CN109259293A - A kind of tealeaves toasts fragrant reconstituted tobacco and its preparation method and application - Google Patents
A kind of tealeaves toasts fragrant reconstituted tobacco and its preparation method and application Download PDFInfo
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- CN109259293A CN109259293A CN201811069030.2A CN201811069030A CN109259293A CN 109259293 A CN109259293 A CN 109259293A CN 201811069030 A CN201811069030 A CN 201811069030A CN 109259293 A CN109259293 A CN 109259293A
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- tealeaves
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- reconstituted tobacco
- fragrant
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Abstract
The present invention relates to a kind of tealeaves to toast fragrant reconstituted tobacco and its preparation method and application, the preparation method is carried out as follows: tealeaves baking Studies of The Aromatic Substances is mixed with reconstituted tobacco coating fluid 1:100~1:20 in mass ratio, 0.5~1 times of the scutelloside that tealeaves bakes Studies of The Aromatic Substances quality is added later, 20~30min is stirred at room temperature, it is placed in and is protected from light 24~48h of shady place alcoholization, above-mentioned coating fluid is spread evenly across in chip base with 20%~40% spreading rate, it dries chopping and toasts fragrant reconstituted tobacco to get to tealeaves.The present invention can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance, obtain pure baking perfume (or spice) note substance.Tealeaves baking Studies of The Aromatic Substances of the invention is compounded with scutelloside, be can significantly reduce free-radical contents in flue gas, is added on reconstituted tobacco, the flavor and taste of abundant cigarette can greatly be improved, the effective baking perfume (or spice) quality for improving tobacco, reduces miscellaneous tolerance, improves the comfort and harmony of cigarette.
Description
Technical field
The present invention relates to a kind of preparation methods of reconstituted tobacco, and in particular to a kind of tealeaves toasts the preparation of fragrant reconstituted tobacco
Method further relates to the tealeaves that the preparation method obtains and toasts fragrant reconstituted tobacco and application, belongs to cigarette auxiliary material field.
Background technique
Reconstituted tobacco is that the manufactured thin slice close to tobacco leaf of scrap feed material in production of cigarettes is reused in production of cigarettes,
The inherent quality for improving cigarette product while reducing consumption of raw materials, reduce cost, reduces the harmful components in flue gas, is cigarette
The important component of tobacco leaf formulation.It can be set off, added volume cigarette perfume taste, be increased by reconstituted tobacco flavoring and casing technology
Add flue gas concentration, improvement is jealous, removes and cover miscellaneous gas, reduces irritation, assigns the good characteristic chicken flavor of product, prominent cigarette
The personalized style of product, promote cigarette sucks satisfaction and pleasure degree.
Toasting fragrant note is to bake one of perfume (or spice) note, is the important component of cigarette flavor.In recent years, there is research
Flavouring is carried out to traditional red date extract using zymotechnic, microbial fermentation technology, Maillard reaction etc., produces fragrant processing,
The note for enriching red date extract to a certain extent increases the content of flavor component.Utilize the common volume such as malt extract
It is fragrant to increase flue gas baking for cigarette additive.But the baking perfume (or spice) note of gained the said goods does not protrude, and wherein still contains
There are the macromolecular substances such as a certain amount of protein, pectin, polysaccharide, these substances can crack generation during cigarette is burnt and sucked
Harmful components, increase cigarette smoking irritation and miscellaneous gas.
Tealeaves is one of maximum beverage of world today's consumption figure, it and coffee, cocoa simultaneously claim the world three big non-alcohol drink
Material.Tea from wild into people's artificial cultivation epoch, by the mankind as health care, prevent and cure diseases and apply.And with the hair of society
Exhibition and people constantly improve the raising that the effect of tea recognizes.Tealeaves is as the important drink in people's daily life, with it
The quality and pleasant sense organ flavor of health are liked by consumer, are widely used.Thus, how to select suitable tealeaves to combine
And handled, it is subsequently used for processing reconstituted tobacco, improves cigarette odor-absorbing, urgent need is studied and explored.
Summary of the invention
In order to solve the above technical problem, the present invention provides the preparation method that a kind of tealeaves toasts fragrant reconstituted tobacco, this hairs
Bright technical solution is specific as follows:
A kind of tealeaves toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
Tealeaves baking Studies of The Aromatic Substances is mixed with reconstituted tobacco coating fluid 1:100~1:20 in mass ratio, the roasting perfume of tealeaves is added later
0.5~1 times of scutelloside of material mass, is stirred at room temperature 20~30min, is placed in and is protected from light shady place 24~48h of alcoholization, will
Above-mentioned coating fluid is spread evenly across in chip base with 20%~40% spreading rate, is dried chopping to get to tealeaves baking is fragrant and is reproduced cigarette
Leaf.
Further, the preparation of the tealeaves baking Studies of The Aromatic Substances is carried out as follows:
10~60 parts of green tea powder, 1~5 part of black tea powder and 5~60 parts of dark green tea powder mixing are weighed, are then added 100~500
The polyalcohol of part parts by weight and the magnesium ion complex of 0.01~1 part of parts by weight stir evenly, cold under 150~250 DEG C of oil baths
0.5~3h of solidifying reflux, the solvent supersonic that 200~2000 parts by weight are then added extract 10~60min, then concussion extraction 10~
60min, then be centrifuged 4~15min, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, by solvent remove to get
Perfumery is toasted to tealeaves.
Further, the green tea is one of Xihu Longjing Tea, Xinyang Maojian Tea and Pilochun (a green tea) or a variety of；Described is red
Tea is one of Keemun black tea, Yunnan black tea and Yixing black tea or a variety of；The dark green tea is that Pu'er tea, Sichuan dark green tea and Hunan are black
One of tea is a variety of.
Further, the polyalcohol is one of ethylene glycol, propylene glycol, glycerol or a variety of.
Further, the magnesium ion complex is that magnesium tartrate ionic complex or ethylenediamine tetra-acetic acid magnesium ion are matched
Close object.
Further, the solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and acetic acid
One of methyl esters is a variety of.
The invention further relates to the obtained tealeaves of above-mentioned preparation method toast fragrant reconstituted tobacco.
The invention further relates to above-mentioned tealeaves toast fragrant reconstituted tobacco and do not burn in cigarette cigarette in conventional cigarette or electric heating
Application.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) tealeaves of the invention is in specific modulated process, it will the substance that distinctive tealeaves toasts fragrant note is generated, to it
Product carries out targeting extraction to it using certain solvent, can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance,
Obtain pure baking perfume (or spice) note substance.
(2) tealeaves of the invention baking Studies of The Aromatic Substances is compounded with scutelloside, can significantly reduce free-radical contents in flue gas, by it
It is added on reconstituted tobacco, can greatly improves the flavor and taste of abundant cigarette, improves the baking fragrance and suction mouthfeel of cigarette,
The effective baking perfume (or spice) quality for improving tobacco, reduces miscellaneous tolerance, improves the comfort and harmony of cigarette, preparation method operation
Simply, product safety is with a wide range of applications.
Specific embodiment
(2) tealeaves of the invention baking Studies of The Aromatic Substances is compounded with scutelloside, can significantly reduce free-radical contents in flue gas, by it
It is added on reconstituted tobacco, can greatly improves the flavor and taste of abundant cigarette, improves the baking fragrance and suction mouthfeel of cigarette,
The effective baking perfume (or spice) quality for improving tobacco, reduces miscellaneous tolerance, improves the comfort and harmony of cigarette, preparation method operation
Simply, product safety is with a wide range of applications.
Embodiment 1
The tealeaves of the present embodiment toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
By 10 parts of Xihu Longjing Tea, 1 part of Keemun black tea, 5 parts of Pu'er tea, 100 parts of ethylene glycol, 0.01 part of magnesium tartrate ionic complex
Round-bottomed flask stirring is added, flask mouth connects condenser pipe, is put into oil bath heating later to 180 DEG C of condensing reflux 2.5h.
Then 200 parts of petroleum ethers are added in above-mentioned reaction product, ultrasonic extraction 60min, then concussion extracts 60min
Afterwards, 15min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, by solvent remove to get
Studies of The Aromatic Substances is toasted to tealeaves.
By in above-mentioned tealeaves baking Studies of The Aromatic Substances 1:100 ratio addition reconstituted tobacco coating fluid in mass ratio, tea is added later
Leaf bake 0.5 times of Studies of The Aromatic Substances quality scutelloside, be stirred at room temperature 20min to dissolution mixing it is uniform, be placed in and be protected from light shady place alcohol
Change for 24 hours.
Above-mentioned coating fluid is spread evenly across in chip base with 20% spreading rate, chopping is dried and is dried to get to required tealeaves
Bake fragrant reconstituted tobacco.
Cigarette is produced in conventional fashion into above-mentioned reconstituted tobacco.
Smoked panel test and shown by reconstituted tobacco (reference examples) comparison fragrant with tealeaves baking is not added with: prepared tealeaves toasts
Fragrant reconstituted tobacco, baking note is prominent, and irritation reduces, and comfort improves.The results are shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, 1 gained sample cigarette of embodiment is free
Base content reduces 23%.
Embodiment 2
The tealeaves of the present embodiment toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
3 parts of Xinyang Maojian Tea and Pilochun (a green tea) is 30 parts each, 2 parts of Yunnan black tea and Yixing black tea, Sichuan dark green tea and Hunan dark green tea is 25 parts each, second
Two pure and mild propylene glycol are 250 parts each, 1 part of addition round-bottomed flask of ethylenediamine tetra-acetic acid magnesium ion complex stirs, and flask mouth connects cold
Solidifying pipe, is put into oil bath heating to 250 DEG C of condensing reflux 0.5h later.
Then 2000 parts of n-hexanes and chloroform, ultrasonic extraction 10min, then concussion extraction are added in above-mentioned reaction product
After 10min, 4min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed,
Obtain tealeaves baking Studies of The Aromatic Substances.
By in above-mentioned tealeaves baking Studies of The Aromatic Substances 1:20 ratio addition reconstituted tobacco coating fluid in mass ratio, tealeaves is added later
The scutelloside of roasting 1 times of Studies of The Aromatic Substances, it is uniform to dissolution mixing to be stirred at room temperature 30min, is placed in and is protected from light shady place and refines 48 h.
Above-mentioned coating fluid is spread evenly across in chip base with 40% spreading rate, dries chopping to get fragrant again to tealeaves baking
Make tobacco leaf.
Cigarette is produced in conventional fashion into above-mentioned reconstituted tobacco.
It is smoked panel test and is shown by the reconstituted tobacco comparison fragrant with tealeaves baking is not added with: the fragrant reconstruction of prepared tealeaves baking
Tobacco leaf, baking note is dense, and miscellaneous gas is reduced, and harmony increases.The results are shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, 2 gained sample cigarette of embodiment is free
Base content reduces 34%.
Embodiment 3
The tealeaves of the present embodiment toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
Xihu Longjing Tea and Xinyang Maojian Tea is 30 parts each, 2 parts of Yunnan black tea, 18 parts of Pu'er tea, 200 parts of glycerol, magnesium tartrate ion complex
0.1 part of addition round-bottomed flask of object, stirring, flask mouth connect condenser pipe, are put into oil bath heating later to 200 DEG C of condensing reflux 1h.
1000 parts of ethyl acetate are added in above-mentioned reaction product, then ultrasonic extraction 30min shakes after extracting 30min,
4min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed to get institute is arrived
The tealeaves needed toasts Studies of The Aromatic Substances.
By in above-mentioned tealeaves baking Studies of The Aromatic Substances 1:50 ratio addition reconstituted tobacco coating fluid in mass ratio, tealeaves is added later
The scutelloside of roasting 0.6 times of Studies of The Aromatic Substances, it is uniform to dissolution mixing to be stirred at room temperature 25min, is placed in and is protected from light shady place and refines 30 h.
Above-mentioned coating fluid is spread evenly across in chip base with 30% spreading rate, chopping is dried and is dried to get to required tealeaves
Bake fragrant reconstituted tobacco.
Cigarette is produced in conventional fashion into above-mentioned reconstituted tobacco.
It is smoked panel test and is shown by the reconstituted tobacco comparison fragrant with tealeaves baking is not added with: the fragrant reconstruction of prepared tealeaves baking
Tobacco leaf, tealeaves toast note foot, and in good taste, irritation reduces.The results are shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows 3 gained sample cigarette of embodiment
Free-radical contents reduce 39%.
Embodiment 4
The tealeaves of the present embodiment toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
Xinyang Maojian Tea and Pilochun (a green tea) is 10 parts each, 2 parts of Yixing black tea, Pu'er tea and Hunan dark green tea it is 30 parts each, 300 parts of propylene glycol,
The 0.2 part of addition round-bottomed flask stirring of ethylenediamine tetra-acetic acid magnesium ion complex, flask mouth connect condenser pipe, are put into oil bath later and add
Heat is to 210 DEG C of condensing reflux 2h.
500 parts of methylene chloride of addition and 1500 parts of methyl acetates in above-mentioned reaction product, ultrasonic extraction 20min, then
After concussion extraction 15min, 8min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, it will be molten
Agent removal toasts Studies of The Aromatic Substances to get to required tealeaves.
By above-mentioned tealeaves baking Studies of The Aromatic Substances in 1:80 ratio addition reconstituted tobacco coating fluid, tealeaves is added later and bakes perfumery
The scutelloside that 0.7 times of matter, be stirred at room temperature 28min ingredient dissolution mixing it is uniform, be placed in be protected from light shady place alcoholization 40h.
Above-mentioned coating fluid is spread evenly across in chip base with 35% spreading rate, chopping is dried and is dried to get to required tealeaves
Bake fragrant reconstituted tobacco.
Cigarette is produced in conventional fashion into above-mentioned reconstituted tobacco.
It is smoked panel test and is shown by the reconstituted tobacco comparison fragrant with tealeaves baking is not added with: the fragrant reconstruction of prepared tealeaves baking
Tobacco leaf, tealeaves toast note and protrude, and irritation reduces, and flue gas is fine and smooth.The results are shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows 4 gained sample cigarette of embodiment
Free-radical contents reduce 35%.
Embodiment 5
The tealeaves of the present embodiment toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
Xihu Longjing Tea and Pilochun (a green tea) is 25 parts each, 4 parts of Yixing black tea, Pu'er tea and Hunan dark green tea it is 28 parts each, 250 parts of glycerol, second
The 0.8 part of addition round-bottomed flask stirring of ethylenediamine tetraacetic acid (EDTA) magnesium ion complex, flask mouth connect condenser pipe, are put into oil bath heating later
To 230 DEG C of condensing reflux 1.5h.
200 parts of n-hexanes are added in above-mentioned reaction product and then 1400 parts of methyl acetates, ultrasonic extraction 15min shake
After swinging extraction 15min, 5min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, by solvent
It removes and toasts Studies of The Aromatic Substances to get to required tealeaves.
By above-mentioned tealeaves baking Studies of The Aromatic Substances in 1:70 ratio addition reconstituted tobacco coating fluid, tealeaves is added later and bakes perfumery
The scutelloside that 0.8 times of matter, be stirred at room temperature 28min ingredient dissolution mixing it is uniform, be placed in be protected from light shady place alcoholization 45h.
Above-mentioned coating fluid is spread evenly across in chip base with 30% spreading rate, chopping is dried and is dried to get to required tealeaves
Bake fragrant reconstituted tobacco.
Cigarette is produced in conventional fashion into above-mentioned reconstituted tobacco.
It is smoked panel test and is shown by the reconstituted tobacco comparison fragrant with tealeaves baking is not added with: the fragrant reconstruction of prepared tealeaves baking
Tobacco leaf, tealeaves toast note and protrude, and irritation reduces, and flue gas is fine and smooth.The results are shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows 5 gained sample cigarette of embodiment
Free-radical contents reduce 42%.
Embodiment 6
The tealeaves of the present embodiment toasts the preparation method of fragrant reconstituted tobacco, is carried out as follows:
45 parts of Pilochun (a green tea), 2 parts of Yunnan black tea, 35 parts of Sichuan dark green tea, 150 parts of propylene glycol, 0.08 part of magnesium tartrate ionic complex are added
Enter round-bottomed flask stirring, flask mouth connects condenser pipe, is put into oil bath heating later to 200 DEG C of condensing reflux 2h.
Then 200 parts of chloroforms are added in above-mentioned reaction product, then ultrasonic extraction 60min shakes after extracting 60min,
15min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed to get tea is arrived
Leaf toasts Studies of The Aromatic Substances.
By in above-mentioned tealeaves baking Studies of The Aromatic Substances 1:80 ratio addition reconstituted tobacco coating fluid in mass ratio, tealeaves is added later
The scutelloside of roasting 0.7 times of Studies of The Aromatic Substances quality, it is uniform to dissolution mixing to be stirred at room temperature 20min, is placed in and is protected from light shady place alcoholization
30h。
Above-mentioned coating fluid is spread evenly across in chip base with 25% spreading rate, chopping is dried and is dried to get to required tealeaves
Bake fragrant reconstituted tobacco.
Above-mentioned reconstituted tobacco is produced in conventional fashion into and heats the cigarette that do not burn.
It is smoked panel test and is shown by the reconstituted tobacco comparison fragrant with tealeaves baking is not added with: the fragrant reconstruction of prepared tealeaves baking
Tobacco leaf, baking note is prominent, and irritation reduces, and comfort improves.The results are shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, 6 gained sample cigarette of embodiment is free
Base content reduces 46%.
Comparative test 1
Comparative sample 1 according in embodiment 1 method preparation targeting extraction baking odor type material, but be added without in preparation process magnesium from
Sub- complex detects targeting extraction in comparative sample 1 and embodiment 1 respectively and toasts protein, pectin and polysaccharide etc. in odor type material
Macromolecular content.As shown in Table 1, protein, pectin and more in targeting extraction baking odor type material are added after magnesium ion complex
The macromoleculars content such as sugar is substantially reduced.
Table 1
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Control 1 | 0.2% | 30 | 24 |
| Embodiment 1 | 0 | 0 | 0.2 |
While cigarette 1 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: opposite 1 cigarette of embodiment, control
Cigarette 1 has certain tealeaves baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 2
Comparative sample 2 is prepared according to method in embodiment 1, but calcium salt complex is changed to calcium chloride in preparation process, detects respectively
The macromoleculars content such as protein, pectin and polysaccharide in targeting extraction baking odor type material in comparative sample 2 and embodiment 1.It can by table 2
Know, using the macromoleculars content appearance such as protein, pectin and polysaccharide is bright in targeting extraction baking odor type material after calcium salt complex
It is aobvious to reduce.
Table 2
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 2 | 0.3% | 28 | 20 |
| Embodiment 1 | 0 | 0 | 0.2 |
While cigarette 2 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: opposite 1 cigarette of embodiment, control
Cigarette 2 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 3
Comparative sample 3 is prepared according to method in embodiment 1, but reaction temperature is 120 DEG C, detects comparative sample 3 and embodiment 1 respectively
The macromoleculars content such as protein, pectin and polysaccharide in middle targeting extraction baking odor type material.As shown in Table 3, the targeting of embodiment 1 extraction
The macromoleculars content such as protein, pectin and polysaccharide in baking odor type material is taken to be substantially reduced.
Table 3
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 3 | 0.3% | 22 | 15 |
| Embodiment 1 | 0 | 0 | 0.2 |
While cigarette 3 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: opposite 1 cigarette of embodiment, control
Cigarette 3 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 4
Comparative sample 4 is prepared according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects comparative sample 4 and embodiment respectively
The macromoleculars content such as protein, pectin and polysaccharide in targeting extraction baking odor type material in 1.As shown in Table 4, embodiment 1 targets
The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in extraction baking odor type material.
Table 4
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 4 | 0.5% | 32 | 20 |
| Embodiment 1 | 0 | 0 | 0.2 |
While cigarette 4 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: opposite 1 cigarette of embodiment, control
Cigarette 4 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is stronger, and comfort is very poor.
Comparative test 5
Comparative sample 5 is prepared according to method in embodiment 1, but ultrasonic extraction, concussion extraction and step with centrifugal separation are changed to use
Separatory funnel carries out conventional extraction, detect in comparative sample 5 and embodiment 1 respectively protein in targeting extraction baking odor type material,
The macromoleculars content such as pectin and polysaccharide.As shown in Table 5, protein, pectin and more in the targeting of embodiment 1 extraction baking odor type material
The macromoleculars content such as sugar is substantially reduced.
Table 5
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 5 | 0.4% | 10 | 8 |
| Embodiment 1 | 0 | 0 | 0.2 |
While cigarette 5 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: opposite 1 cigarette of embodiment, control
Cigarette 5 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is slightly strong, and comfort is slightly worse.
Performance detection
Free-radical contents for compareing cigarette 1-6 detect, as a result such as table 6.
Table 6
| Main flume free-radical contents reduced rate, % | |
| 1 reference substance of embodiment | - |
| Embodiment 1 | 23 |
| Compare cigarette 1 | 6 |
| Compare cigarette 2 | -1 |
| Compare cigarette 3 | 5 |
| Compare cigarette 4 | 4 |
| Compare cigarette 5 | 3 |
| Compare cigarette 6 | 1 |
As can be seen from Table 6, the main flume free-radical contents of 1 product of embodiment are well below control cigarette 1-6.Meanwhile it is logical
Comparison is crossed it can be seen that each component and parameter have good synergistic effect in preparation method of the present invention.
Kinds of cigarettes sensory evaluating smoking's evaluation result in 7 embodiment 1-6 of table
| Sample | Fragrance | Harmony | Miscellaneous gas | Irritation | Pleasant impression |
| Reference examples | 25 | 5 | 9 | 16 | 21 |
| Scutelloside is not used in embodiment 1 | 27 | 4.5 | 8.5 | 16.5 | 21 |
| Embodiment 1 | 28 | 5.5 | 10 | 17 | 22 |
| Embodiment 2 | 28.5 | 6 | 10 | 16.5 | 22 |
| Embodiment 3 | 27 | 5.5 | 9.5 | 16.5 | 23 |
| Embodiment 4 | 27.5 | 6 | 10 | 18.5 | 22 |
| Embodiment 5 | 29 | 5.5 | 11 | 17 | 23 |
| Embodiment 6 | 29 | 5.5 | 9.5 | 19 | 24 |
As can be seen from Table 7, the cigarette tealeaves baking note of opposite 1 cigarette of embodiment, control is prominent without cigarette, and comfort is poor,
Respiratory tract irritation decreases, but obvious without the reduction of embodiment 1.
It is compounded in embodiment 1 without using scutelloside, cigarette obtained in the case that other techniques are all the same, sensory evaluating smoking's
Coordinate, is undesirable in terms of miscellaneous gas, effect is also less than reference examples, it is seen then that scutelloside compounding effect is significant.Especially embodiment 5-6
It has outstanding performance.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (8)
1. the preparation method that a kind of tealeaves toasts fragrant reconstituted tobacco, it is characterised in that: be carried out as follows:
Tealeaves baking Studies of The Aromatic Substances is mixed with reconstituted tobacco coating fluid 1:100~1:20 in mass ratio, the roasting perfume of tealeaves is added later
0.5~1 times of scutelloside of material mass, is stirred at room temperature 20~30min, is placed in and is protected from light shady place 24~48h of alcoholization, will
Above-mentioned coating fluid is spread evenly across in chip base with 20%~40% spreading rate, is dried chopping to get to tealeaves baking is fragrant and is reproduced cigarette
Leaf.
2. preparation method according to claim 1, it is characterised in that: the preparation of tealeaves baking Studies of The Aromatic Substances by below into
Row:
10~60 parts of green tea powder, 1~5 part of black tea powder and 5~60 parts of dark green tea powder mixing are weighed, are then added 100~500
The polyalcohol of part parts by weight and the magnesium ion complex of 0.01~1 part of parts by weight stir evenly, cold under 150~250 DEG C of oil baths
0.5~3h of solidifying reflux, the solvent supersonic that 200~2000 parts by weight are then added extract 10~60min, then concussion extraction 10~
60min, then be centrifuged 4~15min, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, by solvent remove to get
Perfumery is toasted to tealeaves.
3. preparation method according to claim 2, it is characterised in that: the green tea be Xihu Longjing Tea, Xinyang Maojian Tea and
One of Pilochun (a green tea) is a variety of；The black tea is one of Keemun black tea, Yunnan black tea and Yixing black tea or a variety of；Described
Dark green tea is one of Pu'er tea, Sichuan dark green tea and Hunan dark green tea or a variety of.
4. preparation method according to claim 2, it is characterised in that: the polyalcohol is ethylene glycol, propylene glycol, glycerol
One of or it is a variety of.
5. preparation method according to claim 2, it is characterised in that: the magnesium ion complex is magnesium tartrate ion
Complex or ethylenediamine tetra-acetic acid magnesium ion complex.
6. preparation method according to claim 1, it is characterised in that: the solvent be petroleum ether, n-hexane, ethyl alcohol,
One of chloroform, methylene chloride, ethyl acetate and methyl acetate are a variety of.
7. the tealeaves that preparation method described in one of claim 1-6 obtains toasts fragrant reconstituted tobacco.
8. the tealeaves of claim 7 toasts the application that fragrant reconstituted tobacco is not burnt in conventional cigarette or electric heating in cigarette cigarette.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022126958A1 (en) * | 2020-12-14 | 2022-06-23 | 湖北中烟工业有限责任公司 | Composition capable of reducing free radical levels in cigarette smoke and preparation method therefor |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2022126958A1 (en) * | 2020-12-14 | 2022-06-23 | 湖北中烟工业有限责任公司 | Composition capable of reducing free radical levels in cigarette smoke and preparation method therefor |
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