CN108095199A - A kind of gel state tobacco juice for electronic smoke and preparation method thereof - Google Patents

A kind of gel state tobacco juice for electronic smoke and preparation method thereof Download PDF

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Publication number
CN108095199A
CN108095199A CN201810058047.1A CN201810058047A CN108095199A CN 108095199 A CN108095199 A CN 108095199A CN 201810058047 A CN201810058047 A CN 201810058047A CN 108095199 A CN108095199 A CN 108095199A
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CN
China
Prior art keywords
electronic smoke
tobacco juice
gel state
tobacco
glue
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810058047.1A
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Chinese (zh)
Inventor
刘维涓
郭婷婷
晏秀祥
夏荣涛
徐汉峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yunnan Tuobao Science & Technology Co Ltd
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Yunnan Tuobao Science & Technology Co Ltd
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Publication date
Application filed by Yunnan Tuobao Science & Technology Co Ltd filed Critical Yunnan Tuobao Science & Technology Co Ltd
Priority to CN201810058047.1A priority Critical patent/CN108095199A/en
Publication of CN108095199A publication Critical patent/CN108095199A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F47/00Smokers' requisites not otherwise provided for
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Confectionery (AREA)

Abstract

A kind of gel state tobacco juice for electronic smoke and preparation method thereof, the tobacco juice for electronic smoke includes the component of following mass ratio:Natural plant gum 1% 17%, Alevaire 15% 43%, food flavor 2% 20%, pure water 20 60%.Preparation method is to add in natural plant gum, pure water by proportioning, and heating is melted into glue;Flavouring essence for tobacco, Alevaire are added in by proportioning in the glue melted, is uniformly mixed, gel state tobacco juice for electronic smoke is formed after cooling.The gel state tobacco juice for electronic smoke of the present invention can vary with temperature and change solid-liquid state, and tobacco tar liquefaction condition is good, and safe and reliable.

Description

A kind of gel state tobacco juice for electronic smoke and preparation method thereof
Technical field
The invention belongs to the tobacco juice for electronic smoke products of tobacco product technical field, specially a kind of gel state.
Background technology
Electronic cigarette as a kind of on-fuel cigarette substitute, do not burn by it, without tar and a variety of carcinogenic substances, no Many advantages, such as " secondhand smoke " etc. endangers can be generated, is just gradually received and is liked by numerous smokers.Electronic cigarette is also known as electronic fog Change device, be mainly made of lithium battery, atomizer and tobacco juice three parts, be a kind of on-fuel cigarette substitute products, cardinal principle It is to provide the energy by lithium battery, tobacco tar is atomized into smog and is sucked for consumer.Presently commercially available electronic cigarette was using It is present with " leakage " phenomenon in journey, especially after electronic cigarette use environment air pressure changes or puts for a long time, the phenomenon is outstanding To be apparent, due to the leakage of tobacco juice, cause electronic cigarette electrode section loose contact, influence normal use or because " oil leak " makes Into the pollution of consumer's clothing and other articles, electron cigarette user causes great puzzlement, while greatly reduces electricity Sub- cigarette consumes usage experience sense.
To solve the problems, such as electronic cigarette " leakage ", current main resolving ideas is concentrated in the change of smoking set structure, but by It is flowable state at normal temperatures in current tobacco juice for electronic smoke, is put if undergoing air pressure change after opening use or leaving unused for a long time It puts and is still present with tobacco tar Seepage, it is impossible to thoroughly solve the problems, such as " leakage ".
In addition, Chinese patent CN201410205474.X discloses a kind of gel-type solid-liquid electronics smoke grenade and its preparation side Method, it is mentioned that gel type solid tobacco tar, its preparation method is that (poloxamer, card pool nurse, gathers by basic tobacco, base gel Vinyl alcohol, povidone, sodium carboxymethylcellulose, methylcellulose, hydroxyethyl cellulose, sodium hyaluronate, polyethylene glycol, hydroxypropyl first One or more mixtures in cellulose) and flavouring essence for tobacco be mixed evenly to be formed.The gel base used in the patent Matter ingredient is mainly surfactant and thickening compound, and the gel-type vehicle formed does not possess to be solidified under low-temperature condition, high temperature The characteristic melted under state, therefore prepared gel type solid tobacco tar is in always thick glue shape, by the metal for heating electronic cigarette Shell carrys out destructive distillation tobacco gel, generates smog, and due to not undergoing phase transition, tobacco material is coated be subject to gel, causes what is generated Tobacco component content is extremely limited in flue gas, and tobacco flavor volatilization is bad, and suction experience sense is poor.And wherein polyvinyl alcohol, Two kinds of ingredients of povidone have carcinogenic risk, do not have security.Although it is considered using the shape that tobacco tar is carried out to gel solidification Formula, but be atomized since electronic smoke atomizer relies primarily on importing fluid, it can just make tobacco aroma abundant in oil atomization Volatilization makes smoker have preferable experience sense, therefore this gel type solid tobacco tar using effect that will not melt and pays no attention to Think.
The content of the invention
Present invention aims to solve the deficiencies of the prior art, and provides a kind of one kind can vary with temperature and change solid-liquid state, Good and safe and reliable gel state tobacco juice for electronic smoke of tobacco tar liquefaction condition and preparation method thereof.
In order to achieve the above object, the present invention uses following technical scheme:
A kind of gel state tobacco juice for electronic smoke includes the component of following mass ratio:Natural plant gum 1%-17%, Alevaire 15%- 43%, food flavor 2%-20%, pure water 20-60%.
Natural plant gum of the present invention is chitosan, sodium alginate, gelatin, agar, Arabic gum, pectin, carragheen, xanthan One or more mixtures in glue, guar gum.The Alevaire is the mixture of propylene glycol, glycerine or both.
The preparation method of gel state tobacco juice for electronic smoke of the present invention includes the following steps:
(1) natural plant gum, pure water are added in by proportioning, heating is melted into glue;
(2) flavouring essence for tobacco, Alevaire are added in by proportioning in the glue melted, uniformly mixes, formed after cooling Gel state tobacco juice for electronic smoke.
Electronic cigarette liquid prepared by the present invention, in not flow-gel state, becomes working fluid state below room temperature after heated, Temperature is down to below room temperature again in not flow-gel state, is accordingly used in electronic cigarette utensil when room temperature or low temperature do not aspirate heating Tobacco juice is solid gel state, is not in leakage and writes phenomenon freely and easily;And during electronic cigarette utensil aspirates use, it is atomized After device heating, gel tobacco juice melts immediately as liquid, and the normal atomizer that imports carries out atomization use.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention Further it is described in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and do not have to In restriction technical solution of the present invention.
Embodiment 1
A kind of gel state tobacco juice for electronic smoke weighs the component of following mass ratio:Chitosan 2%, gelatin 8%, propylene glycol 15%th, glycerine 20%, tobacco rhythm essence 15%, pure water 40%.
Heating is melted into glue after chitosan, gelatin, pure water are mixed, and it is fragrant that cigarette is then added in the glue melted Essence, propylene glycol, glycerine, uniformly mix, and gel state tobacco juice for electronic smoke is formed after cooling.
Embodiment 2
A kind of gel state tobacco juice for electronic smoke weighs the component of following mass ratio:Sodium alginate 1%, agar 12%, propylene glycol 43%th, Mint Essence 20%, pure water 24%.
Heating is melted into glue after sodium alginate, agar, pure water are mixed, and cigarette is then added in the glue melted uses Essence, propylene glycol, uniformly mix, and gel state tobacco juice for electronic smoke is formed after cooling.
Embodiment 3
A kind of gel state tobacco juice for electronic smoke weighs the component of following mass ratio:Guar gum 1%, glycerine 35%, cocoa are fragrant Essence 8%, pure water 56%.
Heating is melted into glue after guar gum, pure water are mixed, and flavouring essence for tobacco, third are then added in the glue melted Triol uniformly mixes, and gel state tobacco juice for electronic smoke is formed after cooling.
Embodiment 4
A kind of gel state tobacco juice for electronic smoke weighs the component of following mass ratio:Arabic gum 10%, pectin 2%, carragheen 5%th, glycerine 15%, mango essence 8%, pure water 60%.
Heating is melted into glue after Arabic gum, pectin, pure water are mixed, and cigarette is then added in the glue melted uses Essence, glycerine, uniformly mix, and gel state tobacco juice for electronic smoke is formed after cooling.
Embodiment 5
A kind of gel state tobacco juice for electronic smoke weighs the component of following mass ratio:Xanthans 15%, propylene glycol 15%, the third three Alcohol 25%, osmanthus flower fragrance 2%, pure water 43%.
Heating is melted into glue after xanthans, pure water are mixed, and flavouring essence for tobacco, third are then added in the glue melted Glycol, glycerine, uniformly mix, and gel state tobacco juice for electronic smoke is formed after cooling.
Embodiment 6
A kind of gel state tobacco juice for electronic smoke weighs the component of following mass ratio:Chitosan 10%, pectin 7%, propylene glycol 18%th, glycerine 25%, coffee aroma 20%, pure water 20%.
Heating is melted into glue after chitosan, pectin, pure water are mixed, and it is fragrant that cigarette is then added in the glue melted Essence, propylene glycol, glycerine, uniformly mix, and gel state tobacco juice for electronic smoke is formed after cooling.
Natural plant gum of the present invention, Alevaire, food flavor etc. are original commercially available to be obtained.

Claims (4)

1. a kind of gel state tobacco juice for electronic smoke, which is characterized in that include the component of following mass ratio:Natural plant gum 1%-17%, mist Agent 15%-43%, food flavor 2%-20%, pure water 20-60%.
2. a kind of gel state tobacco juice for electronic smoke according to claim 1, it is characterised in that:The natural plant gum for chitosan, One or more mixtures in sodium alginate, gelatin, agar, Arabic gum, pectin, carragheen, xanthans, guar gum.
3. a kind of gel state tobacco juice for electronic smoke according to claim 1, it is characterised in that:The Alevaire for propylene glycol, The mixture of glycerine or both.
4. a kind of such as preparation method of gel state tobacco juice for electronic smoke of any one of them of claims 1 to 3, including walking as follows Suddenly:
(1) natural plant gum, pure water are added in by proportioning, heating is melted into glue;
(2) flavouring essence for tobacco, Alevaire are added in by proportioning in the glue melted, uniformly mixes, gel is formed after cooling State tobacco juice for electronic smoke.
CN201810058047.1A 2018-01-22 2018-01-22 A kind of gel state tobacco juice for electronic smoke and preparation method thereof Pending CN108095199A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810058047.1A CN108095199A (en) 2018-01-22 2018-01-22 A kind of gel state tobacco juice for electronic smoke and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810058047.1A CN108095199A (en) 2018-01-22 2018-01-22 A kind of gel state tobacco juice for electronic smoke and preparation method thereof

Publications (1)

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110664006A (en) * 2019-09-09 2020-01-10 河南中烟工业有限责任公司 Smoking article containing hot-melt atomizing agent
CN111466607A (en) * 2020-03-12 2020-07-31 深圳瀚星翔科技有限公司 Tobacco tar thickener, electronic cigarette tobacco tar and preparation method thereof
CN111672431A (en) * 2020-06-04 2020-09-18 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-amino-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof
CN111672429A (en) * 2020-06-04 2020-09-18 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-aryl-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof
CN111672430A (en) * 2020-06-04 2020-09-18 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-amido-glycosyl-arylidene four-section glycosyl gelling agent and preparation and application thereof
CN112237295A (en) * 2020-11-16 2021-01-19 云南中烟工业有限责任公司 High-liquid-holding-capacity transparent solid tobacco tar and preparation method thereof
WO2021094365A1 (en) * 2019-11-15 2021-05-20 Jt International Sa Hot pressed tobacco substrate
CN113163844A (en) * 2018-12-28 2021-07-23 菲利普莫里斯生产公司 High viscosity nicotine formulations
CN113613514A (en) * 2018-12-17 2021-11-05 菲利普莫里斯生产公司 Tubular element for use with an aerosol-generating article
WO2021243657A1 (en) * 2020-06-04 2021-12-09 云南中烟工业有限责任公司 Atomizing liquid gel having reversible phase transition characteristics, and preparation method therefor and application thereof
CN113907399A (en) * 2021-09-30 2022-01-11 深圳市真味生物科技有限公司 Electronic atomized liquid and preparation method thereof
WO2022165896A1 (en) * 2021-02-04 2022-08-11 云南中烟工业有限责任公司 Gel-state e-liquid preparation device and preparation method capable of reducing bubbles

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CN101461566A (en) * 2009-01-08 2009-06-24 华健 Atomized liquid of electronic smoke
CN102028306A (en) * 2010-12-07 2011-04-27 张志军 Throat nourishing health-care type electronic cigarette liquid
CN104026730A (en) * 2014-07-01 2014-09-10 安徽中烟工业有限责任公司 Scorch sweet aroma electronic cigarette juice
CN104256888A (en) * 2014-08-07 2015-01-07 江苏中烟工业有限责任公司 Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice
CN104382236A (en) * 2014-10-22 2015-03-04 浙江中烟工业有限责任公司 Gel state tobacco cartridge of electronic cigarette and preparation method thereof
US20170099868A1 (en) * 2013-07-19 2017-04-13 Altria Client Services Llc Methods and Systems for Incorporating Nicotine into Oral Products

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CN101461566A (en) * 2009-01-08 2009-06-24 华健 Atomized liquid of electronic smoke
CN102028306A (en) * 2010-12-07 2011-04-27 张志军 Throat nourishing health-care type electronic cigarette liquid
US20170099868A1 (en) * 2013-07-19 2017-04-13 Altria Client Services Llc Methods and Systems for Incorporating Nicotine into Oral Products
CN104026730A (en) * 2014-07-01 2014-09-10 安徽中烟工业有限责任公司 Scorch sweet aroma electronic cigarette juice
CN104256888A (en) * 2014-08-07 2015-01-07 江苏中烟工业有限责任公司 Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice
CN104382236A (en) * 2014-10-22 2015-03-04 浙江中烟工业有限责任公司 Gel state tobacco cartridge of electronic cigarette and preparation method thereof

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113613514A (en) * 2018-12-17 2021-11-05 菲利普莫里斯生产公司 Tubular element for use with an aerosol-generating article
CN113163844A (en) * 2018-12-28 2021-07-23 菲利普莫里斯生产公司 High viscosity nicotine formulations
CN110664006A (en) * 2019-09-09 2020-01-10 河南中烟工业有限责任公司 Smoking article containing hot-melt atomizing agent
WO2021094365A1 (en) * 2019-11-15 2021-05-20 Jt International Sa Hot pressed tobacco substrate
CN111466607A (en) * 2020-03-12 2020-07-31 深圳瀚星翔科技有限公司 Tobacco tar thickener, electronic cigarette tobacco tar and preparation method thereof
CN111672430A (en) * 2020-06-04 2020-09-18 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-amido-glycosyl-arylidene four-section glycosyl gelling agent and preparation and application thereof
CN111672429A (en) * 2020-06-04 2020-09-18 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-aryl-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof
CN111672431A (en) * 2020-06-04 2020-09-18 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-amino-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof
WO2021243657A1 (en) * 2020-06-04 2021-12-09 云南中烟工业有限责任公司 Atomizing liquid gel having reversible phase transition characteristics, and preparation method therefor and application thereof
CN111672429B (en) * 2020-06-04 2022-02-08 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-aryl-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof
CN111672431B (en) * 2020-06-04 2022-04-08 云南中烟工业有限责任公司 Reversible phase-change atomized liquid gel containing alkyl-amino-glycosyl three-stage glycosyl gelling agent and preparation method and application thereof
US11344058B2 (en) 2020-06-04 2022-05-31 China Tobacco Yunnan Industrial Co., Ltd Atomizing liquid gel with reversible phase transition characteristics, preparation method and applications thereof
EP3943186B1 (en) * 2020-06-04 2023-01-11 China Tobacco Yunnan Industrial Co., Ltd Applications of atomizing liquid gel having reversible phase transition characteristics
CN112237295A (en) * 2020-11-16 2021-01-19 云南中烟工业有限责任公司 High-liquid-holding-capacity transparent solid tobacco tar and preparation method thereof
WO2022165896A1 (en) * 2021-02-04 2022-08-11 云南中烟工业有限责任公司 Gel-state e-liquid preparation device and preparation method capable of reducing bubbles
US11717020B2 (en) 2021-02-04 2023-08-08 China Tobacco Yunnan Industrial Co., Ltd Bubble removal preparation device and method for gel-state electronic liquid (e-liquid)
CN113907399A (en) * 2021-09-30 2022-01-11 深圳市真味生物科技有限公司 Electronic atomized liquid and preparation method thereof

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