CN105996115A - Electronic cigarette juice prepared from primary preparation extract of extra-strong tea - Google Patents
Electronic cigarette juice prepared from primary preparation extract of extra-strong tea Download PDFInfo
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- CN105996115A CN105996115A CN201610564484.1A CN201610564484A CN105996115A CN 105996115 A CN105996115 A CN 105996115A CN 201610564484 A CN201610564484 A CN 201610564484A CN 105996115 A CN105996115 A CN 105996115A
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- China
- Prior art keywords
- tea
- extract
- tieguanyin
- folium camelliae
- camelliae sinensis
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A24F47/008—
Abstract
The invention relates to an electronic cigarette juice prepared from primary preparation extract of extra-strong tea and specifically relates to a compound. The compound comprises the following components in percent by weight: 10-15% of primary preparation extract of extra-strong tea, 6-8% of tobacco flavor and 70-84% of atomizing agents. The compound provided by the invention not only can endow the electronic cigarette with elegant extra-strong tea fragrance but also can effectively improve the suction quality and sensory comfortable degree of the electronic cigarette.
Description
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of electricity prepared with thing extract processed at the beginning of TIEGUANYIN tea
Sub-cigarette tobacco juice.
Background technology
The living environment of traditional cigarette is increasingly serious, and whole world tobacco company, in order to seek new outlet, considers full simultaneously
The different consumer demand of foot, the product of various simulation Medicated cigarette continues to bring out, wherein with smokeless tobacco with without burning Medicated cigarette the most
Extensively.Electronic cigarette is exactly one of representative without burning tobacco, and electronic cigarette is to transmit perfume by electronics heater means to respiratory system
The electronics transporter of gas, nicotine etc..As the succedaneum of traditional cigarette, electronic cigarette in external form with traditional cigarette extremely phase
Seemingly.Its simulated cigarette taste, does not but have flue dust, does not falls cigarette end, do not burn, do not have naked light, and harmful substance contents is the lowest.This
Integrate modern microelectronic technology, biotechnology, the electronic cigarette of healthy living theory, firmly hold the psychology of consumer
Feature, meets the consumer psychology demand wanting smoking cessation simultaneously.
Electronic cigarette mainly includes smoking set and cigarette bullet, is mounted with tobacco juice in cigarette bullet, smoking set make tobacco juice atomization produce smoking
Effect.Tobacco juice for electronic smoke is mainly with the product of various essence and flavoring agents allotment, although the smog that tobacco juice for electronic smoke produces exists
The aspect such as fragrance, taste, feels still to have gap with the suction of real Medicated cigarette, but due to the numerous advantage of electronic cigarette, increasingly
Many consumers start accept and use electronic cigarette.
Essence and flavoring agent is widely used in the fields such as Nicotiana tabacum L., food, daily use chemicals, and natural perfume material is due to its composition complexity, fragrance
Abundant, fragrance remaining time is persistently the raw material that preparing essence is indispensable.
China is Folium Camelliae sinensis original producton location, and tea district is vast in territory, a multitude of names, and Tea Processing is divided into just system, refined two stages,
Folium Camelliae sinensis is divided into six big classes according to the difference of Tea Processing technique by Agricultural University Of Anhui famous Folium Camelliae sinensis expert's old rafter professor: green tea,
Yellow tea, Ramulus et Folium Mussaendae Pubescentis, Folium Camelliae sinensis (oolong tea), postfermented tea and black tea.
Fujian is famous Folium Camelliae sinensis high-quality producing region, the whole nation, wherein with TIEGUANYIN and Radix Campylotropis Hirtella (Herba Myrsines Africanae) as Typical Representative.TIEGUANYIN and
Radix Campylotropis Hirtella (Herba Myrsines Africanae) belongs to oolong tea system, and oolong tea belongs to half-fermented teas, its just process processed by dry in sun (withering), do green grass or young crops, complete,
Baking operation forms, different types of Folium Camelliae sinensis through just system, in it chemical composition and physical behavior there are a series of changes,
Thus form the unique color of Folium Camelliae sinensis, shape.
Its material of the different phase of primary processing of tea and fragrance composition are the most different.Wang Wei etc. are to Oolong Tea and solarization
The result of study of the aroma change in young worker's sequence shows, dry in sun can increase aroma component number and essential oil total amount, does green grass or young crops and then can change
Step-down boiling point and the ratio of high boiling point aroma component content；The floral character compound produced in oolong tea rocking of green leaf operation is benzene first
Alcohol, nerolidol, salicylic acid, cis-3-hexene ester, dibutyl phthalate and two kinds of unidentified components.When the gentliest doing green grass or young crops,
Linalool and oxide content thereof are higher；At identical temperature, the green-making enviroment that humidity is 75 DEG C is fragrant high and lasting；Machinery withers journey
Spending with the 7%～10% of fresh leaf dehydration, the fragrance preparing oolong tea is optimal.
Have no the report of the tobacco juice for electronic smoke prepared with thing extract processed at the beginning of TIEGUANYIN tea at present.
Summary of the invention
The present inventor is through substantial amounts of experiment and creative work, with Tie Guanyin tea in just different phase processed
Product is raw material, extracted tea essential oil, tea ethanol extract and the tea extract of obtaining, and using above-mentioned extract prepare can be as electronic cigarette
The compositions of tobacco juice, it can not only give the TIEGUANYIN tea perfume (or spice) note that electronic cigarette is elegant, can be effectively improved taking out of electronic cigarette simultaneously
Inhaling quality and sense organ comfort level, the present invention is i.e. to complete based on above discovery.
The invention mainly relates to the following aspects:
1. a compositions, it comprises by percentage to the quality:
Thing extract 10-15% processed at the beginning of TIEGUANYIN tea；
Flavouring essence for tobacco 6-8%；And
Propellant 70-84%.
In a preferred embodiment of the invention, in described compositions, at the beginning of TIEGUANYIN tea, the content of thing extract processed is
10%, 11%, 12%, 13%, 14% or 15%.
In a preferred embodiment of the invention, in described compositions, the content of flavouring essence for tobacco is 6%, 7% or 8%.
In a preferred embodiment of the invention, in described compositions the content of propellant be 70%, 71%, 72%,
73%, 74%, 75%, 76%, 77%, 78%, 79%, 80%, 81%, 82%, 83% or 84%.
TIEGUANYIN tea belongs to Folium Camelliae sinensis (oolong tea), for half-fermented teas, its just system by dry in sun (withering), do green grass or young crops, complete, dry
Roasting operation composition；The product that TIEGUANYIN tea obtains through each operation of first system is " thing processed at the beginning of TIEGUANYIN tea " of the present invention；Phase
Ying Di, the product " TIEGUANYIN solarization Folium Camelliae sinensis " the most described herein of above-mentioned each operation, " TIEGUANYIN does Folium Camelliae sinensis ", " TIEGUANYIN
Complete tea " and " TIEGUANYIN baking tea "；For simplicity, " solarization Folium Camelliae sinensis ", " doing Folium Camelliae sinensis ", " complete tea " it are referred to as individually below
" baking tea ".
In the preferred embodiment of the application, thing processed at the beginning of described TIEGUANYIN tea selected from shine Folium Camelliae sinensis, do Folium Camelliae sinensis, complete tea and
Bakee tea.
Process of withering refers to be placed in dark brownish green under illumination, ventilation and/or heating condition, makes dark brownish green dehydration wilt.
Doing blue or green process is under the effect of mechanical force, makes dark brownish green or withered tea leaves edge portion damaged, promotes its intension
Polyphenols partial oxidation, polymerization, produce the process on " the red limit of greenery ".Do blue or green process and preferably can include that one or many shakes
Blue or green and stand green grass or young crops processes.Rocking of green leaf refers to put in big bamboo plaque or vibration machine dark brownish green or withered tea leaves, carry out the most hand or
Person's machinery drives rocking of green leaf cage to rotate, and makes the Folium Camelliae sinensis blade after withering constantly circle round, stirs up and down, allow leaf margin and leaf margin, leaf margin with
Compass screen surface mutually rubs, leaf margin cell breakage.Rocking of green leaf can promote that polyphenol compound aoxidizes, and makes tea generation series of physical chemistry
Change.
After doing blue or green process, the stalk base of a fruit of tea water of satisfying is dark green, and vein becomes clear, and mesophyll is yellowish green, and leaf margin becomes vermilion, and the food value of leaf is soft,
Blue or green gas disappears, and fragrance is pure, micro-strip flowers and fruits fragrant.
The process that completes is to use uniform temperature, makes the enzyme in fresh leaf lose activity, or by the process of enzymatic inactivation.Complete place
The method of reason mainly have pot fry complete, roller fixation and steam beating etc..
When being completed by pot stir-fry, on the basis of being fried by tea, killing, frying the most stiff to limb edge by tea, leaf color transfers to
Darker yellow green, tarnishes, blade face slightly wrinkle, leaf stalk softness, and holding leaf has strong feel, and slightly elastic, clearing heat in QI system disappears, and dissipates
Send out delicate fragrance.
Bakee operation and i.e. refer to dehydration further to Folium Camelliae sinensis, eliminate the puckery bitter taste of Folium Camelliae sinensis self, it is simple to the technique of storage.Logical
Often, the mode bakeing general employing baking oven for heating of Tie Guanyin tea, after baked process, substantial amounts of Pyrazine, pyrrole can be formed
Cough up class, pyridines, pyran compounds, make Folium Camelliae sinensis have and roast fragrance.Heating can cause the degraded of Ester, produces multiple
Have high-quality slender joss stick terpenoid, constitute the quiet and tastefully laid out fragrance of oolong tea.
In certain embodiments of the invention, thing extract processed at the beginning of described TIEGUANYIN tea refers to thing warp processed at the beginning of TIEGUANYIN tea
The combination in any more than tea essential oil of thing processed, tea ethanol extract, tea extract at the beginning of the TIEGUANYIN tea that different extraction processes prepare；In order to
For purpose of brevity, being referred to as individually below " tea essential oil ", " tea ethanol extract " and " tea extract ", the most described " tea essential oil " includes
Dry in sun tea essential oil, do Folium Camelliae sinensis quintessence oil, complete tea essential oil and bakee tea essential oil；Described " tea ethanol extract " include shine Folium Camelliae sinensis ethanol extract,
Do Folium Camelliae sinensis ethanol extract, complete tea ethanol extract and baking tea ethanol extract；Described " tea extract " includes dry in sun tea extract, does Folium Camelliae sinensis
Water extract, the tea extract that completes and baking tea extract.
In a preferred embodiment of the invention, thing extract processed at the beginning of described TIEGUANYIN tea selected from tea essential oil, tea ethanol extract,
Tea extract or above combination in any (such as tea essential oil, tea ethanol extract and the combination of tea extract).
In a preferred embodiment of the invention, the extract of thing processed at the beginning of described TIEGUANYIN tea is selected from dry in sun tea essential oil, solarization
Folium Camelliae sinensis ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis quintessence oil, do Folium Camelliae sinensis ethanol extract, do Folium Camelliae sinensis water extract, the tea essential oil that completes, complete
Tea ethanol extract, the tea extract that completes, baking tea essential oil, baking tea ethanol extract, baking tea extract or above combination in any (example
Such as dry in sun tea essential oil, solarization Folium Camelliae sinensis ethanol extract, the tea ethanol extract that completes, baking tea ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis water extract
Combination；Do Folium Camelliae sinensis quintessence oil, do Folium Camelliae sinensis ethanol extract, the tea ethanol extract that completes, bakee tea ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis
The combination of water extract；Complete tea essential oil, the tea ethanol extract that completes, bakee tea ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis water extract,
The compositions of the tea extract that completes；Bakee tea essential oil, the tea ethanol extract that completes, baking tea ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis
Water extract, the combination of baking tea extract；Do Folium Camelliae sinensis quintessence oil, the tea essential oil that completes, shine Folium Camelliae sinensis ethanol extract, baking tea ethanol extract, solarization
Folium Camelliae sinensis water extract, do Folium Camelliae sinensis water extract, the combination of the tea extract that completes).
In a preferred embodiment of the invention, described flavouring essence for tobacco comprises following components by weight percentage:
Ethyl acetate 1.00%；
Ethyl n-butyrate. 0.50%；
Ethyl valerate 0.30%；
Iso-amyl iso-valeriate 0.50%；
Leaf Acetate 0.02%；
Menthyl acetate 0.50%；
Geraniol 0.05%；
Nerolidol 0.20%；
Caryophyllenol 0.10%；
Flos Caryophylli oil 0.05%；
Fennel oil 0.02%；
Acetic acid 0.01%；
Alpha, beta-lonone 0.02%；
β-Damascenone 0.05%；
Megastigmatrienone 0.01%；
Vanillin 0.10%；
Ethylmaltol 0.20%；
Fructus Armeniacae Mume extract 1.00%；
Red date tincture 2.00%；
Herba Cichorii extract 0.50%；
Cloud and mist absolute oil 0.50%；
Zimbabwe's extract 3.00%；
Storesin 0.01%；
Peru's extractum 0.20%；
Tolu concrete 0.10%；
Propylene glycol 30.00%；
Ethanol 59.06%.
In a preferred embodiment of the invention, the propellant during described propellant refers to described compositions is selected from the third two
Alcohol, glycerol or combination.
In a preferred embodiment of the invention, the propellant in described compositions is propylene glycol and glycerol；Further
Preferably, in described compositions, the content of glycerol is 8.0%.
In a preferred embodiment of the invention, described compositions comprises following components by percentage to the quality:
Dry in sun tea essential oil 0.1%-0.5% (such as 0.1%, 0.2%, 0.3%, 0.4%, 0.5%)；
Shine Folium Camelliae sinensis ethanol extract 1.0%-2.0% (such as 1.0%, 2.0%)；
Dry in sun tea extract 2.0%-3.0% (such as 2.0%, 3.0%)；
It is Folium Camelliae sinensis water extract 1.0-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Complete tea ethanol extract 2.0%-5.0% (such as 2.0%, 3.0%, 4.0%, 5.0%)；
Bakee tea ethanol extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Flavouring essence for tobacco 6.0%-8.0% (such as 6.0%, 7.0%, 8.0%)；
Glycerol 8.0%；And,
The propylene glycol of surplus.
In a preferred embodiment of the invention, described compositions comprises following components by percentage to the quality:
Dry in sun tea extract 2.0%-3.0% (such as 2.0%, 3.0%)；
It is Folium Camelliae sinensis quintessence oil 0.1%-0.2% (such as 0.1%, 0.2%)；
It is Folium Camelliae sinensis ethanol extract 2.0%-5.0% (such as 2.0%, 3.0%, 4.0%, 5.0%)；
It is Folium Camelliae sinensis water extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Complete tea ethanol extract 2.0%-5.0% (such as 2.0%, 3.0%, 4.0%, 5.0%)；
Bakee tea ethanol extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Flavouring essence for tobacco 6.0%-8.0% (such as 6.0%, 7.0%, 8.0%)；
Glycerol 8.0%；And
The propylene glycol of surplus.
In a preferred embodiment of the invention, described compositions comprises following components by percentage to the quality:
Dry in sun tea extract 2.0%-3.0% (such as 2.0%, 3.0%)；
It is Folium Camelliae sinensis water extract 1.0-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Complete tea ethanol extract 2.0%-5.0% (such as 2.0%, 3.0%, 4.0%, 5.0%)；
Complete tea essential oil 0.1%-0.2% (such as 0.1%, 0.2%)；
Tea extract 2.0%-3.0% that completes (such as 2.0%, 3.0%)；
Bakee tea ethanol extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Flavouring essence for tobacco 6.0%-8.0% (such as 6.0%, 8.0%)；
Glycerol 8.0%；And
The propylene glycol of surplus.
In a preferred embodiment of the invention, described compositions comprises following components by percentage to the quality:
Dry in sun tea extract 2.0%-3.0% (such as 2.0%, 3.0%)；
It is Folium Camelliae sinensis water extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Complete tea ethanol extract 2.0%-5.0% (such as 2.0%, 3.0%, 4.0%, 5.0%)；
Bakee tea essential oil 0.1%-0.2% (such as 0.1%, 0.2%)；
Bakee tea ethanol extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Bakee tea extract 2.0%-5.0% (such as 2.0%, 3.0%, 4.0%, 5.0%)；
Flavouring essence for tobacco 6.0%-8.0% (such as 6.0%, 7.0%, 8.0%)；
Glycerol 8.0%；And
The propylene glycol of surplus.
In a preferred embodiment of the invention, described compositions comprises following components by percentage to the quality:
Shine Folium Camelliae sinensis ethanol extract 1.0%-2.0% (such as 1.0%, 2.0%)；
Dry in sun tea extract 2.0%-3.0% (such as 2.0%, 3.0%)；
It is Folium Camelliae sinensis quintessence oil 0.1%-0.2% (such as 0.1%, 0.2%)；
It is Folium Camelliae sinensis water extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Complete tea essential oil 0.1%-0.2% (such as 0.1%, 0.2%)；
Tea extract 2.0%-3.0% that completes (such as 2.0%, 3.0%)；
Bakee tea ethanol extract 1.0%-5.0% (such as 1.0%, 2.0%, 3.0%, 4.0%, 5.0%)；
Flavouring essence for tobacco 6.0%-8.0% (such as 6.0%, 8.0%)；
Glycerol 8.0%；And
The propylene glycol of surplus.
The compositions the most of the present invention purposes in preparing tobacco juice for electronic smoke.
3. tobacco juice for electronic smoke, electronic cigarette or a cigarette bullet, it contains compositions of the present invention.
The preparation method of tea essential oil the most of the present invention, it comprises the following steps:
(1) obtain thing processed at the beginning of thing processed at the beginning of TIEGUANYIN tea, described TIEGUANYIN tea include solarization Folium Camelliae sinensis, do Folium Camelliae sinensis, complete tea and baking
Roasting tea；
(2) thing processed at the beginning of steam distillation TIEGUANYIN tea, collects distillate, obtains tea hydrosol；
Preferably, the step that distillate is carried out concentration is also included；
(3) from the tea hydrosol that step (2) obtains, separate (such as extract and separate) and obtain described tea essential oil.
In certain embodiments of the invention, step (3) includes following 3a)～3c) in one or multi-step:
3a) in described tea hydrosol, add saturated NaCl solution, be extracted with ethyl acetate, be then peeled off ethyl acetate extraction
Liquid；
Preferably, step 3a) may be repeated one or many, such as 3-6 time；Preferably, extract acetic acid used every time
The amount of ethyl ester is the 30～50% of solution weight to be extracted；
3b) acetic acid ethyl acetate extract is carried out the first concentrating under reduced pressure, remove ethyl acetate, obtain described tea essential oil；
3c) preferably, also include 3b) step that purifies further of described tea essential oil: described tea essential oil will add second
Alcohol (preferably, the amount of dehydrated alcohol is 4～10 times of tea essential oil weight), then carries out the second concentrating under reduced pressure, removes ethanol,
To described tea essential oil.
In a preferred embodiment of the invention, the preparation method of tea essential oil of the present invention, its have with the next item down or
Multinomial feature:
A) step 3b) in, the vacuum of the first concentrating under reduced pressure is 200-230mbar, such as 200-220mbar；
B) step 3b) in, the temperature of the first concentrating under reduced pressure is preferably 30-40 DEG C, such as 35-40 DEG C；
C) step 3c) in, the vacuum of the second concentrating under reduced pressure is 110-130mbar；
D) step 3c) in, the temperature of the second concentrating under reduced pressure is 35-45 DEG C, such as 40-45 DEG C.
In embodiments of the invention, described tea hydrosol can be prepared by steam distillation, thing processed at the beginning of TIEGUANYIN tea
The volume that feeds intake account for distillation vessel volume 70-80%；In distillation container, gas (includes in thing processed at the beginning of water vapour and TIEGUANYIN tea
The escaping gas contained) steam per hour volume account for distillation vessel volume 5-10%；The distillation time mistake of steam distillation
Short, can cause extraction not exclusively, long then energy consumption is bigger, it is however generally that, the process time of thing processed at the beginning of TIEGUANYIN tea should make to wave
The 90-95% that the amount of steaming is theoretical amount of the property sent out quintessence oil；In a preferred embodiment of the invention, such as, when at the beginning of TIEGUANYIN tea
When thing inventory processed is 15Kg, the speed of response of distillate controls 20～40Kg/h, such as 25-35Kg/h, at the beginning of TIEGUANYIN tea
The process time of thing processed controls at 1-3h, such as 2.5-3h.
The preparation method of tea ethanol extract the most of the present invention, it comprises the following steps:
Thing processed at the beginning of TIEGUANYIN tea or the present invention the 4th aspect are obtained thing processed at the beginning of the TIEGUANYIN tea after tea essential oil the hottest
Extract, obtain ethanol extract, concentrating under reduced pressure, obtain described tea ethanol extract.
Preferably, described ethanol is 95% ethanol；
Preferably, thing processed at the beginning of TIEGUANYIN tea and weight ratio 1:10 of ethanol；
Preferably, described heat is extracted as circumfluence distillation, it is preferable that the heating-up temperature that described heat is extracted is 60-70 DEG C；
Preferably, the time that described heat is extracted is 1-2h；
Preferably, described heat is extracted and is carried out 2 times；
Preferably, described concentrating under reduced pressure temperature is 45～55 DEG C, and vacuum is 40～60mbar；
Preferably, the density controlling concentrating under reduced pressure product is 1.05-1.10g/cm3。
The preparation method of tea extract the most of the present invention, it comprises the following steps:
Thing processed at the beginning of TIEGUANYIN tea or the present invention the 5th aspect are obtained thing processed heat in water at the beginning of the TIEGUANYIN tea after tea ethanol extract
Extract, obtain aqueous extract, concentrating under reduced pressure, obtain described tea extract.
Preferably, thing processed at the beginning of TIEGUANYIN tea is 1:10 with the weight ratio of water；
Preferably, described heat is extracted as circumfluence distillation, it is preferable that the heating-up temperature that described heat is extracted is 80-90 DEG C；
Preferably, the time that described heat is extracted is 1-2h；
Preferably, described heat is extracted and is carried out 2 times；
Preferably, described pressurization thickening temperature is 50～60 DEG C, and vacuum is 40～60mbar；
Preferably, the density controlling concentrating under reduced pressure product is 1.00-1.10g/cm3。
7. tea essential oil, it is prepared by the method described in the present invention the 4th aspect.
8. tea ethanol extract, it is prepared by the method described in the present invention the 5th aspect.
9. tea extract, it is prepared by the method described in the present invention the 6th aspect.
The tea essential oil the most of the present invention purposes in preparing tobacco juice for electronic smoke.
The 11. tea ethanol extract of the present invention purposes in preparing tobacco juice for electronic smoke.
The 12. tea extracts of the present invention purposes in preparing tobacco juice for electronic smoke.
The present invention has quoted in full following document:
GBT 30766-2014 Classification of Tea；
GBT 30357.2-2013 oolong tea part 2: TIEGUANYIN；
Chen Rongbing, Yao Xinen, Huang Fuping. fujian oolong tea kind [J]. Chinese tea, 2002,24 (2): 6-9.
The beneficial effect of the invention
The present invention prepares using thing extract processed at the beginning of TIEGUANYIN tea can be as the compositions of tobacco juice for electronic smoke, and it can not only give
The TIEGUANYIN tea perfume (or spice) note that electronic cigarette is elegant, can be effectively improved suction quality and the sense organ comfort level of electronic cigarette simultaneously.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but those skilled in the art will
Understanding, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.In embodiment unreceipted specifically
Condition person, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or instrument unreceipted production firm person, be
Can by city available from conventional products.
Solarization Folium Camelliae sinensis of the present invention, do Folium Camelliae sinensis, complete tea and bakee tea be commercially, be such as purchased from Xiamen tea ceremony
Younger sister trade Co., Ltd.
At the beginning of TIEGUANYIN tea of the present invention, thing extract processed is independently extracted by Fujian China Tobacco Industrial Co., Ltd..
The preparation of embodiment 1 dry in sun tea essential oil
Weigh 20Kg TIEGUANYIN shine Folium Camelliae sinensis on the dividing plate of extraction system, control bottom lead directly to steam aperture, to be extracted
Material bed be fully contacted, disperse and gasify, the water of formation and the mixed vapour of the volatile essential oil steam from alembic top
Outlet is derived, and condenser temperature controls, at 4 DEG C, to obtain the condensed fluid of primary processing of tea thing, steams flow-control in 30Kg/h, distillation
Time controls at 2h.Primary processing of tea thing condensed fluid is after micro-filtrate membrane filtration removes float, antibacterial, and microfiltration permeate is through reverse osmosis
Membrance concentration obtains concentrated solution.Gained concentrated solution will add a certain amount of saturated aqueous common salt, the 40% of addition concentrated solution weight
Ethyl acetate extracts 5 times, combined ethyl acetate extract, adds anhydrous Na2SO4Dried 35 DEG C, vacuum is 220mbar's
Under the conditions of be evaporated to closely to do into acetic acid ethyl ester extract, add the anhydrous second of 5 times amount of acetic acid ethyl ester extract weight
Alcohol is at temperature 45 C, and vacuum is to continue under conditions of 120mbar to be evaporated to dehydrated alcohol and ethyl acetate close to all
Steaming, obtain dry in sun tea essential oil, quintessence oil yield is 0.08 ‰
According to said method, vegetation has obtained doing Folium Camelliae sinensis quintessence oil, the tea essential oil that completes, bakeing tea essential oil respectively.
Embodiment 2 shines the preparation of Folium Camelliae sinensis ethanol extract
Extract in embodiment 1 and obtain in the extraction system after tea essential oil, after bottom condensed water is released, by shine Folium Camelliae sinensis with
Weight ratio 1:10 of 95% ethanol, adds ethanol, and controlling heating-up temperature is 70 DEG C, and extraction time is 1.5h, circumfluence distillation 2
Secondary, merge the alcohol extract of twice, at 50 DEG C, under conditions of vacuum is 50mbar, use concentrating under reduced pressure, controlling density is
1.06g/cm3, obtaining shining Folium Camelliae sinensis ethanol extract, yield is 11.5%.
According to said method, prepare respectively and done Folium Camelliae sinensis ethanol extract, the tea ethanol extract that completes, bakeed tea ethanol extract.
The preparation of embodiment 3 dry in sun tea extract
Extract in example 2 in the extraction system after obtaining alcohol extract, by solarization Folium Camelliae sinensis and weight ratio 1:10 of pure water, add
Entering pure water, controlling heating-up temperature is 85 DEG C, and extraction time is 2h, circumfluence distillation 2 times, merges the aqueous extract of twice, 55
DEG C, under conditions of vacuum is 50mbar, using concentrating under reduced pressure, control density is 1.08g/cm3, obtain dry in sun tea extract,
Yield is 11.5%.
According to said method, prepare respectively and done Folium Camelliae sinensis water extract, the tea extract that completes, bakeed tea extract.
Through chromatography of gases-Mass Spectrometer Method analysis, TIEGUANYIN does containing of multiple fragrance component in Folium Camelliae sinensis quintessence oil, the tea essential oil that completes
Measuring the highest, the such as content of benzyl alcohol, phenethanol, 1-Phenylethanone., indole and nerolidol is the highest.
Wherein, phenethanol has: gentle hyacinth-Fructus Gardeniae fragrance, flower, earth, Mel fragrance, fruit sample
Taste.Benzyl alcohol has: faint, sweet, the fragrance of fruity, distinctive pleasant fruit aroma.Indole has: connect
The fragrance of nearly jasmin.Nerolidol has: be similar to the faint fragrance of a flower of Flos Rosae Rugosae and Fructus Mali pumilae, the sweetest, the freshest,
Lasting fragrance.1-Phenylethanone. has: have note as May bloom fragrance, Acacia farnesiana Willd. and Herba Mimosae Pudicae.The prompting present invention does Folium Camelliae sinensis
Quintessence oil and the tea essential oil that completes have important function for the suction quality and sense organ comfort level improving electronic cigarette.
The allotment of embodiment 4 flavouring essence for tobacco
Each component is mixed by following mass percent, and under room temperature, stirs 30min, fully mix, obtain described cigarette
Use essence.Wherein each monomer perfume in flavouring essence for tobacco is provided by Hua Bao essence and flavoring agent (Shanghai) Co., Ltd..
Ethyl acetate 1.00%, ethyl n-butyrate. 0.50%, ethyl valerate 0.30%, iso-amyl iso-valeriate 0.50%, acetic acid
Folic alcohol ester 0.02%, menthyl acetate 0.50%, geraniol 0.05%, nerolidol 0.20%, caryophyllenol 0.10%, Flos Caryophylli
Flower bud oil 0.05%, fennel oil 0.02%, acetic acid 0.01%, alpha, beta-lonone 0.02%, β-Damascenone 0.05%, huge bean
Three ketenes 0.01%, vanillin 0.10%, ethylmaltol 0.20%, Fructus Armeniacae Mume extract 1.00%, red date tincture 2.00%, Herba Cichorii
Extract 0.50%, cloud and mist absolute oil 0.50%, Zimbabwe's extract 3.00%, storesin 0.01%, Peru's extractum
0.20%, Tolu concrete 0.10%, propylene glycol 30.00% and ethanol 59.06%.
The preparation of embodiment 5 compositions of the present invention
Each raw material embodiment 1-4 prepared is mixed by following mass percent, and stirs 30min under room temperature, fully
Mixing, obtains described compositions.
Embodiment 6 sensory quality assessment
Blank sample, the compositions for preparing by the formula 1-5 in embodiment 5 is added to electricity as tobacco juice for electronic smoke
Sub-cigarette carries out sensory quality assessment.
Electronic cigarette sensory quality assessment method in the present invention uses GB 5606.4-2005 " Medicated cigarette the 4th part: sense organ
Technology requires " evaluation methodology, its evaluation index " gloss " do not scores, and evaluation number is 11 people, and concrete evaluation result is such as
Shown in table 1.
Described blank sample refers to the tobacco juice for electronic smoke without thing extract processed at the beginning of TIEGUANYIN tea, comprises following mass ratio
Component: flavouring essence for tobacco 8.0%, glycerol 8.0%, surplus is propylene glycol.
Table 1 sensory quality assessment result (GB5606.4-2005)
As can be seen from Table 1, there are the tobacco juice for electronic smoke of the formula 1-5 of thing extract processed, sense organ matter at the beginning of interpolation TIEGUANYIN tea
Measure and point be above blank sample, and every quality index all has improvement；Because of thing extract processed, cigarette at the beginning of the TIEGUANYIN tea that used
Different by essence adding proportion, the aesthetic quality of formula 1-5 all has difference in various degree, according to scoring event, described in formula 5
Formulation composition the most reasonable.
Sensory Quality of Cigarette evaluation result shows: the tobacco juice for electronic smoke prepared with thing extract processed at the beginning of TIEGUANYIN tea, not only
The TIEGUANYIN tea perfume (or spice) note that electronic cigarette is elegant can be given, suction quality and the sense organ comfort level of electronic cigarette can be effectively improved simultaneously.
Although the detailed description of the invention of the present invention has obtained detailed description, it will be understood to those of skill in the art that root
According to disclosed all teachings, those details can be carried out various amendment and replacement, these change all the guarantor of the present invention
Within the scope of protecting.The four corner of the present invention is given by claims and any equivalent thereof.
Claims (13)
1. a compositions, it comprises by percentage to the quality:
Thing extract 10-15% processed at the beginning of TIEGUANYIN tea；
Flavouring essence for tobacco 6-8%；And,
Propellant 70-84%.
2. the compositions of claim 1, thing extract processed at the beginning of wherein said TIEGUANYIN tea is selected from the caffein of thing processed at the beginning of TIEGUANYIN tea
Oil, tea ethanol extract, tea extract or above combination in any (such as tea essential oil, tea ethanol extract and the combination of tea extract).
3. thing chosen from Fe kwan-yin processed at the beginning of the compositions of claim 1 or 2, wherein said TIEGUANYIN tea shines Folium Camelliae sinensis, does Folium Camelliae sinensis, completes
Tea and baking tea.
4. the compositions of claim 3, extract chosen from Fe kwan-yin dry in sun tea essential oil of thing processed, solarization at the beginning of wherein said TIEGUANYIN tea
Folium Camelliae sinensis ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis quintessence oil, do Folium Camelliae sinensis ethanol extract, do Folium Camelliae sinensis water extract, the tea essential oil that completes, complete
Tea ethanol extract, the tea extract that completes, baking tea essential oil, baking tea ethanol extract, baking tea extract or above combination in any (example
Such as TIEGUANYIN dry in sun tea essential oil, solarization Folium Camelliae sinensis ethanol extract, the tea ethanol extract that completes, baking tea ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis
The combination of water extract；TIEGUANYIN is done Folium Camelliae sinensis quintessence oil, is done Folium Camelliae sinensis ethanol extract, the tea ethanol extract that completes, baking tea ethanol extract, dry in sun tea
Extract, do the combination of Folium Camelliae sinensis water extract；TIEGUANYIN complete tea essential oil, the tea ethanol extract that completes, bakee tea ethanol extract, dry in sun tea and carry
Thing, do Folium Camelliae sinensis water extract, the compositions of the tea extract that completes；TIEGUANYIN bakees tea essential oil, the tea ethanol extract that completes, bakees tea alcohol extraction
Thing, dry in sun tea extract, do Folium Camelliae sinensis water extract, bakee tea extract combination；TIEGUANYIN do Folium Camelliae sinensis quintessence oil, the tea essential oil that completes,
Shine Folium Camelliae sinensis ethanol extract, baking tea ethanol extract, dry in sun tea extract, do Folium Camelliae sinensis water extract, the combination of the tea extract that completes).
5. the compositions of claim 1, wherein said flavouring essence for tobacco comprises following components by weight percentage:
Ethyl acetate 1.00%；
Ethyl n-butyrate. 0.50%；
Ethyl valerate 0.30%；
Iso-amyl iso-valeriate 0.50%；
Leaf Acetate 0.02%；
Menthyl acetate 0.50%；
Geraniol 0.05%；
Nerolidol 0.20%；
Caryophyllenol 0.10%；
Flos Caryophylli oil 0.05%；
Fennel oil 0.02%；
Acetic acid 0.01%；
Alpha, beta-lonone 0.02%；
β-Damascenone 0.05%；
Megastigmatrienone 0.01%；
Vanillin 0.10%；
Ethylmaltol 0.20%；
Fructus Armeniacae Mume extract 1.00%；
Red date tincture 2.00%；
Herba Cichorii extract 0.50%；
Cloud and mist absolute oil 0.50%；
Zimbabwe's extract 3.00%；
Storesin 0.01%；
Peru's extractum 0.20%；
Tolu concrete 0.10%；
Propylene glycol 30.00%；
Ethanol 59.06%.
6. the compositions of claim 1, wherein said propellant is selected from propylene glycol, glycerol and combination；Preferably, institute
Stating propellant is propylene glycol and glycerol；It is highly preferred that the content of glycerol is 8% in described compositions.
7. the compositions of claim 4, it comprises following components by percentage to the quality:
TIEGUANYIN dry in sun tea essential oil 0.1%-0.5%；
TIEGUANYIN shines Folium Camelliae sinensis ethanol extract 1.0%-2.0%；
TIEGUANYIN dry in sun tea extract 2.0%-3.0%；
TIEGUANYIN is Folium Camelliae sinensis water extract 1.0-5.0%；
TIEGUANYIN completes tea ethanol extract 2.0%-5.0%；
TIEGUANYIN bakees tea ethanol extract 1.0%-5.0%；
Flavouring essence for tobacco 6.0%-8.0%；
Glycerol 8.0%；And,
The propylene glycol of surplus.
8. the compositions of claim 4, it comprises following components by percentage to the quality:
TIEGUANYIN dry in sun tea extract 2.0%-3.0%；
TIEGUANYIN is Folium Camelliae sinensis quintessence oil 0.1%-0.2%；
TIEGUANYIN is Folium Camelliae sinensis ethanol extract 2.0%-5.0%；
TIEGUANYIN is Folium Camelliae sinensis water extract 1.0%-5.0%；
TIEGUANYIN completes tea ethanol extract 2.0%-5.0%；
TIEGUANYIN bakees tea ethanol extract 1.0%-5.0%；
Flavouring essence for tobacco 6.0%-8.0%；
Glycerol 8.0%；And
The propylene glycol of surplus.
9. the compositions of claim 4, it comprises following components by percentage to the quality:
TIEGUANYIN dry in sun tea extract 2.0%-3.0%；
TIEGUANYIN is Folium Camelliae sinensis water extract 1.0-5.0%；
TIEGUANYIN completes tea ethanol extract 2.0%-5.0%；
TIEGUANYIN completes tea essential oil 0.1%-0.2%；
TIEGUANYIN completes tea extract 2.0%-3.0%；
TIEGUANYIN bakees tea ethanol extract 1.0%-5.0%；
Flavouring essence for tobacco 6.0%-8.0%；
Glycerol 8.0%；And
The propylene glycol of surplus.
10. the compositions of claim 4, it comprises following components by percentage to the quality:
TIEGUANYIN dry in sun tea extract 2.0%-3.0%；
TIEGUANYIN is Folium Camelliae sinensis water extract 1.0%-5.0%；
TIEGUANYIN completes tea ethanol extract 2.0%-5.0%；
TIEGUANYIN bakees tea essential oil 0.1%-0.2%；
TIEGUANYIN bakees tea ethanol extract 1.0%-5.0%；
TIEGUANYIN bakees tea extract 2.0%-5.0%；
Flavouring essence for tobacco 6.0%-8.0%；
Glycerol 8.0%；And
The propylene glycol of surplus.
The compositions of 11. claim 4, it comprises following components by percentage to the quality:
TIEGUANYIN shines Folium Camelliae sinensis ethanol extract 1.0%-2.0%；
TIEGUANYIN dry in sun tea extract 2.0%-3.0%；
TIEGUANYIN is Folium Camelliae sinensis quintessence oil 0.1%-0.2%；
TIEGUANYIN is Folium Camelliae sinensis water extract 1.0%-5.0%；
TIEGUANYIN completes tea essential oil 0.1%-0.2%；
TIEGUANYIN completes tea extract 2.0%-3.0%；
TIEGUANYIN bakees tea ethanol extract 1.0%-5.0%；
Flavouring essence for tobacco 6.0%-8.0%；
Glycerol 8.0%；And
The propylene glycol of surplus.
The compositions of 12. any one of claim 1-11 purposes in preparing tobacco juice for electronic smoke.
13. 1 kinds of tobacco juice for electronic smoke, electronic cigarette or cigarette bullet, it contains the compositions of any one of claim 1-11.
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