CN104256888A - Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice - Google Patents
Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice Download PDFInfo
- Publication number
- CN104256888A CN104256888A CN201410387362.0A CN201410387362A CN104256888A CN 104256888 A CN104256888 A CN 104256888A CN 201410387362 A CN201410387362 A CN 201410387362A CN 104256888 A CN104256888 A CN 104256888A
- Authority
- CN
- China
- Prior art keywords
- tobacco juice
- heat
- tobacco
- electronic tobacco
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
Abstract
The invention discloses heat-sensitivity electronic tobacco juice. The heat-sensitivity electronic tobacco juice comprises, by weight, 5%-8% of tobacco extracting solutions, 0.1%-3.5% of nicotine, 0.1%-2% of acidity regulators, 2%-3% of tobacco essence, 0.4%-8% of thickening agents, 15%-35% of water and the balance propylene glycol; the sum of all components is 100, and the components are evenly mixed to prepare the heat-sensitivity electronic tobacco juice. The thickening agents are one or more of gelatin, agar, acquirable burning rubber and carrageenan. The heat-sensitivity electronic tobacco juice has the heat sensitivity because of containing the thickening agents, and when the heating temperature ranges from 50 DEG C to 80 DEG C, the electronic tobacco juice is in the liquid state; when heating is stopped, the electronic tobacco juice liquidated by heating is cooled to restore to the solid state and is free of random flowing, so that the problems of liquid leakage, backflowing and volatilization of the electronic tobacco juice in the storage process and the transporting process are effectively solved, and a consumer can conveniently take and use the electronic tobacco juice. The heat-sensitivity electronic tobacco juice can be stored for a long time, and the quality, the taste and the like of the electronic tobacco juice all keep unchanged in the storage period.
Description
Technical field
The present invention relates to electronic cigarette technical field.More specifically, a kind of heat-sensitive electronic tobacco juice and preparation thereof is related to.
Background technology
" smoking is with healthy " is people's questions of common concern, is also the focus that tobacco business is paid close attention to.Traditional cigarette smoking mode makes to contain many harmful materials in the flue gas produced during cigarette burning, entering human body, can produce certain harm to human body by sucking.In addition, the side-stream smoke of generation also can make non-smokers' passive smoking.Therefore, smoking is more and more subject to criticism and the restriction of various circles of society in public places.Electronic cigarette is not due to containing tar and CO, the harm not having " second-hand-cigarette " to cause other people and the pollution to environment, and therefore electronic cigarette is day by day universal for cigarette, smoking cessation product as one.The appearance of electronic cigarette, indicates that smoking enters the healthy epoch, is also the response to " 12 " planning Tobacco Control ban on opium-smoking and the opium trade.The electronic cigarette occurred in the market and patent thereof are main mainly with liquid tobacco tar.But this liquid tobacco tar in use can produce liquid suck-back, leakage, storage and transport the problems such as inconvenient, volatile aroma is fast.Further, when liquid smoke oil consumption needs to the greatest extent to change, liquid is easily caused to expose, dangerous, unhygienic.
The electronic smoke atomizer that CN 202354377U invents at the sheathed oil removal sleeve pipe of the open slot end of fiberglass tubes, and in oil removal sleeve pipe outer wrapping one deck second cotton piece, can effectively prevent tobacco tar suck-back.
CN 101933653B has invented a kind of medicinal health type solid electronic aerosolization liquid, comprise propane diols 35-45%, medicament 30-35%, deionized water 10-15%, tobacco leaf extract 3-3.5%, tobacco essence 3-3.5%, excipient 2-3.0%, Calcium Pectate gel 0.2-1.0%, curing agent 0.3-0.8%.Wherein the main one-tenth composition of curing agent is the sodium alginate of 35% propylene glycol alginate and 65%; The main component of excipient is the casein sodium of 35% xanthans and 65%.Although this solid electronic tobacco juice efficiently solves the problem of the leakage of liquid electronic tobacco juice, backflow, storage transport inconvenience, but owing to being in solid form by heating atomization in use procedure, the ease of user when smoking and required atomization quantity and liquid electronic tobacco juice can gaps to some extent.
Therefore, need to provide a kind of electronic cigarette liquid, can ensure to suck effect, the problem such as leakage, suck-back of electronic cigarette in storage, transportation can be solved again.
Summary of the invention
First technical problem that the present invention will solve is to provide a kind of heat-sensitive electronic tobacco juice, and this electronic cigarette liquid is solid gel under storing state, is liquid after heated; Stop heating, the electronic cigarette liquid regelation of heat post liquefaction becomes solid gel.This electronic cigarette liquid changes existing liquid electronic tobacco juice and uses and storage mode, effectively solves the problems that liquid electronic tobacco juice occurs in storage and transportation.And the volatilization of electronic cigarette liquid of the present invention active ingredient when can prevent long storage periods.
Second technical problem that the present invention will solve is to provide a kind of preparation method of above-mentioned electronic cigarette liquid.
For solving above-mentioned first technical problem, the present invention adopts following technical proposals:
A kind of heat-sensitive electronic tobacco juice, it is characterized in that, comprise the following component of percentage by weight: 5-8% tobacco extract, 0.1-3.5% nicotine, 0.1-2% acidity regulator, 2-3% flavouring essence for tobacco, 0.4-8% thickener, 15-35% water, surplus are propane diols.
Preferably, described thickener be selected from gelatin, agar, can fire in glue and carragheen one or more.
Preferably, described acidity regulator is selected from one or more in citric acid, malic acid and oxalic acid.Citric acid, malic acid and oxalic acid are non-volatile organic acids main in tobacco, join the soda acid ratio that can regulate electronic cigarette liquid in electronic cigarette liquid, and being conducive to increases flue gas richness and soft sense.
Preferably, described flavouring essence for tobacco is selected from one or more in phenylacetic acid, vanillic aldehyde, ethyl maltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propyl alcohol and ethyl myristate.The effect that flavouring essence for tobacco used has to be increased tobacco characteristic perfume, increase flue gas richness and soft sense, only has amount of smoke when making up electronic cigarette suction in the past and lacks the defect of aesthetic quality.
Preferably, the serviceability temperature of described electronic cigarette liquid is less than 80 DEG C, effectively ensures that the thermal reversibility of thickener is not by high temperature.
For solving above-mentioned second technical problem, the present invention adopts following technical proposals.
The preparation method of heat-sensitive electronic tobacco juice, comprises the steps:
1) be added to the water by thickener, heating is stirred to dissolving;
2) to step 1) add propane diols in the solution that obtains, constantly stir, and maintenance system temperature is 60-75 DEG C.
3) stop heating, treat step 2) in mixed solution be cooled to 55 DEG C, add 0.1-3.5% nicotine, 0.1-2% acidity regulator, 5-8% tobacco extract, 2-3% flavouring essence for tobacco successively, stir, the obtained heat-sensitive electronic tobacco juice of cooling.
Preferably, step 1) described thickener is selected from gelatin, agar, can fire in glue and carragheen one or more.
Preferably, the electronic cigarette liquid prepared is 0.4-8% containing the percentage by weight of thickener, when gelatin selected by thickener, the percentage by weight of described gelatin is 4-8%, and when agar selected by thickener, the percentage by weight of described agar is 0.4-1.2%, when thickener select can fire glue time, the described percentage by weight that can fire sol solution is 1.5-2.5%, and when carragheen selected by thickener, the percentage by weight of described carrageenan solutions is 0.7-1.2%.In the preferred scope of application, being gel state when thickener used can ensure that electronic cigarette liquid stores, is that mobility is well liquid after heating.
Preferably, step 1) temperature of described heating is 60-75 DEG C, step 2) described in warming temperature be 60-75 DEG C.In this temperature range, heat thickener, can ensure that thickener is effectively dissolved into liquid state, the thermal reversibility of thickener can be ensured again.
Preferably, step 3) described in flavouring essence for tobacco be selected from phenylacetic acid, vanillic aldehyde, ethyl maltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propyl alcohol and ethyl myristate one or more.The effect that preferred flavouring essence for tobacco has to be increased tobacco characteristic perfume, increase flue gas richness and soft sense, only has amount of smoke when making up electronic cigarette suction in the past and lacks the defect of aesthetic quality.
Preferably, step 3) described acidity regulator be selected from citric acid, malic acid and strawberriff one or more.Citric acid, malic acid and oxalic acid are non-volatile organic acids main in tobacco, join the soda acid ratio that can regulate electronic cigarette liquid in electronic cigarette liquid, and being conducive to increases flue gas richness and soft sense.
Beneficial effect of the present invention is as follows:
1. the present invention is that the preparation of solid-liquid electronic cigarette liquid provides an effective approach, effectively changes the storage form of existing liquid electronic tobacco juice.
2. the electronic cigarette liquid that prepared by the present invention has thermal reversibility, is solid gel at normal temperatures, is liquid after heating, makes electronic cigarette liquid be easy to storage, transport, prevents leakage.
3. the electronic cigarette liquid that prepared by the present invention is solid gel at storage period, the volatilization of active ingredient when can prevent long storage periods in tobacco juice.
4. tobacco juice for electronic smoke of the present invention is used for the atomization of electronic cigarette, do not produce tar and CO, greatly reduce the harm of consumer, and the application of this product can not produce the harm of second-hand-cigarette.
Detailed description of the invention
In order to be illustrated more clearly in the present invention, below in conjunction with preferred embodiment, the present invention is described further.It will be appreciated by those skilled in the art that specifically described content is illustrative and nonrestrictive, should not limit the scope of the invention with this below.
Embodiment 1
A kind of heat-sensitive electronic tobacco juice, comprise the following component of percentage by weight: 8% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 6% gelatin, 32% water, 48% propane diols, each component summation is 100 parts, makes after mixing.
The preparation method of tobacco extract adopts conventional method, and detailed process is: get tobacco leaf in 40 DEG C of oven dry, after being cooled to room temperature, grind.Get 50g offal and be placed in 500ml triangular flask, add 250ml deionized water, 65 DEG C of shaking table oscillation extraction 30min.Coextraction 3 times, combining extraction liquid, decompression rotary evaporation is concentrated into 25ml, obtains tobacco extract.
The present invention does not have special restriction to the kind of described flavouring essence for tobacco and source, adopts flavouring essence for tobacco well known to those skilled in the art.In the present invention, described flavouring essence for tobacco preferentially comprises the following composition of percentage by weight: phenylacetic acid 4%, vanillic aldehyde 5%, ethyl maltol 5%, 3,5-lutidines 2%, P-hydroxybenzoic acid 5%, 5 hydroxymethyl furfural 2%, 1-acetoxyl group-2-propyl alcohol 2%, ethyl myristate 2%, 73% ethanol.Said components is mixed fit over together and stir 1h under normal temperature.
Embodiment 2
With embodiment 1, difference is the following component comprising percentage by weight: 5% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 2% can fire glue, 30% water, 57% propane diols, and each component summation is 100 parts, makes after mixing.
Embodiment 3
With embodiment 1, difference is the following component comprising percentage by weight: 8% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 1% agar, 25% water, 60% propane diols, makes after mixing.
Embodiment 4
With embodiment 1, difference is the following component comprising percentage by weight: 8% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 0.85% carragheen, 20% water, 65.15% propane diols, each component summation is 100 parts, makes after mixing.
Electronic cigarette liquid prepared by embodiment 1, embodiment 2, embodiment 3, embodiment 4 is added in electronic cigarette and carries out sensory quality assessment, evaluate in table 1.
Check problem: provide sample and check table to 6 experts that smoke panel test, requires that member of smoking smokes panel test to indices according to form requirement.
Table 1 embodiment of the present invention electronic cigarette liquid smoking result
As shown in Table 1, heat-sensitive electronic tobacco juice of the present invention, it is light that smoking experiences micro-sweet, the assorted gas of abundant, full, mouthfeel, has higher to suck comfort level.
Obviously; the above embodiment of the present invention is only for example of the present invention is clearly described; and be not the restriction to embodiments of the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here cannot give exhaustive to all embodiments, every belong to technical scheme of the present invention the apparent change of extending out or variation be still in the row of protection scope of the present invention.
Claims (10)
1. a heat-sensitive electronic tobacco juice, it is characterized in that, comprise the following component of percentage by weight: 5-8% tobacco extract, 0.1-3.5% nicotine, 0.1-2% acidity regulator, 2-3% flavouring essence for tobacco, 0.4-8% thickener, 15-35% water, surplus are propane diols.
2. heat-sensitive electronic tobacco juice according to claim 1, is characterized in that: described thickener is selected from gelatin, agar, can fire in glue and carragheen one or more.
3. heat-sensitive electronic tobacco juice according to claim 1, is characterized in that: described acidity regulator is selected from one or more in citric acid, malic acid and oxalic acid.
4. heat-sensitive electronic tobacco juice according to claim 1, it is characterized in that: described flavouring essence for tobacco is selected from one or more of phenylacetic acid, vanillic aldehyde, ethyl maltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propyl alcohol and ethyl myristate.
5. heat-sensitive electronic tobacco juice according to claim 1, is characterized in that: the serviceability temperature of described electronic cigarette liquid is less than 80 DEG C.
6. the preparation method of heat-sensitive electronic tobacco juice as claimed in claim 1, is characterized in that, comprise the steps:
1) be added to the water by thickener, heating is stirred to dissolving;
2) to step 1) slowly add propane diols in the solution that obtains, constantly stir, and maintenance system temperature is 60-75 DEG C.
3) stop heating, treat step 2) in mixed solution be cooled to 55 DEG C, add 0.1-3.5% nicotine, 0.1-2% acidity regulator, 5-8% tobacco extract, 2-3% flavouring essence for tobacco successively, stir, the obtained heat-sensitive electronic tobacco juice of cooling.
7. method according to claim 6, is characterized in that: step 1) described thickener is selected from gelatin, agar, can fire in glue and carragheen one or more.
8. method according to claim 6, is characterized in that: step 3) described electronic cigarette liquid is 0.4-8% containing the percentage by weight of thickener.
9. method according to claim 6, is characterized in that: step 1) temperature of described heating is 60-75 DEG C.
10. method according to claim 6, it is characterized in that: step 3) described in flavouring essence for tobacco be selected from one or more of phenylacetic acid, vanillic aldehyde, ethyl maltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propyl alcohol and ethyl myristate; Described acidity regulator is selected from one or more in citric acid, malic acid and oxalic acid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410387362.0A CN104256888B (en) | 2014-08-07 | 2014-08-07 | A kind of heat-sensitive electronic tobacco juice and preparation thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410387362.0A CN104256888B (en) | 2014-08-07 | 2014-08-07 | A kind of heat-sensitive electronic tobacco juice and preparation thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104256888A true CN104256888A (en) | 2015-01-07 |
| CN104256888B CN104256888B (en) | 2016-06-22 |
Family
ID=52148570
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410387362.0A Active CN104256888B (en) | 2014-08-07 | 2014-08-07 | A kind of heat-sensitive electronic tobacco juice and preparation thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104256888B (en) |
Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104585873A (en) * | 2015-01-20 | 2015-05-06 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof |
| CN105361238A (en) * | 2015-12-16 | 2016-03-02 | 浙江中烟工业有限责任公司 | Electronic cigarette smoke solution containing pH conditioning agent and method for improving smoking feeling of electronic cigarette smoke solution |
| CN105394807A (en) * | 2015-10-27 | 2016-03-16 | 广州市雅禾生物科技有限公司 | Preparation method of electronic cigarette liquid with good heat stability |
| CN105455190A (en) * | 2016-02-01 | 2016-04-06 | 湖北中烟工业有限责任公司 | Electronic cigarette liquid |
| CN108095199A (en) * | 2018-01-22 | 2018-06-01 | 云南拓宝科技有限公司 | A kind of gel state tobacco juice for electronic smoke and preparation method thereof |
| CN108185539A (en) * | 2018-03-21 | 2018-06-22 | 福建中烟工业有限责任公司 | Electronic cigarette that a kind of aesthetic quality is improved and preparation method thereof |
| CN108323827A (en) * | 2018-05-18 | 2018-07-27 | 东莞市鸿馥生物科技有限公司 | A kind of electronic cigarette atomizing liquid |
| CN109475187A (en) * | 2016-07-29 | 2019-03-15 | 菲利普莫里斯生产公司 | Aerosol including the device containing cartridge of gel and for cartridge heater generates system |
| CN109576058A (en) * | 2018-12-20 | 2019-04-05 | 湖北中烟工业有限责任公司 | A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill |
| CN110522083A (en) * | 2018-05-25 | 2019-12-03 | 中国科学院理化技术研究所 | A kind of new tobacco products Alevaire and its preparation method and application |
| CN111466607A (en) * | 2020-03-12 | 2020-07-31 | 深圳瀚星翔科技有限公司 | Tobacco tar thickener, electronic cigarette tobacco tar and preparation method thereof |
| CN111672429A (en) * | 2020-06-04 | 2020-09-18 | 云南中烟工业有限责任公司 | Reversible phase-change atomized liquid gel containing alkyl-aryl-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof |
| US10791760B2 (en) | 2016-07-29 | 2020-10-06 | Altria Client Services Llc | Aerosol-generating system including a cartridge containing a gel |
| CN112237295A (en) * | 2020-11-16 | 2021-01-19 | 云南中烟工业有限责任公司 | High-liquid-holding-capacity transparent solid tobacco tar and preparation method thereof |
| WO2021056526A1 (en) * | 2019-09-27 | 2021-04-01 | 深圳雾芯科技有限公司 | Electronic cigarette liquid |
| CN113331464A (en) * | 2021-05-21 | 2021-09-03 | 中国烟草总公司郑州烟草研究院 | Method for reducing aldehyde compounds in electronic smoke sol |
| CN113907398A (en) * | 2021-09-28 | 2022-01-11 | 深圳市真味生物科技有限公司 | Electronic atomized liquid with liquid leakage prevention function |
| CN113907399A (en) * | 2021-09-30 | 2022-01-11 | 深圳市真味生物科技有限公司 | Electronic atomized liquid and preparation method thereof |
| US11589607B2 (en) | 2018-04-06 | 2023-02-28 | Philip Morris Products S.A. | Nicotine gel |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB201718031D0 (en) * | 2017-11-01 | 2017-12-13 | British American Tobacco Investments Ltd | Aerosolisable gel |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101926505A (en) * | 2010-08-09 | 2010-12-29 | 深圳市如烟生物科技有限公司 | Caffeine electronic cigarette liquid |
| CN101933653A (en) * | 2010-08-09 | 2011-01-05 | 深圳市如烟生物科技有限公司 | Officinal health-care solid electronic aerosolization liquid and preparation method thereof |
| CN102551218A (en) * | 2012-01-20 | 2012-07-11 | 易侧位 | Quick smoking cessation atomizing cigarette with prolonged service life |
| CN103751252A (en) * | 2014-01-21 | 2014-04-30 | 江苏中烟工业有限责任公司 | Antiseptic disinfectant wash-free type tobacco gel composition and preparation method thereof |
| CN103960784A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type disposable electronic cigarette cartridge with electric heating wire arranged internally and with liquid fixed and preparation method thereof |
| CN103960783A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type solid-liquid electronic cigarette cartridge and manufacturing method thereof |
-
2014
- 2014-08-07 CN CN201410387362.0A patent/CN104256888B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101926505A (en) * | 2010-08-09 | 2010-12-29 | 深圳市如烟生物科技有限公司 | Caffeine electronic cigarette liquid |
| CN101933653A (en) * | 2010-08-09 | 2011-01-05 | 深圳市如烟生物科技有限公司 | Officinal health-care solid electronic aerosolization liquid and preparation method thereof |
| CN102551218A (en) * | 2012-01-20 | 2012-07-11 | 易侧位 | Quick smoking cessation atomizing cigarette with prolonged service life |
| CN103751252A (en) * | 2014-01-21 | 2014-04-30 | 江苏中烟工业有限责任公司 | Antiseptic disinfectant wash-free type tobacco gel composition and preparation method thereof |
| CN103960784A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type disposable electronic cigarette cartridge with electric heating wire arranged internally and with liquid fixed and preparation method thereof |
| CN103960783A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type solid-liquid electronic cigarette cartridge and manufacturing method thereof |
Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104585873A (en) * | 2015-01-20 | 2015-05-06 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof |
| CN104585873B (en) * | 2015-01-20 | 2017-01-18 | 四川中烟工业有限责任公司 | Electronic cigarette liquid rich in biological active polysaccharide and preparation method thereof |
| CN105394807A (en) * | 2015-10-27 | 2016-03-16 | 广州市雅禾生物科技有限公司 | Preparation method of electronic cigarette liquid with good heat stability |
| CN105361238A (en) * | 2015-12-16 | 2016-03-02 | 浙江中烟工业有限责任公司 | Electronic cigarette smoke solution containing pH conditioning agent and method for improving smoking feeling of electronic cigarette smoke solution |
| CN105455190A (en) * | 2016-02-01 | 2016-04-06 | 湖北中烟工业有限责任公司 | Electronic cigarette liquid |
| US11792894B2 (en) | 2016-07-29 | 2023-10-17 | Altria Client Services Llc | Aerosol-generating system including a cartridge containing a gel |
| CN109475187A (en) * | 2016-07-29 | 2019-03-15 | 菲利普莫里斯生产公司 | Aerosol including the device containing cartridge of gel and for cartridge heater generates system |
| US10791760B2 (en) | 2016-07-29 | 2020-10-06 | Altria Client Services Llc | Aerosol-generating system including a cartridge containing a gel |
| EP3490392B1 (en) | 2016-07-29 | 2022-11-23 | Philip Morris Products S.A. | Aerosol-generating system comprising a gel containing cartridge and a device for heating the cartridge |
| CN108095199A (en) * | 2018-01-22 | 2018-06-01 | 云南拓宝科技有限公司 | A kind of gel state tobacco juice for electronic smoke and preparation method thereof |
| CN108185539A (en) * | 2018-03-21 | 2018-06-22 | 福建中烟工业有限责任公司 | Electronic cigarette that a kind of aesthetic quality is improved and preparation method thereof |
| US11589607B2 (en) | 2018-04-06 | 2023-02-28 | Philip Morris Products S.A. | Nicotine gel |
| CN108323827A (en) * | 2018-05-18 | 2018-07-27 | 东莞市鸿馥生物科技有限公司 | A kind of electronic cigarette atomizing liquid |
| CN110522083A (en) * | 2018-05-25 | 2019-12-03 | 中国科学院理化技术研究所 | A kind of new tobacco products Alevaire and its preparation method and application |
| CN109576058A (en) * | 2018-12-20 | 2019-04-05 | 湖北中烟工业有限责任公司 | A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill |
| WO2021056526A1 (en) * | 2019-09-27 | 2021-04-01 | 深圳雾芯科技有限公司 | Electronic cigarette liquid |
| CN111466607A (en) * | 2020-03-12 | 2020-07-31 | 深圳瀚星翔科技有限公司 | Tobacco tar thickener, electronic cigarette tobacco tar and preparation method thereof |
| CN111672429B (en) * | 2020-06-04 | 2022-02-08 | 云南中烟工业有限责任公司 | Reversible phase-change atomized liquid gel containing alkyl-aryl-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof |
| CN111672429A (en) * | 2020-06-04 | 2020-09-18 | 云南中烟工业有限责任公司 | Reversible phase-change atomized liquid gel containing alkyl-aryl-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof |
| CN112237295A (en) * | 2020-11-16 | 2021-01-19 | 云南中烟工业有限责任公司 | High-liquid-holding-capacity transparent solid tobacco tar and preparation method thereof |
| CN113331464A (en) * | 2021-05-21 | 2021-09-03 | 中国烟草总公司郑州烟草研究院 | Method for reducing aldehyde compounds in electronic smoke sol |
| CN113907398A (en) * | 2021-09-28 | 2022-01-11 | 深圳市真味生物科技有限公司 | Electronic atomized liquid with liquid leakage prevention function |
| CN113907399A (en) * | 2021-09-30 | 2022-01-11 | 深圳市真味生物科技有限公司 | Electronic atomized liquid and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104256888B (en) | 2016-06-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104256888B (en) | A kind of heat-sensitive electronic tobacco juice and preparation thereof | |
| WO2019201290A1 (en) | Method for preparing low-suction-resistance polylactic acid tow filter rod used for reducing temperature of cigarette vapor | |
| RU2671775C1 (en) | Liquid composition for electronic cigarettes | |
| KR101208473B1 (en) | Composition of atomized solution for electronic cigarette | |
| CN108095199A (en) | A kind of gel state tobacco juice for electronic smoke and preparation method thereof | |
| CN101233890B (en) | Hard sugar containing tobacco component | |
| CN104585862B (en) | A kind of without sweet soapy feeling tobacco juice for electronic smoke | |
| CN101862024B (en) | Refreshing tablets containing tobacco components | |
| CN104382236A (en) | Gel state tobacco cartridge of electronic cigarette and preparation method thereof | |
| CN104489912A (en) | Strong-flavor electronic cigarette liquid | |
| CN109619656A (en) | It is a kind of to have effects that the tobacco juice for electronic smoke of antiphlogistic antibacterial | |
| CN108926030A (en) | A kind of tobacco style leaf composition for multiple heating mode cigarette, multiple heating mode cigarette and preparation method thereof | |
| CN103610229A (en) | Nicotine liquid of electronic cigarette | |
| JP7457069B2 (en) | Composition | |
| JPWO2018016069A1 (en) | Cigarette fillings for non-combustion heating smoking articles | |
| CN108669635B (en) | Fruity tobacco composition, smoking segment and heating non-combustion cigarette rod | |
| CN105167176A (en) | Composite tobacco humectant and composite tobacco humectant preparation method and application of composite tobacco humectant | |
| CN107574016A (en) | One kind heats do not burn the savory extract formula of the special peppermint of cigarette and preparation method | |
| US20050263165A1 (en) | Tobacco leaf substitute | |
| CN105361237A (en) | Electronic cigarette tobacco juice with cholesterol reducing function and preparation method thereof | |
| US10952460B2 (en) | Composition for a tobacco-free chew and method of manufacturing same | |
| CN108968136B (en) | Herbal tobacco composition, smoking segment and heating non-combustible cigarette rod | |
| CN103666764B (en) | A kind of cold taste essence for peppermint type cigarette composition | |
| US20210195937A1 (en) | Composition for a tobacco-free chew with liquid synthetic nicotine | |
| CN108669634A (en) | The tobacco compositions of drink style, smoke section and heating are not burnt cigarette cigarette stick |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |