CN109259296A - A kind of electronics tobacco tar and preparation method and application that tealeaves baking is fragrant - Google Patents

A kind of electronics tobacco tar and preparation method and application that tealeaves baking is fragrant Download PDF

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Publication number
CN109259296A
CN109259296A CN201811069031.7A CN201811069031A CN109259296A CN 109259296 A CN109259296 A CN 109259296A CN 201811069031 A CN201811069031 A CN 201811069031A CN 109259296 A CN109259296 A CN 109259296A
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Prior art keywords
tealeaves
preparation
tobacco tar
fragrant
electronics tobacco
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CN109259296B (en
Inventor
陈章玉
王晋
张承明
陈建华
张涛
黄海涛
缪恩铭
向明
耿永勤
蒋次清
王小龙
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Fats And Perfumes (AREA)

Abstract

The present invention relates to the electronics tobacco tar and preparation method and application that a kind of baking of tealeaves is fragrant, which includes the following steps: that step (1), raw material weigh;Step (2) extracts tealeaves baking Studies of The Aromatic Substances;Step (3) prepares electronics tobacco tar.Electronics tobacco tar of the invention can greatly improve the flavor and taste of abundant cigarette, and the effective baking perfume (or spice) quality for improving new tobacco products reduces miscellaneous tolerance, improves the comfort and harmony of cigarette.Preparation method of the present invention is easy to operate, and safe without toxic side effect is with a wide range of applications.

Description

A kind of electronics tobacco tar and preparation method and application that tealeaves baking is fragrant
Technical field
The present invention relates to a kind of preparation method of electronics tobacco tar, especially a kind of preparation for the electronics tobacco tar that tealeaves baking is fragrant Method further relates to the fragrant electronics tobacco tar of the baking of tealeaves made from this method, belongs to tobacco product field.
Background technique
As cigarette consumption person is to the growing interest of own health, and the requirement to cigarette interior quality is higher and higher, Low tar high-quality cigarette has become the emphasis of current tealeaves research.However, being necessarily accompanied with cigarette perfume while low tar Gas loss and comfort level variation.And in quality, country's cigarette product is deposited in terms of sucking quality and sense organ at present In certain deficiency, such as fragrance is faint, dry sensation is strong, sweet degree is inadequate, comfort level is poor.
In order to improve the quality of cigarette, can by perfuming cigarette feeding technique, come set off, added volume cigarette perfume taste, increase Flue gas concentration, improvement is jealous, removes and cover miscellaneous gas, reduces irritation, assigns the good characteristic chicken flavor of product, and prominent cigarette produces The personalized style of product, promote cigarette sucks satisfaction and pleasure degree.
Toasting fragrant note is to bake one of perfume (or spice) note, is the important component of cigarette flavor.In recent years, there is research Flavouring is carried out to traditional red date extract using zymotechnic, microbial fermentation technology, Maillard reaction etc., produces fragrant processing, The note for enriching red date extract to a certain extent increases the content of flavor component.Utilize the common volume such as malt extract It is fragrant to increase flue gas baking for cigarette additive.But the baking perfume (or spice) note of above-mentioned products obtained therefrom does not protrude, and wherein still contains There are the macromolecular substances such as a certain amount of protein, pectin, polysaccharide, these substances can crack generation during cigarette is burnt and sucked Harmful components, increase cigarette smoking irritation and miscellaneous gas.
Tealeaves is one of maximum beverage of world today's consumption figure, it and coffee, cocoa simultaneously claim the world three big non-alcohol drink Material.Tea from wild into people's artificial cultivation epoch, by the mankind as health care, prevent and cure diseases and apply.And with the hair of society Exhibition and people constantly improve the raising that the effect of tea recognizes.Tealeaves is as the important drink in people's daily life, with it The quality and pleasant sense organ flavor of health are liked by consumer, are widely used.Therefore, how tealeaves applied into improvement cigarette Branch is inhaled on taste, is to be worth research.
Summary of the invention
In order to solve the above technical problem, the present invention provides it is a kind of prepare it is simple, at low cost, can significantly improve conventional electricity Sub- cigarette or electric heating do not burn cigarette sensory evaluating smoking the fragrant electronics tobacco tar of tealeaves baking preparation method, technology of the invention Scheme is specific as follows:
A kind of tealeaves toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1), raw material weigh
Raw material is weighed by following weight point: 10~60 parts of green tea powder, 1~5 part of black tea powder and 5~60 parts of dark green tea powder;
Step (2) extracts tealeaves baking perfumery
The raw material of step (1) is added to the container, the polyalcohol and 0.01~1 part of weight of 100~500 parts of parts by weight is then added The magnesium ion complex of part stirs evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths, is then added 200~2000 The solvent supersonic of parts by weight extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4~15min, takes supernatant liquid It after organic membrane filtration, is evaporated under reduced pressure, solvent is removed and toasts perfumery to get to tealeaves;
Step (3) prepares electronics tobacco tar
Tealeaves baking Studies of The Aromatic Substances, polydextrose and the atomized liquid 1-5:5-20:75-94 by weight of step (2) are mixed, It stirs to ingredient and is uniformly dissolved at room temperature, be placed in and be protected from light shady place 24~48 h of alcoholization to get the electronic cigarette fragrant to tealeaves baking Oil.
Further, in step (1), the green tea is one of Xihu Longjing Tea, Xinyang Maojian Tea and Pilochun (a green tea) or more Kind;The black tea is one of Keemun black tea, Yunnan black tea and Yixing black tea or a variety of;The dark green tea is Pu'er tea, Sichuan One of dark green tea and Hunan dark green tea are a variety of.
Further, in step (2), the polyalcohol is one of ethylene glycol, propylene glycol, glycerol or a variety of.
Further, in step (2), the magnesium ion complex is magnesium tartrate ionic complex or ethylenediamine tetrem Sour magnesium ion complex.
Further, in step (2), the solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, acetic acid One of ethyl ester and methyl acetate are a variety of.
Further, in step (3), the atomized liquid is propylene glycol or glycerol.
Further, in step (3), mixing time is 20~30min.
The invention further relates to the obtained tealeaves of above-mentioned preparation method toast fragrant electronics tobacco tar.
The invention further relates to above-mentioned tealeaves toast the application of fragrant electronics tobacco tar, by the electronics tobacco tar according to 0.3-1g It is added to conventional electrical cigarette.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) tealeaves of the invention is in modulated process, it will generates the substance that distinctive tealeaves toasts fragrant note, adopts to its product Targeting extraction is carried out to it with certain solvent, the flue gases such as macromolecular substances irritation or miscellaneous gas substance can be removed, obtained pure Positive baking perfume (or spice) note substance, is added on electronics tobacco tar, can greatly improve the flavor and taste of abundant cigarette.
(2) tealeaves of the invention baking Studies of The Aromatic Substances is compounded with polydextrose, can be substantially reduced stimulation of the tobacco tar to respiratory tract, And the baking fragrance and suction mouthfeel of cigarette can be improved, the baking perfume (or spice) quality of new tobacco products can be effectively improved, is dropped Low miscellaneous tolerance improves the comfort and harmony of cigarette.
(3) preparation method of the present invention is easy to operate, and safe without toxic side effect is with a wide range of applications.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.In the examples where no specific technique or condition is specified, described technology or item according to the literature in the art Part is carried out according to product description.Reagents or instruments used without specified manufacturer is that can be obtained by purchase Conventional products.All sensory evaluations are carried out according to GB5606.4-2005.
Embodiment 1
The tealeaves of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1), raw material weigh
Raw material is weighed by following weight point: 10 parts of Xihu Longjing Tea, 1 part of Keemun black tea and 5 parts of Pu'er tea;
Step (2) extracts tealeaves baking perfumery
Round-bottomed flask is added in above-mentioned raw materials, 100 parts of ethylene glycol and 0.01 part of magnesium tartrate ionic complex stirring are then added Uniformly, flask mouth is then connected into condenser pipe, is put into oil bath heating later to 150 DEG C of condensing reflux 3h.
200 parts of petroleum ethers are added in above-mentioned reaction product, then ultrasonic extraction 60min shakes after extracting 60min, into Row centrifuge separation 15min carry out conventional vacuum distillation after taking the organic membrane filtration of supernatant liquid, by solvent removal to get Perfumery is toasted to required tealeaves.
Step (3) prepares electronics tobacco tar
Tealeaves baking Studies of The Aromatic Substances, polydextrose and the propylene glycol 1:5:94 by weight of step (2) are mixed, stirred at room temperature It mixes that 20min is uniform to dissolution mixing, is placed in and is protected from light shady place alcoholization for 24 hours to get the electronics tobacco tar fragrant to required tealeaves baking.
Above-mentioned 0.5g electronics tobacco tar is prepared into electronic cigarette, (is compareed by the electronics tobacco tar fragrant with tealeaves baking is not added with Example) comparison smokes panel test and shows: after prepared tealeaves baking Studies of The Aromatic Substances is added, electronic cigarette toasts that note is prominent, and comfort improves, and exhales It inhales road irritation to be substantially reduced, the results are shown in Table 1.
Embodiment 2
The tealeaves of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1), raw material weigh
Point raw material is weighed by following weight: Xinyang Maojian Tea and Pilochun (a green tea) is 30 parts each, 2 parts of Yunnan black tea and 3 parts of Yixing black tea, Sichuan dark green tea Each 25 parts with Hunan dark green tea.
Step (2) extracts tealeaves baking perfumery
Round-bottomed flask is added in above-mentioned raw materials, ethylene glycol is then added and propylene glycol is 250 parts each, ethylenediamine tetra-acetic acid magnesium ion is matched It closes 1 part of object to stir evenly, flask mouth is then connected into condenser pipe, is put into oil bath heating later to 250 DEG C of condensing reflux 0.5h.
2000 parts of n-hexanes and chloroform are added in above-mentioned reaction product, wherein n-hexane and chloroform volume ratio are 1:1, Ultrasonic extraction 10min is centrifuged 4min, takes supernatant liquid with organic membrane filtration then after concussion extraction 10min Afterwards, it is evaporated under reduced pressure, solvent is removed and toasts perfumery to get to required tealeaves.
Step (3) prepares electronics tobacco tar
Tealeaves baking Studies of The Aromatic Substances, polydextrose and the glycerol 5:20:75 by weight of step (2) are mixed, stirred at room temperature It is uniform to mix 20min extremely dissolution mixing, is placed in and is protected from light shady place alcoholization 48h to get fragrant electronics tobacco tar is toasted to required tealeaves.
Above-mentioned 0.3g electronics tobacco tar is prepared into electronic cigarette.It (is compareed by the electronics tobacco tar fragrant with tealeaves baking is not added with Example) comparison smokes panel test and shows: after prepared tealeaves baking Studies of The Aromatic Substances is added, electronic cigarette toasts that note is dense, and miscellaneous gas is reduced, and coordinates Property increase, respiratory tract irritation is substantially reduced.The results are shown in Table 1.Remaining is same as Example 1.
Embodiment 3
The tealeaves of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1), raw material weigh
Point raw material is weighed by following weight: Xihu Longjing Tea and Xinyang Maojian Tea is 30 parts each, 2 parts of Yunnan black tea and 18 parts of Pu'er tea.
Step (2) extracts tealeaves baking perfumery
Round-bottomed flask is added in above-mentioned raw materials, then be added 200 parts of glycerol, 0.1 part of magnesium tartrate ionic complex stir evenly, Then flask mouth is connected into condenser pipe, is put into oil bath heating later to 200 DEG C of condensing reflux 1h.
1000 parts of ethyl acetate are added in above-mentioned reaction product, then ultrasonic extraction 30min shakes after extracting 30min, 4min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed to get institute is arrived The tealeaves needed toasts perfumery.
Step (3) prepares electronics tobacco tar
Tealeaves baking Studies of The Aromatic Substances, polydextrose and the propylene glycol 3:10:87 by weight of step (2) are mixed, at room temperature It is uniform to stir 25min extremely dissolution mixing, is placed in and is protected from light shady place alcoholization 30h to get fragrant electronic cigarette is toasted to required tealeaves Oil.
Above-mentioned 0.7g electronics tobacco tar is prepared into electronic cigarette.It is commented by the electronics tobacco tar comparison fragrant with tealeaves baking is not added with Suction shows: after prepared tealeaves baking Studies of The Aromatic Substances is added, electronic cigarette tealeaves toasts note foot, in good taste, respiratory tract irritation It is substantially reduced.The results are shown in Table 1.Remaining is same as Example 1.
Embodiment 4
The tealeaves of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1), raw material weigh
Point raw material is weighed by following weight: Xinyang Maojian Tea and Pilochun (a green tea) is 10 parts each, 2 parts of Yixing black tea and Pu'er tea and Hunan dark green tea Each 30 parts.
Step (2) extracts tealeaves baking perfumery
Round-bottomed flask is added in above-mentioned raw materials, 300 parts of propylene glycol, 0.2 part of ethylenediamine tetra-acetic acid magnesium ion complex is then added It stirs evenly, flask mouth is then connected into condenser pipe, be put into oil bath heating later to 210 DEG C of condensing reflux 2h.
500 parts of methylene chloride of addition and 1500 parts of methyl acetates in above-mentioned reaction product, ultrasonic extraction 20min, then After concussion extraction 15min, 8min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, it will be molten Agent removal toasts perfumery to get to required tealeaves.
Step (3) prepares electronics tobacco tar
Tealeaves baking Studies of The Aromatic Substances, polydextrose and the propylene glycol 5:15:80 by weight of step (2) are mixed, at room temperature It is uniform to stir 24min extremely dissolution mixing, is placed in and is protected from light shady place alcoholization 40h to get fragrant electronic cigarette is toasted to required tealeaves Oil.
Above-mentioned 0.9g electronics tobacco tar is prepared into electronic cigarette.It is commented by the electronics tobacco tar comparison fragrant with tealeaves baking is not added with Suction shows: after prepared tealeaves baking Studies of The Aromatic Substances is added, electronic cigarette tealeaves toasts note and protrudes, and flue gas is fine and smooth, respiratory tract thorn Sharp property is substantially reduced.The results are shown in Table 1.
Different electronic cigarette sensory evaluating smoking's evaluation results in 1 embodiment 1-4 of table
Sample Fragrance Harmony Miscellaneous gas Irritation Pleasant impression
Reference examples 25 5 9 15 21
It is compounded in embodiment 1 without using polydextrose 28 4.5 8.5 16.5 21
Do not make solvent extraction in embodiment 1 27 4 8 15 20
Embodiment 1 28 5.5 10 17 22
Embodiment 2 28.5 6 10 16.5 22
Embodiment 3 28 5.5 9.5 17 24
Embodiment 4 29 5.5 9.5 16.5 23
As a comparison, it is prepared according to method in embodiment 1, but is added without polydextrose in preparation process, extracts without using solvent It takes.Simultaneously according to described in embodiment 1, it is prepared into control electronic cigarette.
As can be seen from Table 1, the control electronic cigarette in opposite embodiment 1, control electronic cigarette tealeaves baking note do not protrude, Comfort is slightly good, and respiratory tract irritation decreases, but reduces obviously without 1 electronic cigarette of embodiment.
In embodiment 1 without using glucose sugar compound other techniques it is all the same in the case where electronics tobacco tar obtained electronics is added After cigarette, the coordination of electronic cigarette sensory evaluating smoking, miscellaneous gas, irritation aspect are undesirable, especially in terms of coordinating with miscellaneous gas, effect Fruit is also less than reference examples, it is seen then that glucose sugar compounding effect is significant.
If not using solvent extraction in embodiment 1, after electronic cigarette is added in obtained electronics tobacco tar, effect is worse, it is seen that molten Agent extraction is also to improve an important factor for inhaling taste.
Comparative test 1
Comparative sample 1 is prepared according to method in embodiment 1, but magnesium ion complex is added without in preparation process, respectively detection pair The macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance is toasted than tealeaves in sample 1 and embodiment 1.As shown in Table 2, it is added Tealeaves toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance and is substantially reduced after magnesium ion complex.
Table 2
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 1 0.2% 30 24
Embodiment 1 0 0 0.2
While electronic cigarette 1 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control Electronic cigarette 1 has certain tealeaves baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 2
Comparative sample 2 is prepared according to method in embodiment 1, but magnesium ion complex is changed to magnesium chloride in preparation process, examines respectively It surveys tealeaves in comparative sample 2 and embodiment 1 and toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.As shown in Table 3, The macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance is toasted using tealeaves after magnesium ion complex to be substantially reduced.
Table 3
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 2 0.3% 28 20
Embodiment 1 0 0 0.2
While electronic cigarette 2 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control Electronic cigarette 2 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 3
Comparative sample 3 is prepared according to method in embodiment 1, but reaction temperature is 120 DEG C, detects comparative sample 3 and embodiment 1 respectively Middle tealeaves toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.As shown in Table 4, the baking of 1 tealeaves of embodiment is fragrant The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in material.
Table 4
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 3 0.3% 22 15
Embodiment 1 0 0 0.2
While electronic cigarette 3 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control Electronic cigarette 3 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 4
Comparative sample 4 is prepared according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects comparative sample 4 and embodiment respectively Tealeaves toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance in 1.As shown in Table 5, the baking of 1 tealeaves of embodiment is fragrant The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in fragrance.
Table 5
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 4 0.5% 32 20
Embodiment 1 0 0 0.2
While electronic cigarette 4 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control Electronic cigarette 4 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 5
Comparative sample 5 is prepared according to method in embodiment 1, but ultrasonic extraction, concussion extraction and step with centrifugal separation are changed to use Separatory funnel carries out conventional extraction, detect respectively tealeaves in comparative sample 5 and embodiment 1 toast protein in fragrant fragrance, pectin and The macromoleculars content such as polysaccharide.As shown in Table 6,1 tealeaves of embodiment toasts the macromoleculars such as protein, pectin and polysaccharide in fragrant fragrance and contains Amount is substantially reduced.
Table 6
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 5 0.4% 10 8
Embodiment 1 0 0 0.2
While electronic cigarette 5 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control Electronic cigarette 5 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (9)

1. the preparation method that a kind of tealeaves toasts fragrant electronics tobacco tar, characterized by the following steps:
Step (1), raw material weigh
Raw material is weighed by following weight point: 10~60 parts of green tea powder, 1~5 part of black tea powder and 5~60 parts of dark green tea powder;
Step (2) extracts tealeaves baking perfumery
The raw material of step (1) is added to the container, the polyalcohol and 0.01~1 part of weight of 100~500 parts of parts by weight is then added The magnesium ion complex of part stirs evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths, is then added 200~2000 The solvent supersonic of parts by weight extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4~15min, takes supernatant liquid It after organic membrane filtration, is evaporated under reduced pressure, solvent is removed and toasts perfumery to get to tealeaves;
Step (3) prepares electronics tobacco tar
Tealeaves baking Studies of The Aromatic Substances, polydextrose and the atomized liquid 1-5:5-20:75-94 by weight of step (2) are mixed, It stirs to ingredient and is uniformly dissolved at room temperature, be placed in and be protected from light shady place 24~48 h of alcoholization to get the electronic cigarette fragrant to tealeaves baking Oil.
2. preparation method according to claim 1, it is characterised in that: in step (1), the green tea be Xihu Longjing Tea, One of Xinyang Maojian Tea and Pilochun (a green tea) are a variety of;The black tea be one of Keemun black tea, Yunnan black tea and Yixing black tea or It is a variety of;The dark green tea is one of Pu'er tea, Sichuan dark green tea and Hunan dark green tea or a variety of.
3. preparation method according to claim 1, it is characterised in that: in step (2), the polyalcohol be ethylene glycol, One of propylene glycol, glycerol are a variety of.
4. preparation method according to claim 1, it is characterised in that: in step (2), the magnesium ion complex is wine Stone acid magnesium ion complex or ethylenediamine tetra-acetic acid magnesium ion complex.
5. preparation method according to claim 1, it is characterised in that: in step (2), the solvent is petroleum ether, just One of hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and methyl acetate are a variety of.
6. preparation method according to claim 1, it is characterised in that: in step (3), the atomized liquid be propylene glycol or Glycerol.
7. preparation method according to claim 1, it is characterised in that: in step (3), mixing time is 20~30min.
8. the tealeaves that preparation method described in one of claim 1-7 obtains toasts fragrant electronics tobacco tar.
9. the application that tealeaves according to any one of claims 8 toasts fragrant electronics tobacco tar, it is characterised in that: by the electronics tobacco tar according to 0.3-1g is added to conventional electrical cigarette or electric heating and does not burn in cigarette.
CN201811069031.7A 2018-09-13 2018-09-13 Electronic cigarette oil with tea baking fragrance and preparation method and application thereof Active CN109259296B (en)

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CN110693071A (en) * 2019-09-30 2020-01-17 深圳市舜宝科技有限公司 Smoking substrate and method of making same
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CN110693070A (en) * 2019-09-30 2020-01-17 深圳市舜宝科技有限公司 Preparation method of tea stem fuming substrate

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