CN101473879A - Preparation method of Yunnan black tea extract and use thereof - Google Patents
Preparation method of Yunnan black tea extract and use thereof Download PDFInfo
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- CN101473879A CN101473879A CNA2008102195526A CN200810219552A CN101473879A CN 101473879 A CN101473879 A CN 101473879A CN A2008102195526 A CNA2008102195526 A CN A2008102195526A CN 200810219552 A CN200810219552 A CN 200810219552A CN 101473879 A CN101473879 A CN 101473879A
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Abstract
The invention relates to a method for preparing extract of yunnan black tea and application thereof. The extract is prepared and obtained by extraction with ultrasonic extraction method and the combination of silica gel chromatographic separation method; the extraction processes comprise fetching of yunnan black tea, ultrasonic extraction, silica gel chromatographic separation, concentration, and obtaining of extract in sequence. When the extract of yunnan black tea is added to the tobacco of cigarettes, the invention can cause the fragrance of cigarettes to be permeable and abundant, the smell of cigarettes to be refined and fine, and the rest smell to be significantly improved in the aspect of comfort. Compared with the traditional extraction method, by using the yunnan black tea which is extracted by the ultrasonic wave of mixed solvent, the dosage ethanol is greatly reduced, the extracting and heating time is shortened, and the extraction efficiency is improved; by combining the silica gel chromatographic separation, the quality and purity of active ingredient is improved. The method relates to uncomplicated equipment, is easy for operation, has no pollution, and provides an improved extraction method which has good effect for the preparation of the extract of yunnan black tea.
Description
Technical field:
The present invention relates to the extraction and the application of tealeaves in the natural perfume material, be specifically related to a kind of preparation method and application thereof of Yunnan black tea extract.
Background technology:
China is the native place of tealeaves, is to find and utilize tealeaves country the earliest.Tealeaves has multiple efficacies such as medicinal, edible.Tea extract contains amino acid and multiple active skull cap components, as polyphenol, catechin, polysaccharide, vitamin, alkaloid etc., have the functions such as benefit think of, permanent tooth preventing decayed tooth, antiphlogistic and bactericidal, the anticancer change of radiation proof of refreshing oneself, and side effect is little, be a kind of broad-spectrum natural plant extracts, extensive in sector applications such as food, beverage, cosmetics.
Yunnan black tea tea is a kind of of China's six big teas; Its extract is a kind of traditional tobacco charging raw material, and it has the effect that lasting is lasting, improve cigarette odor-absorbing and flavouring essence quality.At present domestic most employing low-concentration ethanol continuous extraction legal system is equipped with tea extract, but this method has two big shortcomings: 1. the leaching process time longer, easily make part natural tea fragrance loss; 2. in the product except that fragrance component, also contain some protein, impurity component, dissolubility is bad, makes product be subjected to certain restriction when using.Therefore, how effectively the effective fragrance component in the black tea to be extracted, and improve its fragrance content, improve the black tea extract quality, make it can obtain more perfect utilization, become the development trend of tealeaves spices.
Summary of the invention:
The purpose of this invention is to provide a kind of preparation method and application thereof of Yunnan black tea extract, utilize ultrasonic wave to extract the yield that Yunnan black tea tea can improve Yunnan black tea extract, the binding silica gel chromatography has improved the quality and the purity of active ingredient; And then the interior quality of raising cigarette.
The objective of the invention is to realize by following proposal, is raw material with Yunnan black tea tea, uses mixed solvent, ultrasonic extraction method to obtain, and wherein the preparation method of Yunnan black tea extract prepares as follows:
Step 1: in the ultrasonic wave extractor, add Yunnan black tea tea, add mixed solvent, opening device, temperature remains under 60-70 ℃, extracts 30-60 minute, stops operation, and pours out extract after the cooling slightly, uses strainer filtering, collects extract; Recrement continues to carry out the second time with said method and extracts, and filters and collects extract for the second time;
Step 2: merge extracted twice liquid, on rotary evaporator, concentrate, thickening temperature 60-90 ℃, vacuum 0.03-0.1Mpa;
Step 3: the ethyl acetate mixed processing that benzinum that to be 1.0 ± 0.02 concentrate with the proportion that obtains doubly measure with 0.5-2 and 2-5 doubly measure, remove insoluble matter, and reclaim solvent;
Step 4: this concentrate is placed on the silica gel column chromatography, as solvent, carry out chromatography, behind the recovery solvent, obtain Yunnan black tea extract with benzinum.
The preparation method of above-mentioned Yunnan black tea extract, described concentrate content is: Polyphenols 4-16%, catechin 5-10%, amino acids 0.5-3.0%, carbohydrate 2.0-10%, alkaloid 1-8.0%.
The preparation method of above-mentioned Yunnan black tea extract, described mixed solvent is made up of ethanol, propane diols, water, citric acid.
The preparation method of above-mentioned Yunnan black tea extract, described Yunnan black tea tea raw material is the tealeaves of fermentation, moisture is at 7-20%.
The preparation method of above-mentioned Yunnan black tea extract, solid-liquid ratio was 1:8-1:20 during described ultrasonic wave was handled, and ultrasonic power is 15-60kHz, and extraction time is 30-60min.
Above-mentioned Yunnan black tea extract, the appearance characteristics of described extract is yellow green or dark brown.
A kind of application of Yunnan black tea extract takes by weighing Yunnan black tea extract by the 0.01-0.05% of cigarette shreds, and with the dissolving of 60% ethanol, spray is added in the flue-cured tobacco pipe tobacco, is rolled into the cigarette finished product.
The invention has the advantages that: compare with traditional extracting method, the Yunnan black tea tea that uses mixed solvent, ultrasonic wave to extract greatly reduces consumption of ethanol, reduces and extracts heat time heating time, has improved extraction efficiency; The binding silica gel chromatography has improved the quality and the purity of active ingredient, and the method equipment is uncomplicated, and operation is pollution-free easily, for the Yunnan black tea extract preparation provides a kind of improved, respond well extracting method.Think that through smokeing panel test this product perfuming effect in flue-cured tobacco is obvious: fragrance sends out thoroughly, plentiful, smoke is pure and mild, fine and smooth, pleasant impression comfort aspect has clear improvement.
The specific embodiment
To method afford further instruction of the present invention, but do not place restrictions on the present invention below by example.
Embodiment
The preparation method of Yunnan black tea extract prepares as follows:
Step 1: in the ultrasonic wave extractor, add Yunnan black tea tea, add mixed solvent, the water of its ethanol by 2 times of amounts, the propane diols of 2.5 times of amounts, 4.5 times of amounts, the citric acid of 0.05 times of amount are formed.Opening device, temperature remain under 60 ℃, extract 30 minutes, stop operation, and pour out extract after the cooling slightly, filter with 200 mesh filter screens, collect extract.Recrement continues to carry out the second time with said method and extracts, and filters and collects extract for the second time.
Step 2: merge extracted twice liquid, on rotary evaporator, concentrate 65 ℃ of thickening temperatures, vacuum 0.06Mpa;
Step 3: with the proportion that obtains be 1.0 ± 0.02 concentrate with the benzinum of 1 times of amount and the ethyl acetate mixed processing of 5 times of amounts, remove insoluble matter, and reclaim solvent;
Step 4: this concentrate is placed on the silica gel column chromatography, as solvent, carry out chromatography, behind the recovery solvent, obtain Yunnan black tea extract with benzinum.
Example carries out twice, feed intake to be 1000 grams at every turn, for the first time extract 255 grams (recovery rate 25.5%), for the second time extract 245 grams (recovery rate 24.5%), twice average recovery rate is 25.0%;
Detecting its concentrate content is: Polyphenols is about 11%, and catechin is about 8%, amino acids 0.9%, carbohydrate 2.4%, alkaloid 1.46%.
With the above-mentioned Yunnan black tea extract that makes, press 2/10000ths consumptions of pipe tobacco weight, with the dissolving of 60% ethanol, be sprayed onto equably in the pipe tobacco, pipe tobacco is made cigarette smoke panel test.
Claims (7)
1, a kind of preparation method of Yunnan black tea extract is a raw material with Yunnan black tea tea, uses mixed solvent, ultrasonic extraction method to obtain, and it is characterized in that: the preparation method of Yunnan black tea extract prepares as follows:
Step 1: in the ultrasonic wave extractor, add Yunnan black tea tealeaves, add mixed solvent, opening device, temperature remains under 60-70 ℃, extracts 30-60 minute, stops operation, and pours out extract after the cooling slightly, uses strainer filtering, collects extract; Recrement continues to carry out the second time with said method and extracts, and filters and collects extract for the second time;
Step 2: merge extracted twice liquid, on rotary evaporator, concentrate, thickening temperature 60-90 ℃, vacuum 0.03-0.1Mpa;
Step 3: the ethyl acetate mixed processing that benzinum that to be 1.0 ± 0.02 concentrate with the proportion that obtains doubly measure with 0.5-2 and 2-5 doubly measure, remove insoluble matter, and reclaim solvent;
Step 4: this concentrate is placed on the silica gel column chromatography, as solvent, carry out chromatography, behind the recovery solvent, obtain Yunnan black tea extract with benzinum.
2, the preparation method of Yunnan black tea extract according to claim 1 is characterized in that: described concentrate content is: Polyphenols 4-16%, catechin 5-10%, amino acids 0.5-3.0%, carbohydrate 2.0-10%, alkaloid 1-8.0%.
3, the preparation method of Yunnan black tea extract according to claim 1 is characterized in that: described mixed solvent is made up of ethanol, propane diols, water, citric acid.
4, the preparation method of Yunnan black tea extract according to claim 1 is characterized in that: described Yunnan black tea tea raw material is the tealeaves of fermentation, and moisture is at 7-20%.
5, the preparation method of Yunnan black tea extract according to claim 1 is characterized in that: solid-liquid ratio was 1:8-1:20 during described ultrasonic wave was handled, and ultrasonic power is 15-60kHz, and extraction time is 30-60min, and extracting temperature is 60-70 ℃.
6, Yunnan black tea extract according to claim 1 is characterized in that: the appearance characteristics of described extract is yellow green or dark brown.
7, a kind of application of Yunnan black tea extract as claimed in claim 1 is characterized in that: the 0.01-0.05% by cigarette shreds takes by weighing Yunnan black tea extract, and with the dissolving of 60% ethanol, spray is added in the flue-cured tobacco pipe tobacco, is rolled into the cigarette finished product.
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| CN2008102195526A CN101473879B (en) | 2008-11-28 | 2008-11-28 | Preparation method of Yunnan black tea extract and use thereof |
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| CN2008102195526A CN101473879B (en) | 2008-11-28 | 2008-11-28 | Preparation method of Yunnan black tea extract and use thereof |
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| CN101473879A true CN101473879A (en) | 2009-07-08 |
| CN101473879B CN101473879B (en) | 2012-06-27 |
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Cited By (13)
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| CN101828613A (en) * | 2010-05-10 | 2010-09-15 | 贾向云 | Process for producing Pu'er tea powder |
| CN102919427A (en) * | 2012-11-15 | 2013-02-13 | 戴群 | Black tea extract for effectively retaining original tea aroma and taste and preparation method and application of same |
| CN102940074A (en) * | 2012-11-15 | 2013-02-27 | 戴群 | Tea extract for effectively retaining aroma and taste of original tea and preparation method and application thereof |
| CN104403800A (en) * | 2014-12-04 | 2015-03-11 | 湖北中烟工业有限责任公司 | Preparation method of golden flower fungus fermentation type cigarette tea extract |
| CN104450191A (en) * | 2014-12-04 | 2015-03-25 | 湖北中烟工业有限责任公司 | Lactobacillus-fermented tea leaf extract for cigarettes and preparation method of lactobacillus-fermented tea leaf extract for cigarettes |
| CN104946388A (en) * | 2015-04-29 | 2015-09-30 | 湖北中烟工业有限责任公司 | Fermented black tea spice for cigarettes and preparation method of fermented black tea spice |
| CN105029696A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Black tea glycerol triacetate extract and application thereof in cigarettes |
| CN105707973A (en) * | 2014-09-10 | 2016-06-29 | 邹玉华 | Green tea extract and preparation method thereof |
| CN105996115A (en) * | 2016-07-18 | 2016-10-12 | 福建中烟工业有限责任公司 | Electronic cigarette juice prepared from primary preparation extract of extra-strong tea |
| CN106723352A (en) * | 2016-12-30 | 2017-05-31 | 广东中烟工业有限责任公司 | A kind of method and a kind of cigarette filter for lifting cigarette comfort level |
| CN106753793A (en) * | 2016-11-11 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette preparation method of tealeaves absolute oil |
| CN106867664A (en) * | 2015-12-10 | 2017-06-20 | 澳华达香料科技(广州)有限公司 | A kind of preparation method and application of compound collecting hops tincture |
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
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| CN103300183B (en) * | 2013-06-19 | 2014-08-20 | 广州市名花香料有限公司 | Cool tea concentrated liquid and extraction method thereof |
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| CN1695473A (en) * | 2004-12-01 | 2005-11-16 | 浙江大学 | Method for extracting effective content of tea |
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2008
- 2008-11-28 CN CN2008102195526A patent/CN101473879B/en active Active
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101828613B (en) * | 2010-05-10 | 2013-01-02 | 贾向云 | Process for producing Pu'er tea powder |
| CN101828613A (en) * | 2010-05-10 | 2010-09-15 | 贾向云 | Process for producing Pu'er tea powder |
| CN102919427A (en) * | 2012-11-15 | 2013-02-13 | 戴群 | Black tea extract for effectively retaining original tea aroma and taste and preparation method and application of same |
| CN102940074A (en) * | 2012-11-15 | 2013-02-27 | 戴群 | Tea extract for effectively retaining aroma and taste of original tea and preparation method and application thereof |
| CN102940074B (en) * | 2012-11-15 | 2014-02-19 | 戴群 | Tea extract for effectively retaining aroma and taste of original tea and preparation method and application thereof |
| CN102919427B (en) * | 2012-11-15 | 2014-02-26 | 戴群 | Black tea extract for effectively retaining original tea aroma and taste and preparation method |
| CN105707973A (en) * | 2014-09-10 | 2016-06-29 | 邹玉华 | Green tea extract and preparation method thereof |
| CN104403800A (en) * | 2014-12-04 | 2015-03-11 | 湖北中烟工业有限责任公司 | Preparation method of golden flower fungus fermentation type cigarette tea extract |
| CN104450191A (en) * | 2014-12-04 | 2015-03-25 | 湖北中烟工业有限责任公司 | Lactobacillus-fermented tea leaf extract for cigarettes and preparation method of lactobacillus-fermented tea leaf extract for cigarettes |
| CN104946388A (en) * | 2015-04-29 | 2015-09-30 | 湖北中烟工业有限责任公司 | Fermented black tea spice for cigarettes and preparation method of fermented black tea spice |
| CN105029696A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Black tea glycerol triacetate extract and application thereof in cigarettes |
| CN106867664A (en) * | 2015-12-10 | 2017-06-20 | 澳华达香料科技(广州)有限公司 | A kind of preparation method and application of compound collecting hops tincture |
| CN105996115A (en) * | 2016-07-18 | 2016-10-12 | 福建中烟工业有限责任公司 | Electronic cigarette juice prepared from primary preparation extract of extra-strong tea |
| CN106753793A (en) * | 2016-11-11 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette preparation method of tealeaves absolute oil |
| CN106753793B (en) * | 2016-11-11 | 2020-07-24 | 湖北中烟工业有限责任公司 | Preparation method of tea absolute for cigarettes |
| CN106723352A (en) * | 2016-12-30 | 2017-05-31 | 广东中烟工业有限责任公司 | A kind of method and a kind of cigarette filter for lifting cigarette comfort level |
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
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| CN101473879B (en) | 2012-06-27 |
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Owner name: AOHUADA PERFUMERY TECHNOLOGY (GUANGZHOU) CO., LTD. Free format text: FORMER OWNER: HUAFANG TOBACCO FLAVORS CO., LTD. Effective date: 20120428 |
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Effective date of registration: 20120428 Address after: YUNPU Luogang District YUNPU Industrial District of Guangzhou City, Guangdong province 510530 Road No. 22 Applicant after: Aohuada Perfume Technology (Guangzhou) Co.,Ltd. Address before: 510530 Guangzhou, Guangdong, Po Po Industrial Zone, Po Po Road, No. 22 Applicant before: Huafang Tobacco Flavors Co., Ltd. |
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Address after: YUNPU Luogang District YUNPU Industrial District of Guangzhou City, Guangdong province 510530 Road No. 22 Patentee after: Australian flavor (Guangzhou) Co., Ltd. Address before: YUNPU Luogang District YUNPU Industrial District of Guangzhou City, Guangdong province 510530 Road No. 22 Patentee before: Aohuada Perfume Technology (Guangzhou) Co.,Ltd. |