CN104905400A - Tobacco humectant and preparing method thereof - Google Patents

Tobacco humectant and preparing method thereof Download PDF

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Publication number
CN104905400A
CN104905400A CN201510209794.7A CN201510209794A CN104905400A CN 104905400 A CN104905400 A CN 104905400A CN 201510209794 A CN201510209794 A CN 201510209794A CN 104905400 A CN104905400 A CN 104905400A
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Prior art keywords
parts
tobacco
humectant
water
tobacco humectant
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CN201510209794.7A
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CN104905400B (en
Inventor
杨亚玲
赵娇
刘春波
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

Abstract

The invention discloses tobacco humectant and a preparing method thereof. The tobacco humectant is composed of, by weight, 1-5 parts of water soluble plant oil, 50-80 parts of polyhydric alcohol, 2-5 parts of polyethylene glycol, 2-5 parts of polydextrose, 2-5 parts of maltose, 3-7 parts of inositol and 5-25 parts of absolute ethyl alcohol. The tobacco humectant comprises the hydrophilic humectant polyhydric alcohol and the water soluble plant oil, the hydrophilic humectant absorbs moisture from damp air, the water soluble plant oil forms a protection membrane on the surface of cut tobacco, and the speed of the moisture loss is reduced. The hydrophilic humectant polyhydric alcohol and the water soluble plant oil form an even and stable system under a certain condition and fully play the roles of all components, and a good tobacco leaf moistening effect is achieved.

Description

A kind of tobacco humectant and preparation method thereof
Technical field
The present invention relates to tobacco manufacture field, be specifically related to a kind of tobacco humectant and preparation method thereof.
Background technology
In tobacco processing, the main purpose of NMF is the moisture content maintaining pipe tobacco in process, improves the resist processing of pipe tobacco, improves the moisture content of finished cigarettes, sense organ comfort level.NMF has moisturizing and moistureproof double effects, namely reduces the sensitivity that tobacco moisture percentage changes ambient temperature and humidity, remains that moisture content of cut tobaccos is a metastable scope; Focus on the improvement effect to mouthfeel simultaneously.Mainly adopt the polyhydroxy substances such as glycerine, propane diols, sorbierite as humectant in China's tobacco industry.In recent years, domesticly report some novel humectants, as polydextrose, sucrose ester, plant extracts natural baccy humectant, belong to hygroscopicity humectant from principle, this kind of material has stronger water imbibition, and its effect absorbs moisture content and is stored in cigarette.Chinese patent 201210262126.7 discloses a kind of polydextrose cigarette humectant and using method, makes after mixing with polydextrose and water or propane diols; Chinese patent 201210307164.X discloses a kind of cigarette sense organ flavouring humectant and its preparation method and application, and this flavouring humectant is taro extract; Chinese patent 201210292418.5 discloses a kind of plant oil tobacco humectation and preparation method thereof, is processed by vegetable oil, emulsifying agent and water.These public technologies mostly only have the performance of hydrophilic humectant, namely absorb the effect of moisture, the humectant obtained by vegetable oil emulsification, the selection of emulsifying agent and the selection of vegetable fat and important, otherwise produce excitant peculiar smell during burning.The present invention is both containing hydrophily humectant polyalcohol, again containing oleophilic plant oil, owing to producing the hydrophilic plant oil of peculiar smell when have selected burning hardly, especially do not adopt emulsifying agent, make the tobacco humectant of preparation have excellent humectation function, keep the fragrance of cigarette simultaneously.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, there is provided a kind of tobacco humectant, the constituent of this tobacco humectant and weight portion are: water-soluble plant oil 1 ~ 5 part, polyalcohol 50 ~ 80 parts, polyethylene glycol 2 ~ 5 parts, polydextrose 2 ~ 5 parts, maltose 2 ~ 5 parts, inositol 3 ~ 7 parts, absolute ethyl alcohol 5 ~ 25 parts.
Described water-soluble plant oil is the one in water-soluble sun caul-fat, fiery flaxseed oil, water-soluble jojoba oil, water-soluble corn oil.
Described polyalcohol is one or more mixtures in propane diols, glycerine, xylitol, sorbierite.
Described polyethylene glycol is the one in Macrogol 200, PEG400, Macrogol 600.
Another object of the present invention is to provide the preparation method of above-mentioned tobacco humectant, and concrete operations are as follows:
(1) be warming up to 50 ~ 70 DEG C by after polyalcohol, polyethylene glycol, polydextrose, maltose, inositol mixing, under 800 ~ 1500rpm, stir 10 ~ 20min;
(2) water-soluble plant oil is mixed with absolute ethyl alcohol, under normal temperature, under 800 ~ 1500rpm, stir 20 ~ 40min;
(3) be warming up to 50 ~ 70 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, under 800 ~ 1500rpm, stir 20 ~ 40min, namely obtain tobacco humectant.
The inventive method utilizes hydrophilic humectant polyalcohol and water-soluble plant oil, be prepared from through certain technique, existing water suction humectation effect, form a skim on pipe tobacco surface again, do not produce any peculiar smell when result of combustion of tobacco, play the object that comfort level is sucked in moisturizing and improvement.
Be applied to by tobacco humectant of the present invention in tobacco humectation, 0.1%-0.5% tobacco humectant being pressed pipe tobacco weight mixes with tobacco sauce, and even application, on pipe tobacco, makes cigarette.
relative to prior art, the present invention has following remarkable advantage:
1, the humectation of this tobacco is both containing hydrophily humectant polyalcohol, again containing oleophilic plant oil, does not need to add emulsifying agent, can not bring uncomfortable peculiar smell, give full play to the effect of each composition simultaneously in preparation.
2, because selected raw material is all water miscible, the stable system of preparation.
3, product is as tobacco humectant, better with tobacco sauce compatibility, can dissolve in 75% ethanol, and stable, technique is easy to realize.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further described, but protection scope of the present invention is not limited to this.
embodiment 1:the constituent of this tobacco humectant and weight portion are: water-soluble sun caul-fat 5 parts, polyalcohol 50 parts, polyethylene glycol 5 parts, polydextrose 2 parts, maltose 2 parts, inositol 4 parts, absolute ethyl alcohol 25 parts.
The preparation method of above-mentioned humectant is as follows:
(1) by 30g propane diols, 20 g xylitols, 2g maltose, 5g Macrogol 200,2g polydextrose, the mixing of 4g inositol, be warming up to 60 DEG C, mixing speed is 800rpm, and constant temperature stirs 15min;
(2) water-soluble for 5g sun caul-fat is mixed with 25g absolute ethyl alcohol, under 800rpm normal temperature, stir 30min;
(3) be warming up to 55 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, under 1000rpm, stir 25min, namely obtain tobacco humectant.
(4) tobacco humectant that prepared by step (3) mixes with tobacco sauce by 0.3% of pipe tobacco weight, and even application, on pipe tobacco, makes cigarette, carries out humid keeping performance test.
embodiment 2:the constituent of this tobacco humectant and weight portion are: fiery flaxseed oil 3 parts, polyalcohol 60 parts, polyethylene glycol 3 parts, polydextrose 3 parts, maltose 4 parts, inositol 5 parts, absolute ethyl alcohol 15 parts.
The preparation method of above-mentioned humectant is as follows:
(1) by 40g propane diols, 20 g glycerine, 4g maltose, 3g PEG400,3g polydextrose, the mixing of 5g inositol, mixing speed is 1000rpm, is warming up to 65 DEG C, and constant temperature stirs 12min;
(2) 3g fire flaxseed oil is mixed with 15g absolute ethyl alcohol, under 1000rpm normal temperature, stir 25min;
(3) be warming up to 60 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, under 1000rpm, stir 30min, namely obtain tobacco humectant.
(4) tobacco humectant that prepared by step (3) mixes with tobacco sauce by 0.3% of pipe tobacco weight, and even application, on pipe tobacco, makes cigarette, carries out humid keeping performance test.
embodiment 3: the constituent of this tobacco humectant and weight portion are: water-soluble jojoba oil 3 parts, polyalcohol 65 parts, polyethylene glycol 2 parts, polydextrose 2 parts, maltose 3 parts, inositol 5 parts, absolute ethyl alcohol 20 parts.
The preparation method of above-mentioned humectant is as follows:
(1) by 35g propane diols, 20 g glycerine, 10 g sorbierites, 3g maltose, 2g Macrogol 600,2g polydextrose, the mixing of 5g inositol, mixing speed is 1200rpm, is warming up to 50 DEG C, and constant temperature stirs 20min;
(2) water-soluble for 3g jojoba oil is mixed with 20g absolute ethyl alcohol, under 1200rpm normal temperature, stir 20min;
(3) be warming up to 70 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, stir 40min at 800 rpm, namely obtain tobacco humectant.
(4) tobacco humectant that prepared by step (3) mixes with tobacco sauce by 0.3% of pipe tobacco weight, and even application, on pipe tobacco, makes cigarette, carries out humid keeping performance test.
embodiment 4:the constituent of this tobacco humectant and weight portion are: water-soluble corn oil 2 parts, polyalcohol 80 parts, polyethylene glycol 5 parts, polydextrose 2 parts, maltose 5 parts, inositol 6 parts, absolute ethyl alcohol 10 parts.
The preparation method of above-mentioned humectant is as follows:
(1) by 50g propane diols, 10 g glycerine, 20 g xylitols, 5g maltose, 5g Macrogol 200,2g polydextrose, the mixing of 6g inositol, mixing speed is 900rpm, is warming up to 70 DEG C, and constant temperature stirs 10min;
(2) water-soluble for 2g corn oil is mixed with 10g absolute ethyl alcohol, under 1200rpm normal temperature, stir 30min;
(3) be warming up to 60 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, under 1000rpm, stir 30min, namely obtain tobacco humectant.
(4) tobacco humectant that prepared by step (3) mixes with tobacco sauce by 0.3% of pipe tobacco weight, and even application, on pipe tobacco, makes cigarette, carries out humid keeping performance test.
embodiment 5:the constituent of this tobacco humectant and weight portion are: water-soluble corn oil 1 part, polyalcohol 80 parts, polyethylene glycol 3 parts, polydextrose 5 parts, maltose 2 parts, inositol 3 parts, absolute ethyl alcohol 15 parts.
The preparation method of above-mentioned humectant is as follows:
(1) by 30g propane diols, 30 g glycerine, 20 g sorbierites, 2g maltose, 3g PEG400,5g polydextrose, the mixing of 3g inositol, mixing speed is 800rpm, is warming up to 70 DEG C, and constant temperature stirs 20min;
(2) water-soluble for 1g corn oil is mixed with 15g absolute ethyl alcohol, under 1000rpm normal temperature, stir 40min;
(3) be warming up to 70 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, stir 20min at 800 rpm, namely obtain tobacco humectant.
(4) tobacco humectant that prepared by step (3) mixes with tobacco sauce by 0.3% of pipe tobacco weight, and even application, on pipe tobacco, makes cigarette, carries out humid keeping performance test.
embodiment 6:the constituent of this tobacco humectant and weight portion are: fiery flaxseed oil 5 parts, polyalcohol 60 parts, polyethylene glycol 2 parts, polydextrose 2 parts, maltose 2 parts, inositol 7 parts, absolute ethyl alcohol 25 parts.
The preparation method of above-mentioned humectant is as follows:
(1) by 60g propane diols, 2g maltose, 2g Macrogol 600,2g polydextrose, the mixing of 7g inositol, mixing speed is 1500rpm, is warming up to 50 DEG C, and constant temperature stirs 15min;
(2) 5g fire flaxseed oil is mixed with 25g absolute ethyl alcohol, under 1200rpm normal temperature, stir 30min;
(3) be warming up to 70 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, stir 40min at 800 rpm, namely obtain tobacco humectant.
(4) tobacco humectant that prepared by step (3) mixes with tobacco sauce by 0.3% of pipe tobacco weight, and even application, on pipe tobacco, makes cigarette, carries out humid keeping performance test.
That is prepared by embodiment 1-6 carries out the test of tobacco humectant humid keeping performance, the results are shown in Table 1.
Table 1: tobacco humectant moisture content changes in time
As shown in Table 1, under humectant addition same case, the humectation effect of humectant of the present invention is all better than the contrast pipe tobacco not adding humectant and conventional tobacco humectant propane diols and glycerine, the moisture using humectant can increase pipe tobacco is described, improve the equilibrium moisture content of pipe tobacco, have good humid keeping performance.

Claims (5)

1. a tobacco humectant, is characterized in that: its constituent and weight portion are water-soluble plant oil 1 ~ 5 part, polyalcohol 50 ~ 80 parts, polyethylene glycol 2 ~ 5 parts, polydextrose 2 ~ 5 parts, maltose 2 ~ 5 parts, inositol 3 ~ 7 parts, absolute ethyl alcohol 5 ~ 25 parts.
2. tobacco humectant according to claim 1, is characterized in that: water-soluble plant oil is the one in water-soluble sun caul-fat, fiery flaxseed oil, water-soluble jojoba oil, water-soluble corn oil.
3. tobacco humectant according to claim 1 and 2, is characterized in that: polyalcohol is one or more mixtures in propane diols, glycerine, xylitol, sorbierite.
4. tobacco humectant according to claim 3, is characterized in that: polyethylene glycol is the one in Macrogol 200, PEG400, Macrogol 600.
5. the preparation method of tobacco humectant according to claim 1, is characterized in that comprising the following steps:
(1) be warming up to 50 ~ 70 DEG C by after polyalcohol, polyethylene glycol, polydextrose, maltose, inositol mixing, under 800 ~ 1500rpm, stir 10 ~ 20min;
(2) water-soluble plant oil is mixed with absolute ethyl alcohol, under normal temperature, under 800 ~ 1500rpm, stir 20 ~ 40min;
(3) be warming up to 50 ~ 70 DEG C after liquid prepared by liquid step (1) prepared and step (2) mixes, under 800 ~ 1500rpm, stir 20 ~ 40min, namely obtain tobacco humectant.
CN201510209794.7A 2015-04-29 2015-04-29 A kind of tobacco humectant and preparation method thereof Active CN104905400B (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106490676A (en) * 2016-12-11 2017-03-15 钦州学院 A kind of starchiness humectant for smoke and preparation method thereof
CN108013498A (en) * 2017-11-23 2018-05-11 广西中烟工业有限责任公司 A kind of compound additive for improving reconstituted tobacco physics humid keeping performance
CN108056496A (en) * 2017-11-29 2018-05-22 广西中烟工业有限责任公司 A kind of tobacco humectant and preparation method thereof
CN109105945A (en) * 2018-09-13 2019-01-01 云南中烟工业有限责任公司 A method of tobacco roasting odor type electronics tobacco tar is prepared using organic acid-metal salt compound
CN109259297A (en) * 2018-09-25 2019-01-25 云南中烟工业有限责任公司 A kind of coffee toasts fragrant electronics tobacco tar and its preparation method and application
CN109259296A (en) * 2018-09-13 2019-01-25 云南中烟工业有限责任公司 A kind of electronics tobacco tar and preparation method and application that tealeaves baking is fragrant
CN109805440A (en) * 2019-02-21 2019-05-28 吉林烟草工业有限责任公司 A kind of tobacco fixation humectant and preparation method thereof
WO2024078373A1 (en) * 2022-10-10 2024-04-18 惠州市新泓威科技有限公司 Use of jojoba oil in preparation of e-liquid of electronic cigarette

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CN102613694A (en) * 2012-03-27 2012-08-01 广西中烟工业有限责任公司 Application of natural tobacco additive with effects of increasing aroma and preserving moisture
CN102742928A (en) * 2012-07-27 2012-10-24 红云红河烟草(集团)有限责任公司 Polydextrose cigarette humectant and using method thereof
CN102754915A (en) * 2012-07-27 2012-10-31 红云红河烟草(集团)有限责任公司 Isomalto-oligosaccharide cigarette humectant and application method thereof
CN102783708A (en) * 2012-08-16 2012-11-21 上海烟草集团有限责任公司 Vegetable oil type tobacco humectant and preparation method thereof

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CN102613694A (en) * 2012-03-27 2012-08-01 广西中烟工业有限责任公司 Application of natural tobacco additive with effects of increasing aroma and preserving moisture
CN102742928A (en) * 2012-07-27 2012-10-24 红云红河烟草(集团)有限责任公司 Polydextrose cigarette humectant and using method thereof
CN102754915A (en) * 2012-07-27 2012-10-31 红云红河烟草(集团)有限责任公司 Isomalto-oligosaccharide cigarette humectant and application method thereof
CN102783708A (en) * 2012-08-16 2012-11-21 上海烟草集团有限责任公司 Vegetable oil type tobacco humectant and preparation method thereof

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106490676A (en) * 2016-12-11 2017-03-15 钦州学院 A kind of starchiness humectant for smoke and preparation method thereof
CN108013498A (en) * 2017-11-23 2018-05-11 广西中烟工业有限责任公司 A kind of compound additive for improving reconstituted tobacco physics humid keeping performance
CN108056496A (en) * 2017-11-29 2018-05-22 广西中烟工业有限责任公司 A kind of tobacco humectant and preparation method thereof
CN108056496B (en) * 2017-11-29 2020-12-29 广西中烟工业有限责任公司 Tobacco humectant and preparation method thereof
CN109105945A (en) * 2018-09-13 2019-01-01 云南中烟工业有限责任公司 A method of tobacco roasting odor type electronics tobacco tar is prepared using organic acid-metal salt compound
CN109259296A (en) * 2018-09-13 2019-01-25 云南中烟工业有限责任公司 A kind of electronics tobacco tar and preparation method and application that tealeaves baking is fragrant
CN109105945B (en) * 2018-09-13 2021-09-14 云南中烟工业有限责任公司 Method for preparing tobacco baking fragrance type electronic cigarette oil by adopting organic acid-metal salt compound
CN109259296B (en) * 2018-09-13 2021-10-26 云南中烟工业有限责任公司 Electronic cigarette oil with tea baking fragrance and preparation method and application thereof
CN109259297A (en) * 2018-09-25 2019-01-25 云南中烟工业有限责任公司 A kind of coffee toasts fragrant electronics tobacco tar and its preparation method and application
CN109805440A (en) * 2019-02-21 2019-05-28 吉林烟草工业有限责任公司 A kind of tobacco fixation humectant and preparation method thereof
CN109805440B (en) * 2019-02-21 2022-03-08 吉林烟草工业有限责任公司 Tobacco fragrance-fixing humectant and preparation method thereof
WO2024078373A1 (en) * 2022-10-10 2024-04-18 惠州市新泓威科技有限公司 Use of jojoba oil in preparation of e-liquid of electronic cigarette

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