CN109512015A - A kind of non-ignitable burning solid essence of the heating of cigarette and preparation method thereof - Google Patents
A kind of non-ignitable burning solid essence of the heating of cigarette and preparation method thereof Download PDFInfo
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- CN109512015A CN109512015A CN201811267270.3A CN201811267270A CN109512015A CN 109512015 A CN109512015 A CN 109512015A CN 201811267270 A CN201811267270 A CN 201811267270A CN 109512015 A CN109512015 A CN 109512015A
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- extract
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- ignitable
- weight ratio
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Abstract
The present invention relates to a kind of non-ignitable burning solid essences of heating and preparation method thereof, the non-ignitable burning solid essence of the heating contains natural extract, microcrystalline cellulose, sodium carboxymethylcellulose and smoke agent, the present invention heats non-ignitable burning solid essence and is used in cigarette, keeps fragrance stereovision abundant, thick and solid, compared with smoke grenade is not burnt in existing heating, miscellaneous gas obviously weakens, simple process, is suitable for the heating of different size shape not burner, mode of appearance is novel, meet consumer at heart and psychological need.
Description
[technical field]
The invention belongs to technical field of tobacco processing.More particularly it relates to which a kind of heating of cigarette is not burnt
Solid essence further relates to the non-ignitable preparation method for burning solid essence of heating of the cigarette.
[background technique]
Heating do not burn cigarette be it is a kind of tobacco material rather than the cigarette of burning tobacco substance are heated by electronic equipment,
Open fire and cigarette ash are not generated during this cigarette smoking, it is environmentally friendly, aspirate consumer by electronics heating equipment
Tobacco flavor can be experienced when cigarette, while reducing and generating harmful substance in burning high temperature pyrolysis in conventional cigarette, be consumer
The smoking of healthy formula provide an effective approach, such smoking mode is at home and abroad increasingly come popular, has formed one
The consumer group of considerable scale.
Currently, the fragrant section of the incombustible production of the heating of commercial type mainly uses paper process thin slice, dry method thin slice, thick slurry method
Materials, the substrate of these materials such as thin slice and the forming paper by being coated with are paper fibers, can bring miscellaneous gas when heated, influence to take out
Quality is inhaled, and restores that the aroma substance that goes back is less, is difficult to meet the demand to fragrance and physiology satisfaction of consumption.
Therefore, finally complete present inventor has performed a large amount of test and analysis for many technological deficiencies of the prior art
At the present invention.
[summary of the invention]
[technical problems to be solved]
The object of the present invention is to provide a kind of non-ignitable burning solid essences of the heating of cigarette.
It is a further object to provide the non-ignitable preparation methods for burning solid essence of cigarette heating.
[technical solution]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of non-ignitable burning solid essences of the heating of cigarette.
It is as follows that the present invention heats non-ignitable burning solid essence composition: in parts by weight
The natural extract is yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extraction
The mixture of object, plum extract and Fructus Fici extract；
The smoke agent is the mixture of propylene glycol, glycerine and two acetoglycerides.
A preferred embodiment of the invention, it is as follows that the present invention heats non-ignitable burning solid essence composition: with weight
Part meter
According to another preferred method of implementation of the present invention, in the natural extract, yunyan extract can be can extract
Object, licorice, tree moss extract, Chinese date extract, plum extract and Fructus Fici extract weight ratio be 50~70:
10~20:5~10:1~3:3~9:2~8:5~10.
According to another preferred method of implementation of the present invention, in the natural extract, yunyan extract can be can extract
Object, licorice, tree moss extract, Chinese date extract, plum extract and Fructus Fici extract weight ratio be 55~65:
12~18:6~8:1.6~2.4:4~8:3~6:6~8.
According to another preferred method of implementation of the present invention, in the smoke agent, propylene glycol, glycerine and two acetic acid
The weight ratio of glyceride is 10~30:20~40:50~80.
According to another preferred method of implementation of the present invention, in the smoke agent, propylene glycol, glycerine and two acetic acid
The weight ratio of glyceride is 14~26:24~36:58~72.
The invention further relates to the non-ignitable preparation methods for burning solid essence of the heating.
The step of this method, is as follows:
A, natural extract is prepared
By yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extract, plum extract and nothing
Flowers and fruits extract is mixed to get the day according to 50~70:10 of weight ratio~20:5~10:1~3:3~9:2~8:5~10
Right extract；
B, smoke agent is prepared
Propylene glycol, glycerine and two acetoglycerides are mixed to get institute according to 10~30:20 of weight ratio~40:50~80
The smoke agent stated；
C, it mixes
0.08~2.6 parts by weight microcrystalline cellulose is added in the natural extract that step A is obtained toward 76~130 parts by weight
Element, 0.08~1.0 parts by weight sodium carboxymethylcellulose are uniformly mixed, and in obtained mixture injection mold, are placed in drying box
In, be dried at 105~115 DEG C of temperature water content be by weight 5% hereinafter, be sprayed at that step B obtains again 0.8~
1.6 parts by weight smoke agents, it is dry, obtain the non-ignitable burning solid essence of heating.
A preferred embodiment of the invention, yunyan extract, cocoa extract, licorice, tree moss extract
Object, Chinese date extract, plum extract and Fructus Fici extract weight ratio be 55~65:12~18:6~8:1.6~2.4:4
~8:3~6:6~8.
According to another preferred method of implementation of the present invention, propylene glycol, the weight ratio of glycerine and two acetoglycerides are
14~26:24~36:58~72.
According to another preferred method of implementation of the present invention, the mold have cylinder, pentagon body, rhombogen,
Spherical, cuboid or square shape.
The present invention is described in more detail below.
The present invention relates to a kind of non-ignitable burning solid essences of the heating of cigarette.
It is as follows that cigarette of the present invention heats non-ignitable burning solid essence composition: in parts by weight
The natural extract is yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extraction
The mixture of object, plum extract and Fructus Fici extract；
The yunyan extract is to be free of any additive through what science extraction was process using Yunnan High Quality Tobacco
It can effectively improve cigarette quality and increase reconstituted tobacoo and naturally feel, improve the additive of cigarette cloud and mist flavor.What the present invention used
Yunyan extract is current market sales of product, e.g. by Kaifeng Rui Quan flavors and fragrances Co., Ltd with trade name cloud and mist alcohol
The product of extract sale.The yunyan extract that the present invention uses is to provide tobacco in the basic role heated in non-ignitable burning solid essence
This perfume.In the natural extract, when other components are within the scope of the weight ratio, if the weight ratio of yunyan extract
Lower than 50, then cigarette perfume is thiner；If the weight ratio of yunyan extract is higher than 70, flue gas burr sense increases, and the larynx that occurs choking is existing
As, therefore it is reasonable that the weight ratio of yunyan extract, which is 50~70,.
The cocoa extract that the present invention uses is to increase cigarette in the non-ignitable basic role burnt in solid essence of present invention heating
The solid sense of gas, increasing smoke concentration.The cocoa extract that the present invention uses is current market sales of product, e.g. by
The product that Kaifeng Rui Quan flavors and fragrances Co., Ltd is sold with trade name cocoa alcohol extract.In the natural extract,
When its component is within the scope of the weight ratio, if the weight ratio of cocoa extract is lower than 10, flue gas hair is empty, flue gas concentration
It reduces；If the weight ratio of cocoa extract is higher than 20, flue gas dissipates, and conglobation property is poor；Therefore the weight of cocoa extract
Than being appropriate for 10~20.
The licorice that the present invention uses is to increase cigarette in the non-ignitable basic role burnt in solid essence of present invention heating
The sweet tea rhythm of gas.The licorice that the present invention uses is current market sales of product, e.g. fragrant by the auspicious spring essence that breaks a seal
The product that material Co., Ltd is sold with trade name Radix Glycyrrhizae alcohol extract.In the natural extract, other components are described
When within the scope of weight ratio, if the weight ratio of licorice is lower than 5, flue gas is bitter, and sweet tea rhythm sense is poor；If licorice
Weight ratio be higher than 10, then Radix Glycyrrhizae green gas is heavier in flue gas；Therefore it is suitable that the weight ratio of licorice, which is 5~10,.
The tree moss extract that the present invention uses is abundant cigarette in the non-ignitable basic role burnt in solid essence of present invention heating
Tongue fur fragrance ceases in gas, increases the elegant sense of flue gas.The tree moss extract that the present invention uses is current market sales of product, example
The product sold in this way by the Rui Quan flavors and fragrances Co., Ltd that breaks a seal with trade name tree moss water extract.In the natural extract
In, when other components are within the scope of the weight ratio, if the weight ratio of tree moss extract be lower than 1, flue gas it is rich
It is poor；If the weight ratio of tree moss extract is higher than 3, tongue fur fragrance breath is overweight, uncoordinated with flue gas；Therefore tree moss extract
It is reasonable that weight ratio, which is 1~3,.
The Chinese date extract that the present invention uses is to increase jujube in the non-ignitable basic role burnt in solid essence of present invention heating
Sweet gas breath, covers miscellaneous gas.The Chinese date extract that the present invention uses is current market sales of product, e.g. by the Rui Quan that breaks a seal
The product that flavors and fragrances Co., Ltd is sold with trade name Chinese date alcohol extract.In the natural extract, other components
When within the scope of the weight ratio, if the weight ratio of Chinese date extract is lower than 3, miscellaneous gas is obvious, and oral cavity residual is heavier；If
The weight ratio of Chinese date extract is higher than 9, then jujube sweet gas breath is obvious, presses cigarette perfume；Therefore the weight ratio of Chinese date extract is for 3~9
It is feasible.
The plum extract that the present invention uses is to increase cigarette in the non-ignitable basic role burnt in solid essence of present invention heating
The sour-sweet rhythm of gas reduces stimulation, soft flue gas.The plum extract that the present invention uses is current market sales of product, such as
It is the product sold by the Rui Quan flavors and fragrances Co., Ltd that breaks a seal with trade name plum alcohol extract.In the natural extract
In, when other components are within the scope of the weight ratio, if the weight ratio of plum extract is lower than 2, flue gas stimulation is reinforced,
Flue gas is more quick-fried；If the weight ratio of plum extract is higher than 8, flue gas turns sour, and influences mouthfeel；Therefore the weight of plum extract
Than being reasonable for 2~8.
The Fructus Fici extract that the present invention uses is to increase in the non-ignitable basic role burnt in solid essence of present invention heating
Flue gas sugariness reduces oral cavity residual.The Fructus Fici extract that the present invention uses is current market sales of product, e.g. by
The product that Kaifeng Rui Quan flavors and fragrances Co., Ltd is sold with trade name fig alcohol extract.In the natural extract,
When other components are within the scope of the weight ratio, if the weight ratio of Fructus Fici extract is lower than 5, oral cavity residual weight；Such as
The weight ratio of fruit Fructus Fici extract is higher than 10, then presses cigarette perfume, the property sent out is poor thoroughly for flue gas；Therefore the weight ratio of Fructus Fici extract is
5~10 be suitable.
According to the present invention, in the natural extract, yunyan extract, cocoa extract, licorice, tree moss are mentioned
The weight ratio for taking object, Chinese date extract, plum extract and Fructus Fici extract is 50~70:10~20:5~10:1~3:3
~9:2~8:5~10.
Preferably, in the natural extract, yunyan extract, cocoa extract, licorice, tree moss are extracted
Object, Chinese date extract, plum extract and Fructus Fici extract weight ratio be 55~65:12~18:6~8:1.6~2.4:4
~8:3~6:6~8.
It is heated in non-ignitable burning solid essence in the present invention, the main function of the smoke agent is to provide smog when suction
Amount and flue gas moisture feeling.The smoke agent is the mixture of propylene glycol, glycerine and two acetoglycerides, wherein the work of propylene glycol
With being flue gas moisture feeling；The effect of glycerine is to play atomizing；The effect of two acetoglycerides is to play the role of smoke.This
Inventing propylene glycol, glycerine and two acetoglycerides used is all current market sales of product, e.g. by upper Haikang
Two acetoglycerides that bright Biotechnology Co., Ltd is sold with trade name diacetate ester.
In the smoke agent, when other components are within the scope of the weight ratio, if the weight ratio of propylene glycol is low
In 10, then flue gas is dry, if the weight ratio of propylene glycol is higher than 30, steam is obvious in flue gas, influences to aspirate mouthfeel, therefore third
It is suitable that the weight ratio of glycol, which is 10~30,.Similarly, when other components are within the scope of the weight ratio, if glycerine
Weight ratio be lower than 20, then atomizing effect is poor, and amount of smoke is few；If the weight ratio of glycerine is higher than 40, moisture in flue gas
It is promoted, causes suction mouthfeel bad；Therefore it is feasible that the weight ratio of glycerine, which is 20~40,.Other components are in the weight
When than in range, if the weight ratio of two acetoglycerides is lower than 50, smoke amount is less, if the weight of two acetoglycerides
Than being higher than 80, then smoke amount is excessively high, and suction experience is poor；Therefore it is feasible that the weight ratio of two acetoglycerides, which is 50~80,.
Therefore, in the smoke agent weight ratio of propylene glycol, glycerine and two acetoglycerides be 10~30:20~
40:50~80.
Preferably, in the smoke agent, the weight ratio of propylene glycol, glycerine and two acetoglycerides is 14~26:
24~36:58~72.
It is heated in non-ignitable burning solid essence in the present invention, microcrystalline cellulose heats in non-ignitable burning solid essence in the present invention
Main function is that essence is sticked together as binder.The microcrystalline cellulose that the present invention uses is to sell currently on the market
Product, the product e.g. sold by Shandong Yu Heng cellulose Co., Ltd with trade name microcrystalline cellulose.Carboxymethyl cellulose
Main function of the plain sodium in the non-ignitable burning solid essence of present invention heating is to play solidification as curing agent.The present invention makes
Sodium carboxymethylcellulose is also current market sales of product, e.g. by Shandong Yu Heng cellulose Co., Ltd with quotient
The product of name of an article sodium carboxymethylcellulose sale.
It is heated in non-ignitable burning solid essence in cigarette of the present invention, when other components are in the content range, if
The content of natural extract is lower than 76, then flue gas texture is poor, and flue gas hair is empty；If the content of natural extract is higher than 130,
Flue gas concentration is higher, and oral stimulation is larger, influences to aspirate mouthfeel；Therefore it is reasonable that the content of natural extract, which is 76~130,.
Similarly, when other components are in the content range, if the content of microcrystalline cellulose be lower than 0.08, solid essence compared with
Be it is loose, be unfavorable for aspirating；If the content of microcrystalline cellulose is higher than 2.6, when aspirating, miscellaneous gas is heavier；Therefore microcrystalline cellulose
It is appropriate that the content of element, which is 0.08~2.6,.When other components are in the content range, if sodium carboxymethylcellulose
Content is lower than 0.08, then solid essence quality is softer, frangible, is not easy suction operation；If the content of sodium carboxymethylcellulose is high
In 1.0, then solid essence quality is harder, is unfavorable for smoke；Therefore it is appropriate that the content of sodium carboxymethylcellulose, which is 0.08~1.0,
's.When other components are in the content range, if the content of smoke agent is lower than 0.8, amount of smoke is less, it is difficult to meet
The expectation at heart of consumer；If the content of smoke agent is higher than 1.6, smog is larger, influences suction experience；Therefore smoke agent
It is appropriate that content, which is 0.8~1.6,.
Therefore, it is as follows to heat non-ignitable burning solid essence composition for cigarette of the present invention: in parts by weight
Preferably, it is as follows to heat non-ignitable burning solid essence composition for cigarette of the present invention: in parts by weight
The invention further relates to the non-ignitable preparation methods for burning solid essence of the heating.
The step of this method, is as follows:
A, natural extract is prepared
By yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extract, plum extract and nothing
Flowers and fruits extract is mixed to get the day according to 50~70:10 of weight ratio~20:5~10:1~3:3~9:2~8:5~10
Right extract；
B, smoke agent is prepared
Propylene glycol, glycerine and two acetoglycerides are mixed to get institute according to 10~30:20 of weight ratio~40:50~80
The smoke agent stated；
C, it mixes
0.08~2.6 parts by weight microcrystalline cellulose is added in the natural extract that step A is obtained toward 76~130 parts by weight
Element, 0.08~1.0 parts by weight sodium carboxymethylcellulose are uniformly mixed, and in obtained mixture injection mold, are placed in drying box
In, be dried at 105~115 DEG C of temperature water content be by weight 5% hereinafter, be sprayed at that step B obtains again 0.8~
1.6 parts by weight smoke agents, it is dry, obtain the non-ignitable burning solid essence of heating.
Preferably, yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extract, plum extract
The weight ratio of object and Fructus Fici extract is 55~65:12~18:6~8:1.6~2.4:4~8:3~6:6~8.
Preferably, the weight ratio of propylene glycol, glycerine and two acetoglycerides is 10~30:20~40:50~80.
Details in relation to natural extract, microcrystalline cellulose, sodium carboxymethylcellulose and smoke agent is in front
Description, details are not described herein.
The mold that the present invention uses has cylinder, pentagon body, rhombogen, spherical shape, cuboid or square shape.When
So, it can also select according to actual needs using other shapes of mold, this is for those skilled in the art not
There are any technical difficulties.
The drying box that the present invention uses is current market sales of, and drying box product usually used at present.
In the present invention, the water content is the measurement according to GB/T 23357-2009 tobacco and tobacco product moisture
Detection method detection.
Embodiment sample uses the heating chamber suction unit of different shapes produced by Yunnan bar wild rice, heating temperature 300
DEG C, when heating it is a length of 3 points 30 seconds, control using the IUOC suction unit by seeing intelligent technology limited sale more than Shenzhen,
The photoelectric smoke sensor sold by Beijing emerging Wolong sensor Science and Technology Development Co., Ltd. with trade name smoke alarm, is made into
Closed tee tube, every time with syringe inject 35ml flue gas, using by Beijing emerging Wolong sensor Science and Technology Development Co., Ltd. with
The photoelectric smoke sensor of trade name alarm sale is detected.Amount of smoke is divided into three-level, i.e., rudimentary (bright light), middle rank
(two bright lights) and advanced (three bright lights)；Sensory evaluating smoking is carried out to cigarette according to GB5606.4-2005 standard, the result is shown under
Table 1.
[beneficial effect]
The beneficial effects of the present invention are:
The heating of commercial type at present is not burnt, and to produce fragrant section be mainly paper process thin slice, dry method thin slice, thick slurry method thin slice
The materials such as the forming paper being coated with process, the main substrate of these materials is paper fiber, it can bring miscellaneous gas when heated, influences to take out
Quality is inhaled, and it is less to restore the aroma substance that goes back, and is difficult meet the needs of consumer is to fragrance and physiology satisfaction.The present invention
Solid spice is directly heated, fragrance stereovision is abundant, and thick and solid, compared with smoke grenade is not burnt in commercially available heating, miscellaneous gas obviously weakens,
And simple process is suitable for the heating of different size shape not burner, and mode of appearance is novel, meets the heart of consumer
In and psychological need.
[specific embodiment]
It will be better understood that the present invention by following embodiments.
Embodiment 1: the present invention heats the non-ignitable preparation for burning solid essence
The implementation steps of the embodiment are as follows:
A, natural extract is prepared
By by break a seal Rui Quan flavors and fragrances Co., Ltd sell with trade name cloud and mist alcohol extract yunyan extract, by Kaifeng it is auspicious
Cocoa extract that spring flavors and fragrances Co., Ltd is sold with trade name cocoa alcohol extract, by the auspicious limited public affairs of spring flavors and fragrances that break a seal
Take charge of sell with trade name Radix Glycyrrhizae alcohol extract licorice, by break a seal Rui Quan flavors and fragrances Co., Ltd with trade name tree moss water
The tree moss extract of extract sale is mentioned by Kaifeng Rui Quan flavors and fragrances Co., Ltd with the Chinese date that trade name Chinese date alcohol extract is sold
Take object, the plum extract sold by Kaifeng Rui Quan flavors and fragrances Co., Ltd with trade name plum alcohol extract and by the Rui Quan that breaks a seal
The Fructus Fici extract that flavors and fragrances Co., Ltd is sold with trade name fig alcohol extract is according to weight ratio 50:12:5:1.6:
3:3:5 is mixed to get the natural extract:
B, smoke agent is prepared
By the propylene glycol sold by upper object Science and Technology Ltd., Haikang nangzan with trade name PG, by upper Haikang nangzan object science and technology
Glycerine that Co., Ltd is sold with trade name glycerol with by upper object Science and Technology Ltd., Haikang nangzan with trade name diacetate ester pin
Two acetoglycerides sold are mixed to get the smoke agent according to weight ratio 10:24:50；
C, it mixes
0.08 parts by weight microcrystalline cellulose, 0.2 parts by weight are added in natural extract prepared by step A toward 88 parts by weight
Sodium carboxymethylcellulose is uniformly mixed, and in the cylinder mold of obtained mixture injection circumference 25.0mm, high 50mm, is set
In drying box, it is by weight 4.8% that water content is dried at 105 DEG C of temperature, then sprays 0.8 parts by weight in step B system
Standby smoke agent obtains the non-ignitable burning solid essence of heating.
It is that cylindrical heating is not burnt smoking set that the heating of embodiment preparation is non-ignitable, which to burn solid essence to be added to heating chamber,
In, sensory evaluating smoking's detection then is carried out according to the method for present specification description, testing result is listed in the table below in 1.
Embodiment 2: the present invention heats the non-ignitable preparation for burning solid essence
The implementation steps of the embodiment are as follows:
A, natural extract is prepared
By by break a seal Rui Quan flavors and fragrances Co., Ltd sell with trade name cloud and mist alcohol extract yunyan extract, by Kaifeng it is auspicious
Cocoa extract that spring flavors and fragrances Co., Ltd is sold with trade name cocoa alcohol extract, by the auspicious limited public affairs of spring flavors and fragrances that break a seal
Take charge of sell with trade name Radix Glycyrrhizae alcohol extract licorice, by break a seal Rui Quan flavors and fragrances Co., Ltd with trade name tree moss water
The tree moss extract of extract sale is mentioned by Kaifeng Rui Quan flavors and fragrances Co., Ltd with the Chinese date that trade name Chinese date alcohol extract is sold
Take object, the plum extract sold by Kaifeng Rui Quan flavors and fragrances Co., Ltd with trade name plum alcohol extract and by the Rui Quan that breaks a seal
The Fructus Fici extract that flavors and fragrances Co., Ltd is sold with trade name fig alcohol extract is according to weight ratio 70:18:10:
2.4:9:6:10 being mixed to get the natural extract:
B, smoke agent is prepared
By the propylene glycol sold by upper object Science and Technology Ltd., Haikang nangzan with trade name PG, by upper Haikang nangzan object science and technology
Glycerine that Co., Ltd is sold with trade name glycerol with by upper object Science and Technology Ltd., Haikang nangzan with trade name diacetate ester pin
Two acetoglycerides sold are mixed to get the smoke agent according to weight ratio 14:36:80；
C, it mixes
2.6 parts by weight microcrystalline celluloses, 0.8 parts by weight are added in natural extract prepared by step A toward 112 parts by weight
Sodium carboxymethylcellulose is uniformly mixed, and obtained mixture injects the cuboid mould of long side length 50.0mm Yu the long 18.0mm of short side
It in tool, is placed in drying box, it is by weight 4.5% that water content is dried at 110 DEG C of temperature, then sprays 1.0 parts by weight and exist
The smoke agent of step B preparation, obtains the non-ignitable burning solid essence of heating.
It is that cuboid heats in the smoking set that do not burn that the non-ignitable burning solid essence of heating of embodiment preparation, which is added to heating chamber,
Then sensory evaluating smoking's detection is carried out according to the method for present specification description, testing result is listed in the table below in 1.
Embodiment 3: the present invention heats the non-ignitable preparation for burning solid essence
The implementation steps of the embodiment are as follows:
A, natural extract is prepared
By by break a seal Rui Quan flavors and fragrances Co., Ltd sell with trade name cloud and mist alcohol extract yunyan extract, by Kaifeng it is auspicious
Cocoa extract that spring flavors and fragrances Co., Ltd is sold with trade name cocoa alcohol extract, by the auspicious limited public affairs of spring flavors and fragrances that break a seal
Take charge of sell with trade name Radix Glycyrrhizae alcohol extract licorice, by break a seal Rui Quan flavors and fragrances Co., Ltd with trade name tree moss water
The tree moss extract of extract sale is mentioned by Kaifeng Rui Quan flavors and fragrances Co., Ltd with the Chinese date that trade name Chinese date alcohol extract is sold
Take object, the plum extract sold by Kaifeng Rui Quan flavors and fragrances Co., Ltd with trade name plum alcohol extract and by the Rui Quan that breaks a seal
The Fructus Fici extract that flavors and fragrances Co., Ltd is sold with trade name fig alcohol extract is according to weight ratio 55:10:6:1:4:
2:6 is mixed to get the natural extract:
B, smoke agent is prepared
By the propylene glycol sold by upper object Science and Technology Ltd., Haikang nangzan with trade name PG, by upper Haikang nangzan object science and technology
Glycerine that Co., Ltd is sold with trade name glycerol with by upper object Science and Technology Ltd., Haikang nangzan with trade name diacetate ester pin
Two acetoglycerides sold are mixed to get the smoke agent according to weight ratio 26:20:58；
C, it mixes
0.2 parts by weight microcrystalline cellulose, 0.08 parts by weight are added in natural extract prepared by step A toward 76 parts by weight
Sodium carboxymethylcellulose is uniformly mixed, in the diamond shape mould of obtained mixture injection side length 20.0mm and height 20.0mm,
It is placed in drying box, it is by weight 4.9% that water content is dried at 115 DEG C of temperature, then sprays 1.5 parts by weight in step B
The smoke agent of preparation obtains the non-ignitable burning solid essence of heating.
The heating of embodiment preparation is non-ignitable to burn solid essence and is added to the heating that heating chamber is diamond shape and do not burn in smoking set,
Then sensory evaluating smoking's detection is carried out according to the method for present specification description, testing result is listed in the table below in 1.
Embodiment 4: the present invention heats the non-ignitable preparation for burning solid essence
The implementation steps of the embodiment are as follows:
A, natural extract is prepared
By by break a seal Rui Quan flavors and fragrances Co., Ltd sell with trade name cloud and mist alcohol extract yunyan extract, by Kaifeng it is auspicious
Cocoa extract that spring flavors and fragrances Co., Ltd is sold with trade name cocoa alcohol extract, by the auspicious limited public affairs of spring flavors and fragrances that break a seal
Take charge of sell with trade name Radix Glycyrrhizae alcohol extract licorice, by break a seal Rui Quan flavors and fragrances Co., Ltd with trade name tree moss water
The tree moss extract of extract sale is mentioned by Kaifeng Rui Quan flavors and fragrances Co., Ltd with the Chinese date that trade name Chinese date alcohol extract is sold
Take object, the plum extract sold by Kaifeng Rui Quan flavors and fragrances Co., Ltd with trade name plum alcohol extract and by the Rui Quan that breaks a seal
The Fructus Fici extract that flavors and fragrances Co., Ltd is sold with trade name fig alcohol extract is according to weight ratio 65:20:8:3:8:
8:8 is mixed to get the natural extract:
B, smoke agent is prepared
By the propylene glycol sold by upper object Science and Technology Ltd., Haikang nangzan with trade name PG, by upper Haikang nangzan object science and technology
Glycerine that Co., Ltd is sold with trade name glycerol with by upper object Science and Technology Ltd., Haikang nangzan with trade name diacetate ester pin
Two acetoglycerides sold are mixed to get the smoke agent according to weight ratio 30:40:72；
C, it mixes
2.0 parts by weight microcrystalline celluloses, 1.0 parts by weight are added in natural extract prepared by step A toward 130 parts by weight
Sodium carboxymethylcellulose is uniformly mixed, and obtained mixture injection side length is to be placed in drying box in the square mould of 20.0mm
In, it is by weight 4.2% that water content is dried at 110 DEG C of temperature, then sprays the smoke that 1.6 parts by weight are prepared in step B
Agent obtains the non-ignitable burning solid essence of heating.
The heating of embodiment preparation is non-ignitable to burn solid essence and is added to the heating that heating chamber is square and do not burn smoking set
In, sensory evaluating smoking's detection then is carried out according to the method for present specification description, testing result is listed in the table below in 1.
The sample that embodiment 1-4 is prepared be denoted as respectively 1 sample of embodiment, 2 sample of embodiment, 3 sample of embodiment,
4 sample of embodiment, sample B are that the reconstituted tobacco sold by Fei Mo international corporation with trade name IQOS smoke grenade heats the sample that do not burn
Product, sample C are the cigarette purple cloud sample sold by cigarette industry Co., Ltd in Yunnan with trade name cloud and mist (purple), these samples
Product carry out amount of smoke according to the method that present specification describes and its sensory evaluating smoking detects, and result is listed in the table below in 1 together.
Table 1: kinds of cigarettes sample amount of smoke and sensory evaluating smoking's result
The test result of table 1 shows: being existed using the non-ignitable heating cigarette of not burning for burning solid essence of present invention preparation heating
There is very big promotion on fragrance, after adding smoke agent, smoke amount is relaxed better than existing reconstituted tobacco thin slice and conventional cigarette, mouthfeel
Suitable, fragrance is graceful, meets consumer at heart and psychological need.
Claims (10)
1. a kind of non-ignitable burning solid essence of the heating of cigarette, it is characterised in that it forms as follows: in parts by weight
The natural extract is yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extract, plum
The mixture of seed extract and Fructus Fici extract；
The smoke agent is the mixture of propylene glycol, glycerine and two acetoglycerides.
2. the non-ignitable burning solid essence of heating according to claim 1, it is characterised in that it forms as follows: in parts by weight
3. the non-ignitable burning solid essence of heating according to claim 1 or 2, it is characterised in that in the natural extract
In, yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extract, plum extract and fig mention
The weight ratio for taking object is 50~70:10~20:5~10:1~3:3~9:2~8:5~10.
4. the non-ignitable burning solid essence of heating according to claim 3, it is characterised in that in the natural extract, cloud
Smoke-dipping paste, cocoa extract, licorice, tree moss extract, Chinese date extract, plum extract and Fructus Fici extract
Weight ratio is 55~65:12~18:6~8:1.6~2.4:4~8:3~6:6~8.
5. the non-ignitable burning solid essence of heating according to claim 1 or 2, it is characterised in that in the smoke agent, third
The weight ratio of glycol, glycerine and two acetoglycerides is 10~30:20~40:50~80.
6. the non-ignitable burning solid essence of heating according to claim 6, it is characterised in that in the smoke agent, the third two
The weight ratio of alcohol, glycerine and two acetoglycerides is 14~26:24~36:58~72.
7. heating the non-ignitable preparation method for burning solid essence according to claim 1, it is characterised in that the step of this method such as
Under:
A, natural extract is prepared
By yunyan extract, cocoa extract, licorice, tree moss extract, Chinese date extract, plum extract and fig
Extract is mixed to get according to 50~70:10 of weight ratio~20:5~10:1~3:3~9:2~8:5~10 and described naturally mentions
Take object；
B, smoke agent is prepared
Propylene glycol, glycerine and two acetoglycerides are mixed to get according to 10~30:20 of weight ratio~40:50~80 described
Smoke agent；
C, it mixes
Added in the natural extract that step A is obtained toward 76~130 parts by weight 0.08~2.6 parts by weight microcrystalline cellulose,
0.08~1.0 parts by weight sodium carboxymethylcellulose is uniformly mixed, and in obtained mixture injection mold, is placed in drying box,
Water content is dried at 105~115 DEG C of temperature as by weight 5% hereinafter, being sprayed at 0.8~1.6 weight that step B is obtained again
Part smoke agent, it is dry, obtain the non-ignitable burning solid essence of heating.
8. heating the non-ignitable preparation method for burning solid essence according to claim 7, it is characterised in that yunyan extract, cocoa mention
The weight ratio for taking object, licorice, tree moss extract, Chinese date extract, plum extract and Fructus Fici extract is 55~
65:12~18:6~8:1.6~2.4:4~8:3~6:6~8.
9. heat according to claim 7 it is non-ignitable burn solid essence preparation method, it is characterised in that propylene glycol, glycerine with
The weight ratio of two acetoglycerides is 14~26:24~36:58~72.
10. heating the non-ignitable preparation method for burning solid essence according to claim 7, it is characterised in that the mold has
Cylinder, pentagon body, rhombogen, spherical shape, pentagon body, cuboid or square shape.
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| CN109512015B (en) | 2021-07-20 |
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