CN106539125B - A kind of sweetened humectant additive of cigarette shreds and preparation method thereof - Google Patents
A kind of sweetened humectant additive of cigarette shreds and preparation method thereof Download PDFInfo
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- CN106539125B CN106539125B CN201610915435.8A CN201610915435A CN106539125B CN 106539125 B CN106539125 B CN 106539125B CN 201610915435 A CN201610915435 A CN 201610915435A CN 106539125 B CN106539125 B CN 106539125B
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- sweetened
- cigarette
- humectant
- cigarette shreds
- white
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
- Confectionery (AREA)
- Seasonings (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses sweetened humectant additive of a kind of cigarette shreds and preparation method thereof, the composition of the cigarette shreds additive is in parts by weight white first 1~5 part of conopsea extraction, 1~5 part of wolfberry fruit extract, 10~50 parts of polyalcohol, 0.001~0.005 part of sweetener.The sweetened humectant additive of cigarette shreds prepared by the present invention can improve flue gas moistening degree, aesthetic quality and comfort level.The present invention is easy to operate, and equipment is easy to get, at low cost, is easy to be extended and applied.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of sweetened humectant additive of cigarette shreds and its preparation side
Method.
Background technology
There is some pumping problems for the most cigarette product in China：Moisture in cut tobacco scatter and disappear fast, gas drying sense is apparent,
Pungent thorn larynx, the low and oral cavity abundant expectoration of sweet sense etc..In face of these problems, current solution method is usually to add humectation to cigarette
Agent.Humectant can not only improve the physical property of pipe tobacco, increase cigarette toughness and water holding capacity, moreover it is possible to it is comfortable to improve smoking property of cigarette
Degree reduces irritation.In addition, humectant also has certain lasting effect, the fragrance of addition is made to reduce volatilization, and then makes cigarette
The quality of product keeps relative stability.Cigarette humid keeping performance is an important factor for influencing cigarette fragrance and suction comfort level.At present
The humectant that state's inner wrap strip uses is mainly the polyols such as glycerine, propylene glycol.However, it sees with practical conditions, such guarantor
It is unsatisfactory to the humectation effect of cigarette to moisten agent, there is main flume dry sensation is apparent, pipe tobacco water content declines fast, stimulates
The problems such as property is bigger than normal.This kind of humectant relies primarily on the moisture in these material absorbing environment pipe tobacco to be kept to moisten, therefore, by
The influence of environment is bigger, and has no sweetening function.The sweetened humectant of natural plants will extract separation and moisturizing humid keeping performance
It is combined, in terms of structure cigarette feature note, raising suction comfort level, shows unique advantage and application effect.
Bai Yuancan also known as false bark of ash, Bai Yun Shen, white American ginseng, native Radix Glycyrrhizae, white radix scrophulariae, pungent ginseng etc.；Lijing Nahsi language claims " thick
Bow "；For Labiatae (Lamiaceae) Paraphlomis herbaceous plant, rhizome is plump, knob-like series connection；The western regions of the Yunnan Province, Eastern Tibet are originated in,
The western Sichuan North Sea is pulled out on 2700~3000 meters of grass plot, hayashishita or careless slope, is the sweet-tasting plant of NW YUNNAN specialty.White clouds
Join as Yunnan Tibetan common traditional Tibetan medicine among the people, be used as medicine with root block, it is among the people to control abscess of throat, tripe swollen (food poisoning),
Collywobbles, diarrhea and anemofrigid cold etc.；Spleen and other effects is opened with pharynx-clearing throat-benefiting, kobadrin, stomach invigorating.In hundred radix scrophulariae containing high sweet taste into
Divide hundred radix scrophulariae glucosides, sweet taste is 500 times of sucrose, and sweet taste is lasting, can remain 1h or so in oral cavity；Its extract and sweet taste
Hundred radix scrophulariae glucoside of ingredient can substantially increase the sweet sense of cigarette smoking, have preferable effect of promoting the production of body fluid, but white radix scrophulariae gives birth to applied to cigarette
Production not yet has been reported that.It is an object of the invention to be directed to deficiency of the prior art, with hundred yuan of conopsea extractions and its main sweet taste
Hundred radix scrophulariae glucoside of ingredient is key component, provides a kind of sweetened humectation addition of cigarette shreds easy to operate, being suitble to large-scale production
Agent preparation method.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to improve a kind of sweetened humectant of cigarette shreds, form
Object and parts by weight are：White 1~5 part of conopsea extraction of member, 1~5 part of wolfberry fruit extract, 10~50 parts of polyalcohol, sweetener 0.001~
0.005 part.The present invention utilizes the polysaccharide in extract, and for humectant, the fragrance component in extract is sweetened, can play water suction
The effect of humectation, and the purpose of sense organ comfort level can be improved.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 2~5 parts of absolute ethyl alcohols is added in, using surname extraction, heats back
4~8h is flowed, extracting solution is concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 portion of matrimony vine is ground into powder with pulverizer, 2~5 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux 2
~5h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to wolfberry fruit extract.
The preparation method of the sweetened humectant additive of the cigarette shreds is as follows：
(1) 40~70 DEG C are warming up to after polyalcohol is mixed with sweetener, 5~10min is stirred under 600~1600rpm；
(2) after mixing polyalcohol, white first conopsea extraction, wolfberry fruit extract, ultrasound about 30min, filtering removes insoluble
Object；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 40~70 DEG C after mixing, 600~
5~10min is stirred under 1600rpm to get to the sweetened humectant additive of cigarette shreds.
The present invention and the prior art relatively have the following advantages：Sweetened humectant additive prepared by the present invention can not only be notable
Ground retains moisture in cut tobacco, moreover it is possible to play the role of abundant cigarette perfume, improve suction comfort level.The present invention is easy to operate, and equipment is easy to get,
It is at low cost, it is easy to be extended and applied.
Description of the drawings
Nothing.
Specific embodiment
The present invention is further described with reference to embodiment, but protection scope of the present invention is not limited to this.
Embodiment 1：
The composition of the sweetened humectant of this cigarette shreds is in parts by weight：White 1 part of conopsea extraction of member, wolfberry fruit extract 1
Part, 10 parts of polyalcohol, 0.001 part of sweetener.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 2 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
4h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 portion of matrimony vine is ground into powder with pulverizer, 2 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux 2h,
Extracting solution is concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to wolfberry fruit extract.
The preparation method of the sweetened humectant additive of the cigarette shreds is as follows：
(1) 40 DEG C are warming up to after polyalcohol is mixed with sweetener, stirs 5min at 600 rpm；
(2) after mixing polyalcohol, white first conopsea extraction, wolfberry fruit extract, ultrasound about 30min, filtering removes insoluble
Object；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 40 DEG C after mixing, at 600 rpm
5min is stirred to get to cigarette shreds additive.
The sweetened humectant of tobacco that the present embodiment is worth is mixed by the 0.4% of cigarette shreds weight with tobacco sauce,
It is even to spray on cigarette shreds, cigarette is made, carries out humid keeping performance test.
Embodiment 2：
The composition of the sweetened humectant of this cigarette shreds is in parts by weight：White 3 parts of conopsea extraction of member, wolfberry fruit extract 3
Part, 40 parts of polyalcohol, 0.003 part of sweetener.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 3 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
6h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 portion of matrimony vine is ground into powder with pulverizer, 3 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux 3h,
Extracting solution is concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to wolfberry fruit extract.
The preparation method of the sweetened humectant additive of the cigarette shreds is as follows：
(1) 55 DEG C are warming up to after polyalcohol is mixed with sweetener, 7min is stirred under 1000rpm；
(2) after mixing polyalcohol, white first conopsea extraction, wolfberry fruit extract, ultrasound about 30min, filtering removes insoluble
Object；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 55 DEG C after mixing, under 1000rpm
7min is stirred to get to cigarette shreds additive.
The sweetened humectant of tobacco that the present embodiment is worth is mixed by the 0.4% of cigarette shreds weight with tobacco sauce,
It is even to spray on cigarette shreds, cigarette is made, carries out humid keeping performance test.
Embodiment 3：
The composition of the sweetened humectant of this cigarette shreds is in parts by weight：White 5 parts of conopsea extraction of member, wolfberry fruit extract 5
Part, 50 parts of polyalcohol, 0.005 part of sweetener.The present invention is humectant using the polysaccharide in extract, the fragrance in extract into
Point sweetened, can play the role of absorbing water humectation and improves the purpose of sense organ comfort level.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 5 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
8h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 portion of matrimony vine is ground into powder with pulverizer, 5 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux 5h,
Extracting solution is concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to wolfberry fruit extract.
The preparation method of the sweetened humectant additive of the cigarette shreds is as follows：
(1) 70 DEG C are warming up to after polyalcohol is mixed with sweetener, stirs 10min at 1600 rpm；
(2) after mixing polyalcohol, white first conopsea extraction, wolfberry fruit extract, ultrasound about 30min, filtering removes insoluble
Object；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 70 DEG C after mixing, at 1600 rpm
10min is stirred to get to cigarette shreds additive.
The sweetened humectant of tobacco made from the present embodiment is mixed by the 0.4% of cigarette shreds weight with tobacco sauce,
It is even to spray on cigarette shreds, cigarette is made, carries out humid keeping performance test.
The sweetened humectant of cigarette shreds prepared by embodiment 1-3 is tested for the property, and the results are shown in Table 1；Sense organ is carried out to relax
Appropriateness evaluation, the results are shown in Table 2, which carries out according to national standard, and result is score value, and score value is higher to illustrate sense organ comfort level
Better.
Table 1：Cigarette shreds humectant moisture-retaining capacity is tested
Table 2：Cigarette shreds humectant sense organ Comfort Evaluation
As shown in Table 1, under humectant additive amount same case, the humectation effect of the sweetened humectant of cigarette shreds of the present invention
It is better than and is not added with humectant and the control pipe tobacco of common cigarette shreds humectant propylene glycol and glycerine, illustrates to use humectant
The water content of pipe tobacco can be increased, improve the equilibrium moisture content of pipe tobacco, there is preferable humid keeping performance；By to sense organ comfort level
Test, product of the present invention is overall suitable with reference substance propylene glycol, is partly better than propylene glycol in terms of dry sensation, residual, irritation.
Claims (5)
1. a kind of sweetened humectant additive of cigarette shreds, composition are in parts by weight：White 1~5 part of conopsea extraction of member, matrimony vine
1~5 part of extract, 10~50 parts of polyalcohol, 0.001~0.005 part of sweetener；The extracting method of white first conopsea extraction is
Gained is carried out according to the following steps：1 part of white radix scrophulariae is ground into powder with pulverizer, 2~5 parts of absolute ethyl alcohols are added in, using Soxhlet
Extraction, is heated to reflux 4~8h, and extracting solution is concentrated under the conditions of 25~85 DEG C of temperature, pressure is 0.02~0.04MPa up to white
First conopsea extraction；
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：1 portion of matrimony vine is ground into powder with pulverizer,
2~5 parts of absolute ethyl alcohols are added in, using surname extraction, are heated to reflux 2~5h, extracting solution is in 25~85 DEG C of temperature, pressure 0.02
Under the conditions of~0.04MPa, concentrate up to wolfberry fruit extract.
2. the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：Polyalcohol is glycerine, wood
One or more of sugar alcohol, sorbierite mixture.
3. the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：Sweetener for Sucralose,
One or more of neotame, Talin, steviol glycoside, baiyunoside mixture.
4. the preparation method of the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：
(1) 40~70 DEG C are warming up to after polyalcohol is mixed with sweetener, 5~10min is stirred under 600~1600rpm；
(2) after mixing polyalcohol, white first conopsea extraction, wolfberry fruit extract, ultrasonic 30min, filtering removes insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 40~70 DEG C after mixing, 600~
5~10min is stirred under 1600rpm to get to the sweetened humectant additive of the cigarette shreds.
5. the purposes of the sweetened humectant additive of cigarette shreds according to claim 1, which is characterized in that for improving to cigarette
The humectation effect of silk improves cigarette smoking sensory experience.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610915435.8A CN106539125B (en) | 2016-10-20 | 2016-10-20 | A kind of sweetened humectant additive of cigarette shreds and preparation method thereof |
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| CN201610915435.8A CN106539125B (en) | 2016-10-20 | 2016-10-20 | A kind of sweetened humectant additive of cigarette shreds and preparation method thereof |
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| CN106539125B true CN106539125B (en) | 2018-05-18 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107142153A (en) * | 2017-04-27 | 2017-09-08 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl matrimony vine essence and its application in cigarette |
| CN109805440B (en) * | 2019-02-21 | 2022-03-08 | 吉林烟草工业有限责任公司 | Tobacco fragrance-fixing humectant and preparation method thereof |
| CN109924531A (en) * | 2019-03-11 | 2019-06-25 | 四川中烟工业有限责任公司 | A kind of cigarette flavors composition, preparation method and application |
| CN110477445A (en) * | 2019-08-28 | 2019-11-22 | 广东香龙香料有限公司 | Flavouring essence for tobacco containing wolfberry fruit extract |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101692930A (en) * | 2009-09-01 | 2010-04-14 | 广东神农烟科技术有限公司 | Cigarette containing wolfberry polysaccharide and preparation method thereof |
| CN103859581A (en) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | Tobacco humectant achieving gradient distribution of molecular weights |
| CN104872812A (en) * | 2015-04-29 | 2015-09-02 | 昆明理工大学 | Tobacco aroma enhancement and moisture retention agent and application thereof |
| CN105029698A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Radix scrophulariae and glycerol triacetate extracts and application of radix scrophulariae and glycerol triacetate extracts on cigarettes |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2761737A1 (en) * | 2009-05-11 | 2010-11-18 | U.S. Smokeless Tobacco Company Llc | Method and device for flavoring smokeless tobacco |
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- 2016-10-20 CN CN201610915435.8A patent/CN106539125B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101692930A (en) * | 2009-09-01 | 2010-04-14 | 广东神农烟科技术有限公司 | Cigarette containing wolfberry polysaccharide and preparation method thereof |
| CN103859581A (en) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | Tobacco humectant achieving gradient distribution of molecular weights |
| CN104872812A (en) * | 2015-04-29 | 2015-09-02 | 昆明理工大学 | Tobacco aroma enhancement and moisture retention agent and application thereof |
| CN105029698A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Radix scrophulariae and glycerol triacetate extracts and application of radix scrophulariae and glycerol triacetate extracts on cigarettes |
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