CN109259308A - The coffee for reducing flue gas free-radical contents toasts cigarette with quick-fried pearl and preparation method thereof - Google Patents
The coffee for reducing flue gas free-radical contents toasts cigarette with quick-fried pearl and preparation method thereof Download PDFInfo
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- CN109259308A CN109259308A CN201811116211.6A CN201811116211A CN109259308A CN 109259308 A CN109259308 A CN 109259308A CN 201811116211 A CN201811116211 A CN 201811116211A CN 109259308 A CN109259308 A CN 109259308A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Abstract
The present invention relates to a kind of coffees for reducing flue gas free-radical contents to toast cigarette with quick-fried pearl and preparation method thereof, it is carried out as follows: coffee baking Studies of The Aromatic Substances is dissolved in water or Glycerin, mixed triester with caprylic acid capric acid, it is configured to the solution that mass percent is 5%~15%, the scutelloside that coffee bakes 0.5~1 times of Studies of The Aromatic Substances quality is added later, 20~30min is stirred at room temperature, is placed in and is protected from light 24~48h of shady place alcoholization.The present invention can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance, obtain pure baking perfume (or spice) note substance, be added to cigarette on quick-fried pearl, can greatly improve the flavor and taste of abundant cigarette.Coffee baking Studies of The Aromatic Substances of the invention is compounded with scutelloside, using to cigarette in quick-fried pearl, it can significantly reduce free-radical contents in flue gas, the baking fragrance and suction mouthfeel of cigarette can also be improved simultaneously, the baking perfume (or spice) quality of cigarette products can effectively be improved, miscellaneous tolerance is reduced, the comfort and harmony of cigarette are improved.
Description
Technical field
The present invention relates to a kind of cigarettes with quick-fried pearl and preparation method thereof, and in particular to a kind of coffee for reducing flue gas free-radical contents
Coffee toasts the cigarette preparation method of quick-fried pearl, belongs to cigarette auxiliary material field.
Background technique
Quick-fried pearl cigarette is to be pre-filled with one or more flavored capsules, smoker in filter tip to select in sucking process
Capsule is pinched quick-fried, release fragrance by selecting property.Quick-fried pearl is that cigarette assigns fragrant, flavouring humectation technology new way, is in category construction work
Effective support and cigarette brand rejuvenation of " can perceive ", personalized realization rate.
Even if domestic cigarette product is deposited in terms of sucking quality and sense organ however, joined the quick-fried pearl of cigarette
In certain deficiency, such as fragrance is faint, dry sensation is strong, sweet degree is inadequate, comfort level is poor.
Toast the important component that fragrant note is cigarette flavor.In recent years, there are research and utilization zymotechnic, microbial fermentation
Technology, Maillard reaction etc. carry out flavouring to traditional red date extract, produce fragrant processing, enrich jujube to a certain extent and mention
The note for taking object increases the content of flavor component.Using the common cigarette additive such as malt extract, increase flue gas baking
It is fragrant.But the baking perfume (or spice) note of gained the said goods does not protrude, and wherein still containing a certain amount of protein, pectin,
The macromolecular substances such as polysaccharide, these substances can crack during cigarette is burnt and sucked generates some harmful components, increases cigarette smoking
Irritation and miscellaneous gas.
Coffee is as flavouring, wherein roasting modulated process is the key link for influencing coffee flavor quality.Green coffee
Only more than 40 kinds of the fragrance of itself, but its fragrance component is activated up to more than 300 kinds after roasting modulation.How coffee applied into cigarette
With on quick-fried pearl, improves sensory evaluating smoking's mass, be urgent problem.
Summary of the invention
In order to solve the above technical problem, the present invention provides a kind of coffee baking cigarettes for reducing flue gas free-radical contents to use
The preparation method of quick-fried pearl, technical solution of the present invention are specific as follows:
A kind of coffee baking cigarette preparation method of quick-fried pearl reducing flue gas free-radical contents, is carried out as follows:
Coffee baking Studies of The Aromatic Substances is dissolved in water or Glycerin, mixed triester with caprylic acid capric acid, the solution that mass percent is 5%~15% is configured to, it
The scutelloside that coffee bakes 0.5~1 times of Studies of The Aromatic Substances quality is added afterwards, 20~30min is stirred at room temperature, is placed in and is protected from light shady place alcohol
Change 24~48h；
Above-mentioned solution of alcoholized is prepared into dripping pill using pill dripping machine, dries and is toasted to get to the coffee for reducing flue gas free-radical contents
Cigarette is with quick-fried pearl.
Further, the preparation method of the coffee baking Studies of The Aromatic Substances is carried out as follows:
1~5 part of big grain coffee, 10~60 parts of middle grain coffee and 5~50 parts of arabiancoffee are weighed by weight, and 100- is then added
500 parts of polyalcohols and 0.01-1 parts of Nu-Irons, stir evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths,
Then the solvent supersonic that 200~2000 parts by weight are added extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4
~15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed and toasts perfumery to get to coffee
Matter.
Further, in step (1), big grain coffee is the big grain coffee of the big grain coffee of Greece and/or Taiwan；Middle grain coffee is
Grain coffee in Vietnam, grain coffee in India, one of grain coffee or a variety of in Hainan；Arabiancoffee be Brazilian arabiancoffee,
One or more of Jamaica's arabiancoffee, Yunnan arabiancoffee.
Further, in step (1), the polyalcohol is one or more of ethylene glycol, propylene glycol and glycerol.
Further, in step (1), the Nu-Iron is that dextrin polysaccharide iron complexes or iron dextran are multiple
Close object.
Further, in step (1), the solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, acetic acid
One or more of ethyl ester and methyl acetate.
Further, the diameter of dripping pill is 2.5~4.5mm.
The coffee baking cigarette of the reduction flue gas free-radical contents obtained the invention further relates to above-mentioned preparation method is with quick-fried
Pearl.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) the application combines the coffee species of different-grain diameter, through ovennodulation, generates the object that distinctive coffee toasts fragrant note
Matter carries out targeting extraction to it using certain solvent, can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance, obtain
To pure baking perfume (or spice) note substance, cigarette is added to on quick-fried pearl, can greatly improve the flavor and taste of abundant cigarette.
(2) coffee of the invention baking Studies of The Aromatic Substances is compounded with scutelloside, is used cigarette in quick-fried pearl, be can significantly reduce flue gas
Middle free-radical contents, while the baking fragrance and suction mouthfeel of cigarette can also be improved, it can effectively improve cigarette products
Fragrant quality is toasted, miscellaneous tolerance is reduced, improves the comfort and harmony of cigarette.
(3) preparation method of the invention is easy to operate, and product safety is with a wide range of applications.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.In the examples where no specific technique or condition is specified, described technology or item according to the literature in the art
Part is carried out according to product description.Reagents or instruments used without specified manufacturer is that can be obtained by purchase
Conventional products.The sensory evaluation of all embodiments is all carried out according to GB5606.4-2005.
Embodiment 1
The coffee of the reduction flue gas free-radical contents of the present embodiment toasts the cigarette preparation method of quick-fried pearl, is carried out as follows:
It weighs grain coffee in 10 parts of Vietnam, the big grain coffee of 1 part of Greece, 5 parts of Brazilian arabiancoffee powder and round-bottomed flask mixing is added,
Then 100 parts and 0.01 part dextrin polysaccharide iron complexes of ethylene glycol, stirring are added, flask mouth connects condenser pipe, is put into oil later
Bath is heated to 150 DEG C, is condensed back 3h.
200 parts of petroleum ethers are added in above-mentioned reaction product, then ultrasonic extraction 60min shakes after extracting 60min, into
Row centrifuge separation 15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, solvent is removed to get coffee is arrived
Toast Studies of The Aromatic Substances.
5 parts of above-mentioned coffee baking Studies of The Aromatic Substances are dissolved in water, the solution that mass percent is 5% is configured to, 2.5 is added later
The scutelloside of part, is stirred at room temperature 20min, is placed in and is protected from light shady place alcoholization for 24 hours.
Using pill dripping machine by above-mentioned solution of alcoholized be prepared into diameter be 2.5mm dripping pill, collect molding dripping pill, drying to get
Fragrant cigarette is toasted with quick-fried pearl to coffee.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By be not added with the cigarette identical cigarette of quick-fried pearl
(using 555 cigarette), comparison, which is smoked panel test, to be shown: prepared cigarette toasts note with quick-fried pearl and protrudes, and irritation reduces, and comfort mentions
It is high.Smoking result is shown in Table 7.It is measured by flue gas free-radical contents using electron spin resonance, shows 1 gained of embodiment
Sample cigarette free-radical contents reduce 51%.
Embodiment 2
The coffee of the reduction flue gas free-radical contents of the present embodiment toasts the cigarette preparation method of quick-fried pearl, is carried out as follows:
Weigh in Hainan that grain coffee in grain coffee and Vietnam is 30 parts each, 3 parts of the big grain coffee of 2 parts of the big grain coffee of Greece and Taiwan, tooth
Buy plus round-bottomed flask mixing be added in arabiancoffee and each 25 parts of powder of Yunnan arabiancoffee, be then added 250 parts of propylene glycol and
1 part of dextran iron complexes, stirring, flask mouth connects condenser pipe, is put into oil bath heating later to 250 DEG C, is condensed back
0.5h。
2000 parts of n-hexanes and chloroform are added in above-mentioned reaction product, wherein 1:1 is mixed by volume for n-hexane and chloroform
It closes, ultrasonic extraction 10min, then after concussion extraction 10min, 4min is centrifuged, takes supernatant liquid with organic filter membrane mistake
It after filter, is evaporated under reduced pressure, solvent is removed and toasts Studies of The Aromatic Substances to get to coffee.
15 parts of above-mentioned coffee baking Studies of The Aromatic Substances are dissolved in Glycerin, mixed triester with caprylic acid capric acid, are configured to the solution that mass percent is 15%,
15 parts of scutelloside is added later, 30min is stirred at room temperature, is placed in and is protected from light shady place alcoholization 48h.
Using pill dripping machine by above-mentioned solution of alcoholized be prepared into diameter be 4.5mm dripping pill, collect molding dripping pill, drying to get
Fragrant cigarette is toasted with quick-fried pearl to coffee.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By be not added with the cigarette identical cigarette of quick-fried pearl
Comparison, which is smoked panel test, to be shown: prepared cigarette is dense with quick-fried pearl baking note, and miscellaneous gas is reduced, and harmony increases.Smoking result is shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows that 2 gained sample cigarette free radical of embodiment contains
Amount reduces 56%.
Embodiment 3
The coffee of the reduction flue gas free-radical contents of the present embodiment toasts the cigarette preparation method of quick-fried pearl, is carried out as follows:
Weigh in India that grain coffee in grain coffee and Hainan is 30 parts each, 2 parts of the big grain coffee in Taiwan, 18 parts of Yunnan arabiancoffee of powder
Round-bottomed flask is added in end, is then added 200 parts of glycerol, and 0.1 part of dextran iron complexes, stirring, flask mouth connects condenser pipe,
It is put into oil bath heating later to 200 DEG C, is condensed back 1h.
1000 parts of ethyl acetate are added in above-mentioned reaction product, then ultrasonic extraction 30min shakes after extracting 30min,
4min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed to get coffee is arrived
Coffee toasts Studies of The Aromatic Substances.
Above-mentioned 10 portions of coffee baking Studies of The Aromatic Substances is dissolved in Glycerin, mixed triester with caprylic acid capric acid, being configured to mass percent is 10% solution, it
8 parts of scutelloside is added afterwards, 25min is stirred at room temperature, is placed in and is protected from light 30 h of shady place alcoholization.
Above-mentioned solution of alcoholized is prepared into the dripping pill that diameter is 3mm using pill dripping machine, molding dripping pill is collected, dries to get arriving
Coffee toasts fragrant cigarette with quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By be not added with the cigarette identical cigarette of quick-fried pearl
Comparison, which is smoked panel test, to be shown: prepared cigarette toasts note foot with quick-fried pearl coffee, and in good taste, irritation reduces.Smoking result is shown in Table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows that 3 gained sample cigarette free radical of embodiment contains
Amount reduces 42%.
Embodiment 4
The coffee of the reduction flue gas free-radical contents of the present embodiment toasts the cigarette preparation method of quick-fried pearl, is carried out as follows:
Weigh in Vietnam 10 parts each grain coffee in grain coffee and India, 2 parts of the big grain coffee of Greece, Jamaica's arabiancoffee and Brazil
Round-bottomed flask is added in each 30 parts of powder of arabiancoffee, then 300 parts and 0.2 part of dextrin polysaccharide iron complexes of propylene glycol, stirring,
Flask mouth connects condenser pipe, is put into oil bath heating later to 210 DEG C, is condensed back 2h.
500 parts of methylene chloride of addition and 1500 parts of methyl acetates in above-mentioned reaction product, ultrasonic extraction 20min, then
After concussion extraction 15min, 8min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, it will be molten
Agent removal toasts Studies of The Aromatic Substances to get to coffee.
12 parts of above-mentioned coffee baking Studies of The Aromatic Substances are dissolved in water, the solution that mass percent is 12% is configured to, 10 is added later
The scutelloside of part, is stirred at room temperature 30min, is placed in and is protected from light 40 h of shady place alcoholization.
Above-mentioned solution is prepared into the dripping pill that diameter is 3mm using pill dripping machine, collects molding dripping pill, drying, required coffee
Coffee toasts fragrant cigarette with quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By be not added with the cigarette identical cigarette of quick-fried pearl
Comparison, which is smoked panel test, to be shown: prepared cigarette toasts note with quick-fried pearl coffee and protrudes, and irritation reduces, and flue gas is fine and smooth.Smoking result is shown in
Table 7.It is measured by flue gas free-radical contents using electron spin resonance, shows that 4 gained sample cigarette of embodiment is free
Base content reduces 23%.
Comparative test 1
Comparative sample 1 is prepared according to method in embodiment 1, but Nu-Iron is added without in preparation process, respectively detection pair
Than targeting the macromoleculars content such as protein, pectin and polysaccharide in extract in sample 1 and embodiment 1.As shown in Table 1, polysaccharide is added
The macromoleculars content such as protein, pectin and polysaccharide in extract is targeted after iron complexes to be substantially reduced.
Table 1
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Control 1 | 0.4% | 30 | 20 |
| Embodiment 1 | 0 | 0.1 | 0. |
While quick-fried pearl cigarette 1 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 1 has certain coffee baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is poor.
Comparative test 2
Comparative sample 2 is prepared according to method in embodiment 1, but Nu-Iron is changed to iron chloride in preparation process, examines respectively
It surveys in comparative sample 2 and embodiment 1 and targets the macromoleculars content such as protein, pectin and polysaccharide in extract.As shown in Table 2, it uses
The macromoleculars content such as protein, pectin and polysaccharide in extract is targeted after Nu-Iron to be substantially reduced.
Table 2
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 2 | 0.1% | 29 | 25 |
| Embodiment 1 | 0 | 0.1 | 0.1 |
While quick-fried pearl cigarette 2 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 2 has certain coffee baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, comfort
Difference.
Comparative test 3
Comparative sample 3 is prepared according to method in embodiment 1, but reaction temperature is 120 DEG C, detects comparative sample 3 and embodiment 1 respectively
The macromoleculars content such as protein, pectin and polysaccharide in middle targeting extract.As shown in Table 3, embodiment 1 targets albumen in extract
The macromoleculars content such as matter, pectin and polysaccharide is substantially reduced.
Table 3
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 3 | 0.3% | 22 | 15 |
| Embodiment 1 | 0 | 0.1 | 0.1 |
While quick-fried pearl cigarette 3 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 3 has certain coffee baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, comfort
Difference.
Comparative test 4
Comparative sample 4 is prepared according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects comparative sample 4 and embodiment respectively
The macromoleculars content such as protein, pectin and polysaccharide in extract is targeted in 1.As shown in Table 4, embodiment 1 targets egg in extract
The macromoleculars content such as white matter, pectin and polysaccharide is substantially reduced.
Table 4
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 4 | 0.5% | 32 | 20 |
| Embodiment 1 | 0 | 0.1 | 0.1 |
While quick-fried pearl cigarette 4 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 4 has certain coffee baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is very poor.
Comparative test 5
Comparative sample 5 is prepared according to method in embodiment 1, but ultrasonic extraction, concussion extraction and step with centrifugal separation are changed to use
Separatory funnel carries out conventional extraction, detects target protein, pectin and polysaccharide in extract in comparative sample 5 and embodiment 1 respectively
Etc. macromoleculars content.As shown in Table 5, it is bright to target the macromoleculars content such as protein, pectin and polysaccharide appearance in extract for embodiment 1
It is aobvious to reduce.
Table 5
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 5 | 0.4% | 10 | 8 |
| Embodiment 1 | 0 | 0.1 | 0.1 |
While quick-fried pearl cigarette 5 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 5 has certain coffee baking note but does not protrude, while miscellaneous gas is obvious, and irritation is slightly strong, comfortably
Property is slightly worse.
Simultaneously according to control filter tip 5 is prepared into described in embodiment 1, using 1 middle period of embodiment group and control filter tip 5, preparation
Cigarette 5 is compareed at cigarette.Shown by smokeing panel test: opposite 1 cigarette 1 of embodiment, control cigarette 5 have certain coffee baking note but
It does not protrude, while miscellaneous gas is obvious, irritation is strong, and comfort is poor.
Performance detection
Free-radical contents for compareing cigarette 1-6 detect, as a result such as table 6.
Table 6
As can be seen from Table 6, the main flume free-radical contents of 1 product of embodiment are well below control cigarette 1-5.Meanwhile it is logical
Comparison is crossed it can be seen that each component and parameter have good synergistic effect in preparation method of the present invention.
Different electronic cigarette sensory evaluating smoking's evaluation results in 7 embodiment 1-4 of table
| Sample | Fragrance | Harmony | Miscellaneous gas | Irritation | Pleasant impression |
| Reference examples | 25 | 5 | 7 | 14 | 19 |
| Scutelloside is not used in embodiment 1 | 27 | 4 | 8 | 15 | 20 |
| Embodiment 1 | 28 | 5.5 | 10 | 17 | 22 |
| Embodiment 2 | 28.5 | 6 | 10 | 16.5 | 22 |
| Embodiment 3 | 27 | 5.5 | 9.5 | 16.5 | 23 |
| Embodiment 4 | 27.5 | 6 | 10 | 18.5 | 22 |
The cigarette identical cigarette of quick-fried pearl (using 555 cigarette) is not added with as reference examples, without using scutelloside in preparation process,
According to the method for embodiment 1, it is prepared into cigarette.
As can be seen from Table 7, the cigarette coffee baking note of opposite 1 cigarette of embodiment, control is prominent without cigarette, comfort
Difference, respiratory tract irritation decrease, but obvious without the reduction of embodiment 1.
It is compounded in embodiment 1 without using scutelloside, cigarette obtained in the case that other techniques are all the same, sensory evaluating smoking's
Coordinate, is undesirable in terms of miscellaneous gas, effect is also less than reference examples, it is seen then that scutelloside compounding effect is significant.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of coffee baking cigarette for reducing flue gas free-radical contents preparation method of quick-fried pearl, it is characterised in that: by following
It carries out:
Coffee baking Studies of The Aromatic Substances is dissolved in water or Glycerin, mixed triester with caprylic acid capric acid, the solution that mass percent is 5%~15% is configured to, it
The scutelloside that coffee bakes 0.5~1 times of Studies of The Aromatic Substances quality is added afterwards, 20~30min is stirred at room temperature, is placed in and is protected from light shady place alcohol
Change 24~48h；
Above-mentioned solution of alcoholized is prepared into dripping pill using pill dripping machine, dries and is toasted to get to the coffee for reducing flue gas free-radical contents
Cigarette is with quick-fried pearl.
2. preparation method according to claim 1, it is characterised in that: the preparation method of coffee baking Studies of The Aromatic Substances press with
Lower progress:
1~5 part of big grain coffee, 10~60 parts of middle grain coffee and 5~50 parts of arabiancoffee are weighed by weight, and 100- is then added
500 parts of polyalcohols and 0.01-1 parts of Nu-Irons, stir evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths,
Then the solvent supersonic that 200~2000 parts by weight are added extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4
~15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed and toasts perfumery to get to coffee
Matter.
3. preparation method according to claim 2, it is characterised in that: in step (1), big grain coffee is the big grain coffee of Greece
And/or the big grain coffee in Taiwan；Middle grain coffee be grain coffee in Vietnam, grain coffee in India, in Hainan one of grain coffee or
It is a variety of；Arabiancoffee is one or more of Brazilian arabiancoffee, Jamaica's arabiancoffee, Yunnan arabiancoffee.
4. preparation method according to claim 2, it is characterised in that: in step (1), the polyalcohol be ethylene glycol,
One or more of propylene glycol and glycerol.
5. preparation method according to claim 2, it is characterised in that: in step (1), the Nu-Iron is paste
Smart Nu-Iron or dextran iron complexes.
6. preparation method according to claim 2, it is characterised in that: in step (1), the solvent is petroleum ether, just
One or more of hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and methyl acetate.
7. preparation method according to claim 1, it is characterised in that: the diameter of dripping pill is 2.5~4.5mm.
8. the coffee baking cigarette for the reduction flue gas free-radical contents that preparation method described in one of claim 1-7 obtains is with quick-fried
Pearl.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2022126958A1 (en) * | 2020-12-14 | 2022-06-23 | 湖北中烟工业有限责任公司 | Composition capable of reducing free radical levels in cigarette smoke and preparation method therefor |
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