CN107744172A - A kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its application in cigarette - Google Patents
A kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its application in cigarette Download PDFInfo
- Publication number
- CN107744172A CN107744172A CN201710859929.3A CN201710859929A CN107744172A CN 107744172 A CN107744172 A CN 107744172A CN 201710859929 A CN201710859929 A CN 201710859929A CN 107744172 A CN107744172 A CN 107744172A
- Authority
- CN
- China
- Prior art keywords
- extract
- herba hedyotidis
- cigarette
- hedyotis herb
- hedyotidis chrysotrichae
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
Application the invention discloses a kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its in cigarette.After Goldhair Hedyotis Herb pulverizes and sieves, extract is obtained after diethyl ether solution refluxing extraction, distillation and concentration, is dissolved in after propylene glycol solution is added in cigarette, with cigarette perfume harmony, enhances the alcohol and property of flue gas, while reduces the excitant of flue gas, reduces miscellaneous gas.Present invention process is easy, and equipment is simple, and cost is cheap.
Description
Technical field
The invention belongs to cigarette additive technical field, and in particular to a kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its
Application in cigarette.
Background technology
Goldhair Hedyotis Herb also known as deposited ground Paspalum conjugatum, copper eye lion, mainly contain iridoids, triterpenes, flavonoids, alkaloid
A variety of chemical compositions such as class and sterols.Medically there is the effect of removing damp-heat, removing toxicity for detumescence, activate blood and relax tendons.Although yellow hair
Auricled Hedyotis Herb extract is more in the application of pharmaceutical industry, but Goldhair Hedyotis Herb is applied into cigarette to improve the side of smoking property of cigarette quality
There is not been reported for method.
The content of the invention
The purpose of the present invention is overcome the deficiencies in the prior art, there is provided a kind of preparation method of Herba Hedyotidis Chrysotrichae extract and
Application in cigarette.
The purpose of the present invention is achieved by following technical solution.
A kind of preparation method of Herba Hedyotidis Chrysotrichae extract, comprises the following steps：
(1) Goldhair Hedyotis Herb is crushed, crosses 80~120 mesh sieves and obtain Goldhair Hedyotis Herb powder；
(2) mixed according to the ratio that the mass ratio of Goldhair Hedyotis Herb powder and ether is 1: 5~1: 15, in 50 DEG C~70 DEG C temperature
Lower 60~the 180min of refluxing extraction of degree, is then concentrated, it is Huang to collect cut at a temperature of 30 DEG C~50 DEG C with Rotary Evaporators
Hair Auricled Hedyotis Herb extract.
Application of the described Herba Hedyotidis Chrysotrichae extract in cigarette：By after described Herba Hedyotidis Chrysotrichae extract dilution with
0.1%~0.2% dosage is added in pipe tobacco.
Diluent is propylene glycol solution, is added to after preferably diluting 10 times in pipe tobacco.
The beneficial effects of the invention are as follows：
The Herba Hedyotidis Chrysotrichae extract that the present invention is prepared is applied in cigarette, and cigarette perfume harmony, enhances the alcohol of flue gas
And property, while the excitant of flue gas is reduced, reduce miscellaneous gas.Present invention process is easy, and equipment is simple, and cost is cheap.
Embodiment
Percent concentration of the present invention is mass percent concentration.
By the following specific examples further illustrate the invention.
Embodiment 1
Goldhair Hedyotis Herb is put into pulverizer and crushed, 80 mesh sieves is crossed and obtains Goldhair Hedyotis Herb powder, according to Goldhair Hedyotis Herb powder and
The ratio that the mass ratio of ether is 1: 5 mixes, the refluxing extraction 180min at a temperature of 50 DEG C, then with rotation at a temperature of 30 DEG C
Evaporimeter concentrates, and collects cut, obtains Herba Hedyotidis Chrysotrichae extract.
Embodiment 2
Goldhair Hedyotis Herb is put into pulverizer and crushed, 100 mesh sieves is crossed and obtains Goldhair Hedyotis Herb powder, according to Goldhair Hedyotis Herb powder and
The ratio that the mass ratio of ether is 1: 10 mixes, the refluxing extraction 120min at a temperature of 60 DEG C, then with rotation at a temperature of 40 DEG C
Turn evaporimeter concentration, collect cut, obtain Herba Hedyotidis Chrysotrichae extract.
Embodiment 3
Goldhair Hedyotis Herb is put into pulverizer and crushed, 120 mesh sieves is crossed and obtains Goldhair Hedyotis Herb powder, according to Goldhair Hedyotis Herb powder and
The ratio that the mass ratio of ether is 1: 15 mixes, the refluxing extraction 60min at a temperature of 70 DEG C, then with rotation at a temperature of 50 DEG C
Evaporimeter concentrates, and collects cut, obtains Herba Hedyotidis Chrysotrichae extract.
Embodiment 4
The Herba Hedyotidis Chrysotrichae extract that the present invention is prepared is added to progress perfuming processing in pipe tobacco.The present embodiment is with reality
Exemplified by the Herba Hedyotidis Chrysotrichae extract for applying the preparation of example 2,10 times are diluted with propylene glycol solution, is added to pipe tobacco according to 0.1% dosage
In, while the pipe tobacco not add extract is prepared into cigarette as blank control sample.
Two groups of cigarette are subjected to sensory quality assessment, as a result finds to be compared to the cigarette of blank sample, with the addition of Hedyotis chrysotricha (Palib.) Merr.
The cigarette flavor amount of careless extract be increased, and flue gas becomes soft, fine and smooth, and excitant reduces, and wooden miscellaneous gas is reduced, and cigarette is whole
Body-sensing official's quality-improving is notable.
Above content is to combine the further description that specific preferred embodiment is made to the present invention.For this
For the those of ordinary skill of technical field that the present invention belongs to, the obvious modification made without departing from the inventive concept of the premise,
Performance or purposes are identical, are regarded as protection scope of the present invention.
Claims (6)
1. a kind of preparation method of Herba Hedyotidis Chrysotrichae extract, comprises the following steps：
(1) Goldhair Hedyotis Herb is crushed, crosses 80~120 mesh sieves and obtain Goldhair Hedyotis Herb powder；
(2) mixed according to the ratio that the mass ratio of Goldhair Hedyotis Herb powder and ether is 1: 5~1: 15, at a temperature of 50 DEG C~70 DEG C
60~180min of refluxing extraction, then concentrated at a temperature of 30 DEG C~50 DEG C with Rotary Evaporators, it is Hedyotis chrysotricha (Palib.) Merr. to collect cut
Careless extract.
2. preparation method according to claim 1, it is characterised in that comprise the following steps：
(1) Goldhair Hedyotis Herb is put into pulverizer and crushed, crossed 80 mesh sieves and obtain Goldhair Hedyotis Herb powder；
(2) mixed according to the ratio that the mass ratio of Goldhair Hedyotis Herb powder and ether is 1: 5, the refluxing extraction at a temperature of 50 DEG C
180min, then concentrated at a temperature of 30 DEG C with Rotary Evaporators, collect cut, obtain Herba Hedyotidis Chrysotrichae extract.
3. application of the Herba Hedyotidis Chrysotrichae extract that preparation method according to claim 1 or claim 2 is prepared in cigarette.
4. application according to claim 3, it is characterised in that：By described Herba Hedyotidis Chrysotrichae extract dilution dilution agent
Afterwards, it is added to 0.1%~0.2% dosage in pipe tobacco.
5. application according to claim 4, it is characterised in that：With 10 times of dilution agent of dilution, described diluent is the third two
Alcoholic solution.
6. application according to claim 3, it is characterised in that：Described Herba Hedyotidis Chrysotrichae extract is diluted 10 with propane diols
It is added to after times with 0.1% dosage in pipe tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710859929.3A CN107744172A (en) | 2017-09-21 | 2017-09-21 | A kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its application in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710859929.3A CN107744172A (en) | 2017-09-21 | 2017-09-21 | A kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its application in cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107744172A true CN107744172A (en) | 2018-03-02 |
Family
ID=61254604
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710859929.3A Pending CN107744172A (en) | 2017-09-21 | 2017-09-21 | A kind of preparation method of Herba Hedyotidis Chrysotrichae extract and its application in cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107744172A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109619661A (en) * | 2019-01-11 | 2019-04-16 | 广西中烟工业有限责任公司 | A kind of preparation method of serissa extract and its application in cigarette |
| CN109645550A (en) * | 2019-01-17 | 2019-04-19 | 广西中烟工业有限责任公司 | A kind of preparation method of Japanses beauty-berry grass extract and its application in cigarette |
| CN113789224A (en) * | 2021-09-30 | 2021-12-14 | 山东智汇达海洋生物科技有限公司 | Preparation and application of hypericum japonicum volatile oil |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107048471A (en) * | 2017-05-08 | 2017-08-18 | 广西中烟工业有限责任公司 | A kind of preparation method of mango leaf extract and its application in cigarette |
-
2017
- 2017-09-21 CN CN201710859929.3A patent/CN107744172A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107048471A (en) * | 2017-05-08 | 2017-08-18 | 广西中烟工业有限责任公司 | A kind of preparation method of mango leaf extract and its application in cigarette |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109619661A (en) * | 2019-01-11 | 2019-04-16 | 广西中烟工业有限责任公司 | A kind of preparation method of serissa extract and its application in cigarette |
| CN109645550A (en) * | 2019-01-17 | 2019-04-19 | 广西中烟工业有限责任公司 | A kind of preparation method of Japanses beauty-berry grass extract and its application in cigarette |
| CN113789224A (en) * | 2021-09-30 | 2021-12-14 | 山东智汇达海洋生物科技有限公司 | Preparation and application of hypericum japonicum volatile oil |
| CN113789224B (en) * | 2021-09-30 | 2024-03-01 | 山东智汇达海洋生物科技有限公司 | Preparation and application of Jin Maoer grass volatile oil |
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| Date | Code | Title | Description |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180302 |
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| RJ01 | Rejection of invention patent application after publication |