CN102321503B - Preparation method of fructus momordicae condensate and application thereof - Google Patents
Preparation method of fructus momordicae condensate and application thereof Download PDFInfo
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- CN102321503B CN102321503B CN 201110251471 CN201110251471A CN102321503B CN 102321503 B CN102321503 B CN 102321503B CN 201110251471 CN201110251471 CN 201110251471 CN 201110251471 A CN201110251471 A CN 201110251471A CN 102321503 B CN102321503 B CN 102321503B
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- microwave
- reflux extraction
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- condensate
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- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 88
- 238000010992 reflux Methods 0.000 claims abstract description 61
- 239000007788 liquid Substances 0.000 claims abstract description 42
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 29
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 239000003921 oil Substances 0.000 claims description 36
- 235000009815 Momordica Nutrition 0.000 claims description 26
- 241000218984 Momordica Species 0.000 claims description 26
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 239000007921 spray Substances 0.000 claims description 12
- 239000003643 water by type Substances 0.000 claims description 10
- 239000002562 thickening agent Substances 0.000 claims description 7
- 238000013467 fragmentation Methods 0.000 claims description 5
- 238000006062 fragmentation reaction Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 8
- 239000003208 petroleum Substances 0.000 abstract 4
- 239000008367 deionised water Substances 0.000 abstract 1
- 229910021641 deionized water Inorganic materials 0.000 abstract 1
- 238000000874 microwave-assisted extraction Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 241000208125 Nicotiana Species 0.000 description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 5
- 230000007812 deficiency Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Extraction Or Liquid Replacement (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a preparation method of a fructus momordicae condensate and application thereof, which belong to the technical field of plant chemistry. The preparation method of the fructus momordicae condensate specifically comprises the following process steps of: pretreatment of raw materials; double petroleum ether reflux extraction: fructus momordicae and petroleum ether are put into an extractor with a stirring device to be subjected to double petroleum ether reflux extraction; drying: the fructus momordicae subjected to double extraction by the petroleum ether in the extractor is collected and then is dried; double microwave reflux extraction: the dried fructus momordicae is put into a microwave extractor with a stirring device, and deionized water is added to be subjected to double microwave reflux extraction; filtering: primary microwave reflux extraction liquid and secondary microwave reflux extraction liquid are filtered after being mixed, and deposits are removed; and concentrating: the filtered mixed liquid of double microwave reflux extraction liquids is concentrated by pressure reduction to obtain the fructus momordicae condensate. The preparation method adopts microwave extraction, shortens extraction time, improves extraction effect, improves the intrinsic quality of cigarettes, and does not add incompatible herb flavors to cigarette products, and the equipment in the method is not complicated, is easy to operate and is pollution-free.
Description
Technical field
The present invention relates to a kind of application of extracting process and extract of natural perfume, be specifically related to preparation method and the application thereof of fructus momordicae condensate, be particularly useful for the extraction of tobacco spice, belong to the vegetable chemistry technical field.
Background technology
In tobacco product, the fragrance of tobacco and pleasant impression are vital, perfuming cigarette is reinforced then to be one of core technology of tobacco industry, can remedy the shortcomings and deficiencies on the cigarette tobacco leaf formulation by perfuming, reinforced mode, eliminate assorted gas, make the fragrance of cigarette abundanter, sufficient, thereby inhaling flavor, smelling perfume (or spice) and have individual style.
Fructus momordicae condensate is a kind of traditional tobacco aromatics using, have the Hui Tian of increasing, reduce stimulation, improve the effect of cigarette odor-absorbing, but except useful composition, also contain some impurity components, when improving the cigarette quality in the conventional fructus momordicae condensate, also bring in various degree otherwise negative interaction, particularly it has the herbal of herbal medicine, and when consumption was slightly large, the medicinal herbs breath will reveal.Largely limited in application.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, a kind of preparation method and application thereof of fructus momordicae condensate are provided.
According to technical scheme provided by the invention, the preparation method of described fructus momordicae condensate comprises following processing step, and its component ratio is counted by weight,
(1) raw materials pretreatment: the thin slice that the Grosvenor Momordica fragmentation is sliced into 4 ~ 8 mm thick;
(2) twice sherwood oil reflux extraction: get in 490 ~ 510 portions of Grosvenor Momordicas and the extractor of 3400 ~ 3600 parts of sherwood oil inputs with whipping appts after the processing, carry out the sherwood oil reflux extraction first time, 3.0 ~ 3.5 hours time, be extracted liquid A; Reclaim extraction liquid A, in extractor, again add 2800 ~ 3000 parts of sherwood oils, carry out the sherwood oil reflux extraction second time, 2.0 ~ 2.5 hours time, be extracted liquid B, reclaim extraction liquid B; The stirring velocity of twice sherwood oil reflux extraction is 50 ~ 70 rev/mins;
(3) oven dry: collect the Grosvenor Momordica after twice sherwood oil reflux extraction in the extractor, Grosvenor Momordica was dried under 95 ~ 101 ℃ temperature 3.5 ~ 4 hours;
(4) twice microwave reflux extraction: the Grosvenor Momordica after drying processed is thrown in the microwave extracter with whipping appts, adds 3650 ~ 3750 parts of deionized waters, carries out microwave reflux extraction first time 3.5 ~ 4 hours, the collection extraction liquid first time; In microwave extracter, add 2950 ~ 3150 parts of deionized waters, carry out the microwave reflux extraction second time 3 ~ 3.5 hours, collect for the second time extraction liquid; Collect extraction liquid twice; The stirring velocity of twice microwave reflux extraction is 40 ~ 50 rev/mins, and microwave heating temperature is 100 ~ 102 ℃, and microwave power is 1.5 ~ 2.0kW;
(5) filter: after first, second time microwave reflux extraction liquid mixing with above-mentioned collection, filter with 300 mesh filter screens, remove precipitation;
(6) concentrated: incite somebody to action mixed solution concentrating under reduced pressure in 75 ~ 80 ℃ water-bath thickener of twice microwave reflux extraction liquid after filtering, vacuum tightness is 0.090 ~ 0.095MPa, obtains the product fructus momordicae condensate.
The density of described fructus momordicae condensate is 1.1120 ~ 1.1190 grams per milliliters.
The application of described Chinese fruit enriched material: take by weighing fructus momordicae condensate by 0.04% ~ 0.08% of cigarette shreds quality, adopt throat spray that the propylene glycol solution spray of fructus momordicae condensate is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
Twice sherwood oil reflux extraction Main Function is to remove the entrained medium-height grass flavour of a drug of Grosvenor Momordica.
Beneficial effect of the present invention: the present invention adopts microwave extracting, has shortened extraction time, has improved extraction effect, has improved the interior quality of cigarette, does not increase inharmonic herbal to cigarette product again, and this method equipment and uncomplicated, and operation is pollution-free easily.
Embodiment
The invention will be further described below in conjunction with specific embodiment.
The AE03-B type auto extractive device that extractor used in the present invention adopts Beijing ChinaInvent Instrument Technology Co., Ltd. to produce;
The microwave extracting machine that microwave extracter used in the present invention adopts Guangzhou Supreme Being's prestige industrial microwave apparatus company limited to produce;
The TN50-300T series of heat refluxing extraction thickener that water-bath thickener used in the present invention adopts Wenzhou City Tai Tai chemical to produce;
The throat spray that throat spray used in the present invention adopts Yangzhou safety medicine equipment company limited to produce.
Embodiment 1: the fructus momordicae condensate preparation method comprises following processing step: its component ratio is counted by weight,
(1) raw materials pretreatment: the thin slice that the Grosvenor Momordica fragmentation is sliced into 4 mm thick;
(2) twice sherwood oil reflux extraction: 490 portions of Grosvenor Momordicas and 3400 parts of sherwood oil inputs in the extractor with whipping appts, are carried out the sherwood oil reflux extraction first time, 3 hours time, be extracted liquid A; Take out extraction liquid A, add 2800 parts of sherwood oils in extractor, carry out the sherwood oil reflux extraction second time, time 2 h is extracted liquid B; The stirring velocity of twice sherwood oil reflux extraction is 50 rev/mins;
(3) Grosvenor Momordica after twice extraction of sherwood oil in the collection extractor is dried Grosvenor Momordica 3.5 hours under 95 ℃ temperature;
(4) twice microwave reflux extraction: the Grosvenor Momordica after drying processed is thrown in the microwave extracter with whipping appts, adds 3650 parts of deionized waters, carries out microwave reflux extraction first time 3.5 hours, the collection extraction liquid first time; In microwave extracter, add 2950 parts of deionized waters, carry out the microwave reflux extraction second time 3 hours, collect for the second time extraction liquid; The stirring velocity of twice microwave reflux extraction is 40 rev/mins, and microwave heating temperature is 100 ℃, and microwave power is 1.5kW;
(5) filter: after first, second time microwave reflux extraction liquid mixing with above-mentioned collection, filter with 300 mesh filter screens, remove precipitation;
(6) concentrated: incite somebody to action mixed solution concentrating under reduced pressure in 75 ℃ water-bath thickener of twice microwave reflux extraction liquid after filtering, vacuum tightness is 0.095MPa, obtains the product fructus momordicae condensate.
The application of the fructus momordicae condensate of gained: take by weighing fructus momordicae condensate by 0.04% of cigarette shreds quality, adopt throat spray that the propylene glycol solution spray of fructus momordicae condensate is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
Embodiment 2: the preparation method of fructus momordicae condensate comprises following processing step: its component ratio is counted by weight,
(1) raw materials pretreatment: the thin slice that the Grosvenor Momordica fragmentation is sliced into 6 mm thick;
(2) twice sherwood oil reflux extraction: 510 portions of Grosvenor Momordicas and 3600 parts of sherwood oil inputs in the extractor with whipping appts, are carried out the sherwood oil reflux extraction first time 3.5 hours, be extracted liquid A; Take out extraction liquid A, in extractor, add 3000 parts of sherwood oils, carry out the sherwood oil reflux extraction second time 2.5 hours, be extracted liquid B; The stirring velocity of twice sherwood oil reflux extraction is 70 rev/mins;
(3) Grosvenor Momordica after twice extraction of sherwood oil in the collection extractor is dried Grosvenor Momordica 4.0 hours under 101 ℃ temperature;
(4) twice microwave reflux extraction: the Grosvenor Momordica after drying processed is thrown in the microwave extracter with whipping appts, adds 3750 parts of deionized waters, carries out microwave reflux extraction first time 4 hours, the collection extraction liquid first time; In microwave extracter, add 3150 parts of deionized waters, carry out the microwave reflux extraction second time 3.5 hours, collect for the second time extraction liquid; The stirring velocity of twice microwave reflux extraction is 50 rev/mins, and microwave heating temperature is 102 ℃, and microwave power is 2.0kW;
(5) filter: after first, second time microwave reflux extraction liquid mixing with above-mentioned collection, filter with 300 mesh filter screens, remove precipitation;
(6) concentrated: incite somebody to action mixed solution concentrating under reduced pressure in 80 ℃ water-bath thickener of twice microwave reflux extraction liquid after filtering, vacuum tightness is 0.090MPa, obtains the product fructus momordicae condensate.
The application of fructus momordicae condensate takes by weighing fructus momordicae condensate by 0.08% of cigarette shreds quality, adopts throat spray that the propylene glycol solution spray of fructus momordicae condensate is added in the cigarette shreds, and cigarette shreds is rolled into cigarette.
Embodiment 3: the preparation method of fructus momordicae condensate comprises following processing step: its component ratio is counted by weight,
(1) raw materials pretreatment: the thin slice that the Grosvenor Momordica fragmentation is sliced into 8 mm thick;
(2) twice sherwood oil reflux extraction: 500 portions of Grosvenor Momordicas and 3500 parts of sherwood oil inputs in the extractor with whipping appts, are carried out the sherwood oil reflux extraction first time 3.2 hours, be extracted liquid A; Take out extraction liquid A, in extractor, add 2900 parts of sherwood oils, carry out the sherwood oil reflux extraction second time 2.2 hours, be extracted liquid B; The stirring velocity of twice sherwood oil reflux extraction is 60 rev/mins;
(3) Grosvenor Momordica after twice extraction of sherwood oil in the collection extractor is dried Grosvenor Momordica 3.8 hours under 98 ℃ temperature;
(4) twice microwave reflux extraction: the Grosvenor Momordica after drying processed is thrown in the microwave extracter with whipping appts, adds 3700 parts of deionized waters, carries out microwave reflux extraction first time 3.8 hours, the collection extraction liquid first time; In microwave extracter, add 3050 parts of deionized waters, carry out the microwave reflux extraction second time 3.3 hours, collect for the second time extraction liquid; The stirring velocity of twice microwave reflux extraction is 45 rev/mins, and microwave heating temperature is 101 ℃, and microwave power is 1.7kW;
(5) filter: after first, second time microwave reflux extraction liquid mixing with above-mentioned collection, filter with 300 mesh filter screens, remove precipitation;
(6) concentrated: incite somebody to action mixed solution concentrating under reduced pressure in 78 ℃ water-bath thickener of twice microwave reflux extraction liquid after filtering, vacuum tightness is 0.092MPa, obtains the product fructus momordicae condensate.
The application of gained fructus momordicae condensate: take by weighing fructus momordicae condensate by 0.06% of cigarette shreds quality, adopt throat spray that the propylene glycol solution spray of fructus momordicae condensate is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
Claims (1)
1. the preparation method of fructus momordicae condensate, it is characterized in that: comprise following processing step, its component ratio is counted by weight:
(1) raw materials pretreatment: the thin slice that the Grosvenor Momordica fragmentation is sliced into 4 ~ 8 mm thick;
(2) twice sherwood oil reflux extraction: get in 490 ~ 510 portions of Grosvenor Momordicas and the extractor of 3400 ~ 3600 parts of sherwood oil inputs with whipping appts after the processing, carry out the sherwood oil reflux extraction first time, 3.0 ~ 3.5 hours time, be extracted liquid A; Take out extraction liquid A, in extractor, add 2800 ~ 3000 parts of sherwood oils, carry out the sherwood oil reflux extraction second time, 2.0 ~ 2.5 hours time, be extracted liquid B; The stirring velocity of twice sherwood oil reflux extraction is 50 ~ 70 rev/mins;
(3) oven dry: collect the Grosvenor Momordica after twice sherwood oil reflux extraction in the extractor, Grosvenor Momordica was dried under 95 ~ 101 ℃ temperature 3.5 ~ 4 hours;
(4) twice microwave reflux extraction: the Grosvenor Momordica after drying processed is thrown in the microwave extracter with whipping appts, adds 3650 ~ 3750 parts of deionized waters, carries out microwave reflux extraction first time 3.5 ~ 4 hours, the collection extraction liquid first time; In microwave extracter, add 2950 ~ 3150 parts of deionized waters, carry out the microwave reflux extraction second time 3 ~ 3.5 hours, collect for the second time extraction liquid; Collect extraction liquid twice; The stirring velocity of twice microwave reflux extraction is 40 ~ 50 rev/mins, and microwave heating temperature is 100 ~ 102 ℃, and microwave power is 1.5 ~ 2.0kW;
(5) filter: after first, second time microwave reflux extraction liquid mixing with above-mentioned collection, filter with 300 mesh filter screens, remove precipitation;
(6) concentrated: incite somebody to action mixed solution concentrating under reduced pressure in 75 ~ 80 ℃ water-bath thickener of twice microwave reflux extraction liquid after filtering, vacuum tightness is 0.090 ~ 0.095MPa, obtains the product fructus momordicae condensate;
The density of described fructus momordicae condensate is 1.1120 ~ 1.1190 grams per milliliters;
Take by weighing fructus momordicae condensate by 0.04% ~ 0.08% of cigarette shreds quality, adopt throat spray that the propylene glycol solution spray of fructus momordicae condensate is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104762132A (en) * | 2015-03-05 | 2015-07-08 | 云南中烟工业有限责任公司 | Preparation method and application of Siraitia grosvenorii extract |
| CN105011368A (en) * | 2015-06-17 | 2015-11-04 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette |
| CN105907477A (en) * | 2016-07-06 | 2016-08-31 | 鹰潭华宝香精香料有限公司 | Preparation method of natural flavor |
| CN109090702B (en) * | 2018-06-29 | 2021-08-24 | 郑州轻工业学院 | Preparation method and application of Maillard reaction product of Luo Han Guo extract |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
| CN110339225A (en) * | 2019-07-01 | 2019-10-18 | 上海欧润化妆品有限公司 | A kind of extracting method of Siraitia grosvenorii |
Citations (1)
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| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
Non-Patent Citations (2)
| Title |
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| 刘绍华，等.罗汉果提取物在丙纶滤棒中应用的研究.《中国烟草学报》.2009,第15卷(第3期),第17-21页. * |
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Address after: 214112 Jiangsu city of Wuxi province new Qumei Wu Cun Mei Yuk Road No. 7, room 117 Patentee after: Wuxi Huahai flavor Co., Ltd. Address before: 214112 Jiangsu Province, Wuxi City District Mei Tin Town Hung Road No. 37, No. 3 Patentee before: Wuxi Huahai Flavors Ltd. |
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Effective date of registration: 20170502 Address after: 201821 Road, Jiading Industrial Zone, Shanghai, building C, No. 1299 Patentee after: Shanghai Fobao peacock flavors Co. Address before: 214112 Jiangsu city of Wuxi province new Qumei Wu Cun Mei Yuk Road No. 7, room 117 Patentee before: Wuxi Huahai flavor Co., Ltd. |
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