CN104946388A - Fermented black tea spice for cigarettes and preparation method of fermented black tea spice - Google Patents
Fermented black tea spice for cigarettes and preparation method of fermented black tea spice Download PDFInfo
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- CN104946388A CN104946388A CN201510216540.8A CN201510216540A CN104946388A CN 104946388 A CN104946388 A CN 104946388A CN 201510216540 A CN201510216540 A CN 201510216540A CN 104946388 A CN104946388 A CN 104946388A
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- black tea
- spice
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- cigarette
- fermented
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- 244000269722 Thea sinensis Species 0.000 title claims abstract description 32
- 235000006468 Thea sinensis Nutrition 0.000 title claims abstract description 31
- 235000020279 black tea Nutrition 0.000 title claims abstract description 31
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 31
- 235000013599 spices Nutrition 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000284 extract Substances 0.000 claims abstract description 21
- 238000000605 extraction Methods 0.000 claims abstract description 9
- 238000000855 fermentation Methods 0.000 claims description 17
- 230000004151 fermentation Effects 0.000 claims description 17
- 239000007788 liquid Substances 0.000 claims description 17
- 241000894006 Bacteria Species 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 11
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- 239000008103 glucose Substances 0.000 claims description 8
- 238000005374 membrane filtration Methods 0.000 claims description 8
- 239000011259 mixed solution Substances 0.000 claims description 8
- 230000001954 sterilising effect Effects 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 235000014655 lactic acid Nutrition 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 6
- 238000001556 precipitation Methods 0.000 abstract description 3
- 238000001914 filtration Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 241000208125 Nicotiana Species 0.000 description 6
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 5
- 239000002304 perfume Substances 0.000 description 4
- 150000002576 ketones Chemical class 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 241000186660 Lactobacillus Species 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229940039696 lactobacillus Drugs 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 235000013616 tea Nutrition 0.000 description 2
- 240000006914 Aspalathus linearis Species 0.000 description 1
- 235000012984 Aspalathus linearis Nutrition 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 235000019225 fermented tea Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000000383 hazardous chemical Substances 0.000 description 1
- PGSADBUBUOPOJS-UHFFFAOYSA-N neutral red Chemical compound Cl.C1=C(C)C(N)=CC2=NC3=CC(N(C)C)=CC=C3N=C21 PGSADBUBUOPOJS-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
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Abstract
The invention belongs to the technical field of spice for cigarettes and particularly relates to fermented black tea spice for cigarettes and a preparation method of the fermented black tea spice. The spice is obtained by fermenting the raw material natural black tea extract and performing the treatment such as follow-up alcohol precipitation, filtration and concentration of the fermented product; the spice contains more aroma substances than the spice prepared by a direct extraction method, and the aroma is outstanding in style and gives a layering sense; and by adding the spice into cigarettes, the cigarette aroma can be enriched, the mouthfeel is improved, and the sucking comfort is improved. The preparation method of the spice is simple in process and environmentally friendly; the product quality is easy to control, and the cost is relatively low; and the preparation method is suitable for industrial large-scale production.
Description
Technical field
The invention belongs to tobacco aromatics using technical field, be specifically related to a kind of cigarette fermented type black tea spices and preparation method thereof.
Background technology
Essence and flavoring agent has the effect strengthening cigarette perfume, reduce stimulation, improve mouthfeel etc. in cigarette.Current tobacco industry is all at development natural essence spices energetically, adopt microbial fermentation technology to produce cigarette bioflavours, natural green is environmentally friendly, and technological process is simple to operation, do not produce toxic by-products, pollution-free, be easy to be esthetically acceptable to the consumers and there is certain market competitiveness.
Black tea aroma component compound reaches 300 kinds more than.Black tea aroma component is based on volatile compounds such as alcohols, aldehydes, ketone, ester classes, and mostly they are that in black tea manufacturing process natural oxidation obtains.Black tea is as the full fermented tea of one, knead, produce a large amount of violet ketone hazardous substance and ketone, alcohols etc. in fermenting process, ferment closely similar with tobacco ageing, closely, therefore black tea spices is more suitable for being applied in tobacco industry than other teas aroma component.At present, the black tea spices major part of adding in China tobacco is the direct extract of black tea, and its product fragrance is single, complex process.
Summary of the invention
The present invention aims to provide a kind of cigarette black tea spices utilizing microbial fermentation technology to produce, this spices with neutral red tea extract for raw material ferments, and fermented product is obtained through follow-up alcohol precipitation, filtration, the art breading such as concentrated, the spices obtained compared to direx process contains more various fragrance matter, fragrance style is given prominence to and the sense that has levels, added in cigarette and can be enriched cigarette perfume (or spice), improved mouthfeel, improve and inhale taste comfortableness.
The preparation method of cigarette fermented type black tea spices of the present invention comprises the following steps:
Step one, by black tea with pure water according to 1:(5-8) weight ratio mixes, backflow 90min extracts twice, and united extraction liquid, lets cool to room temperature after ultraviolet lamp sterilising treatment;
Step 2, adds glucose and bacterium powder by black tea extracting solution obtained in step one respectively according to 3% and 1% of extracting solution quality, seals and be placed in 25-30 DEG C of bottom fermentation 10-15 days;
Step 3, fermented liquid step 2 obtained and the ethanol of 95% mix according to the volume ratio of 1:6, after hold over night, mixed solution are passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Bacterium powder in described step 2 is any one bacterium powder in acetic bacteria, milk-acid bacteria or yeast saccharomyces cerevisiae.
Being mixed with 95% ethanol by fermented liquid according to the ratio of 1:6 in described step 3 and leave standstill can Quick stop fermentation reaction have good alcohol precipitation effect.
Cigarette fermented type black tea spices of the present invention can select different bacterial classifications in preparation process, and the overall fragrance style of obtained spices is roughly the same.
Cigarette fermented type black tea spices fragrance of the present invention is unique and can enrich cigarette perfume (or spice), improves mouthfeel, improves and inhale taste comfortableness; Simple and the environmental protection of its preparation method technique, quality product is easy to control, and cost is lower, is applicable to commercial scale production.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but following each embodiment should not be construed as the restriction to technical solution of the present invention.
Embodiment one:
Get 50g Yunnan black tea, i.e. Yunnan black tea, add 250g pure water, backflow 90min extracts twice, and united extraction liquid, lets cool to room temperature after ultraviolet lamp sterilising treatment, add analytical pure glucose and acetic bacteria powder respectively according to 3% and 1% of extracting solution quality, seal and be placed in 25 DEG C of bottom fermentations 10 days.The ethanol of aforesaid fermentation liquid and 95% is mixed according to the volume ratio of 1:6, after hold over night, mixed solution is passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Accurately take above-mentioned medicinal extract 0.04g, with 70% alcohol dilution to 10mL, be evenly sprayed on the blank pipe tobacco of 40g with throat spray, after drying, roll into test cigarette.
Embodiment two:
Get 50g Yunnan black tea, add 300g pure water, backflow 90min extracts twice, united extraction liquid, let cool after ultraviolet lamp sterilising treatment to room temperature, add analytical pure glucose and lactobacillus powder respectively according to 3% and 1% of extracting solution quality, seal and be placed in 28 DEG C of bottom fermentations 12 days.The ethanol of aforesaid fermentation liquid and 95% is mixed according to the volume ratio of 1:6, after hold over night, mixed solution is passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Test by cigarette preparation method with embodiment one.
Embodiment three:
Get 50g Yunnan black tea, add 300g pure water, backflow 90min extracts twice, united extraction liquid, let cool after ultraviolet lamp sterilising treatment to room temperature, add analytical pure glucose and acetic bacteria powder respectively according to 3% and 1% of extracting solution quality, seal and be placed in 25 DEG C of bottom fermentations 15 days.The ethanol of aforesaid fermentation liquid and 95% is mixed according to the volume ratio of 1:6, after hold over night, mixed solution is passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Test by cigarette preparation method with embodiment one.
Embodiment four:
Get 50g Yunnan black tea, add 350g pure water, backflow 90min extracts twice, united extraction liquid, let cool after ultraviolet lamp sterilising treatment to room temperature, add analytical pure glucose and lactobacillus powder respectively according to 3% and 1% of extracting solution quality, seal and be placed in 30 DEG C of bottom fermentations 15 days.The ethanol of aforesaid fermentation liquid and 95% is mixed according to the volume ratio of 1:6, after hold over night, mixed solution is passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Test by cigarette preparation method with embodiment one.
Embodiment five:
Get 50g Yunnan black tea, add 400g pure water, backflow 90min extracts twice, united extraction liquid, let cool after ultraviolet lamp sterilising treatment to room temperature, add analytical pure glucose and S. cervisiae powder respectively according to 3% and 1% of extracting solution quality, seal and be placed in 28 DEG C of bottom fermentations 12 days.The ethanol of aforesaid fermentation liquid and 95% is mixed according to the volume ratio of 1:6, after hold over night, mixed solution is passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Test by cigarette preparation method with embodiment one.
Embodiment six:
Get 50g Yunnan black tea, add 250g pure water, backflow 90min extracts twice, united extraction liquid, let cool after ultraviolet lamp sterilising treatment to room temperature, add analytical pure glucose and S. cervisiae powder respectively according to 3% and 1% of extracting solution quality, seal and be placed in 30 DEG C of bottom fermentations 10 days.The ethanol of aforesaid fermentation liquid and 95% is mixed according to the volume ratio of 1:6, after hold over night, mixed solution is passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
Test by cigarette preparation method with embodiment one.
Get test cigarette obtained in each embodiment respectively, carry out sensory evaluating smoking's test with reference to cigarette standard GB/T 5606.4.Temperature 22 ± 1 DEG C, humidity is, after balancing 48 hours under 60 ± 2% environment, do contrast cigarette teacher please be commented to smoke panel test with the blank cigarette not adding extract.
Sensory evaluating smoking's result shows, the spices that each group embodiment obtains all can enrich cigarette perfume (or spice), improve and inhale taste, and cigarette fragrant breeze lattice is basically identical, and fragrant with light tea.
Claims (2)
1. a cigarette preparation method for fermented type black tea spices, is characterized in that, comprise the steps:
Step one, by black tea with pure water according to 1:(5-8) weight ratio mix, backflow 90min extract twice, united extraction liquid, lets cool to room temperature after ultraviolet lamp sterilising treatment;
Step 2, adds glucose and bacterium powder by black tea extracting solution obtained in step one respectively according to 3% and 1% of extracting solution quality, seals and be placed in 25-30 DEG C of bottom fermentation 10-15 days;
Step 3, fermented liquid step 2 obtained and the ethanol of 95% mix according to the volume ratio of 1:6, after hold over night, mixed solution are passed through 0.8 μm of membrane filtration, and by gained filtrate reduced in volume to medicinal extract shape.
2. a preparation method for cigarette fermented type black tea spices as claimed in claim 1, is characterized in that, described bacterium powder is any one bacterium powder in acetic bacteria, milk-acid bacteria or yeast saccharomyces cerevisiae.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510216540.8A CN104946388A (en) | 2015-04-29 | 2015-04-29 | Fermented black tea spice for cigarettes and preparation method of fermented black tea spice |
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| CN201510216540.8A CN104946388A (en) | 2015-04-29 | 2015-04-29 | Fermented black tea spice for cigarettes and preparation method of fermented black tea spice |
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| CN104946388A true CN104946388A (en) | 2015-09-30 |
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| CN201510216540.8A Pending CN104946388A (en) | 2015-04-29 | 2015-04-29 | Fermented black tea spice for cigarettes and preparation method of fermented black tea spice |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105779307A (en) * | 2016-04-18 | 2016-07-20 | 云南中烟工业有限责任公司 | Trichoderma aureoviride strain and method for preparing Pu'er Tea tobacco flavor |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101103840A (en) * | 2007-08-01 | 2008-01-16 | 陕西省科学院酶工程研究所 | Method for preparing tea flavoring used for cigarette |
| CN101473879A (en) * | 2008-11-28 | 2009-07-08 | 华芳烟用香料有限公司 | Preparation method of Yunnan black tea extract and use thereof |
| CN102191130A (en) * | 2011-05-19 | 2011-09-21 | 湖北中烟工业有限责任公司 | Preparation method of fermented cigarette fructus momordicae extractum |
| CN104450191A (en) * | 2014-12-04 | 2015-03-25 | 湖北中烟工业有限责任公司 | Lactobacillus-fermented tea leaf extract for cigarettes and preparation method of lactobacillus-fermented tea leaf extract for cigarettes |
-
2015
- 2015-04-29 CN CN201510216540.8A patent/CN104946388A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101103840A (en) * | 2007-08-01 | 2008-01-16 | 陕西省科学院酶工程研究所 | Method for preparing tea flavoring used for cigarette |
| CN101473879A (en) * | 2008-11-28 | 2009-07-08 | 华芳烟用香料有限公司 | Preparation method of Yunnan black tea extract and use thereof |
| CN102191130A (en) * | 2011-05-19 | 2011-09-21 | 湖北中烟工业有限责任公司 | Preparation method of fermented cigarette fructus momordicae extractum |
| CN104450191A (en) * | 2014-12-04 | 2015-03-25 | 湖北中烟工业有限责任公司 | Lactobacillus-fermented tea leaf extract for cigarettes and preparation method of lactobacillus-fermented tea leaf extract for cigarettes |
Non-Patent Citations (1)
| Title |
|---|
| 虞飞: ""人工接种发酵金花菌茶的品质分析"", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105779307A (en) * | 2016-04-18 | 2016-07-20 | 云南中烟工业有限责任公司 | Trichoderma aureoviride strain and method for preparing Pu'er Tea tobacco flavor |
| CN105779307B (en) * | 2016-04-18 | 2019-04-05 | 云南中烟工业有限责任公司 | A kind of trichoderma aureoviride bacterial strain and the method for preparing Pu'er tea tobacco aromaticss with it |
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Application publication date: 20150930 |