CN106867664A - A kind of preparation method and application of compound collecting hops tincture - Google Patents
A kind of preparation method and application of compound collecting hops tincture Download PDFInfo
- Publication number
- CN106867664A CN106867664A CN201510937055.XA CN201510937055A CN106867664A CN 106867664 A CN106867664 A CN 106867664A CN 201510937055 A CN201510937055 A CN 201510937055A CN 106867664 A CN106867664 A CN 106867664A
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- China
- Prior art keywords
- hops
- tincture
- compound collecting
- extract
- cigarette
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Abstract
The present invention relates to a kind of preparation method and applications of compound collecting hops tincture, the extract, in proportion with cured tobacco leaf, jujube, Yunnan black tea tea mixed material feeding, cooperates with method to extract and obtains with hops as primary raw material using mixed solvent, ultrasonic-microwave：Hop pellet and other raw materials → ultrasonic-microwave collaboration extraction → concentration → alcohol precipitation freezing → centrifugation → concentration → compound collecting hops tincture.Compound collecting hops tincture of the invention is added in cigarette shreds, cigarette flavor can be made hair is abundant thoroughly, smoke alcohol and, soft fine and smooth, the pleasant impression comfortableness aspect of flue gas has clear improvement.Compared with the extracting method of traditional beer flower tincture, the consumption of ethanol is greatly reduced, reduce and extract the heat time, improve extraction efficiency；In cigarette application harmony and it is rich be obviously improved, improve application value and addition in cigarette, the method is easily operated, pollution-free, and a kind of extracting method that is novel, working well is provided for prepared by hops tincture.
Description
Technical field
The present invention relates to the extraction and application of hops in natural perfume material, and in particular to a kind of preparation side of compound collecting hops tincture
Method and its application.
Background technology
Hops (Humunus lupulus L.) is that the perennial herbaceous stem of Moraceae Humulus is overgrow liana, and its female ball Honoka is referred to as
Hops.The geographical position of hops distribution is north latitude 40-60 degree, originates in Europe, western part of Asia and America etc., in many points of China
Cloth is in provinces and regions such as Xinjiang, Gansu, Shaanxi.Hops has its distinctive fragrance and bitter taste, produces the primary raw material of beer, it
A kind of distinctive bitter taste of beer and delicate fragrance can be given；The leavening that food industry is write music for a song using hops as yeast；In pharmaceuticals industry
A kind of upper important medicinal material, it have invigorating the spleen, diuresis, calmness, calm the nerves, it is sterilized, aid digestion the effects such as, to Gram-positive
Bacterium and knot west economy bacterium have inhibitory action, therefore, using the medicine that hops is primary raw material trial-production to treating pulmonary tuberculosis, drenching
The diseases such as Ba Juhe, tuberculous pleurisy have preferable curative effect.
Hops tincture is to extract ripe hops with low-concentration ethanol, heats continuous circulating reflux extraction, is obtained after recycling design.
Application practice shows：During as tobacco aromaticss, flavoring is played, bad breath is covered, is suppressed excitant, makes smoke soft agreeable to the taste
Effect, be the conventional traditional tobacco aromaticss of perfuming cigarette charging.
It is domestic at present to prepare hops tincture extract using low-concentration ethanol sequential extractions mostly, but this method has two big shortcomings：
1. the extraction process time is more long, easily loses part hops volatility aroma component；2. distinctive some aroma substances of hops
The counter productive such as bitter taste and blue foreign smell breath is also easy to produce in cigarette application, therefore limits its usage amount in cigarette.Therefore,
Effectively the aroma component in hops is extracted by technological means, improves perfume (or spice) of the hops tincture in cigarette application process
Gas and harmony and other effects, are to improve value of the hops in perfuming cigarette charging and extend the necessary ways of its range of application.
The content of the invention
It is it is an object of the invention to provide a kind of preparation method and applications of compound collecting hops tincture, hops is natural with other
Raw material according to ratio compound, using ultrasonic-microwave cooperate with extract, with reference to traditional alcohol precipitation refrigerating refining technique, improve effectively into
The quality and purity divided；And then improve hops application value in cigarette.
The purpose of the present invention be by following proposal realize, with hops as primary raw material, in proportion with cured tobacco leaf, jujube,
Yunnan black tea tea mixed material feeding, using mixed solvent, cooperates with method to extract and obtains, with reference to traditional alcohol precipitation refrigerating refining by ultrasonic-microwave
Technique, the preparation method of wherein compound collecting hops tincture is made by the steps：
Step one：Hop pellet, jujube are crushed respectively using disintegrating machine, chopping are carried out to cured tobacco leaf using filament cutter,
Then it is added sequentially in ultrasonic-microwave collaboration extraction kettle together with Yunnan black tea tea, adds mixed solvent, solid-liquid ratio to be 1: 5-1: 20；
Unlatching equipment, regulation ultrasonic power is 30-70w, and regulation microwave power is 100-500W, is extracted 30-60 minutes, stops making
Industry, extract solution is poured out after slightly cooling down, and with strainer filtering, collects extract solution；Recrement continues method described above carries out second extraction,
Second extract solution is collected by filtration；
Step 2：Merge extract solution twice, concentrate on the rotary evaporator, 60-90 DEG C of thickening temperature, vacuum 0.03-0.1Mpa；
Step 3：The proportion that will be obtained is dissolved for the concentrate of 0.9-1.2 with 95% ethanol of 7-10 times of quality of inventory, and
Freezing alcohol precipitation is carried out under conditions of -20-0 DEG C, cooling time is 10-24h；
Step 4：Precipitation solution after freezing is centrifuged, centrifugal rotational speed is 2500-5000r/min, centrifugation time is 20-50min,
Centrifuged supernatant is collected, centrifuged supernatant is concentrated on the rotary evaporator, 60-90 DEG C of thickening temperature, vacuum 0.03-0.1Mpa,
Stop concentration when concentrate proportion is 0.85-1.05, obtain compound collecting hops tincture.
The preparation method of above-mentioned Yunnan black tea extract, described mixed solvent is made up of ethanol, propane diols, water, glucan.
Above-mentioned compound collecting hops tincture, the appearance characteristics of the extract are in dark-brown or dark brown.
A kind of application of compound collecting hops tincture, compound collecting hops tincture is weighed by the 0.01-1% of cigarette shreds, uses 40-70%
Ethanol is dissolved, and spray is added in flue-cured tobacco pipe tobacco, is rolled into cigarette finished product.
The advantage of the invention is that：Compared with the extracting method of traditional beer flower tincture, cooperateed with using mixed solvent, ultrasonic-microwave
The compound material based on hops is extracted, the consumption of ethanol is greatly reduced, is reduced and is extracted the heat time, improve extraction effect
Rate；Hops and cured tobacco leaf, jujube, Yunnan black tea tea are combined the hops tincture for extract and obtaining, are coordinated in cigarette application
Property and it is rich be obviously improved, improve its application value and addition in cigarette, the method equipment is uncomplicated, easily behaviour
Make, it is pollution-free, for hops tincture prepares extracting method providing a kind of novelty, working well.The product is thought through smokeing panel test
Perfuming effect is obvious in flue-cured tobacco：Hair is abundant thoroughly for fragrance, smoke alcohol and, soft fine and smooth, the pleasant impression comfortableness aspect of flue gas has substantially
Improve.
Specific embodiment
Further instruction is given to the method for the present invention below by example, but does not place restrictions on the present invention.
Embodiment
The preparation method of Yunnan black tea extract is prepared as follows：
Step one：In the extraction kettle of ultrasonic-microwave collaboration extraction equipment, add pretreated hops, cured tobacco leaf,
Jujube, wherein Yunnan black tea raw material, hops：Cured tobacco leaf：Jujube, the ratio of Yunnan black tea tea are 8.5: 0.5: 0.8: 0.2, are added mixed
Bonding solvent, it is made up of the glucans of 3 times of ethanol of amount, 0.5 times of propane diols measured, 4.5 times of water measured, 0.05 times of amount.Open
Equipment, regulation ultrasonic wave and microwave power are respectively 50W and 350W, extract 40 minutes, stop operation, and are poured out after slightly cooling down and carried
Liquid is taken, is filtered with 300 mesh filter screens, collect extract solution.Recrement continues method described above carries out second extraction, is collected by filtration second
Secondary extract solution.
Step 2：Merge extract solution twice, concentrate on the rotary evaporator, 65 DEG C of thickening temperature, vacuum 0.06Mpa；
Step 3：The proportion that will be obtained is dissolved for 1.15 ± 0.02 concentrate with 8 times of 95% ethanol of quality, and at -10 DEG C
Under the conditions of carry out freezing alcohol precipitation, cooling time is 15h；
Step 4：Precipitation solution after freezing is centrifuged, centrifugal rotational speed is 3500r/min, centrifugation time is 30min, is collected
Centrifuged supernatant, centrifuged supernatant is concentrated on the rotary evaporator, 65 DEG C of thickening temperature, vacuum 0.06Mpa, in concentration
Stop concentration when thing proportion is 0.95 ± 0.02, obtain compound collecting hops tincture.
Example twice, feed intake be 1000 grams every time, 455 grams of extract is obtained for the first time and (is received
Yield 45.5%), 445 grams of extract (recovery rate 44.5%) is obtained for the second time, average recovery rate is 45.0% twice；
By compound collecting hops tincture obtained above, by 0.5% consumption of pipe tobacco weight, dissolved with 60% ethanol, equably sprayed
It is spread across in pipe tobacco, pipe tobacco is made into cigarette is smoked panel test.
Claims (8)
1. a kind of preparation method of compound collecting hops tincture, with hops as primary raw material, in proportion with cured tobacco leaf, red
Jujube, Yunnan black tea tea mixed material feeding, cooperate with method to extract and obtain, wherein compound collecting hops tincture using mixed solvent, ultrasonic-microwave
Preparation method be made by the steps：
Step one：Hop pellet, jujube are crushed respectively using disintegrating machine, chopping are carried out to cured tobacco leaf using filament cutter,
Then it is added sequentially in ultrasonic-microwave collaboration extraction kettle together with Yunnan black tea tea, adds mixed solvent, opens equipment, regulation ultrasound
Ripple 30-70w, adjusts microwave power 100-500W, extracts 30-60 minutes, stops operation, and extract solution is poured out after slightly cooling down, and uses
Strainer filtering, collects extract solution；Recrement continues method described above carries out second extraction, and second extract solution is collected by filtration；
Step 2：Merge extract solution twice, concentrate on the rotary evaporator, 60-90 DEG C of thickening temperature, vacuum 0.03-0.1Mpa；
Step 3：The proportion that will be obtained is dissolved for the concentrate of 0.9-1.2 with 95% ethanol of 7-10 times of quality of inventory, and
Freezing alcohol precipitation is carried out under conditions of -20-0 DEG C, cooling time is 10-24h；
Step 4：Precipitation solution after freezing is centrifuged, centrifugal rotational speed is 2500-5000r/min, centrifugation time is 20-50min,
Centrifuged supernatant is collected, centrifuged supernatant is concentrated on the rotary evaporator, 60-90 DEG C of thickening temperature, vacuum 0.03-0.1Mpa,
Stop concentration when concentrate proportion is 0.85-1.05, obtain compound collecting hops tincture.
2. the preparation method of compound collecting hops tincture according to claim 1, it is characterised in that：Wherein hops: roasting
Cigarette tobacco leaf: jujube: the ratio of Yunnan black tea tea is (8-9.5): (0.1-2): (0.1-2): (0.1-2).
3. the preparation method of compound collecting hops tincture according to claim 1, it is characterised in that：Described mixed solvent
It is made up of ethanol, propane diols, water, glucan.
4. the preparation method of Yunnan black tea extract according to claim 1, it is characterised in that：Described ultrasonic-microwave association
It is 1: 5-1: 20 with solid-liquid ratio in extraction process, ultrasonic power is 30-70kHz, and microwave power is 100-500W, extraction time
It is 30-60min.
5. compound collecting hops tincture according to claim 1, it is characterised in that：After ultrasonic-microwave collaboration is extracted
Extract solution be concentrated into proportion for 0.9-1.2, add the 95% ethanol dissolving of 7-10 times of quality of inventory, and in -20-0 DEG C of bar
Freezing alcohol precipitation is carried out under part, cooling time is 10-24h.
6. compound collecting hops tincture according to claim 1, it is characterised in that：Precipitation solution after freezing is centrifuged,
Centrifugal rotational speed is 2500-5000r/min, and centrifugation time is 20-50min, collects centrifuged supernatant, by centrifuged supernatant in rotation
Concentrated on evaporator, 60-90 DEG C of thickening temperature, vacuum 0.03-0.1Mpa, stopped when concentrate proportion is 0.85-1.05 dense
Contracting, obtains compound collecting hops tincture.
7. compound collecting hops tincture according to claim 1, it is characterised in that：The appearance characteristics of the extract are in deep
Brown or dark brown.
8. a kind of application of compound collecting hops tincture as claimed in claim 1, it is characterised in that：By the 0.01-1% of cigarette shreds
Compound collecting hops tincture is weighed, is dissolved with 40-70% ethanol, spray is added in flue-cured tobacco pipe tobacco, is rolled into cigarette finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510937055.XA CN106867664A (en) | 2015-12-10 | 2015-12-10 | A kind of preparation method and application of compound collecting hops tincture |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510937055.XA CN106867664A (en) | 2015-12-10 | 2015-12-10 | A kind of preparation method and application of compound collecting hops tincture |
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| CN106867664A true CN106867664A (en) | 2017-06-20 |
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| CN201510937055.XA Withdrawn CN106867664A (en) | 2015-12-10 | 2015-12-10 | A kind of preparation method and application of compound collecting hops tincture |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN108703402A (en) * | 2018-06-07 | 2018-10-26 | 湖北中烟工业有限责任公司 | The method that alanine solid phase Maillard reaction improves stem quality |
| CN111334373A (en) * | 2018-12-19 | 2020-06-26 | 广州华芳烟用香精有限公司 | Preparation method of natural propolis aroma component and application of natural propolis aroma component in cigarettes |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101473879A (en) * | 2008-11-28 | 2009-07-08 | 华芳烟用香料有限公司 | Preparation method of Yunnan black tea extract and use thereof |
| CN102041173A (en) * | 2010-12-22 | 2011-05-04 | 华芳烟用香料有限公司 | Extraction and separation method of aromatic part in aromatic tobacco extract and application thereof to cigarettes |
-
2015
- 2015-12-10 CN CN201510937055.XA patent/CN106867664A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101473879A (en) * | 2008-11-28 | 2009-07-08 | 华芳烟用香料有限公司 | Preparation method of Yunnan black tea extract and use thereof |
| CN102041173A (en) * | 2010-12-22 | 2011-05-04 | 华芳烟用香料有限公司 | Extraction and separation method of aromatic part in aromatic tobacco extract and application thereof to cigarettes |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN108703402A (en) * | 2018-06-07 | 2018-10-26 | 湖北中烟工业有限责任公司 | The method that alanine solid phase Maillard reaction improves stem quality |
| CN111334373A (en) * | 2018-12-19 | 2020-06-26 | 广州华芳烟用香精有限公司 | Preparation method of natural propolis aroma component and application of natural propolis aroma component in cigarettes |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information |
Address after: YUNPU Luogang District YUNPU Industrial District of Guangzhou City, Guangdong province 510530 Road No. 22 Applicant after: Australian flavor (Guangzhou) Co., Ltd. Applicant after: Guangzhou Hua Fangyan flavor Co. Ltd. Address before: YUNPU Luogang District YUNPU Industrial District of Guangzhou City, Guangdong province 510530 Road No. 22 Applicant before: Aohuada Perfume Technology (Guangzhou) Co.,Ltd. Applicant before: Huafang Tobacco Flavors Co., Ltd. |
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| CB02 | Change of applicant information | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170620 |
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| WW01 | Invention patent application withdrawn after publication |