various natural bioactive polyoses extracts, finally to sky
So bioactive polysaccharide extract carries out vacuum drying treatment.
6., according to the electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide described in claim 5, it is special
Levy and be: the water distillating method extracting natural bioactive polyoses extract in described step a is as follows:
First-selection, natural bioactive polysaccharide is carried out being mixed to form extract than 1:10 according to thing liquid with distilled water；
Then extracted using ultrasonic wave added Hot water extraction, its ultrasonic time is 30 minutes, while extracting,
Control extract ph value between 8, control and extract liquid temp at 80 DEG C；
Ultrasonic finish after i.e. to extract adopt Hot water extraction extract, extraction time be 1.5 hours, extract
Material is separated, after purification process, obtain various natural bioactive polyoses extracts, finally to natural
Bioactive polysaccharide extract carries out vacuum drying treatment.
7., according to the electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide described in claim 4, it is special
Levy and be: the supercritical extraction method extracting natural bioactive polyoses extract in described step a is as follows:
Natural bioactive polysaccharide is put in the ethanol solution that concentration is 20%～100%, the weight of ethanol solution
It is 0.5～2 times of natural bioactive polysaccharide dry matter weight；Then by with natural bioactive polysaccharide
Ethanol solution carries out supercritical extract process, and control extracting pressure is 10～45mpa, and 40 DEG C of extraction temperature～
85 DEG C, co2Flow controls in 10～30l/h, and extraction time controlled at 30～180 minutes, obtained various skies
So bioactive polysaccharide extract, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
8., according to the electronic cigarette liquid and preparation method thereof rich in bioactive polysaccharide described in claim 7, it is special
Levy and be: the supercritical extraction method extracting natural bioactive polyoses extract in described step a is as follows:
Natural bioactive polysaccharide is put in the ethanol solution that concentration is 40%～90%, the weight of ethanol solution is sky
So 0.8～1.8 times of bioactive polysaccharide dry matter weight；Then by with natural bioactive polysaccharide
Ethanol solution carries out supercritical extract process, and control extracting pressure is 30～45mpa, and 60 DEG C of extraction temperature～
85 DEG C, co2Flow controls in 20～25l/h, and extraction time controlled at 90～120 minutes, obtained various skies
So bioactive polysaccharide extract, finally carries out vacuum drying treatment to natural bioactive polyoses extract.
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| CN105146733A (en) * | 2015-08-13 | 2015-12-16 | 深圳市施美乐科技股份有限公司 | Electronic cigarette atomization liquid with anti-aging function and preparation method thereof |
| US20180103681A1 (en) * | 2016-10-18 | 2018-04-19 | Altria Client Services Llc | Methods and systems for increasing stability of the pre-vapor formulation of an e-vaping device |
| CN113383987A (en) * | 2021-07-26 | 2021-09-14 | 云南中烟工业有限责任公司 | Essence formula containing tremella polysaccharide extract and application of essence formula in tobacco flavoring |
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| CN101455397A (en) * | 2009-01-07 | 2009-06-17 | 吉林农业大学 | Animals and plants polysaccharide oligomerization method |
| CN101461566A (en) * | 2009-01-08 | 2009-06-24 | 华健 | Atomized liquid of electronic smoke |
| CN101712727A (en) * | 2009-11-24 | 2010-05-26 | 中国计量学院 | Method for extracting black fungus polysaccharide |
| CN103549649A (en) * | 2013-11-07 | 2014-02-05 | 中国烟草总公司山东省公司 | Health-care gum cigarette |
| CN104026730A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Scorch sweet aroma electronic cigarette juice |
| CN104256888A (en) * | 2014-08-07 | 2015-01-07 | 江苏中烟工业有限责任公司 | Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| ITMI20130214A1 (en) * | 2013-02-15 | 2014-08-16 | Pharmaday S R L | COMPOSITION FOR ELECTRONIC CIGARETTE |
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101455397A (en) * | 2009-01-07 | 2009-06-17 | 吉林农业大学 | Animals and plants polysaccharide oligomerization method |
| CN101461566A (en) * | 2009-01-08 | 2009-06-24 | 华健 | Atomized liquid of electronic smoke |
| CN101712727A (en) * | 2009-11-24 | 2010-05-26 | 中国计量学院 | Method for extracting black fungus polysaccharide |
| CN103549649A (en) * | 2013-11-07 | 2014-02-05 | 中国烟草总公司山东省公司 | Health-care gum cigarette |
| CN104026730A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Scorch sweet aroma electronic cigarette juice |
| CN104256888A (en) * | 2014-08-07 | 2015-01-07 | 江苏中烟工业有限责任公司 | Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice |
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