CN105394807A - Preparation method of electronic cigarette liquid with good heat stability - Google Patents
Preparation method of electronic cigarette liquid with good heat stability Download PDFInfo
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- CN105394807A CN105394807A CN201510704644.3A CN201510704644A CN105394807A CN 105394807 A CN105394807 A CN 105394807A CN 201510704644 A CN201510704644 A CN 201510704644A CN 105394807 A CN105394807 A CN 105394807A
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Abstract
The invention discloses a preparation method of electronic cigarette liquid with good heat stability. The preparation method includes the following steps that 1, by mass, 0.05-1% of tobacco extraction liquid, 1-1.5% of tobacco essence, 0-3% of nicotine, 0.5-1% of pure water, 50-70% of propylene glycol and the balance glycerin are prepared into a solution, and the solution is stirred and filtered to obtain filtrate; 2, a flavoring agent accounting for 0.5-10 ppm of the mass of the electronic cigarette liquid planned to be prepared is added into the filtrate, stirring and mixing are performed for 10-20 min, propylene glycol or glycerin is added for supplementation to obtain the 100% mass of the electronic cigarette liquid planned to be prepared, and after stirring and mixing are performed, a mixed solution is obtained; 3, the obtained mixed solution is put into a reaction kettle, heating reflux is performed for 1-3 h at 50-70 DEG C, and after cooling is performed, the electronic cigarette liquid is obtained. The tobacco aroma of the prepared electronic cigarette liquid is kept pure and natural, and the situation that due to great changes of smoked ingredients, a peculiar taste or discomfort is caused is avoided.
Description
Technical field
The present invention relates to electronic cigarette field, particularly a kind of preparation of electronic cigarette liquid of good thermal stability.
Background technology
In recent years, electronic cigarette, as a kind of trendy product, is attracting increasing consumer, and its development speed is very fast.Only 2014, the market sale of global electronic cigarette just reached 6,000,000,000 dollars.Its strong growth, Ling Ge great tobacco company and electronic cigarette giant strengthen the research to electronic cigarette.
Electronic cigarette popular now, all electronic smoke atomizer is housed, the tobacco juice in atomizer, is actually by such as propane diols, glycerine, alcohol equal solvent mix with a small amount of spices and essence, by electronic smoke atomizer, it is heated, produce " smog " and be supplied to consumer's sensation similar to smoking.To the hobby of electronic cigarette whether consumer, relevant with the essence and flavoring agent in electronic smoke atomizer to a great extent.Therefore, how to keep " tobacco flavor " in electronic cigarette liquid as much as possible here, meeting consumer's pursuit sense of taste similar to sucking true cigarette with this and enjoy, is the whether attractive key of electronic cigarette.
A kind of preparation method of electronic cigarette liquid disclosed in CN102349699A, it uses leaf tobacco extract, and then with under propane diols or polyethylene glycol solvent normal temperature mix, obtaining is the electronic cigarette liquid having tobacco aroma.Namely the solubility by improving working substance in leaf tobacco extract makes to remain with more fragrance in tobacco juice.CN104824834A discloses a kind of preparation method of electronic cigarette liquid.It is ethyl maltol, vanillic aldehyde and 2-(4-methoxyphenoxy by adding certain proportioning) sodium propionate composition, reach and suppress or remove the effect of being brought into sweet soapy feeling in electronic cigarette liquid by solvent, make it in atomization process, retain the smell close with true cigarette.
The preparation method of above electronic cigarette liquid lays particular emphasis on the infiltration capacity strengthening tobacco nature fragrance, or laying particular emphasis on to adopt to add presses down edulcorant to suppress " peculiar smell " in tobacco juice, and ignoring the thermal stability problems should considering its solution in the process preparing electronic cigarette liquid to a greater degree, the important component namely producing " smog " when sucking continuously as consumer can produce the impact of certain change.If the heat endurance of electronic cigarette liquid is poor, consumer is often or when sucking continuously, often can because suck into composition transfer comparatively large and cause mouthfeel to have peculiar smell, such as " chemical taste ", or fragrance becomes the sense of discomfort such as strange.
Summary of the invention
The object of the invention is to become strange for existing electronic cigarette liquid mouthfeel under continuous sucking and fragrance to reduce etc. in deficiency, a kind of preparation method of electronic cigarette liquid of good thermal stability is provided, makes electronic cigarette suck effect more close to traditional cigarette in sucking process.
The technical solution used in the present invention is:
A kind of preparation method of electronic cigarette liquid of good thermal stability, comprise the steps: 1) by 0.05 ~ 1% tobacco extract, 1 ~ 1.5% flavouring essence for tobacco, 0 ~ 3% nicotine, 0.5 ~ 1% pure water, 50 ~ 70% propane diols and surplus glycerine by mass percentage component are mixed with solution, stir, and filter and obtain solution; 2) add the flavoring agent of 0.5 ~ 10ppm of plan preparation electronic cigarette liquid quality to filtrate, be uniformly mixed 10 ~ 20min, the electronic cigarette liquid quality prepared with 100% plan of supplying of propane diols or glycerine, is uniformly mixed and obtains mixed solution; 3) gained mixed solution is placed in reactor, at 50 ~ 70 DEG C, adds hot reflux 1 ~ 3h, cools and obtain electronic cigarette liquid.
Tobacco extract wherein joins in the ethanolic solution of 95% by commercially available tobacco extract, is uniformly mixed solution and makes the concentration of final ethanolic solution be 70% ~ 80%.Filter, obtain extract, filter vacuum being concentrated into proportion is 1.3 namely obtain tobacco extract.
Wherein nicotine is commercially available from tobacco leaf or other is containing a kind of natural alkaloid extracted nicotine plant, and it is the important substance causing smoker's habituation.Therefore, when containing a small amount of highly purified nicotine in tobacco juice, the various bad reactions that just ES causes due to smoking cessation can be alleviated; When nicotine content in tobacco juice is 0, ES can avoid producing the injury that harmful substance brings human body in its combustion process.
As the further improvement of technique scheme, flavoring agent is amino acids flavoring agent.Described amino acids flavoring agent consumption is 0.5 ~ 10ppm of plan preparation electronic cigarette liquid quality.Usually, before flavoring agent is added into electronic cigarette liquid, be first made into 0.01 ~ 0.1% the aqueous solution for subsequent use.
As the further improvement of technique scheme, amino acids flavoring agent is selected from least one in L-PROLINE, glycine, Pidolidone, altheine, L-threonine, L-Histidine, Valine.Further, when amino acids flavoring agent is selected from more than one in L-PROLINE, glycine, Pidolidone, altheine, L-threonine, L-Histidine, Valine, different amino acid is to wait mass mixing.
In addition, owing to containing a large amount of fragrance matters in tobacco extract, carboxylic acids is comprised, alcohols, carbohydrate, aldehydes, amine etc.These materials are under the condition of low-temperature heat, and can accelerate a series of chemical reaction.Comprise the condensation, molecular rearrangement, polymerisation, cracking reaction etc. of sugar and the exchange of amino acid whose Maillard reaction, ester and aldehyde/alcohol/ester, alcohol aldehyde and the condensation of aldehyde aldehyde, aldehyde and amine.The result of described series reaction will produce compound new in a large number, and these new compound compounds that normally molecular weight is larger, there is when being present in mixed solution good stability.The present invention adds hot reflux 1 ~ 3h by mixed solution laying temperature 50 ~ 70 DEG C, thus reach make the fragrance of electronic cigarette liquid become more circle and, the object that fragrance is more stable.As the further improvement of technique scheme, heating reflux temperature is 50 DEG C.
The invention has the beneficial effects as follows: the present invention by having set up the step mixed solution being added with amino acids flavoring agent being added hot reflux in the preparation process of electronic cigarette liquid, each component in mixed solution is mixed to get evenly, make in reaction system, to generate the macromolecular compound with circle and fragrance had good stability further simultaneously, improve the stability of mixed solution.The electronic cigarette liquid finally prepared has good stability, and consumer is often or when sucking continuously, the tobacco flavor of electronic cigarette liquid keeps pure nature, can not because of suck into composition transfer comparatively large and cause sensation mouthfeel to have peculiar smell or sense of discomfort.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail.Unreceipted actual conditions person in embodiment, the condition of conveniently condition or manufacturer's suggestion is carried out.Agents useful for same or the unreceipted production firm person of instrument, be and can buy by commercially available the conventional products obtained.
Embodiment 1
A kind of preparation method of electronic cigarette liquid of good thermal stability is as follows:
The cloud and mist extract of 0.1 gram is dissolved in 50 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 48.4 grams, stirs solution, filters and obtains filtrate.Add the glycine solution of 0.5 gram 0.01% to filtrate, stir 10min, then supply 100 grams of electronic cigarette liquids with propane diols, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C, adds hot reflux 1h.Final for gained mixed solution is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 1
The cloud and mist extract of 0.1 gram is dissolved in 50 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 48.4 grams, stirs solution, filters and obtains filtrate.Add propane diols to filtrate and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 1 of getting 3ml embodiment 1 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 1, and during the electronic cigarette liquid of continuous sucking embodiment 1, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Embodiment 2
A kind of preparation method of electronic cigarette liquid of good thermal stability is as follows:
The cloud and mist extract of 0.5 gram is dissolved in 51.5 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 1 gram of pure water, glycerine 46 grams, stirs solution, filters and obtains filtrate.Add the Pidolidone aqueous solution of 1 gram 0.01% to solution, stir 15min.Supply 100 grams of electronic cigarette liquids with propane diols again, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 70 C condition, adds hot reflux 1h, be cooled to normal temperature, obtain electronic cigarette liquid.
Comparative example 2
The cloud and mist extract of 0.5 gram is dissolved in 51.5 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 1 gram of pure water, glycerine 46 grams, stirs solution, filters and obtains filtrate.Add propane diols to solution and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 2 of getting 3ml embodiment 2 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 2, and during the electronic cigarette liquid of continuous sucking embodiment 2, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml embodiment 1 of simultaneously getting 3ml embodiment 2 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with embodiment 2, and during the electronic cigarette liquid of continuous sucking embodiment 1, tobacco perfume (or spice) is more naturally pure.Both after continuous sucking, fragrance mouthfeel is all consistent and does not have notable difference.
Embodiment 3
A kind of preparation method of electronic cigarette liquid of good thermal stability is as follows:
The cloud and mist extract of 0.1 gram is dissolved in 50 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 48.4 grams, stirs solution, filters and obtains filtrate.The glycine of 0.7 gram 0.01%, the mixed aqueous solution of the quality such as Pidolidone and Valine is added to solution.Stir 20min, then supply 100 grams of electronic cigarette liquids with propane diols, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C condition, adds backflow 3h, final for gained mixed solution is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 3
The cloud and mist extract of 0.1 gram is dissolved in 50 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 48.4 grams, stirs solution, filters and obtains filtrate.Add propane diols to filtrate and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 3 of getting 3ml embodiment 3 adds in electronic smoke atomizer respectively, is smoked panel test by professional.Evaluation result shows: both have tobacco aroma, but compares with comparative example 3, and during the electronic cigarette liquid of continuous sucking embodiment 2, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Embodiment 4
A kind of preparation method of electronic cigarette liquid of good thermal stability is as follows:
The cloud and mist extract of 0.1 gram is dissolved in 50 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 45.4 grams, 3 grams, nicotine, stirs solution, filters and obtains filtrate.Add the glycine solution of 0.5 gram 0.01% to filtrate, stir 10min, then supply 100 grams of electronic cigarette liquids with propane diols, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C, adds hot reflux 1h.Final for gained mixed solution is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 4
The cloud and mist extract of 0.1 gram is dissolved in 50 grams of propane diols, adds 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 45.4 grams, 3 grams, nicotine, stirs solution, filters and obtains filtrate.Add propane diols to filtrate and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 4 of getting 3ml embodiment 4 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 4, and during the electronic cigarette liquid of continuous sucking embodiment 4, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Embodiment 5
The cloud and mist extract of 0.05 gram is dissolved in 70 grams of propane diols, adds the flavouring essence for tobacco of 1.2 grams, 0.5 gram of pure water, glycerine 27.95 grams, stirs solution, filters and obtains solution.The L-PROLINE aqueous solution of 0.06 gram 0.19% is added to solution.Stir 10min, then supply 100 grams of electronic cigarette liquids with glycerine, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C, adds backflow 1.5h.Final for gained mixed liquor is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 5
The cloud and mist extract of 0.05 gram is dissolved in 70 grams of propane diols, adds 1.2 grams of flavouring essence for tobaccos, 0.5 gram of pure water, glycerine 27.95 grams, stirs solution, filters and obtains solution.Add glycerine to solution and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 5 of getting 3ml embodiment 5 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 5, and during the electronic cigarette liquid of continuous sucking embodiment 5, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Embodiment 6
The cloud and mist extract of 0.06 gram is dissolved in 60 grams of propane diols, adds the flavouring essence for tobacco of 1 gram, 0.5 gram of pure water, glycerine 38.44 grams, stirs solution, filters and obtains solution.The L-threonine aqueous solution of 0.08 gram 0.5% is added to solution.Stir 10min, then supply 100 grams of electronic cigarette liquids with glycerine, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C, adds backflow 1.5h.Final for gained mixed liquor is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 6
By the cloud and mist extract of 0.06 gram, be richer than 60 grams of propane diols, add 1 gram of flavouring essence for tobacco, 0.5 gram of pure water, glycerine 38.44 grams, just solution stirs, and filters and obtains solution.Add glycerine to solution and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 6 of getting 3ml embodiment 6 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 5, and during the electronic cigarette liquid of continuous sucking embodiment 5, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Embodiment 7
The cloud and mist extract of 0.07 gram is dissolved in 50 grams of propane diols, adds the flavouring essence for tobacco of 1.5 grams, 0.7 gram of pure water, glycerine 47.73 grams, stirs solution, filters and obtains solution.The L-Histidine aqueous solution of 0.07 gram 0.5% is added to solution.Stir 10min, then supply 100 grams of electronic cigarette liquids with glycerine, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C, adds backflow 1.5h.Final for gained mixed liquor is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 7
By the cloud and mist extract of 0.07 gram, be richer than 50 grams of propane diols, add 1.5 grams of flavouring essence for tobaccos, 0.7 gram of pure water, glycerine 47.73 grams, stirs solution, filters and obtains solution.Add glycerine to solution and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 7 of getting 3ml embodiment 7 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 7, and during the electronic cigarette liquid of continuous sucking embodiment 7, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Embodiment 8
The cloud and mist extract of 0.08 gram is dissolved in 55 grams of propane diols, adds the flavouring essence for tobacco of 1 gram, 0.8 gram of pure water, glycerine 43.12 grams, stirs solution, filters and obtains solution.The altheine aqueous solution of 0.08 gram 0.4% is added to solution.Stir 10min, then supply 100 grams of electronic cigarette liquids with glycerine, be uniformly mixed.Above-mentioned mixed solution is positioned over reactor, under temperature 50 C, adds backflow 1.5h.Final for gained mixed liquor is cooled to normal temperature, obtains electronic cigarette liquid.
Comparative example 8
By the cloud and mist extract of 0.08 gram, be richer than 55 grams of propane diols, add 1 gram of flavouring essence for tobacco, 0.8 gram of pure water, glycerine 43.12 grams, stirs solution, filters and obtains solution.Add glycerine to solution and supply 100 grams of electronic cigarette liquids, be uniformly mixed, obtain contrast electronic cigarette liquid.
The electronic cigarette liquid of the electronic cigarette liquid and 3ml comparative example 8 of getting 3ml embodiment 8 adds in electronic smoke atomizer respectively, is smoked panel test by the personnel that smoke panel test of specialty.Evaluation result shows: both have tobacco aroma, but compares with comparative example 8, and during the electronic cigarette liquid of continuous sucking embodiment 8, tobacco perfume (or spice) is more naturally pure, and fragrance mouthfeel is consistent and does not have notable difference.
Above better embodiment of the present invention is illustrated, but the invention is not limited to described embodiment, those of ordinary skill in the art also can make all equivalent modifications or replacement under the prerequisite without prejudice to spirit of the present invention, and these equivalent modification or replacement are all included in the application's claim limited range.
Claims (5)
1. a preparation method for the electronic cigarette liquid of good thermal stability, comprises the steps:
1) by 0.05 ~ 1% tobacco extract, 1 ~ 1.5% flavouring essence for tobacco, 0 ~ 3% nicotine, 0.5 ~ 1% pure water, 50 ~ 70% propane diols and surplus glycerine by mass percentage component are mixed with solution, stir, and filter and obtain solution;
2) add the flavoring agent of 0.5 ~ 10ppm of plan preparation electronic cigarette liquid quality to filtrate, be uniformly mixed 10 ~ 20min, the electronic cigarette liquid quality prepared with 100% plan of supplying of propane diols or glycerine, is uniformly mixed and obtains mixed solution;
3) gained mixed solution is placed in reactor, at 50 ~ 70 DEG C, adds hot reflux 1 ~ 3h, cools and obtain electronic cigarette liquid.
2. the preparation method of the electronic cigarette liquid of a kind of good thermal stability according to claim 1, is characterized in that: heating reflux temperature is 50 DEG C.
3. the preparation method of the electronic cigarette liquid of a kind of good thermal stability according to claim 1, is characterized in that: flavoring agent is amino acids flavoring agent.
4. the preparation method of the electronic cigarette liquid of a kind of good thermal stability according to claim 1, is characterized in that: flavoring agent is selected from least one in L-PROLINE, glycine, Pidolidone, altheine, L-threonine, L-Histidine, Valine.
5. the preparation method of the electronic cigarette liquid of a kind of good thermal stability according to claim 4, it is characterized in that: when flavoring agent is selected from more than one in L-PROLINE, glycine, Pidolidone, altheine, L-threonine, L-Histidine, Valine, the mass mixings such as different amino acid.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1369237A (en) * | 2002-03-11 | 2002-09-18 | 姚揆一 | Artificial low-position tobacco matrix |
| JP2012005412A (en) * | 2010-06-24 | 2012-01-12 | Jbs:Kk | Chemical liquid used for atomizer, and atomizer |
| CN102349699A (en) * | 2011-07-04 | 2012-02-15 | 郑俊祥 | Preparation method for electronic cigarette liquid |
| CN103284319A (en) * | 2013-06-20 | 2013-09-11 | 昌宁德康生物科技有限公司 | Oral cavity atomized liquid with cytosine replacing nicotine and preparation method thereof |
| CN103404965A (en) * | 2012-12-28 | 2013-11-27 | 昌宁德康生物科技有限公司 | Method for producing pulp applied to electronic smoking set and traditional water pipe with shredded tobacco |
| CN104013095A (en) * | 2014-06-23 | 2014-09-03 | 昌宁德康生物科技有限公司 | Shredded tobacco for water pipes and preparation method of shredded tobacco for water pipes |
| CN104256888A (en) * | 2014-08-07 | 2015-01-07 | 江苏中烟工业有限责任公司 | Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice |
-
2015
- 2015-10-27 CN CN201510704644.3A patent/CN105394807A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1369237A (en) * | 2002-03-11 | 2002-09-18 | 姚揆一 | Artificial low-position tobacco matrix |
| JP2012005412A (en) * | 2010-06-24 | 2012-01-12 | Jbs:Kk | Chemical liquid used for atomizer, and atomizer |
| CN102349699A (en) * | 2011-07-04 | 2012-02-15 | 郑俊祥 | Preparation method for electronic cigarette liquid |
| CN103404965A (en) * | 2012-12-28 | 2013-11-27 | 昌宁德康生物科技有限公司 | Method for producing pulp applied to electronic smoking set and traditional water pipe with shredded tobacco |
| CN103284319A (en) * | 2013-06-20 | 2013-09-11 | 昌宁德康生物科技有限公司 | Oral cavity atomized liquid with cytosine replacing nicotine and preparation method thereof |
| CN104013095A (en) * | 2014-06-23 | 2014-09-03 | 昌宁德康生物科技有限公司 | Shredded tobacco for water pipes and preparation method of shredded tobacco for water pipes |
| CN104256888A (en) * | 2014-08-07 | 2015-01-07 | 江苏中烟工业有限责任公司 | Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice |
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