CN104256888B - A kind of heat-sensitive electronic tobacco juice and preparation thereof - Google Patents
A kind of heat-sensitive electronic tobacco juice and preparation thereof Download PDFInfo
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- CN104256888B CN104256888B CN201410387362.0A CN201410387362A CN104256888B CN 104256888 B CN104256888 B CN 104256888B CN 201410387362 A CN201410387362 A CN 201410387362A CN 104256888 B CN104256888 B CN 104256888B
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- tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
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- General Chemical & Material Sciences (AREA)
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- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
Disclosure one heat-sensitive electronic tobacco juice, following component including percentage by weight: 5-8% tobacco extract, 0.1-3.5% nicotine, 0.1-2% acidity regulator, 2-3% flavouring essence for tobacco, 0.4-8% thickening agent, 15-35% water, surplus are propylene glycol, each component summation is 100, is mixed evenly to prepare。Wherein, described thickening agent be gelatin, agar, can fire in glue, carrageenan one or more。The present invention is because having thermal sensitivity containing above-mentioned thickening agent, and when heating-up temperature is 50-80 DEG C, electronic cigarette liquid is in a liquid state；Stop heating, be reduced to solid-state after the electronic cigarette liquid cooling of heat post liquefaction, will not arbitrarily flow, thus effectively solving leakage, backflow and the volatilization problems that electronic cigarette liquid occurs in storage and transportation, and greatly facilitate consumer and carry with and use。Tobacco juice for electronic smoke of the present invention can preserve for a long time, and in storage life, the quality and taste etc. of electronic cigarette liquid all remains unchanged。
Description
Technical field
The present invention relates to electronic cigarette technical field。More particularly, to a kind of heat-sensitive electronic tobacco juice and preparation thereof。
Background technology
" smoking is with healthy " is people's questions of common concern, is also the focus of tobacco business concern。Traditional cigarette smoking mode makes in the flue gas produced during cigarette burning containing many harmful materials, by sucking entrance human body, human body can produce certain harm。It addition, the side-stream smoke produced also can make non-smokers' passive smoking。Therefore, smoking is increasingly subject to criticism and the restriction of various circles of society in public places。Electronic cigarette is not owing to without tar and CO, having harm that other people cause by " second hand smoking " and the pollution to environment, and therefore electronic cigarette becomes increasingly popular for cigarette, smoking cessation product as one。The appearance of electronic cigarette, indicates that smoking enters the healthy epoch, is also the response that " 12 " plan Tobacco Control ban on opium-smoking and the opium trade。The electronic cigarette occurred in the market and patent thereof, how based on liquid ree-oil。But, this liquid ree-oil in use can produce liquid suck-back, leakage, storage and transport the problems such as inconvenient, volatile aroma is fast。Further, when liquid smoke oil consumption to the greatest extent need change time, easily cause liquid expose, dangerous, unhygienic。
The electronic smoke atomizer of CN202354377U invention at the sheathed oil removal sleeve pipe of the open slot end of fiberglass tubes, and in oil removal sleeve pipe outer wrapping one layer of second cotton piece, can effectively prevent ree-oil suck-back。
CN101933653B has invented a kind of medicinal health type solid electronic aerosolization liquid, including propylene glycol 35-45%, medicament 30-35%, deionized water 10-15%, Nicotiana tabacum L. extracting solution 3-3.5%, tobacco essence 3-3.5%, excipient 2-3.0%, Calcium Pectate gel 0.2-1.0%, firming agent 0.3-0.8%。The wherein sodium alginate that main one-tenth composition is 35% propylene glycol alginate and 65% of firming agent；The sodium caseinate being mainly composed of 35% xanthan gum and 65% of excipient。Although the problem that this solid electronic tobacco juice efficiently solves the leakage of liquid electronic tobacco juice, backflow, storage transport inconvenience, but owing to being be heated atomization in solid form in use procedure, user's ease when smoking and required atomization quantity and liquid electronic tobacco juice can gaps to some extent。
Accordingly, it is desirable to provide a kind of electronic cigarette liquid, both can guarantee that and sucked effect, the problems such as electronic cigarette leakage in storage, transportation, suck-back can have been solved again。
Summary of the invention
First technical problem that the invention solves the problems that is to provide a kind of heat-sensitive electronic tobacco juice, and this electronic cigarette liquid is solid gel under storing state, is liquid after heated；Stopping heating, the electronic cigarette liquid regelation of heat post liquefaction becomes solid gel。This electronic cigarette liquid changes existing liquid electronic tobacco juice and uses and storage mode, effectively solves the problems that liquid electronic tobacco juice occurs in storage and transportation。And the electronic cigarette liquid of the present invention volatilization of effective ingredient when can prevent long storage periods。
The preparation method that second technical problem that the invention solves the problems that is to provide a kind of above-mentioned electronic cigarette liquid。
For solving above-mentioned first technical problem, the present invention adopts following technical proposals:
A kind of heat-sensitive electronic tobacco juice, it is characterized in that, including the following component of percentage by weight: 5-8% tobacco extract, 0.1-3.5% nicotine, 0.1-2% acidity regulator, 2-3% flavouring essence for tobacco, 0.4-8% thickening agent, 15-35% water, surplus are propylene glycol。
Preferably, described thickening agent selected from gelatin, agar, can fire in glue and carrageenan one or more。
Preferably, one or more in citric acid, malic acid and oxalic acid of described acidity regulator。Citric acid, malic acid and oxalic acid are non-volatile organic acids main in Nicotiana tabacum L., join the soda acid ratio that can regulate electronic cigarette liquid in electronic cigarette liquid, are conducive to increasing flue gas richness and soft sense。
Preferably, one or more in phenylacetic acid, vanillin, ethylmaltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propanol and ethyl myristate of described flavouring essence for tobacco。The effect that flavouring essence for tobacco used has to be increased Nicotiana tabacum L. characteristic perfume, increase flue gas richness and soft sense, only has amount of smoke to lack the defect of aesthetic quality when making up the suction of conventional electronic cigarette。
Preferably, the use temperature of described electronic cigarette liquid, less than 80 DEG C, is effectively ensured the thermal reversibility of thickening agent not by high temperature。
For solving above-mentioned second technical problem, the present invention adopts following technical proposals。
The preparation method of heat-sensitive electronic tobacco juice, comprises the steps:
1) being added to the water by thickening agent, heated and stirred is to dissolving；
2) to step 1) solution that obtains adds propylene glycol, it is stirred continuously, and maintenance system temperature is 60-75 DEG C。
3) stop heating, treat step 2) in mixed solution be cooled to 55 DEG C, be sequentially added into 0.1-3.5% nicotine, 0.1-2% acidity regulator, 5-8% tobacco extract, 2-3% flavouring essence for tobacco, stir, cooling prepare heat-sensitive electronic tobacco juice。
Preferably, step 1) described thickening agent selected from gelatin, agar, can fire in glue and carrageenan one or more。
Preferably, the electronic cigarette liquid of the preparation percentage by weight containing thickening agent is 0.4-8%, when thickening agent selects gelatin, the percentage by weight of described gelatin is 4-8%, and when thickening agent selects agar, the percentage by weight of described agar is 0.4-1.2%, when thickening agent is selected and can be fired glue, the described percentage by weight that can fire sol solution is 1.5-2.5%, and when thickening agent selects carrageenan, the percentage by weight of described carrageenan solutions is 0.7-1.2%。Within the scope of preferred use, it is gel state that thickening agent used can guarantee that when electronic cigarette liquid stores, and is the good liquid of mobility after heating。
Preferably, step 1) temperature of described heating is 60-75 DEG C, step 2) described in warming temperature be 60-75 DEG C。In this temperature range, heat thickening agent, both can guarantee that thickening agent was effectively dissolved into liquid, and can guarantee that again the thermal reversibility of thickening agent。
Preferably, step 3) described in one or more in phenylacetic acid, vanillin, ethylmaltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propanol and ethyl myristate of flavouring essence for tobacco。The effect that preferred flavouring essence for tobacco has to be increased Nicotiana tabacum L. characteristic perfume, increase flue gas richness and soft sense, only has amount of smoke to lack the defect of aesthetic quality when making up the suction of conventional electronic cigarette。
Preferably, step 3) one or more in citric acid, malic acid and strawberriff of described acidity regulator。Citric acid, malic acid and oxalic acid are non-volatile organic acids main in Nicotiana tabacum L., join the soda acid ratio that can regulate electronic cigarette liquid in electronic cigarette liquid, are conducive to increasing flue gas richness and soft sense。
Beneficial effects of the present invention is as follows:
1. the present invention is that the preparation of solid-liquid electronic cigarette liquid provides an effective approach, effectively changes the storage form of existing liquid electronic tobacco juice。
2. the electronic cigarette liquid that prepared by the present invention has thermal reversibility, is solid gel at normal temperatures, is liquid after heating, makes electronic cigarette liquid be prone to storage, transport, it is prevented that leakage。
3. the electronic cigarette liquid that prepared by the present invention is solid gel at storage period, the volatilization of the effective ingredient in tobacco juice when can prevent long storage periods。
4. the tobacco juice for electronic smoke of the present invention is for the atomization of electronic cigarette, does not produce tar and CO, the harm of consumer is substantially reduced, and the application of this product will not produce the harm of second hand smoking。
Detailed description of the invention
In order to be illustrated more clearly that the present invention, below in conjunction with preferred embodiment, the present invention is described further。It will be appreciated by those skilled in the art that following specifically described content is illustrative and be not restrictive, should not limit the scope of the invention with this。
Embodiment 1
A kind of heat-sensitive electronic tobacco juice, comprises the following components of percentage by weight: 8% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 6% gelatin, 32% water, 48% propylene glycol, and each component summation is 100 parts, is mixed evenly to prepare。
The preparation method of tobacco extract adopts conventional method, and detailed process is: takes Nicotiana tabacum L. in 40 DEG C of drying, after being cooled to room temperature, grinds。Take 50g offal and be placed in 500ml triangular flask, add 250ml deionized water, 65 DEG C of shaking table oscillation extraction 30min。Coextraction 3 times, combining extraction liquid, decompression rotary evaporation is concentrated into 25ml, obtains tobacco extract。
Kind and the source of described flavouring essence for tobacco are not had special restriction by the present invention, adopt flavouring essence for tobacco well known to those skilled in the art。In the present invention, described flavouring essence for tobacco preferentially includes the following composition of percentage by weight: phenylacetic acid 4%, vanillin 5%, ethylmaltol 5%, 3,5-lutidines 2%, P-hydroxybenzoic acid 5%, 5 hydroxymethyl furfural 2%, 1-acetoxyl group-2-propanol 2%, ethyl myristate 2%, 73% ethanol。Mix said components to fit over and after together, under room temperature, stir 1h。
Embodiment 2
With embodiment 1, being distinctive in that the following components comprising percentage by weight: 5% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 2% can fire glue, 30% water, 57% propylene glycol, each component summation is 100 parts, is mixed evenly to prepare。
Embodiment 3
With embodiment 1, it is distinctive in that the following components comprising percentage by weight: 8% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 1% agar, 25% water, 60% propylene glycol, is mixed evenly to prepare。
Embodiment 4
With embodiment 1, being distinctive in that the following components comprising percentage by weight: 8% tobacco extract, 2% nicotine, 1% malic acid, 3% flavouring essence for tobacco, 0.85% carrageenan, 20% water, 65.15% propylene glycol, each component summation is 100 parts, is mixed evenly to prepare。
Electronic cigarette liquid prepared by embodiment 1, embodiment 2, embodiment 3, embodiment 4 is added to electronic cigarette carries out sensory quality assessment, evaluate in Table 1。
Testing procedure: provide sample and check table to 6 experts that smoke panel test, it is desirable to member of smoking requires indices is smoked panel test according to form。
Table 1 embodiment of the present invention electronic cigarette liquid smoking result
As shown in Table 1, the heat-sensitive electronic tobacco juice of the present invention, smoking experience abundant, full, mouthfeel micro-sweet, miscellaneous QI light, have and higher suck comfort level。
Obviously; the above embodiment of the present invention is only for clearly demonstrating example of the present invention; and be not the restriction to embodiments of the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here cannot all of embodiment be given exhaustive, every belong to apparent change that technical scheme extended out or the variation row still in protection scope of the present invention。
Claims (6)
1. a heat-sensitive electronic tobacco juice, it is characterised in that include the following component of percentage by weight:
5-8% tobacco extract, 0.1-3.5% nicotine, 0.1-2% acidity regulator, 2-3% flavouring essence for tobacco, 0.4-8% thickening agent, 15-35% water, surplus are propylene glycol；
Described thickening agent selected from gelatin, agar, can fire in glue and carrageenan one or more；
The use temperature of described electronic cigarette liquid is less than 80 DEG C。
2. heat-sensitive electronic tobacco juice according to claim 1, it is characterised in that: one or more in citric acid, malic acid and oxalic acid of described acidity regulator。
3. heat-sensitive electronic tobacco juice according to claim 1, it is characterized in that: described flavouring essence for tobacco is selected from one or more of phenylacetic acid, vanillin, ethylmaltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propanol and ethyl myristate。
4. the preparation method of heat-sensitive electronic tobacco juice as claimed in claim 1, it is characterised in that comprise the steps:
1) being added to the water by thickening agent, heated and stirred is to dissolving；
2) to step 1) solution that obtains is slowly added to propylene glycol, it is stirred continuously, and maintenance system temperature is 60-75 DEG C。
3) stop heating, treat step 2) in mixed solution be cooled to 55 DEG C, be sequentially added into 0.1-3.5% nicotine, 0.1-2% acidity regulator, 5-8% tobacco extract, 2-3% flavouring essence for tobacco, stir, cooling prepare heat-sensitive electronic tobacco juice。
5. method according to claim 4, it is characterised in that: step 1) temperature of described heating is 60-75 DEG C。
6. method according to claim 4, it is characterized in that: step 3) described in flavouring essence for tobacco selected from phenylacetic acid, vanillin, ethylmaltol, 3,5-lutidines, P-hydroxybenzoic acid, 5 hydroxymethyl furfural, 1-acetoxyl group-2-propanol and ethyl myristate one or more；One or more in citric acid, malic acid and oxalic acid of described acidity regulator。
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| CN201410387362.0A CN104256888B (en) | 2014-08-07 | 2014-08-07 | A kind of heat-sensitive electronic tobacco juice and preparation thereof |
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| CN201410387362.0A CN104256888B (en) | 2014-08-07 | 2014-08-07 | A kind of heat-sensitive electronic tobacco juice and preparation thereof |
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| CN104256888B true CN104256888B (en) | 2016-06-22 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2019086859A1 (en) * | 2017-11-01 | 2019-05-09 | British American Tobacco (Investments) Limited | Aerosolisable gel |
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| CN113907398B (en) * | 2021-09-28 | 2023-06-27 | 深圳市真味生物科技有限公司 | Electronic atomized liquid with liquid leakage preventing function |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101926505A (en) * | 2010-08-09 | 2010-12-29 | 深圳市如烟生物科技有限公司 | Caffeine electronic cigarette liquid |
| CN101933653A (en) * | 2010-08-09 | 2011-01-05 | 深圳市如烟生物科技有限公司 | Officinal health-care solid electronic aerosolization liquid and preparation method thereof |
| CN102551218A (en) * | 2012-01-20 | 2012-07-11 | 易侧位 | Quick smoking cessation atomizing cigarette with prolonged service life |
| CN103751252A (en) * | 2014-01-21 | 2014-04-30 | 江苏中烟工业有限责任公司 | Antiseptic disinfectant wash-free type tobacco gel composition and preparation method thereof |
| CN103960784A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type disposable electronic cigarette cartridge with electric heating wire arranged internally and with liquid fixed and preparation method thereof |
| CN103960783A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type solid-liquid electronic cigarette cartridge and manufacturing method thereof |
-
2014
- 2014-08-07 CN CN201410387362.0A patent/CN104256888B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101926505A (en) * | 2010-08-09 | 2010-12-29 | 深圳市如烟生物科技有限公司 | Caffeine electronic cigarette liquid |
| CN101933653A (en) * | 2010-08-09 | 2011-01-05 | 深圳市如烟生物科技有限公司 | Officinal health-care solid electronic aerosolization liquid and preparation method thereof |
| CN102551218A (en) * | 2012-01-20 | 2012-07-11 | 易侧位 | Quick smoking cessation atomizing cigarette with prolonged service life |
| CN103751252A (en) * | 2014-01-21 | 2014-04-30 | 江苏中烟工业有限责任公司 | Antiseptic disinfectant wash-free type tobacco gel composition and preparation method thereof |
| CN103960784A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type disposable electronic cigarette cartridge with electric heating wire arranged internally and with liquid fixed and preparation method thereof |
| CN103960783A (en) * | 2014-05-15 | 2014-08-06 | 湖北中烟工业有限责任公司 | Gel type solid-liquid electronic cigarette cartridge and manufacturing method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019086859A1 (en) * | 2017-11-01 | 2019-05-09 | British American Tobacco (Investments) Limited | Aerosolisable gel |
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