CN101878955B - Manufacturing method of rich-fragrance reduced-harmfulness cigarette - Google Patents
Manufacturing method of rich-fragrance reduced-harmfulness cigarette Download PDFInfo
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- CN101878955B CN101878955B CN 200910188722 CN200910188722A CN101878955B CN 101878955 B CN101878955 B CN 101878955B CN 200910188722 CN200910188722 CN 200910188722 CN 200910188722 A CN200910188722 A CN 200910188722A CN 101878955 B CN101878955 B CN 101878955B
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Abstract
The invention relates to a manufacturing method of a reduced-harmfulness cigarette, in particular to a reduced-harmfulness cigarette with products of hawthorn subjected to chemical treatment as main efficacy. The extract of hawthorn and a certain concentration of alcohol are prepared into an extraction liquid to be uniformly sprayed to common tobacco shreds during the material addition and flavoring procedures of tobacco, and then, the reduced-harmfulness cigarette is manufactured by using a common cigarette technology. The extraction method of the total extract of hawthorn comprises the following steps of: after pretreatment of the hawthorn, drying the hawthorn in the air or in the sun, and pulverizing into 10-100 meshes; extracting the powder with water three times for 1-8 h each time at 50-90 DEG C; and concentrating filtrate to a certain concentration so as to obtain the reduced-harmfulness cigarette. The rich-fragrance reduced-harmfulness cigarette is produced by utilizing chemical ingredients contained in the hawthorn and various pharmacological effects of the hawthorn.
Description
Technical field
The present invention relates to a kind of preparation method of low-harm type cigarette, particularly a kind of low-harm type cigarette take the product of hawthorn after chemical treatment as main effect.
Background technology
In cigarette, add the shown curative-effect health-care effect that goes out of natural plant extracts, confirmed by clinical testing and numerous consumers' suction for each medical department of participating in developing.Aspirate the cigarette of adding natural plant extracts as the consumer after, really some disease there are certain alleviation and therapeutic action, relatively be typically the caused cough of smoking, asthma Effects remarkable, this also is the reason place that numerous consumers select to aspirate this class cigarette, and the manufacturing enterprise that produces especially healthy cigarettes occupies the reason place of certain market share in fierce market competition.Add the healthy cigarettes of natural plant extracts, the impact of China's traditional Chinese medical theory and method grows up, and is that China is peculiar.Smoking and health problem more and more concerned today in the our times scope, add the healthy cigarettes of natural plant extracts and created a preferably way, in following cigarette development, present very important effect, have larger development potentiality and space.
Hawthorn is the dry mature fruit of rosaceous plant large-fruited Chinese hawthorn Crataegus pinnatifida Bge.Var.major N.E.Br. or hawthorn Crataegus pinnatifida Bge..Gather during fruit maturation autumn, section, drying.Slightly warm in nature, flavor acid, sweet.Return spleen, stomach, Liver Channel.Function with cure mainly: be used for carnivorous stagnantly, the gastral cavilty turgor rushes down dysentery stomachache, trusted subordinate's shouting pain, stasis of blood gas pain; Hyperlipemia.Pharmacological action: 1, to the effect of cardiovascular system; 2, to the effect of digestive system; 3, to immune effect; 4, antibacterial action; 5, diuresis; 6, antitumaous effect; 7, to the effect of central nervous system; 8, resisting oxygen lack; 9, spasmolysis, sedation.Main chemical compositions: 1, flavonoids: Hyperoside, Quercetin, Vitexin, rutin etc.; 2, organic acid: contain citric acid, chlorogenic acid, ursolic acid, oxalic acid, malic acid etc.; 3, liposoluble constituent: 3-methyl hexane, heptane, hexahydrotoluene etc.; 4, other composition: sugar part, tannin, protein and vitamin C, 17 seed amino acids.
Summary of the invention
The object of the invention is to utilize chemical composition contained in the hawthorn and have various pharmacological actions, produce a kind of high-scent low-harm cigarette.
The objective of the invention is to realize by the following technical solutions: the present invention is the extract that is added with hawthorn in the pipe tobacco of cigarette.
The extract of hawthorn of the present invention be total extract or process with chemical method again after refined products.
The production method of health cigarette of the present invention is as follows:
The extract that the extract of hawthorn and certain density ethanol are mixed with is sprayed on the common pipe tobacco uniformly in the link of tobacco charging, perfuming, then namely makes low-harm cigarette with conventional cigarette process.
The extract of hawthorn among the present invention adopts following extracting method to obtain:
The extracting method of hawthorn total extract:
1, hawthorn is after pre-treatment, dry or dry after be crushed to the 10--100 order;
2, under 50--90 ℃ of condition, water extracts powder, extracts 3 times, and extraction time is respectively 1--8h;
3, filtrate is concentrated into finite concentration and get final product.
The extracting method of hawthorn extract:
First method:
1, hawthorn is after pre-treatment, dry or dry after be crushed to the 10-100 order;
2, under 50--90 ℃ of condition, water extracts powder, extracts 3 times, and extraction time is respectively 1--8h;
3, merging filtrate and be concentrated into finite concentration;
4, with 95% ethanol alcohol precipitation twice, alcohol precipitation concentration is 70%～75% for the first time, filters after leaving standstill 8h, gets supernatant and carries out the alcohol precipitation second time;
5, for the second time alcohol precipitation concentration is 80%～85%, filters after leaving standstill 8h, gets supernatant concentration to finite concentration and gets final product.
Second method:
1, hawthorn is after pre-treatment, dry or dry after be crushed to the 10-100 order;
2, under 50--90 ℃ of condition, water extracts powder, extracts 3 times, and extraction time is respectively 1--8h;
3, merging filtrate and be concentrated into finite concentration;
4, cross macroporous resin column, use first the distilled water wash-out, discard eluent, then change 70%～80% ethanol elution, collect eluent, be concentrated into finite concentration and get final product.
In the present invention, described pre-treatment comprises rejecting impurity, airing.
The extract of hawthorn is brown solid, dissolve in low ethanol, during use extract being added 0.15%～0.25% amount in the link of tobacco charging, perfuming after the dissolving of low ethanol is sprayed on the common pipe tobacco uniformly, then namely make with conventional cigarette process, through the specialty test of smokeing panel test, the fine and smooth soften of flue gas obviously improves, and fragrance matter, perfume quantity, assorted gas, the property sent out, stimulation degree, degree of drying, Hui Tian, pleasant impression also all are improved thoroughly.Through harm reduction experiment, can effectively reduce some harmful components in the tobacco with blank cigarette comparison, and through weight-loss method humectation experiment, haw thorn extract has good humid keeping performance.
The specific embodiment
Embodiment 1:
Get Fructus Crataegi and reject impurity, after drying or drying, be crushed to 10 orders, under 60 ℃ of conditions, water extracts powder, extracts 3 times, and extraction time is respectively 3h, and get filtrate and be concentrated into finite concentration and get final product, and the normal temperature preservation.
Embodiment 2:
After getting Fructus Crataegi rejecting impurity, after drying or drying, be crushed to 50 orders, under 60 ℃ of conditions, water extracts powder, extract 3 times, extraction time is respectively 3h, and merging filtrate is concentrated into finite concentration, twice of ethanol alcohol precipitation with 95%, for the first time alcohol precipitation concentration is 70%, filters after leaving standstill 8h, gets supernatant and carries out the alcohol precipitation second time; For the second time alcohol precipitation concentration is 80%, filters after leaving standstill 8h, get supernatant concentration to finite concentration and get final product, and the normal temperature preservation.
Embodiment 3:
After getting Fructus Crataegi and rejecting impurity, after drying or drying, be crushed to 100 orders, under 60 ℃ of conditions, water extracts powder, extracts 3 times, extraction time is respectively 3h, merging filtrate also is concentrated into finite concentration, crosses macroporous resin column, uses first the distilled water wash-out, discard eluent, then change 70% ethanol elution, collect eluent, be concentrated into finite concentration and get final product.
The preparation method of extract is not limited to the method described in above-described embodiment, and can adopt published other extracting methods in this area.
Claims (8)
1. the preparation method of a rich-fragrance reduced-harmfulness cigarette, in the pipe tobacco of cigarette, be added with the extract of hawthorn, it is characterized in that the extract of described hawthorn and the extract that ethanol is mixed with are sprayed on the common pipe tobacco uniformly in the link of tobacco charging, perfuming, then make low-harm cigarette with conventional cigarette process; The extracting method of described haw thorn extract:
1), hawthorn after pre-treatment, dry or dry after be crushed to the 10--100 order;
2), under 50--90 ℃ of condition, water extracts powder, extracts 3 times, extraction time is respectively 1--8h;
3), the concentrated haw thorn extract of filtrate is with 95% ethanol alcohol precipitation twice, the first time, alcohol precipitation concentration was 70%～75%, filtered after leaving standstill 8h, got supernatant and carried out the alcohol precipitation second time; For the second time alcohol precipitation concentration is 80%～85%, filters after leaving standstill 8h, gets supernatant concentration.
2. the preparation method of rich-fragrance reduced-harmfulness cigarette according to claim 1 is characterized in that: the haw thorn extract that described filtrate is concentrated is crossed macroporous resin column, uses first the distilled water wash-out, discard eluent, then change 70%～80% ethanol elution, collect eluent, concentrate and get final product.
3. the preparation method of rich-fragrance reduced-harmfulness cigarette according to claim 1, it is characterized in that: the extract of described hawthorn is after the ethanol dissolving, add 0.15%～0.25% amount in the link of tobacco charging, perfuming and be sprayed at uniformly on the common pipe tobacco, then namely make with conventional cigarette process.
4. according to claim 1 and 2 or the preparation method of 3 described rich-fragrance reduced-harmfulness cigarettes, it is characterized in that: the extract of described hawthorn is got Fructus Crataegi and is rejected impurity, after drying or drying, be crushed to 10 orders, under 60 ℃ of conditions, water extracts powder, extracts 3 times, extraction time is respectively 3h, gets the concentrated also normal temperature of filtrate and preserves.
5. according to claim 1 and 2 or the preparation method of 3 described rich-fragrance reduced-harmfulness cigarettes, it is characterized in that: after the extract of described hawthorn is got Fructus Crataegi rejecting impurity, after drying or drying, be crushed to 50 orders, under 60 ℃ of conditions, water extracts powder, extracts 3 times, extraction time is respectively 3h, and merging filtrate concentrates.
6. the preparation method of rich-fragrance reduced-harmfulness cigarette according to claim 5 is characterized in that described merging filtrate with 95% ethanol alcohol precipitation twice, and alcohol precipitation concentration is 70% for the first time, filters after leaving standstill 8h, gets supernatant and carries out the alcohol precipitation second time; For the second time alcohol precipitation concentration is 80%, filters after leaving standstill 8h, gets supernatant concentration and normal temperature and preserves.
7. according to claim 1 and 2 or the preparation method of 3 described rich-fragrance reduced-harmfulness cigarettes, it is characterized in that: after the extract of described hawthorn is got Fructus Crataegi rejecting impurity, after drying or drying, be crushed to 100 orders, under 60 ℃ of conditions, water extracts powder, extracts 3 times, extraction time is respectively 3h, and merging filtrate concentrates.
8. the preparation method of rich-fragrance reduced-harmfulness cigarette according to claim 7, it is characterized in that: described merging filtrate is crossed macroporous resin column, uses first the distilled water wash-out, discards eluent, then changes 70% ethanol elution, collects eluent, concentrates and get final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200910188722 CN101878955B (en) | 2009-12-07 | 2009-12-07 | Manufacturing method of rich-fragrance reduced-harmfulness cigarette |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200910188722 CN101878955B (en) | 2009-12-07 | 2009-12-07 | Manufacturing method of rich-fragrance reduced-harmfulness cigarette |
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| CN101878955A CN101878955A (en) | 2010-11-10 |
| CN101878955B true CN101878955B (en) | 2013-01-16 |
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| CN 200910188722 Active CN101878955B (en) | 2009-12-07 | 2009-12-07 | Manufacturing method of rich-fragrance reduced-harmfulness cigarette |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423120A (en) * | 2011-10-11 | 2012-04-25 | 中国烟草总公司郑州烟草研究院 | Rolled haw type smokeless tobacco product |
| CN103351950A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same |
| CN103892454B (en) * | 2014-03-18 | 2017-01-04 | 黄金珍 | Hypertension and hyperlipemia electronic cigarette atomizing liquid and preparation method thereof |
| CN106491752A (en) * | 2016-12-20 | 2017-03-15 | 大连丹特生物技术有限公司 | A kind of Xylitol nicotinamide lozenge and preparation method thereof |
Citations (2)
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| CN85106586A (en) * | 1985-08-20 | 1987-05-13 | 辽宁省中药研究所 | A kind of method of preparation of drinks |
| CN1597678A (en) * | 2003-09-15 | 2005-03-23 | 辽宁鑫泰天然药物研究所 | Extraction method of hawthorn leaf total flarone |
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2009
- 2009-12-07 CN CN 200910188722 patent/CN101878955B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85106586A (en) * | 1985-08-20 | 1987-05-13 | 辽宁省中药研究所 | A kind of method of preparation of drinks |
| CN1597678A (en) * | 2003-09-15 | 2005-03-23 | 辽宁鑫泰天然药物研究所 | Extraction method of hawthorn leaf total flarone |
Non-Patent Citations (6)
| Title |
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| FL-2大孔吸附树脂对山楂总黄酮的分离纯化研究;张吉祥等;《北京中医药大学学报》;20090131;第32卷(第1期);62-64 * |
| 山楂多糖提取的研究;李艳红等;《农产品加工(学刊)》;20060528(第05期);43-46 * |
| 张吉祥等.FL-2大孔吸附树脂对山楂总黄酮的分离纯化研究.《北京中医药大学学报》.2009,第32卷(第1期), |
| 张峻松等.新型山楂香料的定量分析及在卷烟中的应用.《烟草科技》.2003,(第9期，总第194期), |
| 新型山楂香料的定量分析及在卷烟中的应用;张峻松等;《烟草科技》;20031231(第9期，总第194期);23-28 * |
| 李艳红等.山楂多糖提取的研究.《农产品加工(学刊)》.2006,(第05期), |
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