CN106539125A - Sweetened humectant additive of a kind of cigarette shreds and preparation method thereof - Google Patents
Sweetened humectant additive of a kind of cigarette shreds and preparation method thereof Download PDFInfo
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- CN106539125A CN106539125A CN201610915435.8A CN201610915435A CN106539125A CN 106539125 A CN106539125 A CN 106539125A CN 201610915435 A CN201610915435 A CN 201610915435A CN 106539125 A CN106539125 A CN 106539125A
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- Prior art keywords
- sweetened
- cigarette shreds
- humectant
- cigarette
- extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
- Confectionery (AREA)
- Seasonings (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses sweetened humectant additive of a kind of cigarette shreds and preparation method thereof, the composition of the cigarette shreds additive is white 1～5 part of conopsea extraction of unit, 1～5 part of wolfberry fruit extract, 10～50 parts of polyhydric alcohol, 0.001～0.005 part of sweeting agent in parts by weight.The sweetened humectant additive of cigarette shreds prepared by the present invention can improve flue gas moistening degree, aesthetic quality and comfort level.The present invention is simple to operate, and equipment is easy to get, low cost, is easy to be extended and applied.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of sweetened humectant additive of cigarette shreds and its preparation side
Method.
Background technology
The most cigarette product of China has some pumping problems：Moisture in cut tobacco is lost soon, gas drying sense is obvious,
Pungent thorn larynx, sweet sense be low and oral cavity abundant expectoration etc..In the face of these problems, current solution is usually to add humectation to Medicated cigarette
Agent.Humectant can not only improve the physical property of tobacco shred, increase Medicated cigarette toughness and water holding capacity, moreover it is possible to improve smoking property of cigarette comfortable
Degree, reduces zest.Additionally, also there is humectant certain lasting to act on, make the spice of addition reduce volatilization, and then make Medicated cigarette
The quality of product keeps relative stability.Medicated cigarette humid keeping performance is the key factor for affecting Medicated cigarette fragrance and suction comfort level.At present
The humectant that state's inner wrap strip is used is mainly the polyols such as glycerol, Propylene Glycol.However, seeing with practical conditions, such guarantor
Profit agent is unsatisfactory to the humectation effect of Medicated cigarette, there is main flume dry sensation substantially, and it is fast that tobacco shred water content declines, and stimulates
The problems such as property is bigger than normal.This kind of humectant relies primarily on moisture in these material absorbing environment to keep tobacco shred to moisten, therefore, receive
The impact of environment is than larger, and has no sweetening function.The sweetened humectant of natural plants will be extracted and be separated and moisturizing humid keeping performance
Combine, in terms of building Medicated cigarette feature note, improving suction comfort level, show the advantage and application effect of uniqueness.
Bai Yuancan also known as false Radix Gentianae Macrophyllae, Radix Campanumoeae, white Radix Panacis Quinquefolii, native Radix Glycyrrhizae, white Radix Scrophulariae, Xin Can etc.；Lijing Nahsi language claims " thick
Bow "；For Labiatae (Lamiaceae) Paraphlomis herbaceous plant, rhizome plumpness, knob-like series connection；The western regions of the Yunnan Province, Eastern Tibet are originated in,
The western Sichuan North Sea is pulled out on 2700～3000 meters of grass plot, sylvan life or careless slope, is the sweet-tasting plant of NW YUNNAN special product.White clouds
Join as Yunnan Tibetan conventional traditional Tibetan medicine among the people, be used as medicine with root block, it is among the people to control laryngopharynx swelling and pain, tripe swollen (alimentary toxicosis),
Belly pain, diarrhoea and anemofrigid cold etc.；The effects such as spleen is opened with pharynx-clearing throat-benefiting, relieving cough and expelling phlegm, stomach invigorating.In hundred Radix Scrophulariae containing high sweet taste into
Divide hundred Radix Scrophulariae glycosides, its sweet taste is 500 times of sucrose, and sweet taste is persistently, can be in oral cavity residual 1h or so；Its extract and sweet taste
Hundred Radix Scrophulariae glycoside of composition can substantially increase the sweet sense of cigarette smoking, and having, but white Radix Scrophulariae is applied to Medicated cigarette life
Product not yet has been reported that.Present invention aims to deficiency of the prior art, with hundred yuan of conopsea extractions and its main sweet taste
Hundred Radix Scrophulariae glycoside of composition is key component, there is provided a kind of sweetened humectation of cigarette shreds of simple to operate, suitable large-scale production is added
Agent preparation method.
The content of the invention
Present invention aims to the deficiencies in the prior art, improve a kind of sweetened humectant of cigarette shreds, its composition
Thing and weight portion are：White 1～5 part of conopsea extraction of unit, 1～5 part of wolfberry fruit extract, 10～50 parts of polyhydric alcohol, sweeting agent 0.001～
0.005 part.The present invention is humectant using the polysaccharide in extract, and the fragrance component in extract is sweetened, can play water suction
The effect of humectation, can improve the purpose of sense organ comfort level again.
The polyhydric alcohol is Propylene Glycol, glycerol, xylitol, one or more mixture in Sorbitol.
The sweeting agent is sucralose, neotame, Talin, stevioside, one or more mixing in baiyunoside
Thing.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white Radix Scrophulariae pulverizer is ground into into powder, 2～5 parts of dehydrated alcohol is added, using surname extraction, is heated back
4～8h of stream, extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 part of Fructus Lycii pulverizer is ground into into powder, 2～5 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux 2
～5h, extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product wolfberry fruit extract.
The preparation method of the sweetened humectant additive of described cigarette shreds is as follows：
(1) 40～70 DEG C are warming up to after mixed polyhydric alcohol with sweeting agent, 5～10min is stirred under 600～1600rpm；
(2), after by polyhydric alcohol, white unit's conopsea extraction, wolfberry fruit extract mixing, ultrasound about 30min is filtered, and is removed insoluble
Thing；
(3) 40～70 DEG C are warming up to after liquid mixing prepared by the liquid and step (2) for preparing step (1), 600～
5～10min is stirred under 1600rpm, that is, obtains the sweetened humectant additive of cigarette shreds.
The present invention and prior art compare with advantages below：Sweetened humectant additive prepared by the present invention can not only be notable
Ground retains moisture in cut tobacco, moreover it is possible to play abundant cigarette perfume, improves the effect of suction comfort level.The present invention is simple to operate, and equipment is easy to get,
Low cost, is easy to be extended and applied.
Description of the drawings
Nothing.
Specific embodiment
The present invention is further described with reference to embodiment, but protection scope of the present invention is not limited to this.
Embodiment 1：
The composition of the sweetened humectant of this cigarette shreds is in parts by weight：White 1 part of conopsea extraction of unit, wolfberry fruit extract 1
Part, 10 parts of polyhydric alcohol, 0.001 part of sweeting agent.
The polyhydric alcohol is Propylene Glycol, glycerol, xylitol, one or more mixture in Sorbitol.
The sweeting agent is sucralose, neotame, Talin, stevioside, one or more mixing in baiyunoside
Thing.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white Radix Scrophulariae pulverizer is ground into into powder, 2 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux
4h, extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 part of Fructus Lycii pulverizer is ground into into powder, 2 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux 2h,
Extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product wolfberry fruit extract.
The preparation method of the sweetened humectant additive of described cigarette shreds is as follows：
(1) 40 DEG C are warming up to after mixed polyhydric alcohol with sweeting agent, 5min is stirred at 600 rpm；
(2), after by polyhydric alcohol, white unit's conopsea extraction, wolfberry fruit extract mixing, ultrasound about 30min is filtered, and is removed insoluble
Thing；
(3) 40 DEG C are warming up to after liquid mixing prepared by the liquid and step (2) for preparing step (1), at 600 rpm
Stirring 5min, that is, obtain cigarette shreds additive.
The sweetened humectant of Nicotiana tabacum L. that the present embodiment is worth is pressed the 0.4% of cigarette shreds weight to mix with tobacco sauce,
It is even to spray on cigarette shreds, Medicated cigarette is made, humid keeping performance test is carried out.
Embodiment 2：
The composition of the sweetened humectant of this cigarette shreds is in parts by weight：White 3 parts of conopsea extraction of unit, wolfberry fruit extract 3
Part, 40 parts of polyhydric alcohol, 0.003 part of sweeting agent.
The polyhydric alcohol is Propylene Glycol, glycerol, xylitol, one or more mixture in Sorbitol.
The sweeting agent is sucralose, neotame, Talin, stevioside, one or more mixing in baiyunoside
Thing.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white Radix Scrophulariae pulverizer is ground into into powder, 3 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux
6h, extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 part of Fructus Lycii pulverizer is ground into into powder, 3 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux 3h,
Extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product wolfberry fruit extract.
The preparation method of the sweetened humectant additive of described cigarette shreds is as follows：
(1) 55 DEG C are warming up to after mixed polyhydric alcohol with sweeting agent, 7min are stirred under 1000rpm；
(2), after by polyhydric alcohol, white unit's conopsea extraction, wolfberry fruit extract mixing, ultrasound about 30min is filtered, and is removed insoluble
Thing；
(3) 55 DEG C are warming up to after liquid mixing prepared by the liquid and step (2) for preparing step (1), under 1000rpm
Stirring 7min, that is, obtain cigarette shreds additive.
The sweetened humectant of Nicotiana tabacum L. that the present embodiment is worth is pressed the 0.4% of cigarette shreds weight to mix with tobacco sauce,
It is even to spray on cigarette shreds, Medicated cigarette is made, humid keeping performance test is carried out.
Embodiment 3：
The composition of the sweetened humectant of this cigarette shreds is in parts by weight：White 5 parts of conopsea extraction of unit, wolfberry fruit extract 5
Part, 50 parts of polyhydric alcohol, 0.005 part of sweeting agent.The present invention is humectant using the polysaccharide in extract, the fragrance in extract into
Divide sweetened, the humectation that absorbs water can be played a part of, the purpose of sense organ comfort level can be improved again.
The polyhydric alcohol is Propylene Glycol, glycerol, xylitol, one or more mixture in Sorbitol.
The sweeting agent is sucralose, neotame, Talin, stevioside, one or more mixing in baiyunoside
Thing.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white Radix Scrophulariae pulverizer is ground into into powder, 5 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux
8h, extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product white first conopsea extraction.
The extracting method of the wolfberry fruit extract is to carry out gained according to the following steps：
1 part of Fructus Lycii pulverizer is ground into into powder, 5 parts of dehydrated alcohol is added, using surname extraction, is heated to reflux 5h,
Extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product wolfberry fruit extract.
The preparation method of the sweetened humectant additive of described cigarette shreds is as follows：
(1) 70 DEG C are warming up to after mixed polyhydric alcohol with sweeting agent, 10min is stirred at 1600 rpm；
(2), after by polyhydric alcohol, white unit's conopsea extraction, wolfberry fruit extract mixing, ultrasound about 30min is filtered, and is removed insoluble
Thing；
(3) 70 DEG C are warming up to after liquid mixing prepared by the liquid and step (2) for preparing step (1), at 1600 rpm
Stirring 10min, that is, obtain cigarette shreds additive.
Nicotiana tabacum L. obtained in the present embodiment sweetened humectant is pressed the 0.4% of cigarette shreds weight to mix with tobacco sauce,
It is even to spray on cigarette shreds, Medicated cigarette is made, humid keeping performance test is carried out.
The sweetened humectant of cigarette shreds prepared by embodiment 1-3 is carried out into performance test, 1 is the results are shown in Table；Carry out sense organ to relax
Appropriateness is evaluated, and the results are shown in Table 2, and the test is carried out according to national standard, is as a result score value, the higher explanation sense organ comfort level of score value
Better.
Table 1：Cigarette shreds humectant moisture-retaining capacity is tested
Table 2：Cigarette shreds humectant sense organ Comfort Evaluation
As shown in Table 1, under humectant addition same case, the humectation effect of the sweetened humectant of cigarette shreds of the present invention
The control tobacco shred for being not added with humectant and conventional cigarette shreds humectant Propylene Glycol and glycerol is better than, illustrates to use humectant
The water content of tobacco shred can be increased, the equilibrium moisture content of tobacco shred is improved, with preferable humid keeping performance；By to sense organ comfort level
Test, overall product of the present invention are suitable with reference substance Propylene Glycol, partly in dry sensation, are better than Propylene Glycol in terms of residual, zest.
Claims (7)
1. the sweetened humectant additive of a kind of cigarette shreds, its composition is in parts by weight：White 1～5 part of conopsea extraction of unit, Fructus Lycii
1～5 part of extract, 10～50 parts of polyhydric alcohol, 0.001～0.005 part of sweeting agent.
2. the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：Polyhydric alcohol be Propylene Glycol, third
One or more mixture in triol, xylitol, Sorbitol.
3. the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：Sweeting agent be sucralose,
One or more mixture in neotame, Talin, stevioside, baiyunoside.
4. the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：The extraction of white unit's conopsea extraction
Method is to carry out gained according to the following steps：
1 part of white Radix Scrophulariae pulverizer is ground into into powder, 2～5 parts of dehydrated alcohol are added, using surname extraction, it is heated to reflux 4～
8h, extracting solution is in 25～85 DEG C of temperature. and under the conditions of pressure is 0.02～0.04MPa, concentration obtains final product white first conopsea extraction.
5. the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：The extraction side of wolfberry fruit extract
Method is to carry out gained according to the following steps：
1 part of Fructus Lycii pulverizer is ground into into powder, 2～5 parts of dehydrated alcohol are added, using surname extraction, it is heated to reflux 2～
5h, under the conditions of 25～85 DEG C of temperature, pressure are 0.02～0.04MPa, concentration obtains final product wolfberry fruit extract to extracting solution.
6. the preparation method of the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that：
(1) 40～70 DEG C are warming up to after mixed polyhydric alcohol with sweeting agent, 5～10min is stirred under 600～1600rpm；
(2), after by polyhydric alcohol, white unit's conopsea extraction, wolfberry fruit extract mixing, ultrasound about 30min is filtered, and removes insoluble matter；
(3) 40～70 DEG C are warming up to after liquid mixing prepared by the liquid and step (2) for preparing step (1), 600～
5～10min is stirred under 1600rpm, that is, obtains the sweetened humectant additive of the cigarette shreds.
7. the purposes of the sweetened humectant additive of cigarette shreds according to claim 1, it is characterised in that for improving to cigarette
The humectation effect of silk improves cigarette smoking sensory experience.
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| CN201610915435.8A CN106539125B (en) | 2016-10-20 | 2016-10-20 | A kind of sweetened humectant additive of cigarette shreds and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107142153A (en) * | 2017-04-27 | 2017-09-08 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl matrimony vine essence and its application in cigarette |
| CN109805440A (en) * | 2019-02-21 | 2019-05-28 | 吉林烟草工业有限责任公司 | A kind of tobacco fixation humectant and preparation method thereof |
| CN109924531A (en) * | 2019-03-11 | 2019-06-25 | 四川中烟工业有限责任公司 | A kind of cigarette flavors composition, preparation method and application |
| CN110477445A (en) * | 2019-08-28 | 2019-11-22 | 广东香龙香料有限公司 | Flavouring essence for tobacco containing wolfberry fruit extract |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107142153A (en) * | 2017-04-27 | 2017-09-08 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl matrimony vine essence and its application in cigarette |
| CN109805440A (en) * | 2019-02-21 | 2019-05-28 | 吉林烟草工业有限责任公司 | A kind of tobacco fixation humectant and preparation method thereof |
| CN109805440B (en) * | 2019-02-21 | 2022-03-08 | 吉林烟草工业有限责任公司 | Tobacco fragrance-fixing humectant and preparation method thereof |
| CN109924531A (en) * | 2019-03-11 | 2019-06-25 | 四川中烟工业有限责任公司 | A kind of cigarette flavors composition, preparation method and application |
| CN110477445A (en) * | 2019-08-28 | 2019-11-22 | 广东香龙香料有限公司 | Flavouring essence for tobacco containing wolfberry fruit extract |
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| Publication number | Publication date |
|---|---|
| CN106539125B (en) | 2018-05-18 |
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